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HomeMy WebLinkAboutDRC-2021-018843 - 0901a06880f9d5beENERGY FUELS October 28, 2021 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 Di3C -Zo2 (- 01, 43 www.energyfuels.corn Div of Waste and Rad.ation Control Sent VIA OVERNIGIIT DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Re: Transmittal of 3rd Quarter 2021 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 3rd Quarter of 2021 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, 101, ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer October 28, 2021 Sent VIA OVERNIGHT DELIVERY Mr. Doug Hansen Director Division of Waste Management and Radiation Control Utah Department of Environmental Quality 195 North 1950 West Salt Lake City, UT 84116 Energy Fuels Resources (USA) Inc. 225 Union Blvd. Suite 600 Lakewood, CO, US, 80228 303 974 2140 www.energy fuels. om Re: Transmittal of 3rd Quarter 2021 Groundwater Monitoring Report Groundwater Quality Discharge Permit UGW370004 White Mesa Uranium Mill Dear Mr. Hansen: Enclosed are two copies of the White Mesa Uranium Mill Groundwater Monitoring Report for the 3rd Quarter of 2021 as required by the Groundwater Quality Discharge Permit UGW370004, as well as two CDs each containing a word searchable electronic copy of the report. If you should have any questions regarding this report please contact me. Yours very truly, <f<!Uu(Jf~ ENERGY FUELS RESOURCES (USA) INC. Kathy Weinel Quality Assurance Manager cc: David Frydenlund Scott Bakken Logan Shumway Garrin Palmer White Mesa Uranium Mill Groundwater Monitoring Report State of Utah Groundwater Discharge Permit No. UGW370004 3rd Quarter (July through September) 2021 Prepared by: e£RGYFUELS Energy Fuels Resources (USA) Inc. 225 Union Boulevard, Suite 600 Lakewood, CO 80228 October 28, 2021 TABLE OF CONTENTS 1.0 INTRODUCTION ................................................................................................... l 2.0 GROUNDWATER MONITORING ....................................................................... J 2.1 Samples and Measurements Taken During the Quarter. ...................................... I 2.1.1 Groundwater Compliance Monitoring .......................................................... 1 2.1.2 Accelerated Groundwater Monitoring .......................................................... I 2.1.3 Background Well Monitoring ....................................................................... 2 2.1.4 Parameters Analyzed .................................................................................... 2 2.1.5 Groundwater Head Monitoring ..................................................................... 2 2.2 Field Data ............................................................................................................. 3 2.3 Laboratory Results -Quarterly Sampling ............................................................ 3 2.3.1 Copy of Laboratory Results .......................................................................... 3 2.3.2 Regulatory Framework and Groundwater Background ................................ 3 2.3.3 Compliance Status ............................................................................................. 4 2.4 Laboratory Results -Accelerated Monitoring ..................................................... 5 2.4.1 Copy of Laboratory Results .......................................................................... 5 2.4.2 Regulatory Framework and Groundwater Background ................................ 5 2.4.3 Compliance Status ........................................................................................ 6 2.5 Depth to Groundwater and Water Table Contour Map ........................................ 6 3.0 QUALITY ASSURANCE AND DATA VALIDATION ....................................... 6 3.1 Field QC Samples ................................................................................................. 7 3.2 Adherence to Mill Sampling SOPs ...................................................................... 7 3.3 Analyte Completeness Review ............................................................................. 7 3.4 Data Validation .................................................................................................... 8 3.4.1 Field Data QA/QC Evaluation ...................................................................... 8 3.4.2 Holding Time Evaluation ............................................................................ 10 3.4.3 Receipt Temperature Evaluation ................................................................. 10 3.4.4 Analytical Method Checklist ...................................................................... 10 3.4.5 Reporting Limit Evaluation ........................................................................ 10 3.4.6 Trip Blank Evaluation ................................................................................. 10 3.4.7 QA/QC Evaluation for Routine Sample Duplicates ................................... 11 3.4.8 Radiologies Counting Error and Duplicate Evaluation .............................. 11 3.4.9 Other Laboratory QA/QC ........................................................................... 12 4.0 CORRECTIVE ACTION REPORT ...................................................................... 14 4.1 5.0 6.0 7.0 Assessment of Corrective Actions from Previous Period .................................. 14 TIME CONCENTRATION PLOTS ...................................................................... 14 ELECTRONIC DATA FILES AND FORMAT ................................................... 14 SIGNATURE AND CERTIFICATION ................................................................ 15 Table 1 Table 2 Table 3 LIST OF TABLES Summary of Well Sampling for the Period Exceedances and Acceleration Requirements GWCL Exceedances March 2019 to Present i INDEX OF TABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4AIB G-5AIB G-6AIB G-7A/B G-8AIB G-9AIB Field Data QA/QC Evaluation Holding Time Evaluation Laboratory Receipt Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QA/QC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map and Depth Data Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter 11 AWAL coc DWMRC EFRI GEL GWCLs GWDP LCS MS MSD QA QAP QC RPD SOPs USEPA ACRONYM LIST American West Analytical Laboratory Chain-of-Custody Utah Division of Waste Management and Radiation Control Energy Fuels Resources (USA) Inc. GEL Laboratories, Inc. Groundwater Compliance Limits Groundwater Discharge Permit Laboratory Control Spike Matrix Spike Matrix Spike Duplicate Quality Assurance Quality Assurance Plan Quality Control Relative Percent Difference Standard Operating Procedures United States Environmental Protection Agency iii 1.0 INTRODUCTION This is the Routine Groundwater Monitoring Report, as required under Part I.F. l of State of Utah Groundwater Discharge Permit No. UGW370004 (the "GWDP") for the third quarter of 2021 for Energy Fuels Resources (USA) Inc's. ("EFRI's") White Mesa Uranium Mill (the "Mill"). As required under Parts I.E. I, I.E.2, I.E.3, and I.E.5 of the GWDP, this Report includes recorded field measurements and laboratory analyses for well monitoring conducted during the quarter. 2.0 GROUNDWATER MONITORING 2.1 Samples and Measurements Taken During the Quarter A map showing the location of groundwater monitoring wells, piezometers, ex1stmg wells, chloroform contaminant investigation wells and nitrate contaminant investigation wells is attached under Tab A. Groundwater samples and measurements were taken during this repmting period, as discussed in the remainder of this section. 2.1.1 Groundwater Compliance Monitoring Groundwater samples and field measurements collected during the quarter included both quarterly and accelerated monitoring. Accelerated monitoring is discussed below in Section 2.1.2. In this report, samples classified as being collected quarterly include those wells which are routinely sampled every quarter as well as semi-annual wells which are sampled on an accelerated quarterly schedule due to exceedances reported in previous quarterly reports. Wells which are sampled routinely every quarter were analyzed for the parameters listed in Table 2 and Part I.E.1.d) 2)ii of the GWDP dated March 8, 2021. The semi-annual wells which have been accelerated to quarterly are analyzed only for those parameters which exceeded the Groundwater Compliance Limits ("GWCLs") in Table 2 described in previous reports and Exceedance Notices. Table 1 of this report provides an overview of wells sampled during the current period, along with the required sampling frequency applicable to each well during the current monitoring period, the date samples were collected from each well, and the date(s) analytical data were received from the contract laboratory(ies). Table 1 also indicates which sample numbers are associated with the required duplicates. 2.1.2 Accelerated Groundwater Monitoring Accelerated monthly sampling was also performed (quarterly wells accelerated to monthly), and results reported, for the wells indicated in Table 1. The accelerated sampling frequency, analyte list and well list were determined based on the previous analytical results as shown in Table 2 and previous Exceedance Notices. 1 As a result of the issuance of a revised GWDP on March 8, 2021, which sets revised GWCLs, requirements to perform accelerated monitoring under Part I.G. l of the previous GWDP ceased effective on March 8, 2021, and the effect of the issuance of the revised GWDP was to create a "clean slate" for constituents in some wells going forward. The GWCLs for some constituents were not 'reset" and continued on an accelerated sampling frequency as shown on Table 2. Table 1 provides an overview of the wells sampled for the accelerated monthly program along with the routine sampling frequency as well as the accelerated sampling frequency, the date samples were collected from each well, the associated duplicates and the date(s) which analytical data were received from the contract laboratory(ies). 2.1.3 Background Well Monitoring Monitor wells MW-38, MW-39, and MW-40 were installed in the first quarter 2018 pursuant to the March 19, 2019 GWDP Part l.H.2 and quarterly sampling commenced in fourth quarter 2018. The March 19, 2019 GWDP Part 1.H.3 required the completion of a background report for each of these wells after the completion of 8 quarters of sampling. The background reports and resultant GWCLs are to be calculated based on 8 statistically valid data points. The background report for wells MW-38, MW-39 and MW-40 was submitted to DWMRC on March 4, 2021. 2.1.4 Parameters Analyzed Routine quarterly groundwater monitoring samples were analyzed for the parameters listed in Table 2 and Part I.E.l.d) 2) ii of the GWDP. The accelerated monitoring samples were analyzed for a more limited and specific parameter list as shown in Table 2. 2.1.5 Groundwater Head Monitoring Depth to groundwater was measured in the following wells and/or piezometers, pursuant to Part I.E.3 of the GWDP: • The groundwater monitoring wells (including general monitoring wells, quarterly and semi-annual monitoring wells, and (MW-34). • Existing monitoring well MW-4 and the temporary chloroform investigation wells. • Piezometers -P-1, P-2, P-3A, P-4 and P-5. • Nitrate monitoring wells. 2 • The DR piezometers which were installed during the Southwest Hydrogeologic Investigation. • In addition to the above, depth to water measurements are routinely observed in conjunction with sampling events for wells sampled during quarterly and accelerated efforts, regardless of the sampling purpose. Water levels used for groundwater contour mapping were measured and recorded within 5 calendar days of each other as indicated by the measurement dates in the summary sheet under Tab D. 2.2 Field Data Attached under Tab B are copies of field data sheets recorded in association with the quarterly effort for the groundwater compliance monitoring wells referred to in paragraph 2.1.1, above. Sampling dates are listed in Table 1. Attached under Tab C, are copies of field data sheets recorded in association with the accelerated monthly monitoring sampling efforts, referred to in paragraph 2.1.2, above. Sampling dates are listed in Table 1. 2.3 Laboratory Results -Quarterly Sampling 2.3.1 Copy of Laboratory Results Analytical results are provided by two contract analytical laboratories: GEL and American West Analytical Laboratories ("AWAL"). Table 1 lists the dates when analytical results were reported to the Quality Assurance ("QA") Manager for each well. Results from analysis of samples collected under the GWDP (i.e., regular quarterly and accelerated semi-annual samples) are provided in Tab E. Also included under Tab E are the results of analyses for duplicate samples as identified in Table 1. 2.3.2 Regulatory Framework and Groundwater Background Under the GWDP, background groundwater quality has been determined on a well-by- well basis, as defined by the DWMRC-approved flowchart included in the Revised Background Groundwater Quality Report: Existing Wells for Denison Mines (USA) Corp. 's White Mesa Uranium Mill Site, San Juan County, Utah. GWCLs that reflect this background groundwater quality have been set for compliance monitoring wells except MW-38, MW-39, and MW-40. As discussed in Section 2.1.3 above, EFRI submitted the background report for MW-38, MW-39, and MW-40 March 4, 2021. 3 Exceedances of the GWCLs during the preceding quarter determined the accelerated monthly monitoring program implemented during this quarter as noted in Tables 1 and 2 as modified under the renewed GWDP. As a result of the issuance of a revised GWDP on March 8, 2021, which sets revised GWCLs, requirements to perform accelerated monitoring under Part I.G.1 of the previous GWDP ceased effective on March 8, 2021, and the effect of the issuance of the revised GWDP was to create a "clean slate" for constituents in some wells going forward. The GWCLs for some constituents were not 'reset" and continued on an accelerated sampling frequency as shown on Table 2. Exceedances of the GWCLs for this quarter are listed in Table 2 for sampling required under the both GWDPs. Accelerated requirements resulting from this quarter are highlighted for ease of reference. Table 3 documents the accelerated sampling program since the issuance of the March 19, 2019 GWDP. Because the quarter was split between two GWDPs, the information has been retained for this quarter. Beginning with the second quarter report, Table 3 will be limited to only the information collected starting March 8, 2021. It should be noted, however, that, because the GWCLs have been set at the mean plus second standard deviation, or the equivalent, un-impacted groundwater would normally be expected to exceed the GWCLs approximately 2.5% of the time. Therefore, exceedances are expected in approximately 2.5% of sample results, and do not necessarily represent impacts to groundwater from Mill operations. In fact, more frequent sampling of a given analyte will increase the number of exceedances due to statistical variation and not due to Mill activity. Additionally, given the slow velocity of groundwater movement, accelerated sampling monthly may result in resampling of the same water and may lead to repeat exceedances for accelerated constituents not due to Mill activities, but due to repeat sampling of the same water. 2.3.3 Compliance Status MW-12 MW-12 is west of MW-05 on the dike between Cell 3 and Cell 4B. When wells MW-05 and MW-12 were installed the top of the casing ("TOC") for both wells was above the ground surface by several feet. During the construction of the dike of Cell 4B several feet of fill dirt was placed around MW-05 and MW-12. MW-05 and MW-12 were not extended and the TOC of both MW-05 and MW-12 was slightly below the ground surface. MW-05 was extended in May 2017 in response to variable uranium concentrations likely caused by dust and dirt entering the well during sampling activities. Since MW-12 has reported exceedances of uranium similar to MW-05 and due to the proximity of MW-12 to MW-05, prior to completing a Source Assessment Report ("SAR"), EFRI believes it is appropriate to first address potential physical causes. 4 In an effort to address potential physical causes of the exceedances, EFRI made changes to the casing and surrounding area in October 2020. The TOC for MW-12 was slightly below the ground surface and may have inadvertently allowed dust and dirt to enter the well during sampling activities. To address this issue EFRI extended the TOC several feet and regraded the area surrounding the well. After the TOC was extended, the well was overpumped to remove any dirt which may have been introduced during these field activities. These activities were completed after the third quarter 2020 sampling event was conducted. EFRI submitted a Plan and Time Schedule as required by the GWDP for MW-12 to address consecutive exceedances of uranium and selenium in MW-12. The Plan and Time Schedule stated that EFRI would continue accelerated monitoring of selenium and uranium in MW-12 for four quarters beginning with the fourth quarter 2020 through the third quarter 2021. Progress and results will be discussed in the routine quarterly groundwater reports. The Plan and Time Schedule noted that future actions, if necessary, will be discussed in the third quarter 2021 groundwater report and that if the exceedances continue, a separate P&TS will be submitted for DWMRC approval. The third quarter MW-12 results for selenium and uranium were below their respective GWCLs. No further actions for MW-12 are required and no additional Plan and Time Schedule or SAR are required at this time. Results for MW-12 will continue to be reported in the quarterly reports until 8 consecutive results below the GWCL have been collected at which time, EFRI will request removal of those parameters from accelerated monitoring. 2.4 Laboratory Results -Accelerated Monitoring 2.4.1 Copy of Laboratory Results Results from analysis of samples collected for the monthly accelerated sampling (j.e. quarterly accelerated to monthly) are provided in Tab F. Also included under Tab Fare the results of analyses for duplicate samples for this sampling effort, as identified in Table 1. 2.4.2 Regulatory Framework and Groundwater Background As a result of the issuance of a revised GWDP on March 8, 2021, which sets revised GWCLs for some constituents, requirements to perform accelerated monitoring under Part I.G.l of the previous GWDP for certain constituents ceased effective March 8, 2021, and the effect of the issuance of the revised GWDP was to create a "clean slate" for certain constituents in a limited list of wells going forward. This means that accelerated monitoring during this quarter was required under the revised GWDP for constituents which did not have revised GWCLs included in the current GWDP. 5 2.4.3 Compliance Status Analytes that have exceeded the GWCLs for this quarter as set forth in the GWDP are summarized in Table 2. The analytes which exceeded their respective GWCLs during the quarter will be sampled on an accelerated schedule as noted in Table 2. Table 3 summarizes the results of the accelerated sampling program since the March 19, 2019 GWDP for the reasons stated in Section 2.3.2 above. Part I.G.4 c) of the GWDP states, with respect to exceedances of GWCLs, "The Permittee shall prepare and submit within 30 calendar days to the Director a plan and a time schedule for assessment of the sources, extent and potential dispersion of the contamination, and an evaluation of potential remedial action to restore and maintain groundwater quality to insure that Permit limits will not be exceeded at the compliance monitoring point and that DMT or BAT will be reestablished." EFRI submits an Exceedance Notice quarterly and the summary in the Exceedance Notice includes, for each exceedance, a brief discussion of whether such a plan and schedule is required at this time in light of other actions currently being undertaken by EFRI. The determination of whether a Plan and Time Schedule is required is based on discussions with DWMRC Staff in teleconferences on April 27 and May 2, 2011 and the constituents covered by previously submitted Source Assessment Reports. 2.5 Depth to Groundwater and Water Table Contour Map As stated above, a listing of groundwater level readings for the quarter (shown as depth to groundwater in feet) is included under Tab D. The data from Tab D has been interpreted (kriged) and plotted in a water table contour map, provided under Tab H. The water table contour map provides the location and identity of the wells and piezometers for which depth to groundwater is recorded. The groundwater elevation at each well and piezometer, measured in feet above mean sea level, and isocontour lines to delineate groundwater flow directions observed during the quarter's sampling event are displayed on the map. 3.0 QUALITY ASSURANCE AND DATA VALIDATION The Mill QA Manager performed a QA/QC review to confirm compliance of the monitoring program with requirements of the Groundwater Monitoring Quality Assurance Plan ("QAP"). As required in the QAP, data QA includes preparation and analysis of QC samples in the field, review of field procedures, an analyte completeness review, and quality control review of laboratory data methods and data. Identification of field QC samples collected and analyzed is provided in Section 3.1. Discussion of adherence to Mill sampling Standard Operating Procedures ("SOPs") is provided in Section 3.2. Analytical completeness review results are provided in Section 3.3. The steps and tests applied to check laboratory data QA/QC are discussed in Sections 3.4.4 through 3.4.9 below. 6 The Analytical Laboratories have provided summary reports of the analytical QA/QC measurements necessary to maintain conformance with National Environmental Laboratory Accreditation Conference certification and repmting protocol. The analytical laboratory QA/QC Summary Reports, including copies of the Mill's COC and Analytical Request Record forms for each set of Analytical Results, follow the analytical results under Tabs E and F. Review of the laboratory QA/QC information is provided under Tab G. 3.1 Field QC Samples The following field QC samples were generated by Mill personnel and submitted to the analytical laboratory in order to assess the quality of data resulting from the field sampling program: One duplicate sample was collected during quarterly sampling as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same parameters as permit-required samples. One duplicate sample was collected during each of the monthly sampling events as indicated in Table 1. The QC samples were sent blind to the analytical laboratory and analyzed for the same accelerated parameters as the parent sample. One trip blank was provided by AW AL and returned and analyzed with the quarterly monitoring samples. One trip blank for each of the monthly accelerated sample events was provided by AWAL and returned and analyzed with the accelerated monthly monitoring samples. Rinsate samples were not collected during the quarter because equipment used during sample collection was dedicated and did not require decontamination. All wells except MW-20, MW-37 and MW-38 have dedicated pumps for purging and sampling and as such no rinsate blanks samples are required. MW-20, MW-37 and MW-38 were purged and sampled with a disposable bailer and no rinsate blank was required. A deionized field blank was not required because equipment decontamination was not required and deionized water was not used during this sampling event. 3.2 Adherence to Mill Sampling SOPs On a review of adherence by Mill personnel to the existing sampling SOPs, the QA Manager observed that QA/QC requirements established in the QAP were met and that the SOP's were implemented as required. 3.3 Analyte Completeness Review Analyses required by the GWDP for the quarterly and semi-annual wells were performed. The accelerated sampling for the semi-annual wells (semi-annual to quarterly) was 7 completed as required by the GWDP and as shown in Tables 2 and 3. The accelerated quarterly sampling (quarterly to monthly) required for this quarter, as shown in Tables 2 and 3, was performed as required. The monthly accelerated sampling program shown on Tables 2 and 3 is required as a result of exceedances in quarterly well monitoring results reported in previous quarters. 3.4 Data Validation The QAP and GWDP identify the data validation steps and data quality control checks required for the groundwater monitoring program. Consistent with these requirements, the QA Manager completed the following evaluations: a field data QA/QC evaluation, a receipt temperature check, a holding time check, an analytical method check, a reporting limit check, a trip blank check, a QA/QC evaluation of routine sample duplicates, a QA/QC evaluation of accelerated sample duplicates, a gross alpha counting error evaluation and a review of each laboratory's reported QA/QC information. Each evaluation is discussed in the following sections. Data check tables indicating the results of each test are provided under Tab G. 3.4.1 Field Data QA/QC Evaluation The QA Manager performs a review of field recorded parameters to assess their adherence with QAP requirements. The assessment involved review of two sources of information: the Field Data Sheets and the Quarterly Depth to Water summary sheet. Review of the Field Data Sheets addresses well purging volumes and the stability of the following field parameters (based upon the purging method chosen): specific conductance, pH, temperature, redox potential, dissolved oxygen ("DO") and turbidity. Stability of field parameters and well sampling techniques are dependent on the purging technique employed. Review of the Depth to Water data confirms that depth measurements were conducted within a five-day period. The results of this quarter's review are provided in Tab G. There are three purging strategies specified in the QAP that are used to remove stagnant water from the casing during groundwater sampling at the Mill. The three strategies are as follows: 1. Purging three well casing volumes with a single measurement of field parameters 2. Purging two casing volumes with stable field parameters (within 10% [Relative Percent Difference] ("RPD")) 3. Purging a well to dryness and stability (within 10% RPD) of a limited list of field parameters after recovery During both the quarterly sampling event and the two monthly events, the purging technique used was two casing volumes with stable field parameters (pH, Conductivity, Redox, temperature, DO, and turbidity) except for the following wells that were purged to dryness: MW-24, MW-24A and MW-38. 8 MW-24, MW-24A, and MW-38 conformed to the QAP requirement for sampling low yield wells which includes the collection of three field parameters (pH, specific conductance ["conductivity"] and temperature) immediately prior to and immediately following sample collection. Stabilization of pH, conductivity and temperature were within the 10% RPD required by the QAP. MW-24, MW-24A, and MW-38 were purged to dryness and the low yield sampling procedures were used for the collection of field parameters. Stabilization of pH, conductivity and temperature were within the 10% RPD required by the QAP for well MW-24, MW-24A, and MW-38. Additionally, two casing volumes were not purged from MW-26, prior to sampling because MW-26 is a continuously pumped well. If a well is continuously pumped, it is pumped on a set schedule per the remediation plan and is considered sufficiently evacuated to immediately collect a sample; however, if a pumping well has been out of service for 48 hours or more, EFRI follows the purging requirements outlined in Attachment 2-3 of the QAP. The review of the field sheets for compliance with QAP requirements resulted in the observations noted below. The QAP requirements in Attachment 2-3 specifically state that field parameters must be stabilized to within 10% over at least two consecutive measurements. The QAP Attachment 2-3 states that turbidity should be less than 5 NTU prior to sampling unless the well is characterized by water that has a higher turbidity. The QAP Attachment 2-3 does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements greater than 5 NTU below are included for information purposes only. • Turbidity measurements were less than 5 NTU for the quarterly and semi-annual wells except MW-11, MW-25, MW-29, and MW-32. Per the QAP, Attachment 2- 3, turbidity measurements prior to sampling were within a 10% RPD for the quarterly and semi-annual wells. • Turbidity measurements were less than 5 NTU for the accelerated sampling wells except MW-31 in the August monthly event and MW-11 in the September monthly event. Turbidity measurements prior to sampling were within a 10% RPD for the accelerated sampling wells. The other field parameters (conductance, pH, redox potential, DO, and temperature) for the wells were within the required RPD for the quarterly, semi-annual and accelerated sampling. During review of the field data sheets, it was observed that sampling personnel consistently recorded depth to water for the quarterly, semi-annual and accelerated sampling programs to the nearest 0.01 foot. EFRI's letter to DWMRC of March 26, 2010 discusses further why turbidity does not appear to be an appropriate parameter for assessing well stabilization. In response to 9 DWMRC's subsequent correspondence dated June 1, 2010 and June 24, 2010, EFRI has completed a monitoring well redevelopment program. The redevelopment report was submitted to DWMRC on September 30, 2011. DWMRC responded to the redevelopment report via letter on November 15, 2012. Per the DWMRC letter dated November 15, 2012, the field data generated this quarter are compliant with the turbidity requirements of the approved QAP. 3.4.2 Holding Time Evaluation QAP Table 1 identifies the method holding times for each suite of parameters. Sample holding time checks are provided under Tab G. The samples were received and analyzed within the required holding time. All accelerated samples were received and analyzed within the required holding time. 3.4.3 Receipt Temperature Evaluation COC sheets were reviewed to confirm compliance with the QAP requirement in Table 1 that samples be received at 6°C or lower. Sample receipt temperature checks are provided under Tab G. The quarterly, semi-annual and accelerated samples were received within the required temperature limit. As noted in Tab G, samples for gross alpha analyses were shipped without using ice. Per Table 1 in the approved QAP, samples submitted for gross alpha analyses do not have a sample temperature requirement. 3.4.4 Analytical Method Checklist The analytical methods reported by both laboratories were checked against the required methods specified in the QAP. Analytical method check results are provided in Tab G. The review indicated that the quarterly, semi-annual and accelerated samples were analyzed in accordance with Table 1 of the QAP. 3.4.5 Reporting Limit Evaluation The analytical method RLs reported by both laboratories were checked against the RLs specified in the QAP Table 1. RL evaluations are provided in Tab G. The analytes were measured and reported to the required RLs except that several sets of quarterly, semi- annual and accelerated sample results had the RL raised for at least one analyte due to matrix interference and/or sample dilution as noted in Section 3.4.9. In all cases the reported value for the analyte was higher than the increased RL. 3.4.6 Trip Blank Evaluation The trip blank results were reviewed to identify any VOC sample contamination which is the result of sample handling and shipment. Trip blank evaluations are provided in Tab 10 G. The trip blank results associated with the quarterly, semi-annual and accelerated samples were all nondetect for VOCs. 3.4.7 QA/QC Evaluation for Routine Sample Duplicates Section 9 .1.4 a) of the QAP states that RPDs will be calculated for the comparison of duplicate and original field samples. The QAP acceptance limits for RPDs between the duplicate and original field sample is less than or equal to 20% unless the measured results are less than 5 times the detection limit. This standard is based on the EPA Contract Laboratory Program National Functional Guidelines for Inorganic Data Review, February 1994, 9240.1-05-01 as cited in the QAP. The RPDs are calculated for the duplicate pairs for all analytes regardless of whether or not the reported concentrations are greater than 5 times the required detection limits; however, data will be considered noncompliant only when the results are greater than 5 times the required detection limit and the RPD is greater than 20%. The additional duplicate information is provided for information purposes. Field duplicate sample results were assessed as required by the SOP. Duplicate results for the quarterly and semi-annual samples were within the acceptance limits specified in the QAP except for cadmium and zinc in duplicate pair MW-14/MW-65. The cadmium and zinc results were greater than 20% RPD, however, the sample and duplicate results were not greater than 5 times the RL and as such are acceptable. Field duplicate results are shown in Attachment G. The duplicate results were within a 20% RPD in the accelerated samples except for total dissolved solids ("TDS") in duplicate pair MW-31/MW-65. The approved QAP specifies a separate corrective action for duplicate RPDs outside of acceptance limits. The revised procedure for duplicate results outside of acceptance limits was implemented for the results outside of the acceptance limits. The corrective actions that were taken in accordance with the QAP procedure are as follows: the QA Manager contacted the Analytical Laboratory and requested a review of the raw data to assure that there were no transcription errors and the data were accurately reported. The laboratory noted that the data were accurate and reported correctly. Reanalysis was not completed as the samples were out of holding time. Results of the RPD test are provided under Tab G. 3.4.8 Radiologies Counting Error and Duplicate Evaluation Section 9 .14 of the QAP require that gross alpha analysis be reported with an activity equal to or greater than the GWCL and shall have a counting variance that is equal to or less than 20% of the reported activity concentration. An error term may be greater than 20% of the reported activity concentration when the sum of the activity concentration and error term is less than or equal to the GWCL. The quarterly.and semi-annual radiologic sample results met the counting error requirements specified in the QAP. Section 9.4 of the QAP also requires a comparability check between the sample and field duplicate sample results utilizing the formula provided in the text. 11 Results of quarterly and semi-annual, radiologic sample QC are provided under Tab G. The quarterly and semi-annual sample results met the duplicate counting error requirements specified in the QAP. 3.4.9 Other Laboratory QA/QC Section 9.2 of the QAP requires that the laboratory's QNQC Manager check the following items in developing data reports: (1) sample preparation information is correct and complete, (2) analysis information is correct and complete, (3) appropriate analytical laboratory procedures are followed, (4) analytical results are correct and complete, (5) QC samples are within established control limits, (6) blanks are within QC limits, (7) special sample preparation and analytical requirements have been met, and (8) documentation is complete. In addition to other laboratory checks described above, EFRI's QA Manager rechecks QC samples and blanks (items (5) and (6)) to confirm that the percent recovery for spikes and the relative percent difference for spike duplicates are within the method-specific required limits, or that the case narrative sufficiently explains any deviation from these limits. Results of this quantitative check are provided under Tab G. The lab QNQC results from both GEL and AW AL samples for compounds regulated under the GWDP met these requirements. The check samples included at least the following: a method blank, a laboratory control spike ("LCS"), a matrix spike ("MS") and a matrix spike duplicate ("MSD"), or the equivalent, where applicable. It should be noted that: • Laboratory fortified blanks are equivalent to LCSs. • Laboratory reagent blanks are equivalent to method blanks. • Post digestion spikes are equivalent to MSs. • Post digestion spike duplicates are equivalent to MSDs. • Laboratory Duplicates are equivalent to MSDs. The qualifiers, and the corresponding explanations reported in the QNQC Summary Reports for the check samples for the analytical methods were reviewed by the QA Manager. The QAP, Section 8.1.2 requires that a MS/MSD pair be analyzed with each analytical batch. The QAP does not specify acceptance limits for the MS/MSD pair, and the QAP does not specify that the MS/MSD pair be prepared on EFRI samples only. Acceptance limits for MS/MSDs are set by the laboratories. The review of the information provided by the laboratories in the data packages verified that the requirements in the QAP to analyze a MS/MSD pair with each analytical batch was met. While the QAP does not require it, the recoveries were reviewed for compliance with the laboratory established acceptance limits. The QAP does not require this level of review and the results of this review are provided for information only. 12 The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the quarterly and semi-annual samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The requirement in the QAP to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The information from the Laboratory QA/QC Summary Reports indicates that the MS/MSDs recoveries and the associated RPDs for the accelerated samples were within acceptable laboratory limits for the regulated compounds except as indicated in Tab G. The data recoveries and RPDs which are outside the laboratory established acceptance limits do not affect the quality or usability of the data because the recoveries and RPDs above or below the acceptance limits are indicative of matrix interference most likely caused by other constituents in the samples. Matrix interferences are applicable to the individual sample results only. The requirement in the QAP to analyze a MS/MSD pair with each analytical batch was met and as such the data are compliant with the QAP. The QAP specifies that surrogate compounds shall be employed for all organic analyses but the QAP does not specify acceptance limits for surrogate recoveries. The information from the Laboratory QA/QC Summary Reports indicates that the surrogate recoveries for the quarterly and accelerated samples were within acceptable laboratory limits for the surrogate compounds. The information from the Laboratory QA/QC Summary Reports indicates that the LCS recoveries for both the quarterly and accelerated samples were within acceptable laboratory limits for the LCS compounds as noted in Tab G. The QAP, Section 8.1.2 requires that each analytical batch shall be accompanied by a method blank. The analytical batches routinely contain a blank, which is a blank sample made and carried through all analytical steps. For the Mill samples, a method blank was prepared for the analytical methods. Per the approved QAP, contamination detected in analysis of method blanks will be used to evaluate any analytical laboratory contamination of environmental samples. The QAP states that non-conformance conditions will exist when contaminant levels in the samples(s) are not an order of magnitude greater than the blank result. The method blanks for the quarterly samples and the accelerated samples reported no detections of any analyte. Method blank results are included in Tab E and Tab F. Laboratory duplicates are completed by the analytical laboratories as required by the analytical method specifications. Acceptance limits for laboratory duplicates are set by the laboratories. The QAP does not require the completion of laboratory duplicates or the completion of a QA assessment of them. EFRI reviews the QC data provided by the 13 laboratories for completeness and to assess the overall quality of the data provided. Duplicate results are included in the analytical data. The information from the Laboratory QA/QC Summary Reports indicates that there were Continuing Calibration Verification ("CCV") samples outside of the laboratory acceptance limits. The information from the Laboratory QA/QC Summary Reports indicates that there were low Continuing Calibration Verification ("CCV") recoveries for 2-butanone. The CCV recovery affected samples MW-11, MW-14, MW-24, MW-24A, MW-25, MW-26, MW- 30, MW-31, MW-36, MW-39, MW-40, MW-65, and the trip blank. The data were flagged in accordance with the changes specified in EPA Method 8260D. The flagging requirements are new to the revised method and do not adversely affect the data. The data are usable for the intended purpose because butanone has not been detected in samples collected at the Mill and the data are accurate. 4.0 CORRECTIVE ACTION REPORT There are no corrective actions required during the current monitoring period. 4.1 Assessment of Corrective Actions from Previous Period No corrective actions were identified in the previous report. 5.0 TIME CONCENTRATION PLOTS Time concentration plots for each monitoring well for the following constituents: chloride, fluoride, sulfate, and uranium, are included under Tab I. The data points collected to date are reflected on the plots. Time concentration plots included with quarterly groundwater reports prior to and including first quarter 2012 did not include data that were determined to be outliers using the statistical methods used for the background determinations at the Mill. Based on conversations with DWMRC, all of the data have been included in the quarterly time concentration plots since first quarter 2012. 6.0 ELECTRONIC DATA FILES AND FORMAT EFRI has provided to the Director electronic copies of the laboratory results from groundwater quality monitoring conducted during the quarter in Comma Separated Values format, from the analytical laboratories. A copy of the transmittal e-mail is included under Tab J. 14 7.0 SIGNATURE AND CERTIFICATION This document was prepared by Energy Fuels Resources (USA) Inc. Energy Fuels Resources (USA) Inc. By: Scott A. Bakken 1ul:2~ s Date Vice President, Regulatory Affairs 15 Certification: I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. Scott A. Bakken Vice President, Regulatory Affairs Energy Fuels Resources (USA) Inc. 16 Tables T bl IS a e : ummary o e am :>.mg or f W II S r f Q3 2021 Normal Purpose for sampling Well Frequency this quarter Sample Date Date of Lab Re~ort MW-11 Quarterly Quarterly 7/27/2021 (8/24/2021) [8/27/2021] MW-12 Semi-annually Semi-annually 7/21/2021 (8/10/2021) MW-14 Quarterly Quarterly 7/27/2021 (8/24/2021) [8/27/2021] MW-24 Semi-annually Semi-annually 7/29/2021 (8/24/2021) [8/27/2021] MW-24A Semi-annually Semi-annually 7/29/2021 (8/24/2021) [8/27/2021] MW-25 Quarterly Quarterly 7/28/2021 (8/24/2021) [8/27/2021] MW-26 Quarterly Quarterly 7/28/2021 (8/24/2021) [8/27/2021] MW-27 Semi-annually Semi-annually 7/22/2021 (8/16/2021) (9/30/2021) MW-28 Semi-annually Semi-annually 7/23/2021 (8/16/2021) (9/30/2021) MW-29 Semi-annually Semi-annually 7/22/2021 (8/16/2021) (9/30/2021) MW-30 Quarterly Quarterly 7/29/2021 (8/24/2021) [8/2712021 J MW-31 Quarterly Quarterly 7/27/2021 (8/24/2021) [8/27/2021] MW-32 Semi-annually Semi-annually 7/28/2021 (8/24/2021) MW-36 Quarterly Quarterly 7/27/2021 (8/24/2021) [8/27/2021] MW-38 Quarterly Background 7/29/2021 (8/24/2021) [8/27/2021] MW-39 Quarterly Background 7/28/2021 (8/24/2021) [8/27/2021] MW-40 Quarterly Background 7/28/2021 (8/24/202 l) [8/2712021] MW-65 1 per Batch Duplicate ofMW-14 7/27/2021 (8/24/2021) [8/2712021] Accelerated August Monthly MW-11 Monthly Accelerated 8/10/2021 (8/30/2021) MW-26 Monthly Accelerated 8/10/2021 (8/30/2021) MW-30 Monthly Accelerated 8/9/2021 (8/30/2021) MW-31 Monthly Accelerated 8/9/2021 (8/30/2021) MW-65 Monthly Duplicate of MW-30 8/9/2021 (8/30/2021 ) Accelerated September Monthly MW-II Monthly Accelerated 9/7/2021 (9/24/2021) MW-26 Monthly Accelerated 9/9/2021 (9/24/2021) MW-30 Monthly Accelerated 9/8/2021 (9/24/2021) MW-31 Monthly Accelerated 9/7/2021 (9/24/2021) MW-65 I per Batch Duplicate ofMW-31 9/7/2021 (9/24/2021) Notes: When more than I date is shown for a certain laboratory, the date(s) in italics are the resubmission dates. Resubmissions were required to correct reporting errors or to address reanalyses. Date in parenthesis depicts the date that data were reported from American West Analytical Laboratories (A WAL). Date in brackets depicts the date the data were reported from GEL Laboratories. Table 2 Exceedances and Acceleration RcquiremcnlS Monitoring Well GWCLin First Result Routine Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Current Exceeding the (Water Class) GWDP GWCL Frequency Frequency Sample Period Monitoring Quartedy Wells Accelerated to Monlhly Sampling MW-I I (Class II) Total Dissolved Solids (mg/L) 2528 2680 Quarterly Monthly Q3 2021 November 2021 Manganese (uwl.) 237 376 Quarterly Monthly Q3 2021 November 2021 Chloride (mg/L) 39.16 48.4 Quarterly Monthly Q3 2019 Q4 2019 (November) Sulfate (mg/L) 1309 1410 Quarterly Monthly Q3 2019 Q4 2019 (November) MW-25 (Class Ill) Total Dissolved Solids (mg/L) 2976 3100 Quarterly Monthly Q3 2021 November 2021 MW-26 (Class III) Nitrate+ Nitrite (ns N) (mg/L) 0.62 1.3 Quarterly Monthly QI 2010 May2010 Chloroform (usefl.,) 70 700 Quarterly Monthly QI 2010 May 2010 Total Dissolved Solids (mg/L) 3284.19 3390 Quarterly Monthly Q3 2021 November 2021 Chloride (mg/L) 58.31 72 Quarterly Monthly QI 2010 May2010 Carbon Tetrachloride (ug/L) 5 26.1 Quarterly Monthly QI 2021 Q2 2021 Methylene Chloride (ug/L) 5 6.59 Quarterly Monthly Q3 2020 August 2020 MW-30 (Class II) Nitrate+ Nitrite (as N) (ml(/L) 2.5 16.1 Quarterly Monthly QI 2010 May 2010 Chloride (mg/L) 128 134 Quarterly Monthly Ql 2011 May201 l Total Dissolved Solids (mg/L) 1918 2010 Quarterly Monthly Q3 2021 November 2021 Selenium (ug/L) 53.6 56.3 Quarterly Monthly Ql 2021 Q2 2021 Uranium (ug/L) 9.82 10.2 Quarterly Monthly QI 2021 Q2 2021 MW-31 (Class Ill) Nitrate+ Nitrite (n.s N) (mg/L) 5 21.7 Quarterly Monthly QI 2010 May2010 Total Dissolved Solids (mg/L) 2132 2580 Quarterly Momhly Q3 2019 Q4 2019 (November) Uranium (ug/L) 15 15.5 Qunncrly Monthly Q2 2020 Augusi 2020 Sulfate (mg/L) 993 1150 Qunncrly Monthly Q3 2019 Q4 2019 (No,·ember) Chloride (mg/L) 143 145 Quarterly Monthly Ql 2011 May201 l Semi-Annual Wells Accelerated to Quarterly Sampling Monitoring Well GWCLin First Result Sample Accelerated Exceedance Start of Accelerated Constituent Exceeding GWCL Current Exceeding the (Water Class) GWDP GWCL Frequency Frequency Sample Period Monitoring MW-12 (Class III) Uranium (ul?/L) 23.5 23.7 Semi-Annually Quarterly Q2 2017 Q3 2017 Selenium (ug/L) 39 41.2 Semi-Annually Quarterly Q2 2020 Q3 2020 MW-24 (Class III) Cadmium (ug/L) 6.43 6.97 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) Beryllium (uWL) 2 2.42 Semi-Annually Quarterly Q4 2017 Ql 2018 Thallium (ug/L) 2.01 2.44 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) Nickel (ug/L) 50 57.7 Semi-Annually Quarterly Q4 2018 Q3 2019 Sulfate (mg/L) 2903 2960 Semi-Annually Quarterly QI 2020 Q3 2020 Mnngnnesc (ug/L) 7507 7700 Semi-Annually Quarterly Q42019 Ql 2020 Fluoride (mg/L) 0.47 0.797 Semi-Annually Quarterly Q4 2018 Q3 201 9 Gross Alpha (pCi/L) 7.5 9.03 Semi-Annually Quarterly Q42020 Q3 2021 TDS (mg/L) 4450 4460 Semi-Annually Quarterly Q2 2021 Q3 2021 Field pH (S.U.) 5.03 4.45 Semi-Annually Quarterly Q2 2018 Q3 2018 (September) MW-27 (Class Ill) Nitrate+ Nitrite (as N) (mg/L) 5.6 5.8 Semi-Annually Quarterly Q2 2010 Q3 2010 MW-28 (Class Ill) Chloride (mg/L) 105 108 Semi-Annually Quarterly Q2 2010 Q3 2010 Nitrate+ Nitrite (as N) (mg/L) 5 5.14 Semi-Annually Quarterly Q4 2019 Q3 2020 Selenium (ug/L) 11.1 12.4 Semi-Annually Quarterly Q2 2019 Q3 2019 Cadmium (ug/L) 5.2 5.41 Semi-Annually Quarterly Q2 2014 Q42014 Uranium (ug/L) 4.9 61.3 Semi-Annually Quarterly Q2 2014 Q42014 MW-29 (Class Ill) Uranium (ug/L) 15 15.3 Semi-Annually Quarterly Q4 2020 Q3 2021 MW-32 (Class III) Chloride (mg/L) 35.99 36.3 Semi-Annually Quarterly Q2 2014 (QI Q2 2014 2015) Notes: Highlighted text shows accelerated requirements resulting from Q3 2021 sampling event. Monitoring Well (Water Constituent Exceeding GWCL Class) Chloride (mg/L) MW-11 Manganese (ug/L) (Class II) Sulfate (mg/L) TDS (mg/L) MW-25 (Class TDS (mg/L) III) Nitrate+ Nitrite (as N) (mJ?/L) Chloroform (ug/L) MW-26 Chloride (mwl.) (Class III) TDS (mg/L) Carbon Te1rachlorido:: Me1hvlene Chloride (ug/L) Nitrate + Nitrite (as N) (mg/L) MW-30 Chloride (mg/L) (Class II) Selenium (ug/L) TDS (mg/L) Uranium (u,g;/L) Nitrate+ Nitrite (as N) (mg/L) MW-31 Sulfate (mg/L) (Class III) TDS (mg/L) Uranium (uJ?/L) Chloride (m_g/L) MW-12 Uranium (ug/L) (Class III) Selenium (ug/L) Beryllium (ug/L) Cadmium (ug/L) Fluoride (m!!IL) MW-24 Nickel (mg/L) (Class III) Man2ane.~c (u,1L) Thallium (ug/L) Gross Aloha (oCj/L) Sulfate (mg/L) TDS (ml?/L) Field pH (S.U.) MW-27 (Class Ill) Nitrate+ Nitrite (as N) (mg/L) Chloride (mg/L) MW-28 Selenium (uwL) (Class Ill) Nitrate+ Nitrite (as N) (mf?IL) Uranium (u,1L) MW-29 Uranium (ug/L) (Class JJ!) MW-32 (Class !II) Chloride (mg/L) Notes: NS= Not Required and Not Sampled NA= Not Applicable GWCLin March 8, Ql 2021 2021 Sample Date GWDP 39.16 237 1/12/2021 1309 2528 2976 1/11/2021 0.62 70 58.31 3284.19 1/14/2021 5 5 2.5 128 53.6 1/11/2021 1918 9.82 5 993 2132 1/12/2021 15 143 I• 23.5 1/14/2021 39 2 6.43 0.47 50 7507 1/14/2021 2.01 7.5 2903 4450 5.03 -8.5 5.6 1/14/2021 105 11.l 1/15/2021 5 4.9 15 l/15/202 l 35.39 1/14/2021 Table 3 -GWCL Exceedances under the March 8, 2021 GWDP Ql 2021 Results February February March 2021 March 2021 Ql 2021 2021 2021 Monthly Monthly Q22021 Result Monthly Monthly Sample Date Result Sample Date Sample Date Result Required Quarterly Samp.ling Wells 46.4 46.4 46.9 185 254 221 2/9/2021 /8/202 1 4/20/2021 1140 1260 1270 2010 2160 1950 2660 NS NA NS NA 4/14/2021 0.619 0.764 0.617 2200 1930 2190 57.4 71.3 63.9 3100 2/10/2021 2700 3/9/2021 3060 4/21/2021 26.l NA NA 7.65 3.43 1.27 17.7 14.3 17.0 184 189 192 '55.f.,I 2/10/202! .·:: '55.J; 3/9/2021 56.3 4/14/2021 1660 NA NA :.'~ -~.!.--;~~-.]·~ 10.2 17.1 14.3 17.4 1070 1130 1210 2460 2/9/2021 2960 3/8/2021 2400 4/13/2021 19.7 22.2 20.2 354 380 388 Required Semiannual Sampling Wells 25.0 35.l NS NA NS NA 4/20/2021 2.75 NA NA 8.79 NA NA 0.916 NA NA 70.4 NA NA 7460 NS NA NS NA 4/29/2021 2.74 NA NA 2.94 NA NA 2980 NA NA 4260 NA NA 5.08 NA NA 5.16 NS NA NS NA 4/15/2021 128 NA NA 14.0 NS NA NS NA 4/15/2021 3.44 NA NA 10.3 NA NA 16.9 NS NA NS NA 4/14/2021 36.9 NS NA NS NA 4/!3/2021 Q2 2021 Results Q3 2021 Results May 2021 May 2021 June 2021 June 2021 Q32021 August2021 August 2021 September September Q22021 Monthly Monthly Monthly Monthly Sample Q3 2021 Monthly Monthly 2021 2021 Result Sample Date Result Sample Date Result Date Result Sample Date Result Monthly Monthly Sample Date Result Required Quarterly Sampling Wells Required Quarterly Sampling Wells 47.7 46.4 52.1 48.3 57.0 49.6 237 NA NA 376 NA NA 5/10/2021 6/8/2021 7/27/2021 8/10/2021 9/7/2021 1290 1280 1270 1470 1370 1240 2110 2190 1960 2680 NA NA 2720 NS NA NS NA 7/28/2021 3100 NS NA NS NA 1.42 1.06 0.368 0.352 1.42 0.710 777 733 1590 723 996 516 57.5 69.6 54.9 54.0 61.4 59.3 2790 5/11/2021 NA 6/8/2021 NA 7/28/2021 3390 8/10/2021 NA 9/9/2021 NA <1.00 <l.00 <l.00 <1.00 <1.00 <1.00 <l.00 <l.00 1.90 <l.00 1.25 <1.00 17.7 18.6 17.0 20.6 16.5 15.4 162 188 170 188 161 183 55.7 5/11/2021 58.3 6/8/2021 54.1 7/29/2021 56.3 8/9/2021 56.1 9/8/2021 60.4 1580 NA NA 2010 NA NA 10.3 10.7 9.84 9.60 9.38 9.74 18.6 18.9 20.6 18.7 15.7 16.0 1170 1200 1170 1210 1130 1130 2300 5/10/2021 2610 6/7/2021 2400 7/27/2021 3100 8/9/2021 2600 9/7/2021 2870 20.1 21.7 20.8 20.0 19.3 20.2 377 384 374 391 365 356 Required Semiannual Sampling Wells Required Semiannual Sampling Wells 22.9 28.8 NS NA NS NA 7/21/2021 22.2 32.4 NS NA NS NA 2.78 NA NA 2.71 NA NA 8.08 NA NA 9.26 NA NA 0.925 NA NA 1.4 NA NA 72.4 NA NA 76.7 NA NA 7540 NS NA NS NA 7/29/2021 7890 NS NA NS NA 3.02 NA NA 2.91 NA NA 3.18 NA NA l.92 NA NA 2960 NA NA 3050 NA NA 4460 NA NA 4940 NA NA 5.00 NA NA 5.85 NA NA 6.57 NS NA NS NA 7/22/2021 6.32 NS NA NS NA 144 NA NA 152 NA NA 13.4 NS NA NS NA 7/23/2021 18.5 NS NA NS NA 4.09 NA NA 6.09 NA NA 8.52 NA NA 13.80 NA NA 16.2 NS NA NS NA 7/22/2021 15.8 NS NA NS NA 31.8 NS NA NS NA 7/28/2021 36.5 NS NA NS NA INDEX OFT ABS Tab A Site Plan and Perched Well Locations White Mesa Site Tab B Field Data Worksheets Quarterly Sampling Tab C Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring, August 2021 Tab C2 Field Data Worksheets Accelerated Monitoring, September 2021 Tab D Quarterly Depth to Water Tab E Laboratory Analytical Reports -Quarterly Sampling Tab F Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring, August 2021 Tab F2 Laboratory Analytical Reports -Accelerated Monitoring, September 2021 Tab G Quality Assurance and Data Validation Tables G-lA/B G-2A/B G-3A/B G-4A/B G-5A/B G-6A/B G-7A/B G-8 A/B G-9AIB Field Data QNQC Evaluation Holding Time Evaluation Laboratory Temperature Check Analytical Method Check Reporting Limit Evaluation Trip Blank Evaluation QNQC Evaluation for Sample Duplicates Radiologies Counting Error Laboratory Matrix QC Tab H Kriged Current Quarterly Groundwater Contour Map Tab I Groundwater Time Concentration Plots Tab J CSV Transmittal Letter Tab A Site Plan and Perched Well Locations White Mesa Site l:o'!I -.. ~t• TW4-43 temporary perched monitoring well ~ installed September, 2021 TWN-20 temporary perched nitrate monitoring C well installed April, 2021 MW-24A perched monitoring well installed • December 2019 TW4-42 temporary perched monitoring well ¢ installed April 2019 TW4-40 perched chloroform pumping well EB installed February 2018 TW4-19 perched chloroform or EB nitrate pumping well MW-38 -¢-perched monitoring well installed February 2018 MW-5 • perched monitoring well TW4-12 0 temporary perched monitoring well TWN-7 temporary perched nitrate monitoring ◊ well PIEZ-1 perched piezometer Q RUIN SPRING b seep or spring DR-46 " •r , l"Jf_ .,._-..J I 1• I ,•,,c -~ 1' ~ ~, Cel l 1 M\11,@' 0 'JWN-'1S • 0 lWN-11 -~<> .... lW~M4 • M~I ·-ttl• 0 TWN.,-10 lil~8 ~ ~ ~.(19 l'IS01 0 -1• 0 • MW-19 TWN-05 .,l\Ylll~ Q 0 1WN·:1;01WN.'1>1 ~'18 -0~ t ~3 '1 !.. /4.>~ , ~ •-·-2 :rWN ~- 21"---~1_1 ~ ite ~ J, ~r."'-.l, .iw~~P( .. lW4lf8' l'' ~T"-~~-•,.·+I!$ 24 L~"' , "1W4-38 t..,•iwt . , O" ll'4:12 MW'21!.! -~t,; Q .. lolW'3t ~...., ~ iw .. 211, TW.-:_'16""",1~:11 • . ,,,.,,.._1S 0 'l:;~'!Xt4«' o· ' "',..., "'l!W/'°4 ~~~~ ~.,~~ ·-' .· ~4,?,,w.._.,,/ '1• .~ ' ' "ITW'.-,. . . •..w\ ,;JW4•21w4,3; •.r.,~iw~i~ o Jr -= '" C . H ~-~ '<&-3' DR-10 DR•11 "" " DR-U l>fr-13 ~ uJ.,,, . . • MW-21 DR•15 .. • MW.JA • MW,20 ~ 1 mile HYDRO GEO CHEM, INC. ,t .ti, 'IJJ :E -~---f M~-39 rJ.:sa .,. MW"CO • l,IW;n WHITE MESA SITE PLAN SHOWING LOCATIONS OF PERCHED WELLS AND PIEZOMETERS APPROVED DATE REFERENCE H :/718000/nov21 /Uwelloc0921 .srf FIGURA-I TabB Field Data Worksheets Quarterly Sampling ~F-1·. _.~ / .' .-=:.-s; -~ EAIERGY~ ,· ,• ' ' Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration {min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7 /27 /202111:22 7 /27 /202111:23 7 /27 /202111:24 7 /27 /202111:25 [volume of water purged (gals) [ Final Depth to Water (feet) 57.93 58.15 58.37 58.59 Name of Certified Analytical Labe>ratory AWSL Anal~ical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-11 Sampling Program Sampling_ Program MW-11 07272021 Sampling Event Sampling Event 2021 Q3 GW Resample 2021 Q3 GW Resample 7/27/2021 6:55 7 /27 /202111:25 !sampler !!;ampler I TH/DL TH/DL Pump Weather Conditions Sunny QED External Ambient Temperature (C) 20 2 Casings Previous Well Sampled MW-31 29.20 269.14 7.0 Well Depth {ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 85.28 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 3257 7.10 15.00 500 901.0 8.6 3261 7.13 15.00 497 905.1 7.2 3253 7.14 15.01 495 913.5 7.3 3254 7.15 14.99 494 920.6 7.0 Pumpin_g_ Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 85.55 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4 DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y Arrived on site at 0650. Purge began at 0655. Purged well for a total of 270 minutes. Purge ended and sa-mples collected afl" 125. Water was a little murky with little bubbles surfacing. Left site at 1135. Signature of Field Technician --=:),,u~-M~ I e---·~-,-' .... '.:".. _r ./~~--· -•· • -y...,,,_.--S,: S ~-~ .. .' ,' ~ _,-j Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance {micromhos) Date/Time Gallons Purged (gal) 7/21/202113:52 7 /21/202113:53 7/21/202113:54 7/21/202113:55 !Volume of water purged (g_a~) !Final Depth to Water (feet) 27.55 27.77 27.99 28.21 Name of Certified Analytical Laboratory AWSL Analytical ~amples Information Type of Sample/Analysis Heavy Metals -U and Se only Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-12 Sampling Program MW-12 07212021 Sampling Event 7/21/202111:45 7/21/202113:55 !sampler Pump Weather Conditions QED External Ambient Temperature (C) 2 Casings Previous Well Sampled 13.58 125.24 7.0 Well Depth (ft) 4.0 Well Casing Diameter (in) 1000 Depth to Water Before Purging (ft) Conductivity (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) 4175 6.53 16.27 461 0.0 4170 6.57 16.21 455 0.0 4168 6.61 16.29 451 0.0 4165 6.62 16.27 449 0.0 Pumping Rate Calculations - 28.21 Flow Rate (Q = S/60) (gal/min) Time to evacuate 2 Casing Volumes (min) 123.09 Number of casing Volumes Volume, if well evacuated to dryness () Sample Container Collected? Matrix Number T Type Sample Filtered? Type y WATER 1 T 250-ml HOPE y HN03 (pH<2) 2021 Q3 GW TH/DL Partly cloudy 28 MW-26 130.40 4 109.59 Dissolved Oxygen(%) Before/After 19.9 20.5 21.7 22.0 .217 130.00 2.00 0 Preservative I Added? I y [ Arrived on site at__1142. Pt1rge began at 1145. Purged \/\/ell for a total of 1_30 minutes. Purge ended and sample was collected at 1355. Water was clear. Left site at 1401 . Signature of Field Technician -=:) Groundwater Discharge Permit :,:it~" Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-14 Sampling Program Sampling_!'rogram Field Sample ID MW-14 07272021 Sampling Event Sampling Event 2021 Q3 GW Resampte 2021 Q3 GW Resampte Purge Date & Time 7 /27 /202111:59 Sample Date & Time 7/27/2021 14:50 !sampler lsa~e_ler I TH/DL TH/DL I Purging Equipment Pum p Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 29 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 17.55 Calculated Casing Volumes Purge Duration (min) 161.77 pH Buffer 7.0 7.0 Well Depth (ft) 128.70 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 101.82 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 7 /27 /202114:47 36.23 3771 7.12 15.20 484 0 6.0 7/27/2021 14:48 36.45 3768 7.10 15.23 484 0 6.0 7 /27 /202114:49 36.67 3715 7.08 15.18 484 0 5.8 7 /27 /202114:50 36.89 3710 7.06 15.20 484 0 6.0 Pume_ing Rate Calculations !Volume of water purg_ed (galsl 36.89 Flow Rate (0 = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 170.00 !Final [.)epth to Viater (feet) 102.89 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical ~borato_ry AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorga nics y WATER 1 250-ml HDPE u 4DegC y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: [ Arrived on site a~ 1155. Purge began at 1200. Purge_cl_ well fo~total of 170 minutes. Purg_e ensJed and s13_mples collected at 1450. Water was clear. Left site at 1505. Signature of Field Technician ~a,-,_,,_,___,._-h4.a~ Groundwater Discharge Permit t~ ..--~Y, Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-24 Sampling Program Field Sample ID MW-24_07292021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/28/2021 8:20 Sample Date & Time 7/29/2021 7:10 !sampler I TH/DL Purging Equipment Bailer Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C} 22 Purging Method 2 Casings Previous Well Sampled MW-40 Casing Volume (gal) 6.39 calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.20 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 7/28/2021 8:28 5.00 4487 5.53 15.18 533 37.8 89.0 7/29/2021 7:10 4427 5.90 16.95 Before 7/29/2021 7:16 4431 5.85 16.84 After Pumpin_g Rate Calculations !volume of water purged (gals) 13.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () !Final Depth to Water (feet) 119.95 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 13.00 Name of Certified Analytical Laboratory GEL Analyt~c~I Sam_eles Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Comments: Arrived on site at 0816. Bailing began at 0820. Bailed a total of 13 gallons from well. Water started clear and ended up murky. Left site at 0845. Arrived on site at 0708. Depth to water was 110.15. Samples bailed and collected at 0710. Left site at 0723. Signature of Field Technician ~=~~ I .. ;.~ -White Mesa Mill Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan ~ .• ,, ~Y, Field Data Worksheet For Groundwater Location ID MW-24A Sampling Program Field Sample ID MW-24A_07292021 Sampling Event 2021 Q3 GW Resa mple Purge Date & Time 7/28/202115:10 Sample Date & Time 7/29/2021 7:00 !sampler I TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 30 Purging Method 2 Casings Previous Well Sampled MW-26 Casing Volume (gal) 7.01 Calculated Casing Volumes Purge Duration (min) 73.12 pH Buffer 7.0 7.0 Well Depth (ft) 122.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos.) 1000 Depth to Water Before Purging (ft) 111.25 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7 /28/202116:25 14.40 4415 5.86 16.56 422 1.0 97.0 7/29/2021 7:00 4412 5.25 15.28 Before 7/29/2021 7:06 4413 5.27 15.22 After Pumping Rate Calculations [volul'Tl_e_Ef water p__u_r_g_ed (gals) 14.40 Flow Rate (Q = S/60) (gal/min) .192 Time to evacuate 2 Casing Volumes (min) 75.00 §nal Depth to Water (feet) 117.43 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (gals) 14.40 Name of Certified Anal}'tical Laboratory GEL Anal}'tical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4DegC y Comments: Arrived on site at 1506. Purge began at 1510. Purged well for a total of 75 minutes. Purged well dry. Purge ended at 1625. Water was mostly clear. Left site at 1627. Arrived on site at 0655. De_e_th to water was 111.15. Samples collected at 0700. Left site at 0723. Signature of Field Technician ~~+r~~ I ~-~ -,~..-~Y~IIEES I .' • Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 7/28/2021 9:57 7/28/2021 9:58 7/28/2021 9:59 7/28/2021 10:00 @:olume of water purged (gals! I Fin_il_l_ Depth_!_o Water (feet} 44.91 45.13 45.35 45.57 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-25 Sampling Program MW-25 _07282021 Sampling Event 2021 Q3 GW Resample 7/28/2021 6:25 7/28/2021 10:00 !sampler I TH/DL Pump Weather Conditions Partly cloudy QED External Ambient Temperature (C) 20 2 Casings Previous Well Sampled MW-36 21.97 202.52 7.0 Well Depth (ff) 115.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 81.35 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 3185 6.96 15.15 497 8.9 6.5 3166 6.93 15.09 497 9.0 6.0 3162 6.90 15.05 497 9.1 5.9 3170 6.88 15.00 497 9.0 5.8 Pumping Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 83.37 Number of casing Volumes 2.00 Volume. if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 250-ml HOPE u 4DegC y y WATER 1 250-ml HOPE y HN03 (pH<2) y y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y y WATER 1 250-ml HOPE u 4 Deg C y y WATER 1 250-ml HOPE y HN03 y Arrived on site at 0620. Purge began at 0630. Purged well for a total of 210 minutes. Purge ended and samples collected at 1000. Water was mostly clear with tiny little bubbles surfacing. Left site at 1009. Signature of Field Technician ~t.v>~/~ I Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill , ~YF'LIWSTCS Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 07282021 Sam_e_ling Event 2021 Q3 GW Resample Purge Date & Time 7 /28/202112:58 Sample Date & Time 7/28/2021 13:00 [sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C) 29 Purging Method 2 Casings Previous Well Sampled MW-39 Casing Volume (gal) 29.01 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 76.89 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/28/2021 13:00 3344 7.15 18.03 475 0 28.S Pumping Rate Calculations @olull'le of ~ater pur_ged () Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () [Final Depth to Water (fee_!l 110.98 Number of casing Volumes Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 Deg C y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: [ Arrived on site at 1255. Samples collected at 1300. Water was clear. Left site at 1305. Signature of Field Technician ~a,vv,_c....,-/:,1,~ Groundwater Discharge Permit =-~.,. : . y,:;;c ... -..,·~ Groundwater Monitoring Quality Assurance Plan s White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-27 Sampling Program Field Sample ID MW-27 _072.22021 Sampling_ Event 2021 Q3 GW Purge Date & Time 7/22/2021 8:30 Sample Date & Time 7/22/202112:20 [sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 22 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 24.16 Calculated Casing Volumes Purge Duration (min) 222.68 pH Buffer 7.0 7.0 Well Depth (ft) 95.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 58.00 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/22/202112:17 49.25 1161 7.13 15.30 471 0 103.0 7/22/202112:18 49.47 1157 7.15 15.31 470 0 102.8 7 /22/202112:19 49.69 1159 7.17 15.34 470 0 103.3 7 /22/202112:20 49.91 1159 7.18 15.31 470 0 103.2 [volume _of water purged (gals) 49.91 Pumping_ Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 230.00 [Final D~pth to ~ater (feet) 59.48 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Sam.e_les Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Nitrate/nitrite as N y WATER 1 I 250-ml HOPE u H2SO4 {pH<2), 4 Deg C I y Comments: I Arrivecj on si~ a10827. P_urg_e began at 0830. Purged well for a to1a1 of 230 minutes._Purg_e ended and sample was collected at 1220. Water was clear. Left site at 1224. Signature of Field Technician -:3 Groundwater Discharge Permit .. :a-~-. ,,7~~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-28 Sampling_!'rogram Field Sample ID MW-28 07232021 Sam_eling Event 2021 Q3 GW Purge Date & Time 7/23/2021 7:40 Sample Date & Time 7/23/202111:15 [sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 21 Purging Method 2 Casings Previous Well Sampled MW-29 Casing Volume (gal) 23.10 Calculated Casing Volumes Purge Duration (min) 212.93 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 74.62 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/23/2021 11:12 46.00 4200 6.54 16.43 508 0 31.5 7/23/2021 11:13 46.22 4195 6.54 16.40 506 0 31.0 7 /23/202111:14 46.43 4187 6.54 16.36 506 0 30.5 7/23/2021 11:15 46.65 4196 6.53 16.32 505 0 30.0 Pumping Rate Calculations [volume of water purged (gals) 46.65 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 215.00 jFinal Depth to Wa~ (fee!} 77.20 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Heavy Metals -U and Se only y WATER 1 250-mLHDPE y HN03 (pH<2) y Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y Comments: ~rrive_cl_9n site at 0736. Pllrge be9.an ati)7 40. f_urged v.Jell for~ total_c)_f 215 minutes. P_LJ_r_ge ended ancl samples collected at 1115. Water was clear. Signature of Field Technician --=:), .... ~ Groundwater Discharge Permit :a~,·,..· . ,' .-. _ ... ~-y. ·•' Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-29 Sampling Program Field Sample ID MW-29 07222021 Sampling Event 2021 Q3 GW Purge Date & Time 7 /22/2021 10:20 Sample Date & Time 7/22/202113:20 !sampler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 25 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 18.14 Calculated Casing Volumes Purge Duration (min) 167.19 pH Buffer 7.0 7.0 Well Depth (ft) 135.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 107.22 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 7/22/202113:17 38.40 4582 6.83 15.00 421 5.4 3.0 7 /22/202113:18 38.62 4590 6.80 15.05 408 5.2 3.1 7 /22/202113:19 38.84 4575 6.78 15.01 400 5.3 3.1 7 /22/202113:20 39.06 4578 6.77 15.01 394 5.4 3.1 @:olume of wat~~purge_<!_(galsl 39.06 Pumping_ Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min} 180.00 I Final Depth_!o Wate_! (feetl 109.73 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Heavy Metals -U only y WATER 1 I 250-ml HDPE y HN03 (pH<2) I y Comments: [ Arrived on site at 1014. Purge bega_n at 102_0. Purged well for a total_ of 180 _l!linutes._Purge ~nded and samp~ was ce>Uected at 1320. _Water \/\/as mo~ly clear. Left site at 1324. Signature of Field Technician Groundwater Discharge Permit ,~· ~~y~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 07292021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/29/2021 6:20 Sample Date & Time 7/29/20219:50 jsampler I TH/OL I Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-24A Casing Volume (gal) 22.67 Calculated Casing Volumes Purge Duration (min) 208.96 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.28 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/29/20219:47 44.91 2216 6.95 15.00 498 0 56.0 7/29/2021 9:48 45.13 2212 6.97 14.99 497 0 56.0 7/29/20219:49 45.35 2204 6.97 14.97 497 0 57.0 7/29/2021 9:50 45.57 2207 6.98 14.98 496 0 57.0 [volume of water purged (gals) Pumping_ Rate Calculations 45.57 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 !Firlal Dee_th to Wate_rJfeet) 77.65 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratol}'_ AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 OegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 DegC y Gross Alpha y WATER 1 250-ml HOPE y HN03 y Comments: I Arrived on site at _Q616. ~rge b~gan at 0620. P_urged well for a total of 210 rriinutes_._Purge_ended and samples collected at 0950. Water was clear. Left site at 1000. Signature of Field Technician ~~~#~ Groundwater Discharge Permit ~F-::· ~· .r .. jail/I/IT,. . ~.· . .:_ .. ·EJl'tJERIGY~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Field Sample ID MW-31 07272021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/27/2021 6:45 Sample Date & Time 7/27/202112:55 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.60 Calculated Casing Volumes Purge Duration (min) 365.01 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.35 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7/27/202112:52 79.63 3341 7.12 15.50 493 0 120.0 7/27/202112:53 79.85 3338 7.12 15.48 493 0 119.0 7/27/202112:54 80.07 3335 7.11 15.45 491 0 118.0 7/27/202112:55 80.29 3315 7.10 15.40 491 0 118.0 Pumping Rate Calculations IVolume of water purge1:I.Jgals) 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 jFinal Depth to Water Jfeet) 73.58 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytical S~meles Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Total Dissolved Soilds y WATER 1 250-mL HDPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y VOCs -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H25O4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 DegC y Gross Alpha y WATER 1 250-ml HDPE y HNO3 y Comments: I Arrived on site at 0640. Purge beg~n at 0645. Purg~d well_lor a to~I of 37Q_ minut~Purge ended and samples collected at 1255. Water was clear. Left site at 1305. Signature of Field Technician ~U.AA~ Groundwater Discharge Permit e~ ,r -· I . ,.---•· ~· . ' / -' . ' / ~,....~ -=;z: S" A j__ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-32 Sampling_!lrogram Field Sample ID MW-32 07282021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/28/202110:15 Sample Date & Time 7/28/202115:15 lsamp_ler TH/DL Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 24 Purging Method 2 Casings Previous Well Sampled MW-38 Casing Volume {gal) 31.53 Calculated Casing Volumes Purge Duration (min) 290.69 pH Buffer 7.0 7.0 Well Depth (ft) 130.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 82.30 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7 /28/202115:12 64.44 3731 7.07 15.43 266 14.6 33.0 7/28/202115:13 64.66 3719 7.00 15.40 260 14.0 32.0 7/28/202115:14 64.88 3721 6.98 15.41 257 14.3 32.0 7/28/202115:15 65.10 3720 6.95 15.36 254 14.5 31.8 !volume of water_purgecf_(gals) 65.10 Pumping_ Rate Calculations Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 300.00 I Final Depth to Water (feet) 88.25 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analyt_ical Laboratory AWSL Analytical Sam_e_les Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number I Type Sample Filtered? Type I Added? Chloride y WATER 1 I 500-ml Poly u None I N Comments: I Arrived on site at 1012. Purge began at 1015. Purged well for a total of 300 minutes. Purge ended and sample was collected at 1515. Water was a little murky. Left site at 1515. Signature of Field Technician ~~/4~ Groundwater Discharge Permit ;../'_ •.. ~~$ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-36 Sampling Program Field Sample ID MW-36 07272021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/27/202113:10 Sample Date & Time 7 /27 /202114:25 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 30 Purging Method 2 Casings Previous Well Sampled MW-14 Casing Volume (gal) 7.27 Calculated Casing Volumes Purge Duration (min) 67.04 pH Buffer 7.0 7.0 Well Depth (ft) 121.60 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 110.46 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7 /27 /202114:22 15.62 3898 7.20 15.40 488 0 84.0 7 /27 /202114:23 15.84 3899 7.20 15.40 487 0 80.0 7/27/202114:24 16.05 3890 7.20 15.38 486 0 81.0 7 /27 /202114:25 16.27 3908 7.19 15.34 486 0 80.0 ~IIJ_me of ~ter purged (gals) Pumping_ Rate Calculations 16.27 Flow Rate (Q = S/60) (gal/min) .217 1Fil'1al Dep!h to Water (feet) 111.05 Time to evacuate 2 Casing Volumes (min) 75.00 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory GEL Analytical Same_les Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HDPE u 4DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Comments: l Arrived on site at 1307. Purge began at 1310. Purged_well for a total of_J5 minut~s. Purge ~ended and samples collected at 1425. Water was clear. Left site at 1435. Signature of Field Technician ~ufVl...._,,__""7 Groundwater Discharge Permit ~ I,-.•' --=--s I': ~7"~ . Er.JLJ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-38 Sampling Program Field Sample ID MW-38 07292021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/28/2021 9:00 Sample Date & Time 7/29/2021 8:00 !sampler I TH/DL Purging Equipment Bailer Weather Conditions Partly cloudy Pump Type Grundfos External Ambient Temperature (C) 23 Purging Method 2 Casings Previous Well Sampled MW-24 Casing Volume (gal) 2.59 Calculated Casing Volumes Purge Duration () pH Buffer 7.0 7.0 Well Depth (ft) 74.40 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 70.42 Conductivity Dissolved DatefTime Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 7/28/2021 9:10 5.00 4366 7.10 15.60 498 8.7 92.0 7/29/2021 8:00 4373 6.25 16.75 Before 7/29/2021 8:06 4370 6.23 16.70 After Pumping_ Rate Calculations lvolu__rne of !-(Ster p1.1rged_lgals) 5.00 Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () I FJnal Depth to Water (feet) 74.29 Number of casing Volumes 1.93 Volume, if well evacuated to dryness (gals) 5.00 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 4 Deg C y Comments: Arrived on site at 0856. Bailing began at 0900. Bailed a total of 5 gallons from well. Bailed well dry. Water started clear and ended murky. Left site at 0913. Arrived on site at 0756. Depth to water was 70.33. Samples bailed and collected at 0800. Left site at 0807. Signature of Field Technician ~u ... 'U'tl~b~~~ I Groundwater Discharge Permit ~~ ·r • J,• _,.-· /i -_,_ •· ~-~Y~esrs '"-':•_ -~_·.-·-~ t' ~~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-39 Sampling Program Sampling Program Field Sample ID MW-39 07282021 Sampling Event Sampling_ Event 2021 Q3 GW Resample 2021 Q3 GW Resample Purge Date & Time 7/28/202111:00 Sample Date & Time 7 /28/202114:50 !sampler [sampler I TH/DL TH/DL I Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 25 Purging Method 2 Casings Previous Well Sampled MW-32 Casing Volume (gal) 24.63 Calculated Casing Volumes Purge Duration (min) 227.01 pH Buffer 7.0 7.0 Well Depth (ft) 102.50 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 64.78 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 7 /28/202114:47 49.25 4770 5.50 15.80 382 1.2 8.3 7 /28/202114:48 49.47 4764 5.48 15.78 386 1.1 8.2 7 /28/202114:49 49.69 4770 5.45 15.80 389 1.1 8.1 7 /28/202114:50 49.91 4773 5.43 15.78 392 1.1 8.1 lvolu'!le of water_purged {gals) Pumping_ Rate Calculations 49.91 Flow Rate (Q = S/60) (gal/min) .217 Tlme to evacuate 2 Casing Volumes (min) 230.00 [ F_i_nal Depth to Water (f~l 68.23 Number of casing Volumes 2.00 Volume, if well evacuated to dryness() 0 Name of Certified Analytical Laboratory GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HDPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HDPE u 4 DegC y Heavy Metals -Full Suite y WATER 1 250-ml HDPE y HNO3 (pH<2) y voes -Full Suite for GW y WATER 3 40ml VOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HDPE u 4 Deg C y Comments: ~rrived on site at 1056. Purge began at 1100. Purged well for a total of 230 minutes. Purge ended and samples collected at 1450. Water was clear. Left site at 1459. Signature of Field Technician ~~.;...;)~, Groundwater Discharge Permit ~~' r ' t, I ·' !"/ .l i __ ~ , ' .. , ~./ ........ · _·•~ .. ,,,,.~ Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-40 Sampling Program Field Sample ID MW-40 07282021 Sampling Event 2021 Q3 GW Resample Purge Date & Time 7/28/2021 6:35 Sample Date & Time 7 /28/202110:40 !sampler I TH/DL I Purging Equipment Pump Weather Conditions Partly cloudy Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-25 Casing Volume (gal) 26.17 Calculated Casing Volumes Purge Duration (min) 241.27 pH Buffer 7.0 7.0 Well Depth (ft) 120.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 79.91 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 7 /28/202110:37 52.51 3836 7.10 15.20 494 0 117.0 7 /28/202110:38 52.73 3838 7.10 15.18 494 0 118.0 7 /28/202110:39 52.94 3835 7.09 15.18 494 0 117.0 7 /28/202110:40 53.16 3837 7.08 15.13 494 0 117.0 !Volume of water purged (g~ls) Pumping_ Rate Calculations 53.16 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 245.00 I Final Deet!) to Water_(feet) 80.84 Number of casing Volumes 2.00 Volume, if well evacuated to dryness O 0 Name of Certified Analytical Laboratory_ GEL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Gross Alpha y WATER 1 250-ml HOPE y HN03 y Total Dissolved Soilds y WATER 1 250-ml HOPE u 40egC y Heavy Metals -Full Suite y WATER 1 250-ml HOPE y HN03 (pH<2) y VOCs -Full Suite for GW y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Nutrients y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y General lnorganics y WATER 1 250-ml HOPE u 40egC y Comments: I Arrived on site at_0630. Purge b~g~ri at 0635. Puiged well for a total of 245 minutes._Purge ended and samples collected at 1040. Water was clear. Left site at 1049. Signature of Field Technician _=:) -"-M~ ,.~ .•·~~Y, Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume O Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance () DatefTime Gallons Pur_g_ed [volume of water purged Q [Final Depth to Water (~et) Name of Certified Analytical Laboratory AWSL Analytical Samples Information Type of Sample/Analysis Total Dissolved Soilds Heavy Metals -Full Suite VOCs -Full Suite for GW Nutrients General lnorganics Gross Alpha Comments: I Duplicate of MW-14 Signature of Field Technician ..:3~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 MW-65 07272021 7/27/2021 14:50 Conductivity Sample Collected? Matrix y WATER y WATER y WATER y WATER y WATER y WATER Sampling Program Sampling_ Event [sampler Weather Conditions External Ambient Temperature O Previous Well Sampled Well Depth (ft) Well Casing Diameter O Depth to Water Before Purging (ft) pH Tem_e Redox Pumpin9_ Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness () Container Number Type Sample Filtered? 1 250-ml HOPE u 1 250-ml HDPE y 3 40ml VOA u 1 250-ml HOPE u 1 250-ml HOPE u 1 250-ml HDPE y 2021 Q3 GW Resample TH/DL Dissolved Turbidity Oxyg_en I Before/ After Preservative Type Added? 4 Deg C y HN03 (pH<2) y HCI (pH<2), 4 Deg C y H2S04 (pH<2), 4 Deg C y 4 Deg C y HN03 y TabC Field Data Worksheets Accelerated Monitoring Tab Cl Field Data Worksheets Accelerated Monitoring August 2021 Groundwater Discharge Permit e~. ._c.r -_} I . ~· -.· (. /.-.r ' r : · ," EIVIIE5R!l(3Y~ S ,• J..! - Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-11 Samp_lin_g_ Program Field Sample ID MW-11 08102021 Sam_e_ling Event Aug_lJst Monthly Purge Date & Time 8/10/2021 6:40 Sample Date & Time 8/10/202111:10 [sam!Jler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 29.24 Calculated Casing Volumes Purge Duration (min) 269.50 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 85.22 Conductivity Dissolved Date/Time Gallons Purged (gal) (um hos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 8/10/202111:07 57.93 3119 7.28 15.11 328 3.5 6.0 8/10/202111:08 58.15 3128 7.30 15.07 327 3.7 6.1 8/10/202111:09 58.37 3116 7.30 15.01 326 4.0 6.0 8/10/202111:10 58.59 3114 7.29 15.04 326 4.0 5.9 Pumping Rate Calculations [volume of water purged (gals) 58.59 Flow Rate (Q "" S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 [ Final Depth to Water (feet) 85.75 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal}'tical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Sulfate y WATER 1 250-ml HOPE u None N Comments: Arrived on site at 0635. Purge began at 0640. Purged well for a total of 270 minutes. Purge ended and sample was collected at 1110. Water was clear with tiny little bubbles surfacing. Left site at 1115. Signature of Field Technician ~<.<JV~~~ Groundwater Discharge Permit t~ _,.,.,--~y,o:zM51t s- Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 08102021 Sampling_ Event August Monthly Purge Date & Time 8/10/2021 9:29 Sample Date & Time 8/10/2021 9:30 jsampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 25 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 29.33 Calculated Casing Volumes Purge Duration O pH Buffer 7 .0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 76.40 Conductivity Dissolved Date!Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 8/10/2021 9:30 3402 6.94 16.37 507 1.0 34.5 Pumping Rate Calculations jvolume of water purged () Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes {) I Final Depth to Water (feet) 100.12 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Anal~ical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y voes -ChCl3, MeCl2, CCl4 y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Comments: I Arrived on site at 0925. Samples collected at 0930. Water was clear. Left site at 0935. Signature of Field Technician ~~vv__,,___..-r-.,r,.~ Groundwater Discharge Permit e ·~,/ ~ ' ,,.{ . ,· .· ' .• ~y~-ez: :S ' .,, .... Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Pro_gram Field Sample ID MW-30 08092021 Sampling Event August Monthly Purge Date & Time 8/9/2021 7:45 Sample Date & Time 8/9/202111:15 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled MW·31 Casing Volume (gal) 22.77 Calculated Casing Volumes Purge Duration (min) 209.92 pH Buffer 7 .0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.12 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 8/9/202111:12 44.91 2213 6.76 15.10 535 0 55.0 8/9/202111:13 45.13 2213 6.80 15.15 533 0 55.0 8/9/202111:14 45.35 2209 6.82 15.11 532 0 55.0 8/9/202111:15 45.57 2213 6.84 15.10 530 0 55.0 ~olume of water purged (gals) Pumpin9 Rate Calculations 45.57 Flow Rate (Q == S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 [ Final Depth to Water (feet) 77.81 Number of casing Volumes 2.00 Volume, if well evacuated to dryness (} 0 Name of Certified Analytical Laboratory AWSL Analytical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2504 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HOPE y HN03 (pH<2) y Comments: [ Arrived on site at 0740. Purge began at 0745 .. Purged well for a total of 21 O minutes. Purge ended and samples collected at 111 5. Water was clear. Left site at 11 21. Signature of Field Technician ~~~ Groundwater Discharge Permit 'F-:_,· ~-· .... --.):::::ap. ..-~Y, ,,._. -. Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Sampling Program Sampling Pro_9.ram Field Sample ID MW-31_08092021 Sampling Event Sampling_ Event August Monthly Aug_LJst Mon!hly Purge Date & Time 8/9/2021 7:30 Sample Date & Time 8/9/202113:40 !sampler ~a111_e_ler I TH/DL TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 20 Purging Method 2 Casings Previous Well Sampled N/A Casing Volume (gal) 39.66 Calculated Casing Volumes Purge Duration (min) 365.61 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.25 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 8/9/202113:37 79.63 3185 7.15 15.43 sos 14.0 115.0 8/9/202113:38 79.85 3237 7.15 15.45 505 14.0 115.0 8/9/202113:39 80.07 3250 7.13 15.43 504 13.0 116.0 8/9/202113:40 80.29 3260 7.13 15.45 504 13.0 116.0 Pumping_ Rate Calculations !volume o_f watel'_purgecl__(gals) 80.29 Flow Rate (Q = S/60) (gal/mln) .217 Time to evacuate 2 Casing Volumes (min) 370.00 !Final Depth_t~ Water (feet) 73.15 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Analytic~ Same_les Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HDPE u H2S04 (pH<2), 4 Deg C y Sulfate y WATER 1 250-ml HDPE u None N Total Dissolved Soilds y WATER 1 250-mLHDPE u 4 Deg C y Heavy Metals -U only y WATER 1 250-ml HOPE y HN03 {pH<2) y Comments: Arrived on site at 0725. Purge began at 0730. Purged well for a total of 370 minutes. Purge ended and samples collected at 1340. Water was mostly clear with tiny little bubbles surfacing. Left site at 1346. Signature of Field Technician ~. I IF-: ..... • . • L.. ~--• ,, ._.,/ _,/~Y. Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume () Calculated Casing Volumes Purge Duration () pH Buffer 7.0 pH Buffer 4.0 Specific Conductance () Date!Time Gallons Purged [volume of wate! purged() [Final Depth to Water (feet) Name of Certified Anal~ical Laboratory AWSL Anal}'!ical Samples Information Type of Sample/ Analysis Chloride Nitrate/nitrite as N Heavy Metals -u and Se only Comments: [Duplicate of MW-30 Signature of Field Technician ~~,Go,~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 Sampling_Pro_gram MW-65 08092021 Sampling Event 8/9/202111:15 [sampler Weather Conditions External Ambient Temperature () Previous Well Sampled Well Depth (ft) Well Casing Diameter() Depth to Water Before Purging (ft) Conductivity _e_H Temp Redox Turbidity Pum_eing Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness () Sample Container Collected? Matrix Number Type Sample Filtered? Type y WATER 1 500-ml Poly u None August Monthly TH/DL Dissolved Oxygen Preservative Before/After Added? N y WATER 1 250-ml HDPE u H2SO4 (pH<2), 4 Deg C y y WATER 1 250-ml HDPE y HN03 (pH<2) y TabC2 Field Data Worksheets Accelerated Monitoring September 2021 ------------· t~· :, .~~y~-=--s- Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume (gal) Calculated Casing Volumes Purge Duration (min) pH Buffer 7.0 pH Buffer 4.0 Specific Conductance (micromhos) Date/Time Gallons Purged (gal) 9/7/202113:17 9/7/202113:18 9/7/202113:19 9/7/202113:20 jvolume of water purged Q !Bnal Deptl!_!o W_!ter (feet) 57.93 58.15 58.37 58.59 Name of Certified Analytical Laboratory AWSL Analyt_ical Samples Information Type of Sample/Analysis Chloride Sulfate Comments: Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-11 Sam_eling Prog_ram MW-11 09072021 Sampling_ Event September Monthly 9/7/20218:50 9/7/202113:20 [sampler TH/DL Pump Weather Conditions Sunny Grundfos External Ambient Temperature (C) 21 2 Casings Previous Well Sampled MW-31 29.20 269.14 7.0 Well Depth (ft) 130.00 4.0 Well Casing Diameter (in) 4 1000 Depth to Water Before Purging (ft) 85.28 Conductivity Dissolved (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/ After 3129 6.85 15.06 481 89.0 7.8 3124 6.90 15.07 478 91.0 7.7 3129 6.95 15.10 476 92.0 7.6 3123 7.00 15.08 474 94.0 7.6 Pum_eing Rate Calculations 58.59 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 270.00 85.40 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Sample Container Preservative Collected? Matrix Number Type Sample Filtered? Type Added? y WATER 1 500-ml Poly u None N y WATER 1 250-ml HOPE u None N Arrived on site at 0846. Purge began at 0850. Purged well for a total of 270 minutes. Purge ended and samples collected at 1320. Water was a little murky with little bubbles surfacing. Left site at 1324. Signature of Field Technician -::3~ Groundwater Discharge Permit ~ ,-er---~,,-/ • • r C ' r ' ' • ~y~ .) .- Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-26 Sampling Program Field Sample ID MW-26 09092021 Sampling Event September Monthly Purge Date & Time 9/9/2021 7:59 Sample Date & Time 9/9/2021 8:00 !sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type Grundfos External Ambient Temperature (C) 19 Purging Method 2 Casings Previous Well Sampled MW-30 Casing Volume (gal) 29.45 Calculated Casing Volumes Purge Duration () pH Buffer 7 .0 7.0 Well Depth (ft) 121.33 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 76.23 Conductivity Dissolved Date/Time Gallons Purged (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 9/9/2021 8:00 3487 6.54 15.95 488 0 27.0 Pumping Rate Calculations !volume of water purged() Flow Rate (Q = S/60) (gal/min) 16.00 Time to evacuate 2 Casing Volumes () I Final Depth~ Water (feet) 99.32 Number of casing Volumes Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laborato_ry AWSL Analytical Samples Information Sample Container Preservative Type of Sample/ Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2S04 (pH<2), 4 Deg C y voes -ChCl3, MeCl2, CCl4 y WATER 3 40mlVOA u HCI (pH<2), 4 Deg C y Comments: I Arrived on site at 0756. Samples collected at 0800. Water was clear. Left site at 0805. Signature of Field Technician -:3 Groundwater Discharge Permit -e -F-:· .--,r .. )· .. -,..-f i ./,_,• ___ •" ~Y~FiTS Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-30 Sampling Program Field Sample ID MW-30 _ 09082021 Sampling Event September Monthly Purge Date & Time 9/8/2021 8:50 Sample Date & Time 9/8/202112:20 !sampler TH/OL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 22 Purging Method 2 Casings Previous Well Sampled MW-11 Casing Volume (gal) 22.71 Calculated Casing Volumes Purge Duration (min) 209.32 pH Buffer 7.0 7.0 Well Depth (ft) 110.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 75.22 Dissolved Date/fime Gallons Purged (gal) >nductivity (umhos/c pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 9/8/202112:17 44.91 2244 6.60 15.04 468 0 54.0 9/8/2021 12:18 4S.13 2242 6.64 15.02 467 0 55.5 9/8/2021 12:19 45.35 2243 6.67 15.00 466 0 55.3 9/8/202112:20 45.57 2240 6.70 15.00 465 0 55 .5 Pumping Rate Calculations !Volume of water purged (gals) 45.57 Flow Rate (Q = $/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 210.00 !Final Depth to ~aterJ!eet) 77.86 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal}'tical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y Heavy Metals -U and Se only y WATER 1 250-ml HOPE y HN03 (pH<2) y Comments: [ Arrive_cj_ on si~ at 0845. Pl.!'"9~ began at 0850._Purged well t0 a tot~ of 21Q minutes. Purge ended and samples collected at 1220. Water was clear. Left site at 1225. Signature of Field Technician ~L<.AA,,~~ Groundwater Discharge Permit e .... ~\. _.,, ., ~ . ' ~ . '.· .' .. ·· ~y~ '. _,,, J Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater Location ID MW-31 Saml)ling _f>rogram Field Sample ID MW-31 09072021 Sampling_ Event September Monthly Purge Date & Time 9/7/20218:10 Sample Date & Time 9/7/202114:20 [sampler TH/DL Purging Equipment Pump Weather Conditions Sunny Pump Type QED External Ambient Temperature (C) 21 Purging Method 2 Casings Previous Well Sampled NA Casing Volume (gal) 39.56 Calculated Casing Volumes Purge Duration (min) 364.65 pH Buffer 7.0 7.0 Well Depth (ft) 130.00 pH Buffer 4.0 4.0 Well Casing Diameter (in) 4 Specific Conductance (micromhos) 1000 Depth to Water Before Purging (ft) 69.41 Conductivity Dissolved Date/Time Gallons Purged (gal) (umhos/cm) pH (pH Units) Temp (deg C) Redox (mV) Turbidity (NTU) Oxygen(%) Before/After 9/7/202114:17 79.63 3396 6.59 15.10 462 5.0 115.0 9/7/202114:18 79.85 3395 6.60 15.16 461 5.1 114.0 9/7/202114:19 80.07 3399 6.61 15.13 460 4.8 114.0 9/7/202114:20 80.29 3399 6.62 15.13 459 4.8 114.0 Pumping Rate Calculations - [volume of \!_ater ei,.irgec:l_(gals} 80.29 Flow Rate (Q = S/60) (gal/min) .217 Time to evacuate 2 Casing Volumes (min) 370.00 [Final Depth _to Wa!er (feet) 73.35 Number of casing Volumes 2.00 Volume, if well evacuated to dryness () 0 Name of Certified Analytical Laboratory AWSL Anal~ical Samples Information Sample Container Preservative Type of Sample/Analysis Collected? Matrix Number Type Sample Filtered? Type Added? Chloride y WATER 1 500-ml Poly u None N Nitrate/nitrite as N y WATER 1 250-ml HOPE u H2SO4 (pH<2), 4 Deg C y Sulfate y WATER 1 250-ml HOPE u None N Total Dissolved Soilds y WATER 1 250-ml HOPE u 4 DegC y Heavy Metals -U only y WATER 1 250-ml HOPE y HNO3 (pH<2) y Comments: I Arrived on site at 0806. Purge began at 0810. Purged well for a total of 370 minutes. Purge ended and samples collected at 1420. Water was mostly clear. Left site at 1432. Signature of Field Technician ~CA.-~ w;::_, r~_,, ' , ,•, _,'f EAl'E:JRIG'Y~ Location ID Field Sample ID Purge Date & Time Sample Date & Time Purging Equipment Pump Type Purging Method Casing Volume O Calculated Casing Volumes Purge Duration O pH Buffer 7.0 pH Buffer 4.0 Specific Conductance O Date!Time I Volume of water purged O [Fi_11al Depth to Wa_!e_rjfeet) Gallons Purged Name of Certified Analyt~al Labo!atory AWSL Analytical Samples Information Type of Sample/Analysis Chloride Nitrate/nitrite as N Sulfate Heavy Metals -U Total Dissolved Solids Comments: I Duplicate of MW-31 Signature of Field Technician --=3='""~Md~ Groundwater Discharge Permit Groundwater Monitoring Quality Assurance Plan White Mesa Mill Field Data Worksheet For Groundwater MW-65 MW-65 09072021 9/7/202114:20 Conductivity Sample Collected? Matrix y WATER y WATER y WATER y WATER y WATER Sampling Pr<>_gram Sampling Event [sampler Weather Conditions External Ambient Temperature() Previous Well Sampled Well Depth (ft) Well Casing Diameter () Depth to Water Before Purging (ft) pH Temp Redox Pumping Rate Calculations Flow Rate (Q = S/60) () Time to evacuate 2 Casing Volumes () Number of casing Volumes Volume, if well evacuated to dryness () Container Number Type Sample Filtered? 1 500-ml Poly u 1 250-ml HOPE u 1 250-ml HOPE u 1 250-ml HOPE y 1 250-ml HOPE u September Monthly TH/DL Dissolved Turbidity Oxygen I Before/After Preservative Type Added? None N H2S04 (pH<2), 4 Deg C y None N HN03 (pH<2) y 4 Deg C y TabD Quarterly Depth to Water Name: Tanner Hollidny. Deen Lyman Date: 8/11/2021 -8/13/2021 Depth to Depth to Date Time Well Water (ft.) Date Time Well Water (ft.) 8/11/2021 1002 MW-01 64.86 8/13/2021 656 MW-04 81..68 8/11/2021 903 MW-02 109.52 8/13/2021 701 TW4-0I 103,33 8/11/2021 1319 MW-03A 84.14 8/13/2021 652 TW4-02 98.10 8/1 I /2021 733 MW-05 108.14 8/13/2021 751 TW4-03 64.62 8/11/2021 834 MW-11 85.31 8/13/2021 708 TW4-04 81 06 8/11/2021 737 MW-12 109,60 8/13/2021 746 TW4-05 72.D2 8/11/2021 821 MW-14 101.78 8/13/2021 718 TW4-06 79,11 8/11/2021 817 MW-15 105.36 8/13/2021 711 TW4-07 82.07 8/11/2021 1311 MW-17 72.13 8/13/2021 715 TW4-08 85.28 8/11/2021 1010 MW-18 73.85 8/13/2021 742 TW4-09 70,05 8/11/2021 1028 MW-19 66.13 8/13/2021 738 TW4-I0 69.35 8/11/2021 1247 MW-20 86,33 8/13/2021 647 TW4-II 89,90 8/11/2021 1256 MW-22 66.39 8/13/2021 918 TW4-12 55.88 8/11/2021 742 MW-23 113.84 8/13/2021 914 TW4-13 56.95 8/11/2021 937 MW-24A 11 I.I I 8/13/2021 906 TW4-14 77.52 8/11/2021 934 MW-24 110.05 8/13/2021 734 TW4-16 73.70 8/1 1/2021 830 MW-25 81.28 8/13/2021 800 TW4-18 73.11 8/11/2021 916 MW-26 75.40 8/13/2021 945 TW4-19 73.40 8/11/2021 948 MW-27 58.03 8/13/2021 620 TW4-21 72.33 8/11/2021 920 MW-28 74.65 8/13/2021 634 TW4-22 68.20 8/11/2021 908 MW-29 107.15 8/13/2021 730 TW4-23 75.74 8/11/2021 712 MW-30 75.18 8/13/2021 630 TW4-24 68.71 8/11/2021 841 MW-31 69.33 8/13/2021 625 TW4-25 69.25 8/11/2021 846 MW-32 82.18 8/13/2021 722 TW4-26 73.95 8/11/2021 755 MW-33 DRY 8/13/2021 843 TW4-27 79.18 8/11/2021 806 MW-34 107.38 8/13/2021 922 TW4-28 49.36 8/11/2021 749 MW-35 112.25 8/13/2021 902 TW4-29 78.48 8/11/2021 746 MW-36 110.51 8/13/2021 850 TW4-30 75.16 8/11/2021 810 MW-37 106.06 8/13/2021 847 TW4-31 76.41 8/11/2021 1237 MW-38 70.28 8/13/2021 927 TW4-32 56.43 8/11/2021 1230 MW-39 64.65 8/13/2021 839 TW4-33 78.25 8/11/2021 1218 MW-40 79.85 8/13/2021 858 TW4-34 76.71 8/13/2021 854 TW4-35 75.42 MW-26 = TW4-15 8/13/2021 910 TW4-36 58.28 MW-32=TW4-17 8/13/2021 638 TW4-37 72.15 Comments: 8/13/2021 755 TW4-38 60.06 8/13/2021 642 TW4-39 74.55 8/13/2021 726 TW4-40 72.32 8/13/2021 705 TW4-41 88.87 8/13/2021 835 TW4-42 69.93 Date Time 8/11/2021 1033 8/11/2021 1021 8/11/2021 1411 8/11/2021 1354 8/11/2021 1349 8/11/2021 1424 8/11/2021 1421 8/11/2021 1417 8/11/2021 1408 8/11/2021 1016 8/11/2021 957 8/11/2021 1049 8/11/2021 1044 8/11/2021 1403 8/11/2021 919 8/11/2021 1059 8/11/2021 1111 8/11/2021 906 8/11/2021 859 8/11/2021 1158 8/11/2021 851 8/11/2021 847 8/11/2021 840 8/11/2021 1335 8/11/2021 1330 8/11/2021 1325 8/11/2021 822 8/11/2021 834 8/11/2021 815 8/11/2021 750 8/11/2021 746 8/11/2021 730 8/11/2021 757 8/11/2021 737 8/11/2021 804 Well PIEZ-01 PIEZ-02 PIEZ-03A PIEZ-04 PIEZ-05 TWN-01 TWN-02 TWN-03 TWN-04 TWN-06 TWN-07 TWN-14 TWN-16 TWN-18 TWN-19 TWN-20 TWN-21 DR-05 DR-06 DR-07 DR-08 DR-09 DR-10 DR-II DR-12 DR-13 DR-14 DR-15 DR-17 DR-19 DR-20 DR-21 DR-22 DR-23 DR-24 Depth to Water (ft.) 67.30 46,17 57.27 67.35 66.06 69.25 58.35 42.84 62.32 80.69 80.55 59.48 47.85 62.44 54.03 77.95 79.19 83.18 94.08 91.91 51.32 86,52 78.38 97.93 91.88 69.82 76.19 92.85 64.68 63.28 55.45 100.54 DRY 69.05 44.51 TabE Laboratory Analytical Reports -Quarterly Sampling INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-001 Client Sample ID: MW-l 1_07272021 Collection Date: 7/27/2021 1125h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual )alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/2021 1 506h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1506h E200.8 0.000500 < 0.000500 Cadmium mg/L 8n/2021 943h 8/13/202 I J359h E200.8 0.000500 < 0.000500 Phone: (801) 263-8686 Calcium mg/L 8/2/202 l 943h 8/10/2021 1541h E200.7 10.0 178 Chromium mg/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/202 l 1359h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 I 359h E200.8 0.0100 < 0.0100 !-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/202 l l 506h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/202 I 1506h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1656h E200.7 0.100 62.1 Manganese mg/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.0100 0.376 Mercury rng/L 8/2/2021 1214h 8/3/2021 11 l 4h E245.1 0.000500 < 0.000500 Jennifer Osborn Molybdenum rng/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.0100 < 0.0100 Laboratory Director Nickel rng/L 8/2/2021 943h 8/1 3/202 l 1359h E200.8 0.0200 < 0.0200 Potassium rng/L 8/2/202 l 943h 8/10/202 l 1656h E200.7 1.00 10.6 Jose Rocha Selenium rng/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.00500 < 0.00500 QA Officer Silver rng/L 8/13/2021 1610h 8/16/2021 1012h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 154 l h E200.7 10.0 520 Thallium mg/L 8/2/2021 943h 8/13/202 l 1506h E200.8 0.000500 < 0.000500 Tin rng/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.100 < 0.100 Uranium rng/L 8/2/2021 943h 8/13/2021 l 506h E200.8 0.000500 0.00221 Vanadium mg/L 8/2/202 J 943h 8/10/202 l l 656h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1359h E200.8 0.0100 < 0.0100 Report Date: 8/24/2021 Page 9 of 72 All llJlolyses applicable to the CWA. SOW A. n.nd RCRA are perlOrmed in accordance to NELAC pro1Mols. Pc.1111\cnl sampling inforouuion is located on Lhe anoched COC. Confidenliol Business lnfonm11ion: This report is provided for 1he C'~duJJ\C use of the ~ddressec. Pri,·ile~es of sub,_seq~enl ~1~e ofth~ •~~io or this _crn~p:my or nn~· 1~mber of ils slafT, or rcproducti~ ~~1his repo~ in ~n?\3Clroo .. wilh lhe ~~•er1ise~enl. P:?moli~n ~r ~aJe of ~2!~prod1!ct or p1:?Cess, ~r in ~onn:c~ion w}lh th~ r~•p~blkotion of lhis report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-001 Client Sample ID: MW-11_07272021 ANALYTICAL LABORATORIES Collection Date: 7/27/2021 1125h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1337h E350.I 0.0500 0.483 Bicarbonate (as mg/L 8/2/2021 I I00h SM2320B 1.00 320 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 1100h SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 8/10/2021 2012h E300.0 5.00 48.3 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 451h E300.0 0.200 0.354 Fax: (801) 263-8687 Ion Balance % 8/11/2021 I 058h Cale. -100 -2.01 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/202 I 14 I 9h E353.2 0.100 0.924 Sulfate mg/L 8/l 0/2021 2012h E300.0 25.0 1,470 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 38.4 Total Cations, meq/L 8/11/2021 1058h Cale. 36.9 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 2,680 Jennifer Osborn Total Dissolved Solids 8/11/2021 l 058h Cale. 1.08 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 2,480 Calculated QA Officer Report Date: 8/24/2021 Page 22 of 72 All analyses applicable 10 lhe CWA. SDW,\, nnd RC-RA we performed in accordance to NELAC p101ocols. PcttinL,11 snmpliny infonnalion is localed on t.he ntlached COC. C'onliW.~uial Business Jnfonnalion: This report is pro,•ided for the exdusl\e use of1he ~ddressee. Pri,·ile~es or sub_..seq~ent ~~e of thc_~:'f.•~ o(this _co1~pany or nny ~mller or its slarT, or r~producltO(! ~f 1his rq,o'! in ~on~ection ... \\ith lhe ~~•ertise~enl, p~~moti<!' er s.1I~ of ?1!~: _frod~I or P~?cess. ~r in ~nn:c!ion \\"!lh th~ r:-puhlfQIIOo or this repon ORGANIC ANALYTICAL REPORT 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-00lA Client Sample ID: MW-l 1_07272021 Collection Date: 7/27/2021 1125h Received Date: 7/30/2021 11 00h Analytical Results Analyzed: 7/30/2021 1415h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osborn Toluene Laborat01y Director Xylenes, Total Contact: Tanner Holliday Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qua! 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 2.25 l 08-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.9 55.1 46.2 49.1 50.00 95.8 80-136 50.00 110 85-121 50.00 92.3 78-132 50.00 98.2 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 36 of 72 All am1lyses applicable to lhe CWA. SDWA4 Md ncRA are perfonned in accordance to NELAC protocols. Pcrum:nt sampling inforu\1111011 is located 011 Lhe auached COC. C-onritknliul Business lnfa1m lion: This report is proYided for the r~c-htSn't use of1he ~ddressee. PJi,·ile~es o,r sub ... seq~enl ~1~e or1h" ~!~~1t of this _c01~pany or nny ~mber of its staff, or re-prqducl1°!! ~(\his repo~ in ~on~CChOJ~ ,vilh the ~~'ertisement, P~?motio.11 "!u.lc of ?1!Y. ~rod~ct o, pr,?Cess, ~r in 7onm;.c~ion w!th th~ r:-publicialiOu orthis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company : Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW --MW-11 07272021 551444001 Ground Water 27-JUL-21 11:25 02-AUG-21 Client ---------- Parameter ----Qualifier Result Uncertainty --------------MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.188 0.556 RL 1.00 Project: Client ID: DNMIO0I00 DNMIO0l --------- Units PF DF Analyst Date Time Batch Method pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods were performed: __ -~ ________ _ -----------Method DescrjQ!Lo'-'-n'-----______ __ Anal _t Comm~tL _________ _ EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 102 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (1-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 13 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107637-001 Client Sample ID: MW-12_07212021 Collection Date: 7/21/2021 1355h Received Date: 7/26/2021 1055h Analytical Results Compound Selenium Uranium Units mg/L mg/L Date Prepared 7/27/2021 1057h 7/27/2021 1057h Date Analyzed 8/2/2021 I 350h 8/2/2021 1450h -------- Contact: Tanner Holliday DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.00500 0.0324 E200.8 0.000300 0.0222 Report Date: 8/10/2021 Page 4 of 8 All onnlyses opplicnl>tc:i l(, lht, CWA. SDWt\, And RCRA nl'e pi!rl'ormi:d in ac..:ordonce to NBLAC 1uo1ot('I• 11M1nen1 sllJTlpliny inforl\\nmUl is locnlcd mi the nnnched COC. Conlidentinl Business lnfonnntion: This r~port is provided for the e.~clusiq~ use or1he ~ddressee. P1irile~es of iul~cq~1ent ~1~~ ot'd1c ~~.n" or !his 1 cor~pn11y or nny 1~~1!1ber ori1s s1nff, or rcprodl1ch0!! ~ lhis rero~ in foniux:11°'~ \\•ilh lhe n~~·or1ise1!1ent. P~?mo1i~n ~r ~aJc, of~!)'. ~rod~cl or P~?cess, ?r ii, 7011n:c~ion w!th th~ r~-p~blicntion or lhis ri.,porl INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-002 Client Sample ID: MW-14_07272021 ANALYTICAL LA0ORATOR1£$ Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1510h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/202 1 943h 8/13/2021 1319h E200.8 0.000500 0.00163 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 1543h E200.7 10.0 505 Chromium mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0100 < 0.0100 Fax: (80 I) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 151 Oh E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 1510h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 94 3 h 8/10/2021 1543h E200.7 1.00 157 Manganese mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0100 1.84 Mercury mg/L 8/2/2021 1214h 8/3/2021 1128h E245.I 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/10/2021 1658h E200.7 1.00 14.7 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 l3l 9h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 1016h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1543h E200.7 10.0 334 Thallium mg/L 8/2/2021 943h 8/13/2021 1510h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.100 < 0.100 Uranium mg/L 8/2/202 1 943h 8/13/2021 1510h E200.8 0.000500 0.0600 Vanadium mg/L 8/2/2021 943h 8/10/2021 1658h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1319h E200.8 0.0100 0.0152 2 -Ana/yte concentration is too high for accurate matrix spike recovery and/or RPD. Report Date: 8/24/2021 Page 10 of72 All analyses applicable to lhe CWA. SOWA. Nxi R(RA are J)Cf(onned in accordance to NELAC protocols. P(!rifnenl sampling infommuon is located on the attached COC. •onflckruial Business lnformalion: This repon is provided for Jhe cxe:huh'r use of lhe ~ddressee. P1fri\e~es or sub,_5eq~ent ~1~e of the ~~.ne or this ,con,,ptHW or nny 1~~ber of its slnIT, or reproducli~ ~:1his repo~ in ~on~1ccuon .. "ith the a~~·ertise~enl, P~?motio_n ~ sale of ?1!Y. ~rod~cl or p1:~ess, ~r in ?'""~~ion w!lh 1h~ r!-pubficAlio-11 of I his repon INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-002 Client Sample ID: MW-14_07272021 Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual :,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1339h E350.I 0.0500 < 0.0500 Bicarbonate (as mg/L 8/2/202 I 1 IO0h SM2320B 1.00 355 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 1100h SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 8/10/202 I 2035h E300.0 10.0 19.0 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 514h E300.0 0.100 0.109 Fax: (80 I) 263-8687 Ion Balance % 8/I I /2021 I 058h Cale. -100 -0.381 :-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/202 l 1420h E353.2 0.100 < 0.100 Sulfate mg/L 8/10/2021 2035h E300.0 50.0 2,200 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/202 I 1058h Cale. 53.4 Total Cations, meq/L 8/11/2021 1058h Cale. 53.0 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 3,810 Jennifer Osborn Total Dissolved Solids 8/11/202 I 1058h Cale. 1.11 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 3,440 Calculated QA Officer Report Date: 8/24/202 I Page 23 of 72 All analyses applicable to lhe CWA. SDWA. And RCRA are performed in accordance to NELAC protocols Pe11inenl sampling information is located on the allached COC Confidential Business Information: This report is provided for 1he exclusire use of the ~dctressee. Pririle~es o_f sub~seq~enl ~,~e of lhr.! ~:"."Cl of this 0con_1pany or any ~mber of its slafT, or reprOOuclio~ ~~lhis repo~ in ~~eclion,. wilh the a~~'ertise~enl P~?molio.n ~r sale of ~~~~-~rod~cl or p1:?cess, ~r in ~nn~c!ion \\'!lh 1h~ r~-publicatio11 of this report ORGANIC ANALYTICAL REPORT Client: Energy Fuels R.esources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-002A American West Client Sample ID: MW-14_07272021 ANALYTICAL LAeoRAToR1es Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 11 00h 3440 South 700 West ;;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1435h Units: µg!L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Jose Rocha QA Officer Surrogate Units: µg/L Surr: l,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260D-W-DENIO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual ---- 47.7 50.00 95.4 80-136 54.4 50.00 109 85-121 45.9 50.00 91.8 78-132 49.4 50.00 98.7 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 37 of72 All ano.lyses applicable to the CWA. SOW , 1111d R RA are perfonned in accordance to NELAC protocols. f'crlmft'II sampling inromi:i1100 is locnled on t.he attached COC. Conri~tcntial Business Information: This repon is provided for the o.chohe use of the ~ddressee. PriYile~es o~ su~q~enl ~~e of the '!~~tc of this .co~pnny or nny ~mber of its slaff, or reproductf"!! ~~ 1his rep~~ in ~w~1ec11on_ '"ith the a~~•ertisement. P~?moliOfl ~ S4le of~-l_)«ldl~Cl or p1:?cess, ~r in ~nn~~!ion w!lh th~ r~-p~bUn1 on of this repon GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW --MW-14 07272021 551444002 Ground Water 27-JUL-21 14:50 02-AUG-21 Client Parameter ---__ gualifier Result Uncertainty -----Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.386 The following Analytical Methods were performed: MDC 0.935 ----- Project: Client ID: DNMIO0l00 DNMIO0l ----------- RL Units PF DF Analyst Date Time Batch Method ----- 1.00 pCi/L JXC9 08/23/21 1725 2157704 Method Desc1-'"·i ""'t--'--'io'---'-n'-------_________ --------'-'Anal st Commen_ts __________ _ EPA 903.0 Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 88.9 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 14 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-010 Client Sample ID: MW-24_07292021 ANALYTICAL LABORATORIF S Collection Date: 7/29/2021 710h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/2021 l 846h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/202 l 943h 8/13/2021 l 846h E200.8 0.000500 0.00271 Cadmium mg/L 8/2/2021 943h 8/13/2021 1508h E200.8 0.000500 0.00926 Phone: (801)263-8686 Calcium mg/L 8/2/2021 943h 8/l 0/202 J I 625h E200.7 10.0 502 Chromium mg/L 8/2/202 l 943h 8/J 3/2021 l 508h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/202 l I 508h E200.8 0.0100 0.130 Fax:(801)263-8687 Copper mg/L 8/2/2021 943h 8/13/202 I 1508h E200.8 0.0100 0.0172 ~-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 l 846h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 1846h E200.8 0.00100 0.00260 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1625h E200.7 1.00 195 Manganese mg/L 8/2/2021 943h 8/1 3/202 J 1432h E200.8 0.0100 7.89 Mercury mg/L 8/2/2021 1214h 8/3/202 l 1149h E245.I 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 1508h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1508h E200.8 0.0200 0.0767 Potassium mg/L 8/2/2021 943h 8/12/2021 1307h E200.7 2.00 15.4 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 1508h E200.8 0.00500 0.00774 QA Officer Silver mg/L 8/13/2021 l 6 J Oh 8/16/202 l J057h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/202 l 943h 8/10/2021 1625h E200.7 10.0 454 Thallium mg/L 8/2/202 l 943h 8/13/2021 I 846h E200.8 0.000500 0.00291 Tin mg/L 8/2/2021 943h 8/13/2021 I 508h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/l 3/202 J 1846h E200.8 0.000500 0.00593 Vanadium mg/L 8/2/202 J 943h 8/J 1/2021 1 802h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/202 l 943h 8/13/202 l J 508h E200.8 0.0100 0.146 Report Date: 8/24/2021 Page I 8 of 72 All analyses applicnble to lhe CWA. SDWA. and RCRA are performed in accordance 10 NELAC prn1oc.ols. Pt.Ulnea, sampling information is localed on lhe attached COC. onfickmiul Business lnrormalion: This report is provided for the e."\:clUSl\'e use of the ~ddressee. Pri,·ile~es o_f su~seq~ent ~1~e or lhe ~~e of lhis .cor,:,p:my or any ~mber of its stnIT, or rcproducll~! ~• 1h1s repo~ in _co~ection .. \\ilh lhe a<!~•ertisement. P~?moti~ nr stale of ?1!Y. ~rod~cl or P~?cess, ?r in ~onn:c!ion w!lh 1h~ r1;-publicEL11011 or I his report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-010 American West Client Sample ID: MW-24_07292021 ANALYTICAi. LABORATORlf6 Collection Date: 7/29/2021 710h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ~alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 134 7h E350.l 0.0500 0.0773 Bicarbonate (as mg/L 8/2/2021 1100h SM23208 1.00 < 1.00 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 11 00h SM23208 1.00 < 1.00 Phone: (801)263-8686 Chloride mg/L 8/11/2021 118h E300.0 20.0 48.1 Toll Free: (888) 263-8686 Fluoride mg/L 8/I I /2021 823h E300.0 0.500 1.40 Fax: (801) 263-8687 Ion Balance % 8/11/2021 I 058h Cale. -100 -2.84 :-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/6/2021 1444h E353.2 0.100 0.369 '@ Sulfate mg/L 8/l l /2021 l\ 8h E300.0 100 3,050 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/202 I 1058h Cale. 64.8 Total Cations, meq/L 8/l I /2021 1058h Cale. 61.3 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 4,940 Jennifer Osborn Total Dissolved Solids 8/1 1 /202 I I 058h Cale. 1.16 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 I 058h Cale. 4,260 Calculated QA Officer @ -High RPD due to suspected sample non-homogeneity or matrix interference. 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 8/24/2021 Page 3 I of 72 All analyses applicnble 10 the CWA, SDWA. Md R RA are perfom1ed in accordance to NELAC prnlQCols. Pcr1ina,,t sampling informalion is locnted on lhe atlached COC. Confidential Bus111css lnform.:alion: This repon is proyided rot 1ho exclusive use or the ~ddressee. Prfrile~es or~ll~SC'q~ienl .u~e or1hc ~!1CI or1his .cor,:ipany or My l~f;lber orils sl:tIT, onc:1Uudutl1~ of this repoi; in ~on?eclion .. with the n~~1ertise~ent. P~?molio.n ~r ~ale of?'!}. l?"°-d~ct OI 1i1.?Cess, ~r in ~onn!c!ion w!lh lh! r~•publicaJion of lhis report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-0lOA American West Client Sample ID: MW-24_07292021 ANALvr1cAL LABORAT0R1Es Collection Date: 7/29/2021 710h Received Date: 7/30/2021 1100h 3440 South 700 West ~alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1713h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENlO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer ---------- Surr: l,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 45.3 57.7 43.2 47.2 50.00 90.6 80-136 50.00 115 85-121 50.00 86.5 78-132 50.00 94.3 81-123 $ · This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 45 of 72 All analyses applicable to lhe CWA. SOWA. tind H.CRA are performed in accordance 10 NELAC pl'OLOCOls. Pcr1lnent samphnu informalion is localed on 1he attached COC. Conlidenlial Business lnfonnulion: This repon is provided for the C'Sdusi\'r me of1he ~ddressee. Pri\·ile~es o!su~seq~tenl ~~e or the ~~or this _co1~pany or nny •~~ber of its stnff, a: rqHOOucth:»~ ~f this rep,c»! i11 _con?eclion .. wilh the n~~•ertise1_~enl. P~?motio,n ~r saJe of :31~Y. ~rod~cl or P~?cess, ~r in ~nn:c~ion \\'!lh th~ r~-publinhon or1his report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Contact: Project: ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-24 07292021 551444010 Ground Water 29-JUL-21 07:10 02-AUG-21 Client ---------------Parameter Qualifier Result Uncertainty MDC Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 1.92 +/-0.359 0.594 Project: Client ID: RL 1.00 pCi/L DNMIO0l00 DNMIO0l JXC9 08/23/21 1649 2157704 The following Analytical Methods were performe'!:__ ____________________ _ Method Descri tion Anal st Comments '---------------------'--"=.;.-=:....=;::=:.;=c.:.=.-----------EPA 903.0 Surrogate/Tracer Recov~ Test __ ------------Result Nominal Bnrium arrier GFP Totnl Alpha Radium, Liquid "A Received" IOI (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = ample Reporting Limit. For metals analysis only. When the ample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: DilutiOJl Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 22 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporti11g Limit SQL: ample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-011 Client Sample ID: MW-24A_07292021 Collection Date: 7/29/2021 700h Received Date: 7/30/2021 l l00h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/16/2021 1148h £200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/202 J 943h 8/l 6/202 l l 200h £200.8 0.000500 0.00519 Cadmium mg/L 8/2/2021 943h 8/13/2021 1512h £200.8 0.000500 0.0103 Phone:(801)263-8686 Calcium mg/L 8/2/2021 943h 8/10/202 I 1627h £200.7 10.0 466 Chromium mg/L 8/2/202 J 943h 8/13/2021 I 5 J 2h £200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 l5J2h £200.8 0.0100 0.136 Fax: (801) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1512h £200.8 0.0100 0.0210 !-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/J 3/2021 1902h £200.8 0.0300 < 0.0300 Lead mg/L 8/2/202 I 943h 8/13/2021 1902h £200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/l 0/202 I 1627h £200.7 1.00 183 Manganese mg/L 8/2/2021 943h 8/13/202 l 1457h £200.8 0.0100 7.74 Mercury mg/L 8/2/2021 1214h 8/3/2021 l15lh £245.1 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/202 l 943h 8/13/2021 l5l2h £200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1512h £200.8 0.0200 0.0695 Potassium mg/L 8/2/2021 943h 8/12/2021 1309h £200.7 2.00 14.4 Jose Rocha Selenium mg/L 8/2/202 l 943h 8/13/2021 1512h £200.8 0.00500 0.00702 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 1 IOlh £200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1627h £200.7 10.0 448 Thallium mg/L 8/2/202 J 943h 8/13/202 I 1902h £200.8 0.000500 0.00269 Tin mg/L 8/2/202 l 943h 8/13/2021 l5J2h £200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 I 902h £200.8 0.000500 0.00899 Vanadium mg/L 8/2/2021 943h 8/11/2021 1804h £200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/202 I 15 I 2h £200.8 0.0100 0.0624 Report Date: 8/24/2021 Page I 9 of72 All analyses applicable lo the CWA. SDW, Md RCRA are performed in accordance to NELAC fHOU>eols. Pemnr:nl sarnplif\S information is located on the allached COC. 'onOdcntial Bu-rmess Information: This repor1 is provided for the c-:uluspc use of the ~ddrcssee. Pri,·ile~es o_f sub__seq~nl ~t~e of 11.C r~~1c of lhis ,con:ipDny or any 1~'!1ber of its slnIT, or rq)mduclio.! ~rlhis rcpo~ in ~on?ectIon~ \\•ilh the a~~1ertise~enl, P:?moti""!' ~~c of !1'!r ~1od~cl or P~?cess, ~r in ~nn~c.Lion w!Lh th~ r~-publ cllllOH Of lhis report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-011 Client Sample ID: MW-24A_07292021 Collection Date: 7/29/2021 700h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual :;alt Lake City, UT 84119 Ammonia (as N) mg.IL 8/4/2021 1050h 8/4/2021 1348h E350.l 0.0500 0.0709 Bicarbonate (as mg.IL 8/2/202 I 11 OOh SM2320B 1.00 7.40 CaCO3) Carbonate (as CaCO3) mg.IL 8/2/2021 11 OOh SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg.IL 8/11/2021 142h E300.0 20.0 45.6 Toll Free: (888) 263-8686 Fluoride mg.IL 8/11/2021 1614h E300.0 0.500 0.868 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 -5.67 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg.IL 8/6/2021 1448h E353.2 0.100 0.373 Sulfate mg.IL 8/11/2021 142h E300.0 100 3,060 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 65.2 Total Cations, meq/L 8/11/2021 1058h Cale. 58.2 Measured Total Dissolved Solids mg.IL 7/30/2021 1345h SM2540C 20.0 4,490 Jennifer Osborn Total Dissolved Solids 8/11/2021 1058h Cale. 1.06 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg.IL 8/1 1/2021 1058h Cale. 4,220 Calculated QA Officer Report Date: 8/24/2021 Page 32 of72 All analyses applicnblu h) lh!! CWA. SOW nnd RCRA nre performed in accordance to NELAC protocols. PtnlMc:tll sampling infonn.,iian is located on the auached COC. Confiden1ial Lhmncss Inf onnallon: This repon is provided ror the tixtlusi\c-U3e of 1he ~ddressee. Pri,·ile~es o_r,~seq~enl ~1~e or 1he~;11.1k! of this _cm~pany or nny ~7mber of its staff, or reproduclitf!! ~r1his repo~ in ~on~tcllQT~ \\ith the a~~•enisen_ient. p~~motio_n ~r ~ale of~y ~od~ct or p~~cess. ~r in ~nn~c~ion w!lh th~ r~-p~blicouun of1his report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-01 IA American West Client Sample ID: MW-24A_07292021 ANALvr1cAL LAeoRAToR1Es Collection Date: 7/29/2021 700h Received Date: 7/30/2021 11 00h 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1733h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENI00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 ---- Surrogate Units: ftg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.2 55.5 46.5 49.6 50.00 96.3 80-136 50.00 111 85-121 50.00 93.0 78-132 50.00 99-3 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 46 of72 All anolyses applic.1blc lo lhe: CWA. SOWA. Md RCRA are perfom,ed in accordance to NELAC protocols. Per1inent sAmplini:; infornmtion is located 011 the attached COC. Confidential Business lnformal100-This report is prol'ided for 1ho c!\--c-lushci use of the !ddressee. Pririle~es f "u~~cq~1enl ~~e of lhe ~!?'!'e or !his .co~pcmy or nny ,~mber of its s1arr, or reproduclio~ ~~ 1his tepo1! in .con!1ec1ion .. \\·ith 1he a~~'ertise~enl. P~?molio_n ~r ~ale of ~!Y._~rOO~cl or P'_?'Ce!S. ~r in :°nn:_c~ion w!lh th~ 1~pubJie1li011 or !his report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company: Address: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW -------Client Sample ID: MW-24A 07292021 Sample ID: 551444011 Matrix: Ground Water Collect Date: 29-JUL-21 07:00 Receive Date: 02-AUG-21 Collector: Client Project: Client ID: DNMIO0IO0 DNMIO0l ---------------Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method -------------'---------------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.77 +/-0.475 The following Analytical Methods were performed: Method D--'--'es ___ c_ri~ti-"-o"'"n ______ _ EPA 903.0 Test 0.751 1.00 Sun-og~te/Tracer Recove1y Barium Carrier ---------------~ GFPC, Total Alpha Radium, Liquid "As Received" Notes: Counting Uncertainty is calculated at the 68% confidence level (}-sigma). pCi/L JXC9 08/23/21 1649 2157704 Anal st Comments _________ _ Result Nom_in_a_l _ Recovery% ~cceptab!:._ Limits 103 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: OF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 23 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-006 Client Sample ID: MW-25_07282021 Collection Date: 7/28/2021 1000h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/16/2021 1116h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/1 6/2021 1215h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/1 3/2021 14 1 Oh E200.8 0.000500 0.00149 Phone:(801)263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 I 6 I 6h E200.7 10.0 355 Chromium mg/L 8/2/2021 943h 8/13/2021 1410h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/202 l 943h 8/13/2021 141 Oh E200.8 0.0100 < 0.0100 Fax:(801)263-8687 Copper mg/L 8/212021 943h 8/13/2021 1410h E200.8 0.0100 < 0.0100 :-mail: awa1@awal-labs.com Iron mg/L 8/2/2021 943h 8/1 6/2021 1215h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/1 6/2021 1215h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/1 0/2021 1616h E200.7 1.00 121 Manganese mg/L 8/2/2021 943h 8/13/2021 1410h E200.8 0.0100 1.48 Mercury mg/L 8/2/2021 1214h 8/3/202 J 1136h E245.I 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 14 I Oh E200.8 0.0100 0.0169 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1410h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/12/2021 1258h E200.7 1.00 11.3 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 I 4 I Oh E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 8/13/2021 1610h 8/1 6/2021 1031h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 16 I 6h E200.7 10.0 292 Thallium mg/L 8/2/2021 943h 8/1 6/2021 12 I 5h E200.8 0.000500 0.000829 Tin mg/L 8/2/2021 943h 8/13/2021 1410h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/1 6/2021 1215h E200.8 0.000500 0.00621 Vanadium mg/L 8/2/2021 943h 8/10/2021 1 722h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/202 I 14 IOh E200.8 0.0100 < 0.0100 ----- Report Date: 8/24/2021 Page 14 of72 All analyses applic.ible 10 lhe CWA. SDWA. and RCKA are performed in accordance to NELAC protocols. Pcnmc,U sampling jnfomuH,on is locoted on the nunched COC. Conlidentinl Business lnfo1mation: This repon is pro,·ided for the exclusive use of the ~ddressee. P1frile~es of' sub~seq~1ent ~•;e or du: !~:u.1WJ.\J( this .co1~pany or any ~t;mber or its staff, or reproduclla~ ~! 1his repo~ in ~on~ecHon_ with the 0~~1ertise~enl. P~?motio,n ~r ~ale of ?-1!Y. prodl'.CI or p~~ess, ~r in ~onn~c!ion w!lh lh~ r~-f)~blicalion of lhis reporl INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-006 Client Sample ID: MW-25_07282021 Collection Date: 7/28/2021 1000h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1343h E350. l 0.0500 0.374 Bicarbonate (as mg/L 8/2/2021 II OOh SM2320B 1.00 335 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 II OOh SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 8/10/2021 2257h E300.0 10.0 34.2 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 649h E300.0 0.200 0.331 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 -1.26 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1425h E353.2 0.100 < 0.100 Sulfate mg/L 8/10/2021 2257h E300.0 50.0 1,640 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 41.7 Total Cations, meq/L 8/11/2021 1058h Cale. 40.7 Measured Total Dissolved Solids mg/L 7 /30/202 I 1345h SM2540C 20.0 3,100 Jennifer Osborn Total Dissolved Solids 8/11/2021 1058h Cale. 1.17 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 2,650 Calculated QA Officer Report Date: 8/24/2021 Page 27 of 72 All analyses applicable to 1he CW A SOW,\. Md llC'RA are perrom1ed in accordance to NELAC pro1ocols. Pc,dnmt sampling infonnm1on is located <Ml I.he auached COC. Confidential Business Jnfonnation: This report is provided for the exclusi\·e use of the ~ddressee. PriYile~es or~ll~q~ent ~1;e of lhC ~!~111c of lhis _cot~pany or any ~mber of its sl:1ff, or ITi>loducli~! ~f 1his repo~ in .con~cc:1ion .. with the a~~1er1ise~ent. P~?mo1io_n ~r ~ale of ~~Y. ~rodl)Cl or P~?cess, ~r in ~onn~c~ion with th~ r~-p~blicalion of I his report ORGANIC ANALYTICAL REPORT 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-Iabs.com Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-006A Client Sample ID: MW-25_07282021 Collection Date: 7/28/2021 1000h Received Date: 7/30/2021 11 00h Analytical Results Analyzed: 7/30/2021 1554h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total ------------- Jose Rocha QA Officer Surrogate Units: µg/L Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Tofuene-d8 CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260D-W-DENIO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qua! 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked %REC Limits Qual 46,9 50.00 93.7 80-136 59,9 50.00 120 85-121 44.7 50.00 89.4 78-132 48,9 50.00 97.7 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 41 of 72 All annlyses applicablt IQ tho CWA. SDW ,\. and RCRA are performed in accordance to NE LAC pro1oco11-1'ertnn,.,,t s0mphns information is located on lhe allached COC. Confidential 811:1mcss Informal ion; This report is provided for lhl" e..~thm,·e use of lhe ~ddressee. Pri\·ile~es <•!su~tq~enl ~~e ortha ~:-i.nc: er lhis _con:1pnny or nny ~mber or ils staff, or r~ruduct ~ ~( 1his rcp,ot! In ~on~eclion~ wilh the n~~1ertise~ent. P~?moli~n ~r saJe of ?'f ~wod~t or P~?cess, ~r in ~nn:c~ion w~th th~ ~publicmfon or this repon GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ---Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: -------- MW-25 07282021 551444006 Ground Water 28-JUL-21 10:00 02-AUG-21 Client ---------- Project: Client ID: Report Date: August 25, 2021 DNMIO0lO0 DNMIO0I -------- Parameter _ __ _9ualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ---------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.213 0.526 1.00 pCi/L The following Analytical Methods were performed: ---Method __ ___ De-"s"""'c,~·i ~t~io'-n __ _ ---~ ---------EPA 903.0 Surrogate/Tracer Recovery Barium Carrier Notes: Test GFPC, Total Alpha Radium, Liquid "As Received" Counting Uncertainty is calculated at the 68% confidence level ()-sigma). Result JXC9 08/23/21 1649 2157704 Anal st Co:..:.111""111"-'e=n=ts,,___ ______ _ Nominal Recoveryo/~ Acceptable Limits 101 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 18 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-007 Client Sample ID: MW-26_07282021 Collection Date: 7/28/2021 1300h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/202 I 17 56h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 I 7 56h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.000500 0.000595 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 16 I 8h E200.7 10.0 513 Chromium mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0100 < 0.0100 Fax: (801)263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0100 < 0.0100 !-mail : awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.100 0.575 Lead mg/L 8/2/2021 943h 8/13/2021 I 7 56h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1618h E200.7 1.00 171 Manganese mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0100 1.07 Mercury mg/L 8/2/2021 1214h 8/3/202 I 1138h E245.l 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/!2/2021 1300h E200.7 1.00 13.8 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 1035h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1618h E200.7 10.0 179 Thallium mg/L 8/2/2021 943h 8/13/2021 1756h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 1756h E200.8 0.000500 0.0464 Vanadium mg/L 8/2/2021 943h 8/10/2021 1724h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1414h E200.8 0.0100 < 0.0100 Report Date: 8/24/2021 Page 15 of72 All analyses applicabfe 101he CWA. SOWA. Md R RA are performed in accordance to NELAC prolocols. Pemnml sampling information is located on the nunched COC. Conndl.'.nlinl Business lnformalion: This report is pm,·ided for Llh::exclusi\·e use of the ~ddressee. Prfrile~es Of !'iu~scq~enl ~~e or 1he ~:".11e or1his ,co1~pony or any ~~~her of its slofT, or reproductl~ ~( tliis repo~ in .con~ection,. ,,ith lhe a~~·ertise1'!1enl. l'~?moti~ or ~It of~!): ~rod~cl or p1:?cess. ~r in 7°nnt;c~io11 w!lh ,1~ r~•publicaLion of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 202 I Lab Sample ID: 2107791-007 Client Sample ID: MW-26_07282021 Collection Date: 7/28/2021 1300h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual :;alt Lake City, UT 84 l l 9 Ammonia (as N) mg/L 8/4/2021 I 050h 8/4/202 I 1345h E350.I 0.0500 0.459 Bicarbonate (as mg/L 8/2/202 I J I OOh SM2320B 1.00 360 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 11 OOh SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 8/11/2021 008h E300.0 10.0 54.0 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 713h E300.0 0.200 0.234 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 0.789 :-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/202 I I 4 2 8h E353.2 0.100 0.352 Sulfate mg/L 8/11/202 I 008h E300.0 50.0 1,840 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 47.1 Total Cations, meq/L 8/11/202 I 10581, Cale. 47.8 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 3,390 Jennifer Osborn Total Dissolved Solids 8/11/202 I I 058h Cale. 1.13 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/202 I I 058h Cale. 2,990 Calculated QA Officer Report Date: 8/24/2021 Page 28 of 72 All analyses applicable lo lh~ CWA. SDW A. and RCRA are performed in accordance to NELAC rnoiOL:ols. Per11ncnt sornµting inro,n1.i.1lon is located on the attached COC. Couridtotial )Jusanr:ss Information: This •~JM>n Is prm·ided for 1he ~dmi\'t use of the ~ddressee. Pri,·ile~es or 9.u~q~enl ~1~e of lhe ~~e of !his _co':'pimy or nny ~mber of its slaff, orrc-1uocJu,cdO!! ~f 1his ''P3i1 t.n ~OIJ~ttnon .. \\·ith the a~:ertisement, P~?motio.n or ,_,"'lie of?'!> J_MOd~ct or p1:~cess, ~r in ~~-e~ion w~lh th~ r~-p~bli~tion of this report 3440 South 700 West ~alt Lake City, UT 84119 ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-007A Client Sample ID: MW-26_07282021 Collection Date: 7/28/2021 1300h Received Date: 7/30/2021 1100h Analytical Results Analyzed: 8/2/2021 944h Units: µg/L Compound Chloroform Extracted: Dilution Factor: JO CAS Contact: Tanner Holliday Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D Reporting Analytical Number Limit Result Qual 67-66-3 10.0 723 ------ Phone: (80 I) 263-8686 Surrogate -------Units: µg/L CAS Result Amount Spiked %REC Limits Qual Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 I 868-53-7 2037-26-5 482 500.0 534 500.0 468 500.0 502 500.0 --The reporting limits were raised due to high analyte concentrations. Analyzed: 7/30/2021 1614h Extracted: Units: µg/L Dilution Factor: CAS Compound Number 2-Butanone 78-93-3 Acetone 67-64-1 Benzene 71-43-2 Carbon tetrachloride 56-23-5 Chloromethane 74-87-3 Methylene chloride 75-09-2 Naphthalene 91-20-3 Tetrahydrofuran 109-99-9 Toluene 108-88-3 Xylenes, Total 1330-20-7 ----- 96.4 80-136 107 85-121 93.5 78-132 IOI 81-123 Method: SW8260D Reporting Analytical Limit Result Qual 20.0 <20.0 $ 20.0 <20.0 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: l,2-Dichloroethane-d4 17060-07-0 46,2 50.00 92.4 80-136 Surr: 4-Bromofluorobenzene 460-00-4 57.1 50.00 114 85-121 Surr: Dibromofluoromethane 1868-53-7 45.8 50.00 91.5 78-132 Surr: Toluene-d8 2037-26-5 48.2 50.00 96.4 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concenlration is estimated and may be biased low. Report Date: 8/24/2021 Page 42 of 72 AU anolyses applicable to 1hr CWA. SOWA. llDd RCRA ure perfonned in accordance to NE LAC protocols. J>er1inC'f1l sampling informalion is located on the al\ached COC. Confidenuot Business lnformalion: This repon is provide41 for tht t'..\c1USl\c use of the ~ddressee. PriYile~es Of sub!c:q~enl ~~e of lltc ~:u.nc orlhis _co1~pany or any •~~mber of its staIT, or reproducll°!! ~flhis repo~ in ~on~eclion_, wilh the a~~•ertiser~enl, P~?moli~n ~r ~ale o(:1'!Y. rrod~cl or p~~ess, ~r in ~nn:_c!ion \\'!lh lh~ r:publkallon of1his repon GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW Report Date: August 25, 2021 -------------------------------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW-26 07282021 551444007 Ground Water 28-JUL-21 13:00 02-AUG-21 Client Project: Client ID: DNMIO0l00 DNMIO0l ------------------- Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ---- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha I. 71 +/-0.339 0.591 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods w_er_e_p_e_rfi_o_rm_e_d_: _______________________________ _ Method Desg:iption_ _ _______________ Anal stComments EPA 903.0 urrogate/Tracer Recovery Barium Carrier Test ---------___ Result __1-Jominal Recovery% Acceptable Limits GFPC, Total Alpha Radium, Liquid "As Received" 106 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = ample Repo1ti11g Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either Lhe adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 19 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail : awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer ' INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107668-00 I Client Sample ID: MW-27 _ 07222021 Collection Date: 7/22/2021 1220h Received Date: 7/27/2021 955h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Nitrate/Nitrite (as N) mg/L 8/2/2021 I 41 2h E353.2 0.100 6.32 ----- Report Date: 9/30/2021 Page 6 of 15 All anolyses applicnblc 10 1hc CWA. SDWA. nnd RCRA are performed in accordance to NELAC pral«ols Pc111n1:11t sampling information is locoted on the allached COC. Confidential Business Informu.iion: This repor1 is provided for the exclusive use of the ~ddressee. Pri\'ile~es ()f t!U~SCq~enl ?~e of lhe ~:":'U! of lhis .co1~pnny or nny 1~ryiber of its stnrr, or 1c1Jroducti"!! ~rthis repo~ in ~Oll)leclion .. "~lh the n~~•ertise,~ent, P~?moli~n ~r ~ale of ?'!Y. ~rod~t or P~?cess, ~r in ~nn:c!ion w!lh 1h~ r~-publicaliOll or lhis repon 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107668-002 Client Sample ID: MW-28_07232021 Collection Date: 7/23/2021 1115h Received Date: 7/27/2021 955h Analytical Results Date Compound Selenium Uranium Units mg/L mg/L Prepared 7/27/2021 1057h 7/27/2021 1057h Date Analyzed 8/2/202 J 1409h 8/2/2021 1409h Contact: Tanner Holliday DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.00500 0.0185 E200.8 0.00200 0.0138 Report Date: 9/30/2021 Page 4 of 15 All analyses upi,lico.ble ro lhl) CWA. SDWA. and RCRA nre perfom,ed in accordance 10 NELAC pmlQCol'j. Pcnmml siunphno infonnnth>I} is locnted on the allached COC. onfid~rllial Business 1nrormo11on: This repon is pro,•ided for 1he exclusiYe use of the ~ddressee. P1frile~es of sub.se:q!1en1 ~•~e of lhe ~~1e of lhis .co~pony or nny •~'!'her of its sloff, or rqnodlktl~! ~~I his rtpor! in _con!1eo1loc~ with the ~~'ertise1~ent. P~?moti~ o, :lit:. of ~!Y .. ~rod~cl or P•.?Cess, ~r in ~nn~c!ion w!lh th~ r~-p~blication or lhis report 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107668-002 Client Sample ID: MW-28_07232021 Collection Date: 7 /23/202 l 1115h Received Date: 7/27/2021 955h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 8/3/2021 231 lh E300.0 10.0 152 Nitrate/Nitrite (as N) mg/L 8/2/2021 1413h E353.2 0.100 6.09 '@ --------- @ -High RPD due to suspected sample non-homogeneity or matrix interference. 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Report Date: 9/30/2021 Page 7 of 15 All nnnlyses applicnble lo lhe CWA. SOW A. and RCRA nre perl'ormed in I\Ccordonce lo NELAC prolocols. Per1inent sampling infomunion is locnled on the nuached COC. Confidential Business Jnformalion: This repore is provided for lhe c.,clusi\ci use of lhe !ddressee. PriYile~es o,rsub .. seq~ent ~~e of 1he ~~e of !his ,co1~pnnr or MY ,~mber of ils stnIT, or reproduclio~ ~! 1his repo~ in _con~t~tton ... with the IU;~'eliise~ent. P~?moli~ or salt of ~!Y. ~rod~cl or P~?cess, ~r in ~nn:c~ion w!th th~ r~-p~btica1lo11 or lhis repon 3440 South 700 West ~alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107668-003 Client Sample ID: MW-29 _07222021 Collection Date: 7/22/2021 1320h Received Date: 7/27/2021 955h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Uranium mg/L 7/27/2021 1057h 8/2/2021 I 424h E200.8 0.000300 0.0158 --- Report Date: 9/30/202 I Page 5 of 15 All annlyses applicable 10 1ho CWA. SOWA. .utd RCRA ore JlCf romted in accordance to NE LAC protocofs.. Pertinenl sampling inlbrmatio11 is locnled 011 lhe nltached COC. Conndcntial OUJinc:.u: lnformnlion: This report is pro,•ided ro, the exclusin, use of the ~ddressee. Pri,·ile~es of !uti:cq~1ent ~~e of lht' J!:"_l•t or I his _c(u~pn~· or nny ~~mber of ils stnff, orrc,1roduc:ti~ ~( this repm~ in ~on~ection,. with the n~~·ertise~enl. P~?moti~ ~ ltafo of!";~: ~rod1'.cl or P~?Cess, ~r in ~nn~!ion \\'!lh th! •;1Xlblication of 1his repon INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-012 Client Sample ID: MW-30_07292021 Collection Date: 7/29/2021 950h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/16/2021 1204h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1917h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.000500 < 0.000500 Phone: (801)263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 1629h E200.7 10.0 294 Chromium mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 I 425h E200.8 0.0100 < 0.0100 Fax:(801)263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 1917h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 1917h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 J 629h E200.7 1.00 78.8 Manganese mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.0100 < 0.0100 Mercury mg/L 8/2/2021 1214h 8/3/2021 1153h E245.l 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/202 I 943h 8/13/2021 1425h E200.8 0.0200 <0.0200 Potassium mg/L 8/2/2021 943h 8/12/2021 131 lh E200.7 1.00 7.89 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 l 425h E200.8 0.00500 0.0563 QA Officer Silver mg/L 8/13/2021 I 61 Oh 8/16/2021 ll2lh E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/202 I 1629h E200.7 10.0 107 Thallium mg/L 8/2/2021 943h 8/13/2021 I 917h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 1917h E200.8 0.000500 0.00960 Vanadium mg/L 8/2/2021 943h 8/10/2021 1735h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1425h E200.8 0.0100 < 0.0100 ---------- Report Date: 8/24/2021 Page 20 of 72 All analyses applic.iblt.•h) th1.1 CWA. SOWA_ and RCRA .ire perl0m1ed in accordance to NELAC pmuxol Pt rtinmt sampling info1m:u1011 is located on the auached COC. Conlidcntial l3usmess 111rornu11on: This report is proyided for the e~clusive use of the ~ddressee. Pri\·ile~es o! soh,.5c-q~ent ~~e of the ~'.'1:"e of this _cori:1p::my or any ~mber of its stnff, or re11roducll~~ ~r ihis repo~ in ~011!1«t[on_ ,,.ith the a~~1er1isemenl. P~?moli~ ~ De of !"U!,\ ~10dl~cl Of pr_?C"ess, ~r in ~onn:,c!ion w!th th~ r~·p~blication of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-012 Client Sample ID: MW-30_07292021 Collection Date: 7/29/2021 950h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qua! ,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1349h E350.l 0.0500 0.133 Bicarbonate (as mg/L 8/2/202 J 1 J OOh SM2320B 1.00 200 CaCO3) Carbonate (as CaCO3) mg/L 8/2/202 1 11 OOh SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 8/11/2021 1503h E300.0 5.00 188 foll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 958h E300.0 0.100 0.318 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 1.30 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1455h E353.2 0.500 20.6 Sulfate mg/L 8/1 1/2021 1503h E300.0 25.0 754 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 25.3 Total Cations, meq/L 8/11/2021 1058h Cale. 26.0 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 2,010 Jennifer Osborn Total Dissolved Solids 8/11/202 I 1058h Cale. 1.28 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 1,570 Calculated QA Officer Report Date: 8/24/2021 Page 33 of 72 All analyses applicable 10 lhc CWA. SDW A. Md RCRA are perfom1ed in accordance lo NE LAC protocols. Pet1fm.·11t sam1lllng information is located on the attached COC. {'onfidcntial Ulmne~ lnformalion: This report is pro"ided for the exclusive use of the ~ddressee. Prl\'ile~es t:if .s:u~~q~enl ~•~e or the ~~car this _co1~pany or any ~f!lbcr of its slaff, or reproducli°!! ~!'Lhis rcpo(_! in ~on~1ection~ \\~lh lhe a~~·enise~nl. P~?molio:'1 ~ ~:ale of !DJ' ~tod~cl or p~~ss, ~r in ~nn:c!ion w!lh 1h~ r:-publication of this report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-012A American West Client Sample ID: MW-30_07292021 ANALvT1c.-L LAeoRAToR 1es Collection Date: 7/29/2021 950h Received Date: 7/30/2021 11 00h 3440 South 700 West ~alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1753h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 ------ Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 45.8 50.00 56.2 50.00 44.0 50.00 47.7 50.00 ----- 91.6 80-136 112 85-121 88.0 78-132 95.5 81-123 $ -This compound exceeded (low) the control limit/or the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 4 7 of 72 All analyses applicablci 10 lhc CWA. SDWA. and RCJtA are perfom,ed in accordance to NELAC prolocols. P<!nmm\l smnplin,u information is localed on the auached COC. Confid.cnlial Business lnrorm:itton: This report is provided for the exclusi,-e use of1he ~ddressee. Pririle~es f sul~q~enl ~~e or1lu: ~~-ncofthis.cm~p:my or any ~mber of i1s slnfT, or reproduch"!! ~fl.his rq,o~ in ~0~1:et.on ... nilh lhe ~~'ertisemenl. P~?moti~1 ~sale of ?'!Y. ~rod~cl or µi~ess, ~r in ~onn:c~ion w!lh lh~ r:-p~blication of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company: Address: Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW ----------------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW -30 07292021 551444012 Ground Water 29-JUL-21 09:50 02-AUG-21 Client -------------------------Parameter Qualifier -------'- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.208 0.659 1.00 _The following Analytical Methods were per_fo_rm_e_d: __________ _ Project: Client ID: DNMIO0l00 DNMIO0l -------------- Units PF _ ~ Analyst Date Time Batch Method pCi/L JXC9 08/23/21 1649 2157704 Method Descri tion EPA 903.0 ---------------~ __ Analyst Comments Surrogateffracer Recovery __ T_e_s_t Result Nomi~ Recovery% Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 103 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of eitJ1er the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 24 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 202 l Lab Sample ID: 2 l 07791-003 Client Sample ID: MW-31_07272021 Collection Date: 7/27/2021 1255h Received Date: 7/30/2021 l l00h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual Salt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/2021 133 7h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/202 I 943h 8/13/2021 1514h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 133 7h E200.8 0.000500 < 0.000500 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/202 I 1554h E200.7 10.0 395 Chromiwn mg/L 8/2/2021 943h 8/13/2021 1337h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/202 I 943h 8/13/2021 1337h E200.8 0.0100 < 0.0100 Fax:(801)263-8687 Copper mg/L 8/2/2021 943h 8/13/202 I 133 7h E200.8 0.0100 < 0.0100 !-mail: awa1@awal-labs.com Iron mg/L 8/2/202 I 943h 8/13/2021 1514h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 1514h E200.8 0.00100 <0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1554h E200.7 1.00 182 Manganese mg/L 8/2/202 I 943h 8/13/2021 I 33 7h E200.8 0.0100 < 0.0100 Mercury mg/L 8/2/202 I 12 I 4h 8/3/2021 1130h E245.1 0.000500 <0.000500 Jennifer Osborn Molybdenum mg/L 8/2/202 I 943h 8/13/2021 1337h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/202 I 943h 8/13/202 I I 337h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/202 I 943h 8/10/2021 1705h E200.7 1.00 9.58 Jose Rocha Selenium mg/L 8/2/202 I 943h 8/13/2021 1337h E200.8 0.00500 0.0865 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 1020h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1554h E200.7 10.0 132 Thallium mg/L 8/2/2021 943h 8/13/2021 1514h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/13/2021 1337h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 1514h E200.8 0.000500 0.0200 Vanadium mg/L 8/2/2021 943h 8/10/2021 1705h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/202 I 1337h E200.8 0.0100 < 0.0100 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Report Date: 8/24/2021 Page 11 of 72 All tinnlyses applicable lo !he CWA. SDWA. Md R{'RA ore pmfomted in accordance to NE LAC protocols. Pei11.o,cnt s11f1lplm8, informalion is located on the o.llached COC. tonridL•ntial Bw-mcss Information: This repor1 is prO\·ided for lhe exclusi,·e use of the ~ddressee. P1iYile~es o[ sub ... seq~1ent ~1~e of the '!:U.uc-Qfthis ,con,lpnn~ or any ~r:iber of its s1nrr. or reproduc1!~ ~t•his tq,Ot! in ~on~ection,. with the n~~'ertise'"!"ent. P~?mo1i~1 ~ SAtcof ~!~:~rad1~c1 or p1:?Cess, ~r in ~nn~c.tion \\'!th th~ r~-publico.tion or this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, lnc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 202 l Lab Sample ID: 2107791-003 Client Sample ID: MW-3 l _ 07272021 Collection Date: 7/27/2021 1255h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/202 I I 340h £350.1 0.0500 < 0.0500 Bicarbonate (as mg/L 8/2/202 I 11 OOh SM2320B 1.00 205 CaCO3) Carbonate (as CaCO3) mg/L 8/2/202 I 1 I OOh SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 8/101202 I 2059h £300.0 10.0 391 Toll Free: (888) 263-8686 Fluoride mg/L 8/1 1/202 l 538h £300.0 0.200 0.623 Fax: (80 I) 263-8687 Ion Balance % 8/J 1/202 I l 058h Cale. -100 -0.0274 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1421h £353.2 0.100 18.7 Sulfate mg/L 8/J 0/2021 2059h £300.0 50.0 1,210 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 40.7 Total Cations, meq/L 8/11/2021 1058h Cale. 40.7 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 3,100 Jennifer Osborn Total Dissolved Solids 8/J 1/202 I l058h Cale. 1.26 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/J 1/2021 I 058h Cale. 2,460 Calculated QA Officer Report Date: 8/24/2021 Page 24 of72 All analyses applicable to lhe CWA. SOW,\, :ind RCRA are performed m accordance 10 NELAC prolocols. Pcnuncnl sampling ln(ormauon is located on the attached COC. ConfiderHial nusml.'lss Information: This r.cpon tJ pro\'ided for the exdusiYe use of lhe ~ddressee. Prhile~es o!' sub~seq~ent ~~e or the ~~I.Hr! or this _co".1pany or rmy ~mber or its slQff, or reproducll~ ~r1l11s repo~ in ~1eetfon .. \\~th I.he a~~·ertisemenl. P~?moli~ ~ sillr of:"!~ J_X"Od~cl or p•:?cess, ~r in ~m~c~lo11 \\'!lh th~ r::•p~blication or this report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-003A American West Client Sample ID: MW-31_07272021 ANA1vrrcAL r.AaoAAToArrs Collection Date: 7/27/2021 1255h Received Date: 7/30/2021 1100h 3440 South 700 West ,alt Lake City, UT 84119 Phone: (80 l) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1455h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENIO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 ------- Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 ---- 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.0 53.1 45.2 49.2 50.00 94.1 80-136 50.00 106 85-121 50.00 90.4 78-132 50.00 98.5 81-123 $ -This compound exceeded (low) !he con/rol /imit for the CCV. The compound concentralion is estimaled and may be biased low. Report Date: 8/24/2021 Page 3 8 of 72 All analyses applicnbl~ u, !ho CWA. SOWA. :md Re.RA are performed in accordance to NELAC prolocols. P~nioent sampling information is loco1ed on the attached COC. ConlicWn1ial B\1!1Mss Jnformolion: This repon is pro,•ided for the exclusiYe use of the ~ddressee. Pii \'ile~es o;su1!,ffl1~ent ~1~e orlho ~~c of this _co1~pany or any 1~mber or ils staff, or reproducll~ ~~ this repo~ in .con~eclion~ \\ilh the a~~1ertise1~e11t, P~?moli~ ~r sale of~!'. l,ffodl'.Cl or p1:?Cess, ~r in ~nn~c~ion w!lh 1h! r:-publication or this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company: Address: Contact: Project: ----Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-31_07272021 551444003 Ground Water 27-JUL-21 12:55 02-AUG-21 Client -------Project: Client ID: DNMIO0l00 DNMIO0l ------------- Parameter Qualifier Result Uncertainty __ M_D_C ___ RL ____ U_n_its _P_F_ DI~:-Analyst Date Time Batch Method Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.190 0.568 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods were performed: ------------------Method Descri tion__ _ _Anal st Comments EPA 903.0 Surrogate(D·acer Recovery Test Result Nominal Recovery% Accept~ble Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 108 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column header are defined as follows: OF: Dilution Fa<::lor DL: Detection Limit MDA : Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 15 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit American West ANALYTICAL LA80RATORIE6 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-015 Client Sample ID: MW-32_07282021 Collection Date: 7/28/2021 1515h Received Date: 7/28/2021 1515h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 8/11/2021 340h E300.0 2.00 36.5 ------------------- Report Date: 8/24/2021 Page 3 5 of 72 All analyses applicable ~o lhci CWA. SDWA, ~ml RCRA are perfonned in accordance lo NELAC p(010C-ols. P.:nlnml sampling infllfm. ton is localed on lhe auached COC. ('onfidtntial Om:1114,.-ss lnformalion: This repon is pro\'ided for 1he a.,clu.sh·~ use of the ~ddressee. PtiYile~es o; Allb_.s~q~ent ~~e of !he ~:1'.11e of lhis _con:ipany or MY ~'!1ber of its sl:uf, orr'tJlmducuoc~ ~r this repo~ in ~1?«h01~ \\ilh the u~~•ertise~enl. P~?moti~, ~-snli: of :"1> J?fod~cL or P~?cess, ~r in ':°nn~c!ion w!th th~ r~-p~blico1ion of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-004 Client Sample ID: MW-36_07272021 ANALYTICAL LABORATORIES Collection Date: 7/27/2021 1425h Received Date: 7/30/2021 l l00h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 841 I 9 Arsenic mg/L 8/2/202 I 943h 8/13/2021 1741h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 I 5 I 8h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1403h E200.8 0.000500 < 0.000500 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/202 I 1600h E200.7 10.0 443 Chromium mg/L 8/2/2021 943h 8/13/2021 1403h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1403h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 8/2/202 I 943h 8/13/2021 1403h E200.8 0.0100 < 0.0100 !-mail: awal@awal-Iabs.com Iron mg/L 8/2/2021 943h 8/13/2021 1518h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 1518h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/202 I 943h 8/10/202 I 1600h E200.7 1.00 142 Manganese mg/L 8/2/2021 943h 8/13/2021 1403h E200.8 0.0100 < 0.0100 Mercury mg/L 8/2/2021 1214h 8/3/2021 1132h E245.l 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/202 I 943h 8/13/2021 1403h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1403h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/202 I 943h 8/10/2021 1711h E200.7 1.00 13.2 Jose Rocha Selenium mg/L 8/2/202 I 943h 8/13/2021 1403h E200.8 0.00500 0.228 QA Officer Silver mg/L 8/13/2021 161 Oh 8/16/2021 1024h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1600h E200.7 10.0 678 Thallium mg/L 8/2/2021 943h 8/13/2021 15 I 8h E200.8 0.000500 0.000590 Tin mg/L 8/2/202 I 943h 8/13/2021 1403h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 1518h E200.8 0.000500 0.0241 Vanadium mg/L 8/2/2021 943h 8/10/2021 1711h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/1 3/202 I 1403h E200.8 0.0100 < 0.0100 Report Date: 8/24/2021 Page 12 of 72 All Malyses applicable lo lhe CWA SOWA. Md RCRA are performed in accordance to NELAC pmlC'ICOhl, Ptnlnmt sampling informtt.Litlft is located on the auached COC. ConlidCnlint Uusrncss lnform:111on: This report is provided for the exclusire use of1he ~ddressee. P1irile~es o_f sub .. seq~ent ~~e or the !!~J•ll Qf this ,cm~pnny or any ~'!1ber of its staff, or rt!producti~ ~~ 1his repo~ in ~011!1ec:110~ with the a~~•ei1isement, p~~moti~ ~rule of !1'J ~Odl~cl or p,!'ess, ?r in :°nn:c~ion w!th th~ r1;-p~blicatio11 or this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-004 Client Sample ID: MW-36_07272021 ANAlVllCAl LAfl OR/ITORIES Collection Date: 7/27/2021 1425h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1341 h E350.J 0.0500 < 0.0500 Bicarbonate (as mg/L 8/2/2021 11 OOh SM2320B 1.00 300 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 11 OOh SM2320B 1.00 < 1.00 Phone:(801)263-8686 Chloride mg/L 8/10/2021 2210h E300.0 20.0 58.4 foll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 602h E300.0 0.100 0.255 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -JOO -0.673 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1422h E353.2 0.100 0.200 Sulfate mg/L 8110/2021 22 !0h E300.0 100 2,730 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 I 058h Cale. 64.4 Total Cations, meq/L 8/11/202 I I 058h Cale. 63.6 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 4,560 Jennifer Osborn Total Dissolved Solids 8/11/2021 1058h Cale. 1.07 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 I 058h Cale. 4,240 Calculated QA Officer Report Date: 8/24/2021 Page 25 of 72 All analyses applicable IO 1lu: CWA. SDW ,\. and RC-RA are performed in accordance to NELAC protocols. Ptnmcnl s11mpling infornmlion is localed on the attached COC. Confidential Business lnfonnalion: This report is proYided for the exclusiYe use of the ~ddressee. Prfrile~es ~! \.V1!_SC'q~cnl ~~e of du!I ~?'.u,: or this _cm~pany or nny 1~mber or its stnff, or rie1)roduct10!! ~ this ,cpo~ In .co~1eclion,.. with the n~~•ertise,~ent, P~?moli~n ~r ~ale of ?'!·Y. ~rod~cl or P~?ce~s. ~r in ~nn:c,lion w!lh th~ r:~publication of this report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-004A American West Client Sample ID: MW-36_07272021 ANALvr1cAL LABORATOR1Es Collection Date: 7/27/2021 1425h Received Date: 7/30/2021 1100h 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 7/30/2021 1514h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DEN100 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dB 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.4 54.8 46.4 49.9 50.00 96.9 80-136 50.00 110 85-121 50.00 92.7 78-132 50.00 99.7 81-123 $ -This compound exceeded (low) the control limit f or the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 39 of 72 All analyses applicable to thr CWA. SOW,\, aml RCRA are perfom1ed in accordance to NELAC-pro1ocol:s.. rer1ineo1 so.mJll1ns informndon is localed on the attached COC. Con0~itnlial Business lnfornwtion: This repor, is provided for 1he t'l(dwi,•e UJe of the ~ddressee. Pri\·ile~esarsu~q~1ent .u~e orLhe ~~'t(l or1his_co1~pany or My ~mber orils slalT, or 1cpt0ducti°!! ~flhis ,cp01! in ~on?..:ction_ with the u~~·ertise~enl. P~?moliOfl Ofta:lc of ?1r ~rodl'.cl or P~?cess, ~r in ~nn:_c~ion w~lh th~ r:_-public:011011 of'lhis report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-36 07272021 551444004 Ground Water 27-JUL-21 14:25 02-AUG-21 Client ------Project: Client ID: Report Date: August 25, 2021 DNMIO0l00 DNMIO0l Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ---------------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.205 0.590 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods we!:~yerformed: _________ _ Method __ Descri tion ____ Anal st Comments _______ _ EPA 903.0 un-ogar~rrrac r Recovery __ T_e_st __ Result Nominal _B.ecovery% _!cceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 101 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL = Sample Reporting Limit. For metals analy is only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 16 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-013 American West Client Sample ID: MW-38_07292021 ANALYTICAL LABORATORlfS Collection Date: 7/29/2021 800h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943 h 8/13/2021 1932h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1932h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.000500 < 0.000500 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 1631 h E200.7 10.0 472 Chromium mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0100 < 0.0100 ~-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 1932h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/202 I 943h 8/13/2021 1932h E200.8 0.00100 <0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1631h E200.7 1.00 183 Manganese mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0100 < 0.0100 Mercury mg/L 8/2/2021 1214h 8/3/2021 1 I 55h E245.l 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/202 l 1428h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/12/2021 1313h E200.7 1.00 33.0 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.00500 0.145 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 I 144h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/202 I 943h 8/10/2021 1631h E200.7 10.0 432 Thallium mg/L 8/2/2021 943h 8/13/2021 1932h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/202 I 943h 8/13/2021 1428h E200.8 0.100 < 0.100 Uranium mg/L 8/2/202 I 943h 8/13/2021 1932h E200.8 0.000500 0.00575 Vanadium mg/L 8/2/2021 943h 8/10/2021 1737h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1428h E200.8 0.0100 < 0.0100 Report Date: 8/24/2021 Page 21 of 72 All analyses applicable 10th.: CWA" SOWA. and RCRA are perfom,ed in accordance to NELAC JlfOloc.ols. l1e1Hncn1 s:1111n1•llnu 11,form..11ion is located on lhe altached COC. onridf.'T'ltial Busuwss Information: This report is prO\·ided for the exclusfre use of the ~ddressee. Pri,·ile~es of su~Jii!q~enl ~~e or the ~~1e or this _cot~pany or any 1~mber or its stnff, at rq,roducli~ ~!' lhis rq,o.! In ~CN~icehon .. "ilh the a~~•ertise~lefll. P~?moli~ ~We of ~l>. ~rod~cl or p~~s. ~r in ~onn:c~ion \\·!th th~ r1;-publication or this repon INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-013 Client Sample ID: MW-38_07292021 Collection Date: 7/29/2021 800h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 1050h 8/4/2021 1350h E350.l 0.0500 0.0562 Bicarbonate (as mg/L 8/2/2021 I 1 00h SM2320B 1.00 110 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 1 1 00h SM2320B 1.00 < l.00 Phone:(801)263-8686 Chloride mg/L 8/11/2021 316h E300.0 20.0 44.3 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 1021h E300.0 0.500 0.728 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 -0.152 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/6/2021 1452h E353.2 0.200 17.2 Sulfate mg/L 8/11/2021 3 16h E300.0 100 2,630 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 58.4 Total Cations, meq/L 8/l 1/2021 1058h Cale. 58.3 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 4,860 Jennifer Osborn Total Dissolved Solids 8/11/2021 1058h Cale. 1.25 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 I 058h Cale. 3,880 Calculated QA Officer ----- Report Date: 8/24/2021 Page 34 of 72 All analyses applicab\e.10 lhc CWA. SOWA. ni'KJ R RA are performed in accordance to NELAC protocols. PerUnrnl sampling information is loCDted on lhe attached COC. onfidcnlial Business In(o,ni.udon: TI1is report is provided for the exclusiYe use of the ~ddressee. Pri,·ile~es af S\1~q~en1 ~~e of 1h~ ~~\C or !his .co1~pany or M)' •~':1ber of its slaff, or reproducll~ ~I'd.tis repo~ in ~o~leclion,. wilh lhe n~~•ertisemenl. P~?moli~n o:r~,le of ~!Y. ~rod~t or Pf'.O(ess, ~r in ~nn~c~ion \\'!lh th7 r~-p~blication or this report ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-0BA American West Client Sample ID: MW-38_07292021 ANALvr,cAL LAsoAAroA1es Collection Date: 7/29/2021 800h Received Date: 7 /30/202 I I IO0h 3440 South 700 West ;;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Analytical Results Analyzed: 8/2/2021 924h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Jose Rocha QA Officer Surrogate Units: µg/L Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dB Extracted: Dilution Factor: CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Contact: Tanner Holliday Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Result Amount Spiked ¾REC Limits Qual 47.6 50.00 95.2 80-136 53.7 50.00 107 85-121 46.1 50.00 92.3 78-132 49.3 50.00 98.7 81-123 Report Date: 8/24/2021 Page 48 of72 All analyses applicable 10 1hc CWA. SDW 1\. ru1d RC'RA are performed in accordance to NE LAC 1iro1ocols. l'cmm.111 sampling information is located on Lhe au ached COC. Confldr:ntinl Business Information: This repon is pro,•ided for lhe e.xclusire use of lhe ~ddressee. Pri,·ile~es <'tr ~u~q~nf ~~e of the ~~r.ne of this .con,1pa11y or any 1~7~ber of its staff, o(n::productlo~ ~this repo~ in .co~ection~ H·ith the ~~'ertise-:1en1. P:?moti°'.° ~r :i;oJe or~!Y. ~rod~ct or P~?cess, ~r in :onn:c~ion w~lh th~ r~-publication of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Certificate of Analysis Report Date: August 25, 2021 Company : Address: Contact: Project: Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW -----------------Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: MW -38 07292021 551444013 Ground Water 29-JUL-21 08:00 02-AUG-21 Client Project: Client ID: DNMIO0lO0 DNMIO0l -------------- Parameter Qualifier Result Uncertainty Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.236 The following Analytical Methods were performed: Method Descri tion EPA 903.0 MDC RL Units PF D!._ Analyst Date Time Batch Method 0.528 1.00 pCi/L JXC9 08/23/21 1649 2157704 Anal st Comment_ _________ _ Surrogate/Tracer Recovery Barium Carrier Test Result N_o_m_in_a_l _Recoveryo/o Acceptable Limits --------GFPC, Total Alpha Radium, Liquid "As Received" 108 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL = Sample Repmting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defi~ed as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 25 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: ample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-008 Client Sample ID: MW-39 _07282021 ANALYTICAL LAOORATORIES Collection Date: 7/28/2021 1450h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/16/2021 1132h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1800h E200.8 0.000500 0.00562 Cadmium mg/L 8/2/2021 943h 8/13/2021 I 417h E200.8 0.000500 0.00303 Phone: (801) 263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 1621h E200.7 10.0 452 Chromium mg/L 8/2/2021 943h 8/131202 I 14 17h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/212021 943h 8/1312021 1417h E200.8 0.0100 0.0669 Fax: (80 I) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 14 I 7h E200.8 0.0100 0.0277 !-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 1454h E200.8 1.00 13.4 Lead mg/L 8/2/2021 943h 8/13/2021 1800h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/212021 943h 8/l 0/2021 1621 h E200.7 1.00 206 Manganese mg/L 8/2/2021 943h 8/13/2021 1454h E200.8 0.0200 2.68 Mercury mg/L 8/2/2021 1214h 8/3/202 I 1144h E245.1 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8113/2021 1417h E200.8 0.0100 < 0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/202 I 14 I 7h E200.8 0.0200 0.0364 Potassium mg/L 8/2/2021 943h 8/12/2021 1302h E200.7 2.00 16.4 Jose Rocha Selenium mg/L 81212021 943h 8/1312021 1417h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 8113/2021 1610h 8/16/2021 1038h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1621h E200.7 10.0 508 Thallium mg/L 8/2/2021 943h 8/131202 I 1800h £200.8 0.000500 0.00348 Tin mg/L 8/2/2021 943h 8/13/2021 1417h E200.8 0.100 < 0.100 Uranium mg/L 812/2021 943h 8/13/2021 1800h £200.8 0.000500 0.0117 Vanadium mg/L 8/2/2021 943h 8/11/202 I 1800h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/1312021 1417h E200.8 0.0100 0.234 Report Date: 8/24/202 I Page 16 of 72 All analyses applic.Jble 10 lhe CWA. SOWA. ood RCRA me perfom1ed in accordance lo NELAC protocols. rcninmt sampling inforn11uiun is located on the atlached COC. Confidenliul Business Information: This repon is provided for the exclusi\"e use of the ~ddressee. Pri,·ile~es of sub~seq~1enl ~1~e of lhc-?.~1c or this _co~pany or nny 1~mber of ils slnff, 01 reproducll~~ ~r this repo~ in _con?~<1ior~ \,ith the "~'.'ertise1~enL P~?motio_n ~r sale of ~!Y. ~rodL~cl or p~~cess. ~r in 7orm:c~ion w~th th~ r~·publication of Lhis repor1 INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-008 Client Sample ID: MW-39 _07282021 Collection Date: 7/28/2021 1450h Received Date: 7/30/2021 l IO0h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia ( as N) mg/L 8/4/2021 1050h 8/4/202 I 1346h E350.l 0.0500 0.187 Bicarbonate (as mg/L 8/2/2021 I 100h SM2320B 1.00 < 1.00 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 11 OOh SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 8/11/2021 031h E300.0 20.0 42.7 Toll Free: (888) 263-8686 Fluoride mg/L 8/l 1/2021 736h E300.0 0.500 0.727 Fax:(801)263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 -4.35 !-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1430h E353 .2 0.100 2.50 Sulfate mg/L 8/11/2021 031h E300.0 100 3,190 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 67.7 Total Cations, meq/L 8/1 l/2021 1058h Cale. 62.0 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 5,080 Jennifer Osborn Total Dissolved Solids 8/11/2021 1058h Cale. 1.15 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 4,420 Calculated QA Officer Report Date: 8/24/2021 Page 29 of 72 All analyses applicable 10 1he CWA. SDWA. and RCRA are perfom1ed in accordance to NELAC p1olorols. renlnml samplinu informal ion is located on t.he attached COC. ConOliential Business Lnformalion: TI1ls report is proyided for lhe e..,,:('l~,\~ use of lhe ~ddressee. Pri\·ile~es 9f su~q~enl ~~e of the ~~1e of this _co1~pa11y or M)' ~mber or its slaIT, o, •~111oduc11~ ~r 1his ,cpor! in .co~1eclion~ wilh the a~~·ertisemenl. P~?moti~, ! SillC of ~!Y. ~rodl~ct or p1:?Cess, ~r in ':°nn:c.1io11 w!lh th~ r~•p~htlccJion or this report ORGANIC ANALYTICAL REPORT 3440 South 700 West ;alt Lake City, UT 841 I 9 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-008A Client Sample ID: MW-39 _07282021 Collection Date: 7/28/2021 1450h Received Date: 7/30/2021 1 IO0h Analytical Results Analyzed: 7/30/2021 1634h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Contact: Tanner Holliday Test Code: 8260D-W-DENI00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 ------ 17060-07-0 460-00-4 1868-53-7 2037-26-5 47.0 52.9 44.7 48.8 50.00 94.0 80-136 50.00 l06 85-121 50.00 89.3 78-132 50.00 97.5 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 43 of 72 All analyses applicable 101he ('WA, SOWA. an,1 RCRA are performed in accordance to NELAC prorocols. Pertinenl sau\J)fin.g information is located on the auached COC. Confidenlial Business lnformalion: This report is provided for thecu:lu1.l\c I.lie of \he ~ddressee. Prfrile~es or ~u~sc-q~tm• ~~(! oflhc l!~•.na-of I his .co,~pany OT nny ~mber or ils staff', or ~oduclio~ ~~ I his re,~; ln fOL~eclion __ ,,,ith the n~~·er1ise~enl, P~?motio,n ~r sale of ?1!Y. ~rod~ct or p1:?Cess. ~r in ~onn~c!ion \\'~th th~ r;,-publi(:atiOO or this repon GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-39 07282021 551444008 Ground Water 28-JUL-21 14:50 02-AUG-21 Client ---------- ------------------ Project: Client ID: Report Date: August 25, 2021 DNMIO0I00 DNMIO0I Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method -------- Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha 2.50 +/-0.412 0.573 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods were performed: ------------------Method Descri tion Anal st Commen.=tc::..s _________ _ I EPA 903.0 Surrogate/Tracer Recovery_ Test ___ _ __ R_e_s_u_lt __ N_o_min~ecovery% ~ceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 101 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). RL = Sample Repo1ting Limit. For metals analysi only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 20 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-009 Client Sample ID: MW-40_07282021 ANALYTICAL LABORATORIES Collection Date: 7/28/2021 1040h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/13/2021 1826h E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/13/2021 1826h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.000500 < 0.000500 Phone:(801)263-8686 Calcium mg/L 8/2/2021 943h 8/10/2021 1623h E200.7 10.0 459 Chromium mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.0100 < 0.0100 Fax: (80 l) 263-8687 Copper mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.0100 0.0113 ~-mail: awal@awal-labs.com Iron mg/L 8/2/2021 943h 8/13/2021 1826h E200.8 0.0300 < 0.0300 Lead mg/L 8/2/2021 943h 8/13/2021 I 826h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1623h E200.7 1.00 187 Manganese mg/L 8/2/2021 943h 8/13/2021 1421 h E200.8 0.0100 0.0732 Mercury mg/L 8/2/2021 1214h 8/3/2021 1146h E245.J 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.0100 <0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/12/2021 1305h E200.7 1.00 9.94 Jose Rocha Selenium mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.00500 0.202 QA Officer Silver mg/L 8/13/2021 1610h 8/16/2021 1053h E200.8 0.0100 < 0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1623h E200.7 10.0 315 Thallium mg/L 8/2/2021 943h 8/J 3/2021 1826h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/13/2021 1421h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/13/2021 1826h E200.8 0.000500 0.0199 Vanadium mg/L 8/2/2021 943h 8/10/2021 1729h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/2021 1826h E200.8 0.0100 < 0.0100 Report Date: 8/24/2021 Page 17 of 72 All analyses applicable to lhc CWA. SOW,\. ;uKI RCRA .ire performed in accordance to NELAC pro-tocols. Pt:ninent sampling information is located on the auached COC. C'o11J1dcntial BuiHWss Information: This repon is provided for the exclusiYe use of the ~ddressee. Prhile~es of s~~q~1ent ~1~e or lhC' !!:1'.neor this _con:ipany or nny '~f!!ber orits slnff, or 1ep1gduc1I~ ~~•his repo~ in ~on~ection~ wilh tile ~~'ertisement p~omoli~ oc snle of~ rrod~ct or P~?cess. ~r in ~onn~!ion \\'!lh th~ n;:•publicalion of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2 02 1 Lab Sample ID: 2107791-009 Client Sample ID: MW-40_07282021 Collection Date: 7/28/2021 1040h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ;alt Lake City, UT 84119 Ammonia ( as N) mg/L 8/4/2021 1050h 8/4/2021 1346h E350.l 0.0500 < 0.0500 Bicarbonate (as mg/L 8/2/2021 I l OOh SM2320B 1.00 235 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 l l OOh SM2320B 1.00 < 1.00 Phone: (80 I) 263-8686 Chloride mg/L 8/11/2021 055h E300.0 10.0 35.9 Toll Free: (888) 263-8686 Fluoride mg/L 8/l l /2021 800h E300.0 0.500 0.722 Fax: (80 I) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 2.29 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1433h E353.2 0.100 2.85 Sulfate mg/L 8/11/2021 055h E300.0 50.0 2,120 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale. 49.9 Total Cations, meq/L 8/11/2021 1058h Cale. 52.3 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 4,290 Jennifer Osborn Total Dissolved Solids 8/l 1/2021 I 058h Cale. 1.31 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 3,270 Calculated QA Officer Report Date: 8/24/2021 Page 30 of 72 All analyses applico.blt" 10 iho CWA_ SDW .A. tv1d RC-RA are perfonned in accordance to NELAC protocols. Penmen I samplin!l information is located on the alL.1ched COC. tOfHidcntial Uusmess Information: This report is provided for the C.'i:ChD.I\C: use or the ~ddressee. PriYile~es of su~eq~ent ~~e of 1hc !!~w., or t~is _co,~pany or any ~r:nber or its slaff, or reproduct °!! ~r1his rep01! in ~on~eclion,. with the a~~·ertisemenl. P~?moli°!1 or Rle of !'1~ _ t)f()d~cl or P~?cess, ~r in ~nm;_c~ion w!lh lh~ r~-p~bl•cation of lhis report ORGANIC ANALYTICAL REPORT 3440 South 700 West ;alt Lake City, UT 84 I 19 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-009A Client Sample ID: MW-40_07282021 Collection Date: 7/28/2021 1040h Received Date: 7/30/2021 11 O0h Analytical Results Analyzed: 7/30/2021 1653h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Contact: Tanner Holliday Test Code: 8260D-W-DENJ00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.6 50.00 59.8 50.00 46.3 50.00 50.5 50.00 ----- 97.2 80-136 120 85-121 92.6 78-132 IOI 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 44 of 72 All analyses applicnble to the CW A. SDWA .. Md R.CltA are performed in accordance 10 NELAC protocols. Pc.-nmtnl si:implm.G_ infonnn1ion is located on the auached COC. Conlidimliol Business lnfonn:iuon: This report is pro,•ided for the C.\(htii\~ Lile of lhe ~ddressee. Pri,·ile~es o,r su~seq~1ent ~e or 1J1t' ~??'."t or1his _co~pany or any ~mber of ils slaff, or rel)roducll~! ~this ropot! in ~on~~l10t~ with the ~~1crtise1~ent. P~?moti~!'' ornle or ~!Y. ~rod~ct (It P•.~ess. ~r in ~onn~c~ion w~lh th~ r~•publiaitioo of I his repon GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company: Address: Contact: Project: ----Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Ms. Kathy Weinel White Mesa Mill GW MW-40 07282021 551444009 Ground Water 28-JUL-21 10:40 02-AUG-21 Client Project: Client ID: Report Date: August 25, 2021 DNMI00100 DNMI001 ----------------------------------------Parameter Qualifier Result Uncertainty MDC RL Units PF DF Analyst Date Time Batch Method ------Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.202 0.416 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods were performed: Method ___ De-=-sc=r=i -'-'ti=o=n ___________________ ...:..A"'-'n0~a=l st Comments _________ _ EPA 903.0 Surrogate/Tracer Recovery Barium Carrier Notes: Test --------------GFPC, Total Alpha Radium, Liquid "As Received" Counting Uncertainty is calculated at the 68% confidence level (I-sigma). Result Recovery% Acceptable Limits -------~---Nominal 105 (25%-125%) SRL = Sample Reporting Limit. For metals analysis only. When th sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined as follows: DF: Dilution Factor DL: Detection Limit MDA: Minimum Detectable Activity MDC: Minimum Detectable Concentration Page 21 of27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Repo1ting Limit SQL: Sample Quantitation Limit INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-005 Client Sample ID: MW-65_07272021 ANALYTICAL LABORATORIES Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 1100h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ~alt Lake City, UT 84119 Arsenic mg/L 8/2/2021 943h 8/16/2021 l I OOh E200.8 0.00500 < 0.00500 Beryllium mg/L 8/2/2021 943h 8/16/2021 1231h E200.8 0.000500 < 0.000500 Cadmium mg/L 8/2/2021 943h 8/13/2021 1407h E200.8 0.000500 0.00130 Phone:(801)263-8686 Calcium mg/L 8/2/202 J 943h 8/10/2021 1614h E200.7 10.0 508 Chromium mg/L 8/2/2021 943h 8/13/2021 1407h E200.8 0.0250 < 0.0250 Toll Free: (888) 263-8686 Cobalt mg/L 8/2/2021 943h 8/13/2021 1407h E200.8 0.0100 < 0.0100 Fax: (801) 263-8687 Copper mg/L 8/2/2021 943h 8/13/202 I 1407h E200.8 0.0100 <0.0100 ~-mail: awal@awal-labs.com Iron mg/L 8/2/202 l 943h 8/16/202 J 123 I h E200.8 0.0300 <0.0300 Lead mg/L 8/2/2021 943h 8/16/2021 1231h E200.8 0.00100 < 0.00100 web: www.awal-labs.com Magnesium mg/L 8/2/2021 943h 8/10/2021 1614h E200.7 1.00 160 Manganese mg/L 8/2/2021 943h 8/13/2021 1407h E200.8 0.0100 1.85 Mercury mg/L 8/2/2021 1214h 8/3/2021 J I 34h E245.l 0.000500 < 0.000500 Jennifer Osborn Molybdenum mg/L 8/2/2021 943h 8/13/202 J 1407h E200.8 0.0100 <0.0100 Laboratory Director Nickel mg/L 8/2/2021 943h 8/l 3/202 I 1407h E200.8 0.0200 < 0.0200 Potassium mg/L 8/2/2021 943h 8/12/2021 1256h E200.7 1.00 14.3 Jose Rocha Selenium mg/L 8/2/202 J 943h 8/13/2021 1407h E200.8 0.00500 < 0.00500 QA Officer Silver mg/L 8/13/2021 1610h 8/16/202 J 1027h E200.8 0.0100 <0.0100 Sodium mg/L 8/2/2021 943h 8/10/2021 1614h E200.7 10.0 338 Thallium mg/L 8/2/2021 943h 8/16/2021 1231h E200.8 0.000500 < 0.000500 Tin mg/L 8/2/2021 943h 8/l 3/2021 1407h E200.8 0.100 < 0.100 Uranium mg/L 8/2/2021 943h 8/16/2021 1231 h E200.8 0.000500 0.0573 Vanadium mg/L 8/2/2021 943h 8/10/2021 1720h E200.7 0.0150 < 0.0150 Zinc mg/L 8/2/2021 943h 8/13/202 l 1407h E200.8 0.0100 0.0211 Report Date: 8/24/2021 Page 13 of 72 All analyses applicable lo lhe CWA. SOW A. nnd R RA are performed in accordance to NELAC protocols. Pemnml sampling inform.itioo is locoted on lhe 11\lnched COC. CO(Jfidcntiol liu,:m~s lnfonnolion: This reror1 is pro\'ided for the exclusire use or the ~ddressee. Pri,·ile~es of ,:u~q!1ent ~1~e of ll1c_2~ or this ,coi~pnny or nny ~mber of ils stoff, or fCIH~ucl)~ ~~ lhis rep~~ in .con~~lion. \\ilh the a~~·ertise~ent. P~?moti°!' ~r ~e of~·. ~11och'.ct or p1:?cess, ?r in ~onn~!ion w!lh th~ r~-publication of Jhis repori INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Sample ID: 2107791-005 Client Sample ID: MW-65_07272021 Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 1100h Analytical Results Date Date Method Reporting Analytical 3440 South 700 West Compound Units Prepared Analyzed Used Limit Result Qual ,alt Lake City, UT 84119 Ammonia (as N) mg/L 8/4/2021 I 050h 8/4/2021 1342h E350.I 0.0500 < 0.0500 Bicarbonate (as mg/L 81212021 1 1 om, SM2320B 1.00 415 CaCO3) Carbonate (as CaCO3) mg/L 8/2/2021 II OOh SM2320B 1.00 < 1.00 Phone: (801) 263-8686 Chloride mg/L 8/10/2021 2233h E300.0 10.0 19.2 Toll Free: (888) 263-8686 Fluoride mg/L 8/11/2021 1419h E300.0 0.100 0.103 Fax: (801) 263-8687 Ion Balance % 8/11/2021 1058h Cale. -100 -0.883 ~-mail: awal@awal-labs.com Nitrate/Nitrite (as N) mg/L 8/2/2021 1424h E353.2 0.100 < 0.100 Sulfate mg/L 8/l 0/2021 2233h E300.0 50.0 2,190 web: www.awal-labs.com Total Anions, Measured meq/L 8/11/2021 1058h Cale, 54.5 Total Cations, meq/L 8/11/2021 1058h Cale. 53.5 Measured Total Dissolved Solids mg/L 7/30/2021 1345h SM2540C 20.0 4,230 Jennifer Osborn Total Dissolved Solids 8/1 1/2021 1058h Cale. 1.22 Laboratory Director Ratio, Measured/Calculated Jose Rocha Total Dissolved Solids, mg/L 8/11/2021 1058h Cale. 3,480 Calculated QA Officer Report Date: 8/24/2021 Page 26 of72 All analyses applicable lu !he CW A. SDWA. and RCRA are perfom1ed in accordance to NELAC protocols. 11c11int.'11l sampling inforrn1111on is located on the au ached COC. Confidential Business Information: This repon is provided for the e:xdusi\·e use of !he ~ddrcssee. Pri,·ile~es o,r,ub .. ~q~enl ~•~e or the ~~w: n(1his _c01~pany or nny 1~mber of its st:tff, or reproductiUf! ~~lhis repo~ in ~"!'«h n ... \1-ith 1he n~~•er1isemen1, P~?moli~ or sale of~!). ~rod~ct or P~?Cess, ?r in ~nn~~~ion w!Lh th~ r~-p~blicaLion or lhis report ORGANIC ANALYTICAL REPORT 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Client: Energy Fuels Resources, Inc. Project: 3rd Quarter Ground Water 2021 Lab Sample lD: 2107791-005A Client Sample ID: MW-65_07272021 Collection Date: 7/27/2021 1450h Received Date: 7/30/2021 1100h Analytical Results Analyzed: 7/30/2021 1534h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osborn Toluene Laboratory Director Xylenes, Total Contact: Tanner Holliday Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 108-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 --------------- Jose Rocha QA Officer Surrogate Units: µg/L Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 CAS 17060-07-0 460-00-4 1868-53-7 2037-26-5 Result Amount Spiked ¾REC Limits Qual ---- 46.6 50.00 93.1 80-136 54.8 50.00 110 85-121 44.6 50.00 89.2 78-132 48.6 50.00 97.1 81-123 $ -This compound exceeded (low) the control limit for the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 40 of 72 All Rnillyses applicabh.,10 lhc CWA. SDWA. :md ltC'ltA are performed in accordance to NELAC ptOlocols. Pot1incnl samplu\,g infontmuoo is localed 011 t11e auached COC. Conl'idt-ntial Business Information: This report is pro\'ided for the csclush--c use oflhe ~ddressee. PriYile~es of subfCq~enl ~•?e of the ~!~1e or lhis ,co1~pnny or any ~~ber of its sl.iff, or reproduc(iO!! ~r1his rl:~ fn ~on~tcl100 .. ,~·ith lhe a~~1ertise~ent. P~?moli~ Ot' lJIJe of :U!Y. ~rod~ct or P~?Cess. ~r in 7°nm;c!ion w~lh th~ r~-p~hfieru1on of this report GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Company : Address: Certificate of Analysis Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Contact: Ms. Kathy Weinel Project: White Mesa Mill GW Report Date: August 25, 202 I ---------------------------Client Sample ID: MW-65 07272021 Project: DNMIO0 100 Sample ID: 551444005 Client ID: DNMIO0I Matrix: Ground Water Collect Date: 27-JUL-21 14:50 Receive Date: 02-AUG-21 Collector: Client -------Parameter __ Qualifier Result Uncertain_ty..c-_ __ M_DC __ RL ___ U_n_it_s __ P_F_DF Analyst Date Time _Ba_tc_h Method Rad Gas Flow Proportional Counting GFPC, Total Alpha Radium, Liquid "As Received" Gross Radium Alpha U 1.00 +/-0.143 0.523 1.00 pCi/L JXC9 08/23/21 1649 2157704 The following Analytical Methods were performed: ------------------------Method Descri tio1_1 _________ _ Anal st Comments _________ _ EPA 903.0 Surro~ate/Tracer Recov~ry __ T_e_st ___ _ _ ____ R_esult __ N_omin_al __ R_e_coveryo/~ Acceptable Limits Barium Carrier GFPC, Total Alpha Radium, Liquid "As Received" 105 (25%-125%) Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). SRL = Sample Reporting Limit. For metals analysis only. When the sample is U qualified and ND, the SRL column reports the value which is the greater of either the adjusted MDL or the CRDL. Column headers are defined a follows: DF: Dilution Factor DL: Detection Limit MDA : Minimum Detectable Activity MDC: Minim.um Detectable Concentration Page 17 of 27 SDG: 551444 Le/LC: Critical Level PF: Prep Factor RL: Reporting Limit SQL: Sample Quantitation Limit ORGANIC ANALYTICAL REPORT 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. 3rd Quarter Ground Water 202 I 2107791-014A Client Sample ID: Trip Blank Collection Date: 7/27/2021 I 125h Received Date: 7/30/2021 I 100h Analytical Results Analyzed: 7/30/2021 1355h Units: µg/L Compound 2-Butanone Acetone Benzene Carbon tetrachloride Chloroform Chloromethane Methylene chloride Naphthalene Extracted: Dilution Factor: Tetrahydrofuran Jennifer Osbom Toluene Laboratory Director Xylenes, Total Contact: Tanner Holliday Test Code: 8260D-W-DENIO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 78-93-3 20.0 <20.0 $ 67-64-1 20.0 <20.0 71-43-2 1.00 < 1.00 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 74-87-3 1.00 < 1.00 75-09-2 1.00 < 1.00 91-20-3 1.00 < 1.00 109-99-9 1.00 < 1.00 I 08-88-3 1.00 < 1.00 1330-20-7 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Jose Rocha QA Officer Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.2 52.4 46.5 49.9 50.00 96.4 80-136 50.00 105 85-121 50.00 92.9 78-132 50.00 99.7 81-123 $ -This compound exceeded (low) the control limit/or the CCV. The compound concentration is estimated and may be biased low. Report Date: 8/24/2021 Page 49 of 72 All analyses applic□blci to 1h~1 CWA. SOWA. and RCRA are perrom1ed in accordance to NELAC pro1ocols. P~rhr\enl somptms infonmulon is located on the allached COC. oolidrntial BU"111t-ss lnfomm.\lon: This k'IK1111s provided for the exclusiYe use oflhe ~ddressee. Pri,·ile~es o[ J.u~cq~enl ~~e of lhe ~~1e of lhis _co,~p.Jny or any 1~mber of its slnff, or rc:produch~ ~r !his fq>of~ ln _con~1C<'IIOI~ "ilh lhe ~~·ertise1~enL p~~moti~ or s:i.lc of~!}: r,od~cl o, JM;~ess, ~r in ~,:<~ion w'.lh th~ r~-p~blicalion of this repon 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 l) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 3rd Quarter Ground Water 2021 Dear Tanner Holliday: Lab Set ID: 2107637 American West Analytical Laboratories received sample(s) on 7/26/2021 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the repo1t is equival ent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Digitally signed by J • f . Jennifer Osborn e n n I e r DN; cn=Jennlfer Osborn, o=AWAL, ou=Organics, 0 b . email=jenn@awal-labs. S Or r:'\ com, c=US I I Date: 2021 .08.1 o Approved by: 12:41 :34-oe·oo· Laboratory Director or designee Report Date: 8/10/2021 Page I of8 All noU>i)~CI applltolllrio lhu CWA, SOWA, nnd I\CRA m" 1><rrom"'d m nccardonco 10 l!I.A(' p,01o«>I~ l'<ninontJrim111in~ ln(ornuufo,, l0<·n1•d ll<I the ~ll~cho<I COC\ ('o,10d,•mlnl llus ,,.., l11fo11111ulu,r ,1, r~11u11 I, pm,ldod (ortho oxclus110 .so oflho ~ddn.'ii-cc l11wllt-~~af $n~c-q~111 ~ of the ~!~e or 1hli. .eon,,pa:n} ,1rnnr ~1!'bcrofi~$Ulrf, or ,~1mxluct1on ()f1l11J rerun in connccuon with 1hc n,hcct C11k.'m.1K"omollon ,,r :\lcor~!>" ~,~t.hkt or pl(M.°clS, nr m to4U~c.uon ,,tth 1ht n:,pubticc1ion orthl, r~pon 3440 South 700 West ;aJt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mai I: awnl@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer SAMPLE SUMMARY Client: Project: Lab Set ID: Energy Fuels Resources, Inc. 3rd Quarter Ground Water 2021 2107637 Date Received: 7/26/2021 1055h Lab Sample ID Client Sample ID Date Collected 2107637-00IA MW-12 07212021 7/21 /2021 1355h Contact: Tanner Holliday Matrix Analysis Aqueous-ICPMS Metals, Dissolved Report Date: 8/10/2021 Page 2 of 8 All anol)·m •11/dlcahlc 1~ 111, CW/\, Sl)Wi\, ond RCRi\ (11011'rfom,ud m nt<onL,nca 10 Nlil.i\(' 1un1<H:ol, Pct1m<1>\ 1nmplin~ i11r,1nu,d<H> 1, loco1ed 011 1hCD11o<h<d C'O<' ('onOMnlinl llu11n 1nrorr11Ai1011 Thb ra1>011 l1 J>1\'J1hled ronh•«•lnmc u,c or the !ddtmt!C. f>r'i,· It~~ of Sl.l~C'fl~U ~ or1hc ~~ of1h .('()f~l-01~ Of~· -~~\l~c,(lb stt\lT, 0~ rquoducll~ ~f this rcro~ in Yo''!lr..'fllon .. wuh lhc ~,on Cl~Wm. J\~011\0111'1~1 '>! lllet or!"P f!ID(fL~I or P•.~~ , ~r Ill ~111~'{;~1on "!th I~ •~P~hfkQdOn of 1hlr. "'JWI 3440 South 700 West Salt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awol@awnl-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: 3rd Quarter Ground Water 2021 2107637 7/26/2021 7/21/2021 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 8/10/2021 Page 3 of 8 All OIW)'$.,. •Pflhcoblo 10 ihc rw,,.' OWA. Md RCRA .,. µ,rf\)mk'\110 OC<Ordonto 10 Nnt,,\(' pm1oco1, l'onmcnt >alllplin~ lnrOt1111tU011 ,. loc111cJ Oh ~•-•11nch<d (,'()(' C'ooOdc111lnl Uu,ln<>1 lnfom10I UII. 11,1, 1q>on • pro11d,d for ih< <«lu,no "" ortho ~dtlt~ Pridl!.!~~ ori:ul!.5C\l~~u ~Ji: orlht ~~,1,1 or1h1s1tot~11m1~ or 0.1\\' 1~!~\IK"f"Orh~ ,t~rr. or r'cjUOl.lucll~! ~flhi1 rcpot! in ~tM~lilChon .. whh tho 11!\"tUI c1w.,u, 1•~oh1U41a:', ~-Hl~ Of!1J!r p1CMh~I Of P~?C , ~ 111 ~1u1~C~1on ''!lh 1~ t~J\ubllcntlon ofth S ,~po,n Client: Energy Fuels Resources, Inc. Lab Set ID: 2107637 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: LCS-78567 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.192 Uranium 0.198 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com ..QC SUMMARY REPORT Contact: Dept: QC Type: ---- Reporting Amount Spiked Units Method MDL Limit 08/02/2021 1346h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 Tanner Holliday ME LCS Spike Ref. Amount %REC 0 95.8 0 98.9 Limits 85 -115 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Repon Date: 8/10/2021 Page 5 of 8 a~yscs:,ppliclble 101hcCWA. SOWA. and RCRA an, pt'ffom1cd m ucco.-dancc 10 NEL-\Cpro1«ols Pmmcnl S3tllplmg inform:iuon is IOC21Cd on d,eattacbodCOC. Confrdcnti:Jl Business lnform:ilion This report ospmvodod fonhcc,cdus,,·c uscofthc:odmt:sstt Prh'ilq,,,esof~ oseoftt ncoftlus coml)Ml)I or any mm,berofitsstnff.orrcproduwon of1his r,-pon m conno:c1,on ,.,l.h 1hc311vmiscmcnl. prornouon Cll"s:tlc ofrnry produa or process. or m conrx-ction \\11.h thc rc-publlcnion ofdus rrpon for:,nypurp«sc otha 111:in for the ~will bcgr.,rudonly on.--Tiris Client: Energy Fuels Resources, Inc. Lab Set ID: 2107637 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB-78567 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium < 0.000200 Uranium < 0.000200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686. Toll Free: (888) 263-8686. Fax: (801 ) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC_SJ1MMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 08/02/2021 I 342h 07/27/2021 1057h mg/L E200,8 0.0000508 0.000200 mg/L E200.8 0.0000176 0.000200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/ I 0/2021 Page 6 of 8 an:d>""5;q,plic,ble101hcCWA. SOWA.and RCRA rn-c performed in accordance 10 )1£1.AC rrotocols. Penincm sampling information is located oo the attachedCOC. Confldmtial Business lnformaliQn This report ispro,•idc:J (ormc Cl<cl11<nc uscor1hcaddr<:sstt. Pri,'11<'£<Sof~ uscorit ncor11uscomp3ny or nny mcmbcroOts:smff. orrc-producuon of1h,srcpon in oonncctioo "'"h 1hc od\'attSeffle"1. i;rornot1<1n ors:ilc or any podud 0< process. or in connttl"'" w,1h lhc r,,.publication ofth,,.-rcpon (o,-~• plJIJIOSC c,mc, th.in for the oddn:ssttwdl beJl"l'l'<'ll cmlyon c-oract. T111s ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107637 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107637-00IAMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.234 Uranium 0.224 Lab Sample ID: 2107668-00JAMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.200 Uranium 0.219 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@,awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 08/02/2021 140th 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 08/02/2021 1428h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200,8 0.000176 0.00200 0.2000 Tanner Holliday ME MS Spike Ref. Amount %REC 0.0324 101 0.0222 101 0.00035 100 0.0158 102 Limits 75 -125 75 -125 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/10/2021 Page 7 of 8 analyses spphc:,blt 10 the CWA. SOWA. ond RCRA an, perfom,ed m accordmic<: 10 NELAC r,n,IOC(lls. Pertinent sampling information is located on the attached COC. Confodcn11al Business lnform;11ioa This rq,ort is l'""''idcd r« th<e c,cclusme use <>fthe adm:sstt. P1n-ilei,es of~ use of ti- ne of this company« :my mcmb<,r or its Slaff. er rcpraducuon of this rcpon m connc:a,on" 1th the :>d\<11iscmcnt. pn,mouon or s:ik of 1111)' l'{oduct or process. or m coonoc1,on wi1h thc ro-p11blicatim or llns ropon for any purpose 01bcr th:an for the nddr= win he gr.,nicJ only on CMl:>CI.. ThJS Client: Energy Fuels Resources, Inc. Lab Set ID: 2107637 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107637-00IAMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.251 Uranium 0.246 Lab Sample ID: 2107668-003AMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.193 Uranium 0.207 3440 South 700 West Salt Lake City, UT 84 J J 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com. web: www.awal-labs.com C SUMMARY REPORT_ Contact: Dept: QC Type: Reporting Amount Spiked Units Method MDL Limit 08/02/2021 1405h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200,8 0.000176 0.00200 0.2000 08/02/2021 1435h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 Tanner Holliday ME MSD Spike Ref. Amount %REC 0.0324 109 0.0222 112 0.00035 96.4 0.01 58 95.5 Limits 75 -125 75 -125 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit 0.234 7.09 20 0.224 9.38 20 0.2 3.65 20 0.219 5.74 20 Qual Report Date: 8/10/202 1 Page 8 of 8 nn.il)._ applicable 10 the CWA. SOWA. and RCRA an, pcrfonnc:d m 3CCQfdonco 10 NEL.\C-r,n><O<ols Pertinent sampling infom,arion is located on the attached COC. Conf oclc:ntial Business lnforma1ion Th,s rcpon is prm'1d<d for the e>:Oll1SJYc, us.-of the :iddr<:sstt. Pri•~'e$ of subsi,qucnl us,: o(l)- nc of1hiscomp.1ny «any m<1nbc<-of itsRalT. o,rq,roduction of this roJ>Ofl mcom~uon wuh 1hca,fron.1~cnt.. prnnlOUonotsnlcohny Jl'Odud o,pvccss. or incooncc1ion with the re-publication of this ropotl forony p,a-pose Nhcr than fortlx~,'111 btgr.nNlon~· on~ Thi, American West Analytical Laboratories Rpt Emailed: WORK ORDER Summary WorkOrder: 2107637 Client: Energy Fuels Resources, Inc. Due Date: 8/9/2021 Client ID: ENE300 Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 QC Level: III WO Type: Project Comments: QC 3 (no chromatograms). EDD-Denison. Email Group; (USE PROJECT for special DLs). Do not use "*R_" samples as MS/MSD.; Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 2107637-00lA l\1W-12_07212021 7/21/20211355h 7/26/2021 1055h 200.8-DIS Aqueous-Dissolved DF-Metals 2 SEL Analf_les: SE U 200.8-DIS-PR DF-Metals UL Denison Page 1 of 1 --'l.., Printed: 07126/21 13:45 LABORATORY CHECK: %M □ RT □ CN □ TAT O QC O LUO □ HOK ___ HOK __ _ HOK___ COC Emailed~---- American West Analytical Laboratories 463 W. 3600 S. Salt Lake City. UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 L-~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: thoWday@e:ll.ergyfuels.com; kweinel@energyfuels.com; Project Name: 3rd Quarter Ground Water 2021 Project#: PO#: Sampler Name: Tanner Holliday Date Samole ID: Samoled 15 MW-12_07212021 7/21/2021 I,_ 7/21/'20'21 17 18 19 !C !1 ' 22 1.3 I !!, !l, Rolinquiahod by._),. Ill ./#./ ./ Date: Slgnaturo ---•.a.a•-llu 7/2212021 , Time: Prln!Nllmo: Tann« Hoffld.sv 1100 Rolnqu!ahod by: Date: ls1gna!uro Time: P,tntNomo; Rollnquishod by. Dare: Slgnoturo [Time: Print Marne: Relinquished by: Date: Signature Time: Prlnl Name,: I Time Samoled 1355 . Received by: Signab.lro CHAIN OF CUSTODY All analysis wlll be conducted using NELAP accredited methods and all data wlll be reported using AWAL's standard analyte llsts and reporting llmfts (POL) unless speclflcally requested olh8M4se on this Chain of Custody and/or attached documentadon. QC Level: I Turn Around Time: Unless other arrangements have been made, Signed reports v,;11 be emailed by 5:00 pm on 3 Standard the day they are due. i:: X Include EDD: 0 LOCUS UPLOAD 1 EXCEL CJ X Field Filtered For: .; Dissolved Metals 5 00 0 00 ~ ~ ~ 0 0 0 II For Compliance With: N 0 0 0 a D NELAP ..._ 0 C'I C'I o' t'--N 0 0 ..._ j:::-j:::-ci .. D RCRA 0 t'--0 0 0 JI D CWA ~ 0 0 0 (') 11 D SOWA 0 ~ ~ ... A§' 4l £!, 0 D ELAP /A2LA • ] II g a l) o' -I() D NLLAP ~ ! o' .e ~ 0 SC"! D Non-Compliance ci ii a a 0 0 .. ~ ~ 5 ~ 0 (') ,l! II D Other: 0 ~ ... lt) ... ,1. li! OJ D' ~ 'St-0 e :s ~ ... m " i 0 0 ~ 0 0 .. C (') ... 0 i1; ... ,a ... 0 :a JI ]§ 0 II II II 4l II lt) ::e .:: 0 ~ .:: .:: ... CJ ~ Known Hazards C :z; lt) ~ ;: ::t. 0 ., -0 ::t. 0 0 .. If u a. N ., Ul ., = • 0 ... CJ .. & ti E g ., ti e .. iS ::s 0 0 ~ .. A i5 i5 ?>: fll > .. Samole Comments .. en 1 w X X y .J IW 7 .... Pate: Special Instructions: llme: ~/6V~~7 AWAL Lab Sample Set# Page--2:::::'.i of ~/ I'"' Date, Laboratory Use Only s,,~ .. :, t..t y!:f 1 <;;; or hand do!lverod 2 Arnblente 3 Tomp,on,luro .Q Q~ 0 •c 4 Received Brokenfleaklng (Improperly Sealed~ y N-l 5 Prope<ly Pr...,..O<I f) N Ch<lckodotbench y N 6 Rtoolv<ldWllhln ~dtr,gllmea N 1 Pr"""'11 on ~Packago C) N NA 2 Gbrckon on Outer Package N NA /JtnS~mple (3 4 ~nbroken on :•mple 8 Discrepancies Betw&En Sample Label!,· and COC R9COrd? y 0 Print Name: , Sample containers for metals were field filtered. See the Rooo!v~~ ,/ r1' J ../ 0,/4 thil Analytical Scope of Work for Reporting Limits and VOC analyte lstgnlliulO . /I f/J~ ~ ~ ✓ list. ·~ ;rime: fOS:.5 Print Name: 2 {{1,.,, ,a / i,J. ~ Received by: I I Data: Signeh.lre Time: Prf_nlName: Received by: Date: SiP,nah.Jre Time: Pr:iolName: I Analysis Ammonia COD Cvanide Metals NOiLNO1 O&G Phenols Sulfide TKN TPO4 CrVI+ ProcedW'e: Frequency: Pi-_eservation Check Sheet s le SetE Preservative I oH<2H2SO4 oH <2 Hi.SO4 oH>l0NaOH oH<2HNO3 y...., oH<2Hi8O◄ t ' oH<2HCL pH<2 H2SO4 oH >9 NaOH ZnAC oH<2H2SO4 0H<2H2SO4 oH >9 (NH4 hSQ4 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid dpH 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + • # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH > __ due to the sample matrix interference. Lab Set ID: pH Lot#: 2./01 Cr~7 0...Q Cl rev I 0-28-2020 3440 South 700 West ~alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 3rd Quarter Ground Water 2021 Dear Tanner Holliday: Lab Set ID: 2107668 American West Analytical Laboratories received sample(s) on 7/27/2021 for the analyses presented in the following report. American West Analytical Laboratories (AW AL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. This is a revision to a report originally issued 8/13/2021. Information herein supersedes that of the previously issued reports. Pages 1, 7, and 12-15 have been revised. Chloride has been added to this report. Thank You, Approved by: J G Digitally signed 0$9 . by Jose G. Rocha Rocha Date: 2021.09.30 16:33: 16 -06'00' Laboratory Director or designee Report Date: 9/30/2021 Page I of 15 All wmlyses applicable lo the CWA. SDWA, and RCRA are perfonned in accordance to NE LAC protocols. Per1inent snmpllniij infomllllion is locnled on lhe attached COC. ('onridcnlial Uu,mcss Information: This repon is provided for the e..'<dush tt ldt' of the ~ddressee Prfrile~es o,r su~seq~ent ~~e of lhe ~~e of 1his ,cm~pany or nny 1~mber of its staff, or reproductio~ ~~this~ in .con!ll!ChOI~ \\·ilh the a~~1ertisemen1, P~?moli~t ~ S,1lc of~!). tJfod~cl or p1:?Cess, ~r in :onn~c~ion w!lh th~ r~-publico1ion or1his report 3440 South 700 West ~alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 !-mail: awal@awal-labs.com web: www.awal-Iabs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer SAMPLE SUMMARY Client: Project: Lab Set ID: Energy Fuels Resources, Inc. 3rd Quarter Ground Water 2021 2107668 Date Received: 7/27/2021 955h Lab Sample ID Client Sample ID Date Collected 2107668-001 A MW-27 07222021 7/22/2021 1220h 2107668-002A MW-28 07232021 7/23/2021 1115h 2107668-0028 MW-28 07232021 7/23/2021 1115h 2107668-002C MW-28 07232021 7/23/2021 1115h 2107668-003A MW-29 07222021 7/22/2021 1320h Contact: Tanner Holliday Matrix Analysis Aqueous Nitrite/Nitrate (as N), E353.2 Aqueous Nitrite/Nitrate (as N), E353.2 Aqueous Anions, E300.0 Aqueous ICPMS Metals, Dissolved Aqueous ICPMS Metals, Dissolved Report Date: 9/30/2021 Page 2 of 15 All llllnlyses applicnbrf 10 1hc CW A. SDWA. and RCRA nre perfonned in accordance to NELAC prolocols. Pe11lnmt s11mplin&. information is located on the altached COC. Conlidentinl Business Jn(orm.111ion: This report is pro,•ided for the cscl~\t' use of the ~ddressee. Pri,·ile~es <>f su~tq~ent .u~e of the ~~'I! or this .co1~pony or nny ~mber of its slnff, or rel)roducti~ ~(lhis rc1>0~ in _con~ection~ with the a~:enisement, P~?motio,n ~r ~ale of ~!Y. ~rod~ct or P•_?Cess, ~r in ~onm:c~ion w!th th~ r!·public,ndon or 1his report 3440 South 700 West ~alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: 3rd Quarter Ground Water 2021 2107668 7/27/2021 7 /22-7/23/2021 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike/ Man·ix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relati e Percent Differences) were inside established limits, with the following exception: San'lple ID Analyte QC Explanation 2107668-002A Nitrate/Nitrite MS/RPD Sample matrix interference or sample non-homogeneity Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 9/30/2021 Page 3 of 15 All analyses applicable 10 lh-:. CWA. SOWA, tu1d RCRA are performed in accordance 10 NELAC prolocols. Pcm nent s11mpliny informalion is locn1ed on 1he ott.:iched CDC. onr.dcntiol Business lnf(N'nlll.tioo· This repon is pro,•ided for the exclusi,·e use or the ~ddressee. Pririle*es of Jll~q~ent ~~e or •~e: •~~o or lhis ,co•~pany or nny •~~ber or its st:ilT, or reproducti~! ~f 1his repo~ in .con~eclion~ \\·ilh lhe n~~·ertisef!lenl. P~?moti~1 O!~lc or ?1!Y. ~rod~cl or p~ocus, ~r in ~onn:c~ion '''!th th~ r~-p~blica1ion of lhis repor1 Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: LCS-78567 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.192 Uranium 0.198 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC_Sll_MMARY REPORT Contact: Dept: QC Type: ----- Reporting Amount Units Method MDL Limit Spiked 08/02/2021 1346h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 Tanner Holliday ME LCS Spike Ref. Amount %REC 0 95.8 0 98.9 Limits 85 -115 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 9/30/2021 Page 8 of 15 analyses applicable to the CWA. SOWA, :ind RCRA nn, paiom1ed m ocoorrlance 10 NELAC-protOC:Ols Ptrtinct11 s.1mpling infonmuon is located on the attached COC Confidential Business Information: This report is p<Q\•1di:d fo, thee.,clusive use of the addressee. Privileges of subsequet11 use oftt ne of this compony or any member or 11sstaff. or rcproducuon of1his n.'P()ft m connccloon w11h 1he :td,•c-nisem"'11. promotion or snk of ony product or process. or in connection with the re-publication of this repon for ony P<lfJJOSO Olhcr thon for the addressee will be granted only on contact This ANALYTICAl Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB-78567 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium < 0.000200 Uranium < 0.000200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMAR~PORT_ Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/02/2021 1342h 07/27/2021 1057h mg/L E200.8 0.0000508 0.000200 mg/L E200,8 0.0000176 0.000200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report. Date: 9/30/2021 Page 9 of 15 analyses opphc;il)le to the CWA. SOWA, 1111d RCRA arc pcrfom,cd in acco~ 10 NELAC protocols l'cnincnt smnpling infonnat,on ls loc:ntcd on the lllll!Chcd COC Coufrdc,ntial Business Information: 1111.s rcpon is provided for the exclusive use ofll,c ~ Pnvilc-JC$Of subs,qucm ,..., oftt ne of this c001pnny or any member of Its staff, or reproduc11on of 1h1s report in conncetion wnh the Jld,•c,usnnenL J1mmo1io,i or sale of any prodLtd or process. or m conncc1ion with the re-publication of this report for any purp()SC o,hcr 1han for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107637-00IAMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.234 Uranium 0.224 Lab Sample ID: 2107668-00JAMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.200 Uranium 0.219 3440 South 700 West Salt Lake City, UT 841 I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com !JC SUMMARY REPQRT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/02/2021 1401h 07/27/2021 1057h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200,8 0.000176 0.00200 0,2000 08/02/2021 1428h 07/27/2021 1057h mg/L E200.8 0,000508 0.00200 0.2000 mg/L E200 8 0.000176 0.00200 0.2000 Tanner Holliday ME MS Spike Ref. Amount %REC 0.0324 IOI 0.0222 IOI 0.00035 100 0.0158 102 Limits 75 -125 75 -125 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit Qual Report Date: 9/30/2021 Page IO of I 5 analyses :,ppl,coble to the CWA, SOWA. ll/ld RCRA an., pcrfom1ed in oa:ordnnco to NE LAC pro1ocols. Pertinent samplini; information is located on the :>11acb«I COC, Confidential Business Information: This rcpon is provided (or the exclusive use of the addressee. Privileges of subsequen( use of tt ne of this compnny or any member of i~ stnO-, or n:ptOdoction of this rcpon m comtCCtion with the advertisement. prom(llion or sale of any product or pr= or m connc<:tion with the re-publication of this repon for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107668 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: MSD ------ Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2107637-00IAMSD Date Analyzed: 08/02/2021 1405h Test Code: 200.8-DIS Date Prepared: 07/27/2021 1057h Selenium 0.251 mg/L E200.8 0.000508 0.00200 0.2000 0.0324 109 75 -125 0.234 7.09 20 Uranium 0.246 mg/L E200.8 0.000176 0.00200 0.2000 0.0222 112 75 -125 0.224 9.38 20 -Lab Sample ID: 2107668-00JAMSD Date Analyzed: 08/02/2021 1435h Test Code: 200.8-DIS Date Prepared: 07/27/2021 1057h Selenium 0.193 mg/L E200,8 0.000508 0.00200 0.2000 0.00035 96.4 75 -125 0.2 3.65 20 Uranium 0.207 mg/L E200,8 0.000176 0.00200 0.2000 0.0158 95.5 75 -125 0.219 5.74 20 Report Date: 9/30/2021 Page 11 of 15 analyses applk,bl~ 10 the CW A. SDWA, and RCRA are p,:<fonncd in accorw,nc,~ to NliLAC protocols Pen mom sampling infonnmion is located on the attached COC Confidential Business lnfonnation: This rcpon is provided for tlie t.<dusive use of 1l,e addressc,,:, l'rnoleges Of$<lb5'<lU<nl use of ti- ne of this company or any member of its staff~ or reproducuon of1h1s report 10 conncchon with the advcniscmcru. promotion or Sll~ or •my product or process. or in connection with the re~publication of this n::pon for any purpoS4!l Ol.hcr lh.nn for the .:tddrcssec will be gr.s:n1«l only on conttid This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Method MDL Reporting Limit Contact: Dept: QC Type: Amount Spiked Tanner Holliday WC LCS Spike Ref. Amount %REC Lab Sample ID: LCS-Rl55082 Date Analyzed: 08/03/2021 1853h Test Code: 300.0-W Chloride 4.98 mg/L E300,0 0.0198 0.100 5.000 0 99.7 Lab Sample ID: LCS-Rl54940 Date Analyzed: 08/02/2021 1359h Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) L02 mg/L E353.2 0.00541 0.0100 1.000 0 102 Limits 90 -110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 9/30/2021 Page 12 of 15 analyses applicable to the CWA. SDW A, and RCRA are perfonncd in accord3nce 10 NE LAC protocols Pcnincnt snmplln~ infonnatron 1s located on the attached COC. Confidential Business lnfonn11tion: This r"l'Ort is pro,·,dcd for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this comp;my or .;my member of its staff, or reproduction af 1,h1s repon m conncct1on with the adveni.scmcnt. pconionon ot saJ~ or ;s.ny product or process. or in connection with there-publication of this rcpon for any purposr.! otht'f than for the addressee will be granted only on contact. Thls Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 - Analyte Result Lab Sample ID: MB-R155082 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Lab Sample ID: MB-R154940 Date Analyzed: Test Code: N02/NO3-W-353.2 Nitrate/Nitrite (as N) < 0.0100 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Tanner Holliday Dept: WC QC Type: MBLK Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 08/03/2021 1829h mg/L E300,0 0.0198 0.100 08/02/2021 1357h mg/L E353.2 0.00541 0.0100 Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt ¾RPD Limit Qual Report Date: 9/30/2021 Page 13 of 15 analyses applicable to tlu: CWA. SDWA, and RCRA ore pcrfom1c:d in accord:incc 10 NEL,\C pt<>lucols. Pc:runcnt samplins information is located on the attached COC Conr1<1cn1111I Business Information: Tl11s rcpon is provided for 1hc exclusive use of the addressee Privileges of subsequent use of& ne of this com puny or nn~ member of its staff, or rcproduet1on of th,s report 111 conncct1Qn with ihc ;,d\lt11iSC'tno:nt. pl't.)motlon or sale of any product or process. or in conncc1ioo with tho re-publication of this repon for any purpose-other 1lmn for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Tanner Holliday WC MS ------- Reporting Amount Spike Ref. Analyte Result Units Method MDL Limit Spiked Amount %REC Lab Sample ID: 2107668-002BMS Date Analyzed: 08/03/2021 2335h Test Code: 300.0-W Chloride 1,160 mg/L E300 0 3.96 20.0 1,000 152 100 Lab Sample ID: 2107668-002AMS Date Analyzed: 08/02/2021 1414h Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 19.3 mg/L E353.2 0.0541 0.100 10.00 6.09 132 Lab Sample ID: 2107791-006DMS Date Analyzed: 08/02/2021 1426h Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 9.74 mg/L E353 2 0.0541 0.100 10.00 0 97.4 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 90 -I IO 90-110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 9/30/2021 Page 14 of 15 analyses applicable to the CWA. SOWA, and RCRA nr,: pttfom1ed in accordnocc 10 NELAC 11ro10:ols Pertinent sampling information is located on the attached COC Confidential Business Information: Th,s rcpon is provided for die e.,clusive use of the addre$Stt Priv~eges orsubs,qutnt use oftt nc of1his company or any member of its staff, or rcprt.'Klucuon of1h1s report m oonn~1ion with 1hc advertisement. promotion or sale of any product or process, or in connection with the re-publication of thi!i rt:port for any purpose other 1han for the addressee will bcgmntl"d only on contod.... This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107668 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107668-002BMSD Date Analyzed: Test Code: 300.0-W Chloride 1,150 Lab Sample ID: 2107668-002AMSD Date Analyzed: Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) 16.0 Lab Sample ID: 2107791-006DMSD Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as NJ 10.5 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com .QC SUMMARY REPORT_ Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/03/2021 23 5 8h mg/L E300.0 3.96 20.0 1,000 -08/02/2021 1415h mg/L E353,2 0.0541 0.100 10.00 08/02/2021 1427h mg/L E353.2 0.0541 0.100 10.00 Tanner Holliday WC MSD Spike Ref. Amount %REC 152 99.7 6.09 99.1 0 105 @ -High RPD due to suspected sample non-homogeneity or matrix interference. Limits 90 -110 90 -110 90-I IO Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 1160 0.578 20 19.3 18.7 10 9.74 7.51 IO Qual @ Report Date: 9/30/2021 Page 15 of 15 analyses applicable to the CW A, SOWA. and RCRA are performed in accordanc:e 10 NELAC pro1oeols Pertinent sampling information is located on the attached COC, Confidential Business Informt1tion: This ropon is pr0\•1ded (OI' the c,xclusive use of !he addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduc:l1on uf 1his report m conneeuon with the ad,1ertisement, promotion or sale of any product or process. or in connection with the re-publication of this r(1)0f1 ror any pu:rposc Ollw.-r 1lum for the addressee will be granted only on contact. This American West Analytical Laboratories Rpt Emailed: UL Denison_ WORK ORDER Summary Work Order: 2107668 Page 1 of 1 Client: Energy Fuels Resources, Inc. Due Date: 8/10/2021 Client ID: ENE300 Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 QC Level: III WO Type: Project Comments: QC 3 (no chromatograms). EDD-Denison. Email Group; (USE PROJECT for special DLs). Do not use "*R_" samples as MS/MSD.; Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage -- 2107668-00lA MW-27_07222021 7/22/2021 1220h 7/27/2021 0955h NO2/NO3-W-353.2 Aqueous df • no2/no3 & nh3 1 SEL Analytes: N03N02N 2107668-002A MW-28_07232021 7/23/2021 1115h 7/27/2021 0955h NO2/NO3-W-353.2 Aqueous df -no2/no3 & nh3 1 SEL Analytes: N03N02N 2107668-002B 300.0-W df-cl 1 SEL Ana/ytes: CL 2107668-002C 200.8-DIS df-metals 2 SEL Analytes: SE U 200.8-DIS-PR df -metals 2107668-00JA MW-29 _ 07222021 7/22/2021 1320h W.7/2021 0955h 200.8-DIS Aqueous OF-Metals 1 SEL Analytes: U 200.8-DIS-PR OF-Metals Printed: 07/27/21 10:21 LABORATORY CHECK: %M O RT □ CN □ TAT O QC O LUO □ HOK ___ HOK __ _ HOK___ COG Emailed~--- American West Analytical Laboratories CHAIN OF CUSTODY ~ I u7 ~i? AWAL Lab Sample Set# 463 W. 3600 S. Salt Lake Cily, lfT 84115 Phone# (801) 263-8686 Toll Free# (888)263-8686 All analysis wtll be c:onduc:tod using NEtAP accmdiod molhods end ell data Will be reportod using AWAJ.'• standard ano1ylo lists and reporting Amllo (POI.) unlosa opoclfleolly requoolod otherwise on this Chain of Cuslody andlo< a\!ll.C:hed documentation. Page 1 of 1 ~ Fax # (801) 263-8687 Email awal@awal~abs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: {435) 678-2221 Cell#: -------Email: tboWday@energyfuels.com; kweinel@energyfuels.com; Project Name: 3rd Quarter Ground Water 2021 Project#: QC Level: 3 ~ g 00 ci 0 N --t--ci 0 £!. = Ill Sample ID: Date Sampled Time Sampled PO#: 1 Sampler Name: Tanner Holliday I j I j I I 5 ~ (.) C. 0 ~ 'U: (l)_ '2. Cl) i ! J "Cl .e : iS IIIW-27 _07222021 7/22/2021 1220 1 IW I X 3IIIIW-28_07232021 7/23/2021 1115 3 IW I X 4 IIIIW-29_07222021 7/22/2021 1320 l IW 5 9 o' c 0 "l ... 0 0 0 l() :t. 0 X G' 0 ~ ~ m Q E-4 00 ci 0 N --t--ci 0 £!. j "Cl Ill .l!: 0 • .!l Q X X Turn Around Time: co g C'I ~ g t:!. e ~ 0 "Cl ~ II • Q Standard co g ~ ~ c:i 0 t:!. -I ~ m "Cl ~ ! X o' g "l ~ u ~ ~ '1-::s. ] t: o' g "l ... 0 0 0 l() :t. 0 m 8 5 { i ! iS g -I() ~~ Unless other amingements have been mede· 11D ue Date: signed reports Will be emailed by 5:00 pm on the day they are due. X Include EDD: LOCUS UPLOAD EXCEL ){ Field Filtered For: Dissolved Metals For Compliance With: □ NELAP 0 RCRA □ CWA 0 SDWA □ ELAPIA2LA D NLLAP □ Non-Compliance D Other: Laboratory Use Only l5omp1M Won,: (.,( (15. 1 ~ hand delivocod 2 Amblf/flt~ 3 TompomlU!O /,<?" 4 Received Broken/Leaking (Improperly Sealed);:;\ y ~/ 5 _,J?.Q;,perty Pres8t'Ved \.r_' N ,2 Ill O-c:1l------------7I .. 'C .s 0 Checked at bench y N ~-0 ij .... 0 J1 0 Ill >f-<_ Known Hazards & Sample Comments 6 Received Within ~ding Times c) N 1 Pr"'ool on CMo, Paolu,,,o 0 N NA 2 Anbroken on Outer Package 0 N NA 3 Present on Sample ~ y N ~I 4 Unbroken on Sample 1..:, '. y N ~,' ~ I I 111 I II I 111 I I I 1~~c5· ~ellclqlll&hod by. --\ --IZ // ~ lonalure ~tu'IN~ rT,?f'LH'~ Data: 77 ITima: 1Recaived by: 712612021 ISi!i.nehJre !Pete: !Time: Special Instructions: ·c P~n, Name: . ToMD< Hollld<> 'Sample containers for metals were field filtered. See the uhlhod t,y. _ z_ / Analytical Scope of Work for Reporting Limits and voe analyte -. ~ c:irn,mamo: 1W1nqubhod by. ls1gna1uro ~rtnlNa,no; Rolinqultl,od by. ls!!!_nohne PdnlNa:mo: ;Doto: !nm•: Data: T,mo: PiiiitName: _ /,Z,., ,1.. o...,'t.._1_'c;.,v. _ ·r 5 5· Received by: $!gn.alure Prln!Name: Received by: $~nature ·Print Name: / I !Dato: lnme: Date: IT,me: Analysis Ammonia COD Cyanide Metals NC½/NO; O&G Phenols Sulfide TKN TPO4 CrVI+ Procedure: Frequency: Pr~~ervation Check_S_beet s le Set E Preservative I 2... .:}J oH<2fuSO4 pH<2H2SO4 oH>l0NaOH pH<2HNO3 Yes ~<. oH<2H2SO4 v~s V,.,.,5 / oH<2HCL I/ I/ 0H<2H2SO4 pH >9 NaOH, ZnAC oH<2 H2SO4 oH<2H2SO4 oH >9 {NH4)2SO4 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or Ud dpH 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + "1. # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH > __ due to the sample matrix interference. Lab Set ID: pH Lot#: 2 tO-) Ci·Gf {r)oc, rev 10-28-2020 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: 3rd Quarter Ground Water 2021 Dear Tanner Holliday: Lab Set ID: 2107791 American West Analytical Laboratories received sample(s) on 7/30/2021 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQ ). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, J G Digitally signed 0$9 . by Jose G. Rocha Rocha Date: 2021.08.24 16:11 :46 -06'00' Approved by: .._ ___________ ~ Laboratory Director or designee Report Date: 8/24/2021 Page I of 72 All analyses applicable 10 lhe CWA_ SDW r\. Nld RCI\A are performed in accordance to NELAC l>r'Otoc:ols. rcnmcnl sampling infon1U111on is located on the atlached COC. Confidrutial Busmess lnform:suoo• This repon is pro\'ided for the~<"IUSl\f use of the ~ddressee. Pri,ile~es of sul~q~nt .u~e or1hti ~:U!l:C or lhis _co1~pany or nny ~mber of ils staff, or rcproductl~ ~'. •his rep~~ in ~01~«hn~ ,,~lh the n~~1ertise~enl. P~?moti~ or snl~ of~~ rrad~ct Cir ~dS. ~r in ~nn~c~ion ,,·!lh th~ r:•publicoliah of this report SAMPLE SUMMARY American West Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday ANALYTICAL LAOORATORI ES Project: 3rd Quarter Ground Water 2021 Lab Set ID: 2107791 Date Received: 7/30/2021 11 00h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 2107791-00lA MW-11 07272021 7/27/2021 1125h Aqueous VOA by GC/MS Method ;att Lake City, UT 84119 8260D/5030C 2107791-001B MW-11 07272021 7/27/2021 1125h Aqueous Anions, E300.0 2107791-00JB MW-11 07272021 7/27/2021 1125h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level Phone:(801)263-8686 2107791-001 C MW-11 07272021 7/27/2021 1125h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 2107791-00lD MW-11 07272021 7/27/2021 1125h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (80 I) 263-8687 2107791-00lD MW-11 07272021 7/27/2021 1125h Aqueous Ammonia, Aqueous !-mail: awal@awal-labs.com 2107791 -00 IE MW-11 07272021 7/27/2021 1125h Aqueous ICPMS Metals, Dissolved 2107791-00lE MW-11 07272021 7/27/2021 1125h Aqueous Mercury, Drinking Water web: www.awal-labs.com Dissolved 2107791-00JE MW-11 07272021 7/27/2021 1125h Aqueous ICP Metals, Dissolved 2107791-00lE MW-11 07272021 7/27/2021 1125h Aqueous Ion Balance Jennifer Osborn 210779 I -002A MW-14_07272021 7/27/2021 1450h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 2107791-002B MW-14 07272021 7/27/2021 1450h Aqueous Anions, E300.0 210779 l -002B MW-14 07272021 7/27/2021 1450h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 210779 I -002C MW-14 07272021 7/27/2021 1450h Aqueous Total Dissolved Solids, A2540C 2107791-002D MW-14 07272021 7/27/2021 1450h Aqueous Ammonia, Aqueous 210779 l -002D MW-14 07272021 7/27/2021 1450h Aqueous Nitrite/Nitrate (as N), E353.2 2 I 07791-002E MW-14 07272021 7/27/2021 1450h Aqueous Mercury, Drinking Water Dissolved 2 I 0779 I -002E MW-14 07272021 7/27/2021 1450h Aqueous ICPMS Metals, Dissolved 2107791-002E MW-14 07272021 7/27/2021 1450h Aqueous Ion Balance 210779 I -002E MW-14 07272021 7/27/2021 1450h Aqueous ICP Metals, Dissolved 210779 l-003A MW-31 07272021 7/27/2021 1255h Aqueous VOA by GC/MS Method 8260D/5030C 210779 l-003B MW-31_07272021 7/27/2021 1255h Aqueous Anions, E300.0 2107791-003B MW-31 07272021 7/27/2021 1255h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 210779 l -003C MW-31 07272021 7/27/2021 1255h Aqueous Total Dissolved Solids, A2540C 210779 l-003D MW-31 07272021 7/27/2021 1255h Aqueous Nitrite/Nitrate (as N), E353.2 2107791-003D MW-31 07272021 7/27/2021 1255h Aqueous Ammonia, Aqueous 2107791-003E MW-31 _ 07272021 7/27/2021 1255h Aqueous Ion Balance 2107791-003E MW-31 07272021 7/27/2021 1255h Aqueous ICP Metals, Dissolved 2107791-003E MW-31 07272021 7/27/2021 1255h Aqueous ICPMS Metals, Dissolved Report Date: 8/24/2021 Page 2 of72 All anolyses applicable 10 1hc CWA. SDWA .. and R('R.A are performed in accordMce to NELAC ptlH(')GOII. ~mcnl sampling infonnnllon is located on Lhe auached COC. Confidential Ousin~ss lnformalion: This repon is pro,•ided for lhee.xclusi,-e use of the ~ddressee. Pri,·ile~es (J!'fu~q~enl ~~e of1hc ~~t~or this _con:1pany or an)· ~~ber of its stnff, or rcpmduch°'! ~flhis repo~ in .con~eclion_ wilh lhe a~~'ertisemenl, P~?moli~ ~r ~aJe of !11~ ~od~ct or p1:?Cess, ~r in 7°nn:,c~ion w!th th~ r;-p~blicalion of this reporL Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Set ID: 2107791 Date Received: 7/30/2021 11 00h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 2107791-00JE MW-31 07272021 7/27/2021 1255h Aqueous Mercury, Drinking Water 3440 South 700 West Dissolved 2107791-004A MW-36 07272021 7/27/2021 1425h Aqueous VOA by GC/MS Method ,alt Lake City, UT 84119 8260D/5030C 2 I 0779 l-004B MW-36 07272021 7/27/2021 1425h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 2107791-004B MW-36 07272021 7/27/2021 1425h Aqueous Anions, E300.0 Phone: (801)263-8686 2107791-004C MW-36 07272021 7/27/2021 1425h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 210779 l-004D MW-36 07272021 7/27/2021 1425h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 2107791-004D MW-36 07272021 7/27/2021 1425h Aqueous Ammonia, Aqueous !-mail: awal@awal-labs.com 2107791-004E MW-36 07272021 7/27/2021 1425h Aqueous Ion Balance 2107791-004E MW-36_07272021 7/27/2021 1425h Aqueous ICP Metals, Dissolved web: www.awal-labs.com 2107791-004E MW-36 07272021 7/27/2021 1425h Aqueous ICPMS Metals, Dissolved 2107791-004E MW-36 07272021 7/27/2021 1425h Aqueous Mercury, Drinking Water Dissolved Jennifer Osborn 2107791-00SA MW-65 07272021 7/27/2021 1450h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 2107791-00SB MW-65 07272021 7/27/2021 1450h Aqueous Anions, E300.0 2107791-00SB MW-65 07272021 7/27/2021 1450h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 2107791-00SC MW-65 07272021 7/27/2021 1450h Aqueous Total Dissolved Solids, A2540C 2107791-00SD MW-65 07272021 7/27/2021 1450h Aqueous Nitrite/Nitrate (as N), E353.2 2107791-00SD MW-65_07272021 7/27/2021 1450h Aqueous Ammonia, Aqueous 2107791-00SE MW-65 07272021 7/27/2021 1450h Aqueous ICPMS Metals, Dissolved 2107791-00SE MW-65 0727202 l 7/27/2021 1450h Aqueous Mercury, Drinking Water Dissolved 2107791-00SE MW-65 07272021 7/27/2021 1450h Aqueous Ion Balance 2107791-00SE MW-65 07272021 7/27/2021 1450h Aqueous ICP Metals, Dissolved 210779 l -006A MW-25 07282021 7/28/2021 1000h Aqueous VOA by GC/MS Method 8260D/5030C 210779 l -006B MW-25 07282021 7/28/2021 1000h Aqueous Anions, E300.0 210779 l -006B MW-25 07282021 7/28/2021 1000h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 210779 l -006C MW-25 07282021 7/28/2021 1000h Aqueous Total Dissolved Solids, A2540C 2107791-006D MW-25 07282021 7/28/2021 1000h Aqueous Nitrite/Nitrate (as N), E353.2 2107791-006D MW-25 07282021 7/28/2021 1000h Aqueous Ammonia, Aqueous 2107791-006E MW-25 07282021 7/28/2021 1000h Aqueous Ion Balance 210779 l -006E MW-25 07282021 7/28/2021 1000h Aqueous Mercury, Drinking Water Dissolved Report Date: 8/24/2021 Page 3 of72 All analyses applicable 101hcCWA. SOWA. and RCRA are performed in accordance to NELAC protocols. Pe,1£netll sampling information is localed on the auached COC. Confidtntial 8u,iurrss Information: This report is proYided for the exclusi,·e use of lhe ~ddressee. Pri,·ile~es 0~1ub_Rq~enl ~?e of the n~!•eofthis _con:ipany or nny_ •~'!1ber of its stnIT, or reproducti~ ~rt.his repo~ in .coi~1eclion,.. with the a~~1ertise~nt. P~?moH°!1 ~~e of:"!~ frod~cl or p•:?Cess, ~r in ~nn:c~ion w~Lh th~ r~-p~blication of lhis repor1 Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 American West Lab Set ID: 2107791 ANALYTICAL LABORATORIES Date Received: 7/30/2021 1100h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 210779 l -006E MW-25 07282021 7/28/2021 1000h Aqueous ICP Metals, Dissolved 3440 South 700 West 210779 l -006E MW-25 07282021 7/28/2021 1000h Aqueous ICPMS Metals, Dissolved ,alt Lake City, UT 84119 2107791-007A MW-26 07282021 7/28/2021 1300h Aqueous VOA by GC/MS Method 8260D/5030C 210779 I -007B MW-26 0728202 I 7/28/2021 1300h Aqueous Anions, E300.0 210779 l -007B MW-26 07282021 7/28/2021 1300h Aqueous Alkalinity/ Bicarbonate/ Phone:(801)263-8686 Carbonate, Low Level 210779 l-007C MW-26 _ 07282021 7/28/2021 1300h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 210779 l -007D MW-26 0728202 I 7/28/2021 1300h Aqueous Nitrite/Nitrate (as N), E353 .2 Fax: (801) 263-8687 2107791-007D MW-26 07282021 7/28/2021 1300h Aqueous Ammonia, Aqueous ~-mail: awal@awal-labs.com 210779 l -007E MW-26 07282021 7/28/2021 1300h Aqueous ICP Metals, Dissolved 2107791-007£ MW-26 07282021 7/28/2021 1300h Aqueous ICPMS Metals, Dissolved web: www.awal-labs.com 210779 l -007E MW-26 07282021 7/28/2021 1300h Aqueous Mercury, Drinking Water Dissolved 210779 I -007E MW-26 07282021 7/28/2021 1300h Aqueous Ion Balance Jennifer Osborn 2107791-008A MW-39 07282021 7/28/2021 1450h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 210779 l -008B MW-39 07282021 7/28/2021 1450h Aqueous Anions, E300.0 210779 l-008B MW-39 07282021 7/28/2021 1450h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 210779 l -008C MW-39 07282021 7/28/2021 1450h Aqueous Total Dissolved Solids, A2540C 210779 l-008D MW-39 07282021 7/28/2021 1450h Aqueous Nitrite/Nitrate (as N), E353.2 210779 l-008D MW-39 07282021 7/28/2021 1450h Aqueous Ammonia, Aqueous 210779 l -008E MW-39 07282021 7/28/2021 1450h Aqueous Ion Balance 210779 l -008E MW-39 07282021 7/28/2021 1450h Aqueous ICP Metals, Dissolved 210779 l -008E MW-39 07282021 7/28/2021 1450h Aqueous ICPMS Metals, Dissolved 2107791-008£ MW-39 07282021 7/28/2021 1450h Aqueous Mercury, Drinking Water Dissolved 2107791-009A MW-40 07282021 7/28/2021 1040h Aqueous VOA by GC/MS Method 8260D/5030C 210779 l -009B MW-40 07282021 7/28/2021 1040h Aqueous Anions, E300.0 210779 l -009B MW-40 07282021 7/28/2021 1040h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 210779 l -009C MW-40 07282021 7/28/2021 1040h Aqueous Total Dissolved Solids, A2540C 210779 l -009D MW-40 07282021 7/28/2021 1040h Aqueous Nitrite/Nitrate (as N), E353.2 210779 l -009D MW-40 07282021 7/28/2021 1040h Aqueous Ammonia, Aqueous 2107791-009£ MW-40 07282021 7/28/2021 1040h Aqueous Mercury, Drinking Water Dissolved 210779 l -009E MW-40 07282021 7/28/2021 1040h Aqueous Ion Balance Report Date: 8/24/2021 Page 4 of72 All analyses applicable 10 d1d CWA. SOWA. tiud RCRA are perfonned in accordance lo NELAC pfOlotols. Pc11lntrU sampling information is located on the annched COC. Conlidenlial Business Information: This report is provided for lhe c-.xdU5h c-u&e of the ~ddressee. Prfrile~es c_rsu'!,_~q~1enl ~~e or the ~?'.n.: or this ,con:ipany or any ~~ber of its stnff, or re1uoducti~~~r !his repo1; in ~on~ection .. with the a~~1ertise1'!1enl. P~?molio.n ~r sale of ?-1!Y. ~rodl)Cl or P~?Cess. ~r in ~onn~c~ion w'.lh th~ r~•publkmiou of lhis report Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 American West Lab Set ID: 2107791 ANALYTICAL LABORATORIES Date Received: 7/30/2021 1100h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 210779 l-009E MW-40 0728202 l 7/28/2021 1040h Aqueous ICP Metals, Dissolved 3440 South 700 West 2107791-009E MW-40 07282021 7/28/2021 1040h Aqueous ICPMS Metals, Dissolved ;alt Lake City, UT 84119 2107791-0l0A MW-24 07292021 7/29/2021 710h Aqueous VOA by GC/MS Method 8260D/5030C 2107791-01 OB MW-24 07292021 7/29/2021 710h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 2107791-0l0B MW-24 07292021 7/29/2021 710h Aqueous Anions, E300.0 Phone: (801)263-8686 2107791-01 oc MW-24 07292021 7/29/2021 710h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 2107791-0l0D MW-24 07292021 7/29/2021 710h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (80 I) 263-8687 2107791-01 OD MW-24 07292021 7/29/2021 710h Aqueous Ammonia, Aqueous ~-mail: awal@awal-labs.com 2107791-01 OE MW-24 07292021 7/29/2021 710h Aqueous Mercury, Drinking Water Dissolved web: www.awal-labs.com 2107791-0 l OE MW-24_07292021 7/29/2021 710h Aqueous ICPMS Metals, Dissolved 2107791-0l0E MW-24 07292021 7/29/2021 710h Aqueous ICP Metals, Dissolved 2107791-01 OE MW-24 07292021 7/29/2021 710h Aqueous Ion Balance Jennifer Osborn 2107791-01 lA MW-24A 07292021 7/29/2021 700h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 2107791-01 lB MW-24A 07292021 7/29/2021 700h Aqueous Anions, E300.0 2107791-0118 MW-24A 07292021 7/29/2021 700h Aqueous Alkalinity/ Bicarbonate/ Jose Rocha Carbonate, Low Level QA Officer 2107791-01 lC MW-24A 07292021 7/29/2021 700h Aqueous Total Dissolved Solids, A2540C 2107791-01 lD MW-24A_07292021 7/29/2021 700h Aqueous Ammonia, Aqueous 2107791-01 lD MW-24A 07292021 7/29/2021 700h Aqueous Nitrite/Nitrate (as N), E353.2 2107791-01 lE MW-24A 07292021 7/29/2021 700h Aqueous Mercury, Drinking Water Dissolved 2107791-01 lE MW-24A 07292021 7/29/2021 700h Aqueous ICPMS Metals, Dissolved 2107791-01 lE MW-24A_07292021 7/29/2021 700h Aqueous Ion Balance 2107791-0llE MW-24A 07292021 7/29/2021 700h Aqueous ICP Metals, Dissolved 2107791-012A MW-30 07292021 7/29/2021 950h Aqueous VOA by GC/MS Method 8260D/5030C 2107791-012B MW-30 07292021 7/29/2021 950h Aqueous Anions, E300.0 2107791-012B MW-30 07292021 7/29/2021 950h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 2107791-012C MW-30 07292021 7/29/2021 950h Aqueous Total Dissolved Solids, A2540C 2107791-012D MW-30 07292021 7/29/2021 950h Aqueous Nitrite/Nitrate (as N), E353.2 2107791-012D MW-30 07292021 7/29/2021 950h Aqueous Ammonia, Aqueous 2107791-012E MW-30 07292021 7/29/2021 950h Aqueous Ion Balance 2107791 -012£ MW-30 07292021 7/29/2021 950h Aqueous ICP Metals, Dissolved 2107791-012E MW-30 07292021 7/29/2021 950h Aqueous ICPMS Metals, Dissolved Report Date: 8/24/2021 Page 5 of72 All analyses applicable 10 lh CW A, SOWA. Md RCRA are perfonned in accordance to NE LAC protocols. Pi!1tln1.111 sampling information is located on lhe auached COC. Conli<tential Business Information: This report is provided for the exclusiYe use or the ~ddressee. Pri\·ile~esoti:ub_sc'q~1enl ~?e of1he. ~~.1H:1 of this _con:ipany or any ~mber of its slaff, or 11:pmducll°!! ~flhis repo~ in ~on~1ec1ion .. \\ilh the a~~·ertisemenl, P~?moli~i ~s.iJcof ~!Y. ~rod~cl or p1:?Cess. ~r in ~nn~c~ion w!th th~ r~-publicalion of lhis report Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: 3rd Quarter Ground Water 2021 Lab Set ID: 2107791 Date Received: 7/30/2021 1100h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 2107791-012E MW-30 07292021 7/29/2021 950h Aqueous Mercury, Drinking Water 3440 South 700 West Dissolved 2107791-013A MW-38_07292021 7/29/2021 800h Aqueous VOA by GC/MS Method ,alt Lake City, UT 841 I 9 8260D/5030C 2107791-0 I 3B MW-38 07292021 7/29/2021 800h Aqueous Alkalinity/ Bicarbonate/ Carbonate, Low Level 2107791-013B MW-38 07292021 7/29/2021 800h Aqueous Anions, E300.0 Phone: (801) 263-8686 2107791-0 l 3C MW-38 07292021 7/29/2021 800h Aqueous Total Dissolved Solids, A2540C Toll Free: (888) 263-8686 2107791-013D MW-38 07292021 7/29/2021 800h Aqueous Ammonia, Aqueous Fax: (801) 263-8687 2107791-013D MW-38 07292021 7/29/2021 800h Aqueous Nitrite/Nitrate (as N), E353.2 ~-mail : awal@awal-labs.com 2107791-013E MW-38 07292021 7/29/2021 800h Aqueous Ion Balance 2107791-013E MW-38 07292021 7/29/2021 800h Aqueous ICP Metals, Dissolved web: www.awal-labs.com 2107791-013E MW-38 07292021 7/29/2021 800h Aqueous ICPMS Metals, Dissolved 2107791-013E MW-38 07292021 7/29/2021 800h Aqueous Mercury, Drinking Water Dissolved Jennifer Osbom 2107791-014A Trip Blank 7/27/2021 1125h Aqueous VOA by GC/MS Method 8260D/5030C Laboratory Director 2107791-0ISA MW-32 07282021 7/28/2021 1515h Aqueous Anions, E300.0 Jose Rocha QA Officer Report Date: 8/24/202 I Page 6 of 72 All analyses applicable I.) 1hc CWA. SDWA. Md RCRA are performed in accordance to NELAC prolocols. Per1inen1 sampling i11formation is localed on Lhe nu ached COC. Confidential Business Jnformahon· This repon is provided for the e.'(dush-e use or the ~ddressee. Pririle~es or1ub_!:<1q~ent ~~e or the ~:V,no o( this .con:ipany or any 1~~mber of ils slaIT. or reproduclio~ ~~this repo~ in ~~1eclion,. with the a~~'ertise~nl. p~~moli<>_n ~r ~ale of ~!Y. ~rodl!cl or P•.~ ~r in ~nnt;c!ion w!lh 1h~ n;:-pubhCl)JtOO of I his repon Client: Contact: Inorganic Case Narrative Energy Fuels Resources, Inc. Tanner Holliday American West Project: 3rd Quarter Ground Water 2021 2107791 ANALvr1cAL LAeoRAroR1es Lab Set JD: 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: 7/30/2021 7/27-7/29/2021 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: Sample ID Analyte QC Explanation 2107668-002A Nitrate/Nitrite MS/RPD Sample matrix interference and/or sample non-homogeneity 2107791-002£ Calcium MSD High analyte concentration 2107791-002E Magnesium MSD High analyte concentration 2107791-002£ Manganese MS/MSD High analyte concentration 2107791-002£ Sodium MSD High analyte concentration 2107791-003£ Calcium MS/MSD High analyte concentration 2107791-003E Magnesium MSD High analyte concentration 2107791-0IOD Nitrate/Nitrite MS/MSD Sample matrix interference and/or sample non-homogeneity Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 8/24/202 1 Page 7 of 72 All analyses applicabltt 10 the CW/\ .. SOWA. Md RCRA are perfom1ed in accordance to NELAC prolocols. Pcnr11en1 sampling i11f0fm1tt on is lc>enled on Lhe aunched COC. Conrirlcn1iol Business Jnforn~llon: Thh l'l!pQn ,i p10,·lckd ror I~ c, c:ht!i,~ tM orthe ~ddressee. Pri,·ife~es or iu~cq~I !'~e orchc !!?~,~ orrhis _co~pany or any ~mber or ils stnff 0~ reproducti~~ ~r111is repo~ in ~°"!'oc11on_ \\ilh lhe a~~'ertise~enl. P~?moliO!l ~ ~ale of~!)'. .~rodl~Cl or p~o~I. ~r tn ~•~!1(111 "!•h I~ ~publirntlon of 1hi1 reporl 3440 South 700 West ;aft Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: 3rd Quarter Ground Water 2021 2107791 7/30/2021 7/27-7/29/2021 Intact None SW-846 8260D/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requit-ements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all sample were performed within the method holding times following the method tated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibra6on check requirements were met, with CCV exceptions noted on the reports. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPO, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 8/24/2021 Page 8 of 72 All analyses applicablt: to lht! CWA. SOW A. and RCRA are perfom1ed in accordance to NELAC p,otocols. P~inenl sampling inforn\lStion is locoted on the nllnched COC. Coon~ntinl Bus-rnc~-s lnfonnnlion: This report is provided' far 1he e:xclusiYe use of the ~ddressee. Prl\·ile~es of~u~q~ent ~1~e of the ~~1e of lhis .co1~pany or nny •~mber of ils staff, or RProducl1ot? ~•his repo~ in ~onrectlet~ ,,ith !he a~~•ertise~enl, P~?moli~ ~r)D.fc of!"!) ~och~cl or P~?cess, ~r in ~nn~c.tio11 w!th th~ -:11ub/ication of this report 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha _QC SUMMARY REPORT QA Officer Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: LCS -------- Reporting Amount Spike Ref. RPDRef. RPO Analyte Result Units Method MDL Limit Spiked Amount ¾REC Limits Amt ¾RPD Limit Qual Lab Sample ID: LCS-78683 Date Analyzed: 08/10/2021 1449h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Calcium 10.2 mg/L E200 7 0.0434 1.00 10.00 0 102 85 -115 Magnesium 10.2 mg/L E200.7 0.0138 0.100 10.00 0 102 85 -115 Potassium 10.2 mg/L E200.7 0.177 1.00 10.00 0 102 85 -115 Sodium 9.91 mg/L E200,7 0.323 1.00 10.00 0 99.1 85 -I 15 Vanadium 0.202 mg/L E200.7 0.00137 0.00500 0.2000 0 101 85 -l 15 Lab Sample ID: LCS-78684 Date Analyzed: 08/13/2021 1316h Test Code: 200.8-DIS Date Prepared: 08/02/2021 943h Arsenic 0.205 mg/L E200.8 0.000298 0.00200 0.2000 0 102 85 -l 15 Beryllium 0.199 mg/L E200.8 0.000198 0.00200 0.2000 0 99.6 85 -115 Cadmium 0.201 mg/L E200.8 0.0000742 0.000500 0.2000 0 100 85 -115 Chromium 0.201 mg/L E200.8 0.000920 0.00200 0.2000 0 100 85 -115 Cobalt 0.192 mg/L E200.8 0,000300 0.00400 0.2000 0 95.8 85 -115 Copper 0.199 mg/L E200.8 0.00111 0.00200 0.2000 0 99.4 85 -115 Iron 1.00 mg/L E200 8 0.0312 0.100 1.000 0 100 85 -I 15 Lead 0.193 mg/L E200.8 0.000588 0.00200 0.2000 0 96.4 85 -II 5 Manganese 0.202 mg/L E200 8 0.000930 0.00200 0.2000 0 101 85 -115 Molybdenum 0.203 mg/L E200 8 0.000884 0.00200 0.2000 0 102 85 -115 Nickel 0.198 mg/L E200.8 0.000584 0.00200 0.2000 0 98.9 85 -115 Selenium 0.193 mg/L E200.8 0.000508 0.00200 0.2000 0 96.4 85 -115 Thallium 0.191 mg/L E200,8 0.000418 0.00200 0.2000 0 95.6 85 -115 Tin 0.962 mg/L E200.8 0.000968 0.00400 1.000 0 96.2 85 -115 Uranium 0.196 mg/L E200,8 0.000176 0.00200 0.2000 0 98,2 85 -115 Zinc 1.00 mg/L E200.8 0.00418 0.00600 1.000 0 100 85 -115 Report Date: 8/24/2021 Page 50 of72 nnn1yscs applicable to the CWA. SOWA, and RCRA are pffionncd in accorcbncc to NELAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business lnfomiation: This report is provlded for the exclusive use or the addressee. Privileges of subsequent use oft~ nc of 1h)s company or any member of its staff, or reproduction Q(this report in conncc::uon with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addl'CS~e will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: LCS-78951 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Silver 0.190 Lab Sample ID: LCS-78693 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00330 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Units Method 08/16/2021 1009h 08/13/2021 16 I Oh mg/L E200.8 08/03/2021 1112h 08/02/2021 1214h mg/L E245.l MDL 0.000232 0.0000396 Reporting Limit 0.00200 0.0000900 Contact: Dept: QC Type: Amount Spiked 0.2000 0.003330 Tanner Holliday ME LCS Spike Ref. Amount ¾REC 0 95.2 0 99.1 Limits 85 -ll5 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 8/24/2021 Page 51 of 72 analyses apphcablo 10 1he CWA. SDWA, and RCRA are pcrfomicd in accordsnec 10 Nfil.J\C pro1ocols. Pertinent sampling infonnatlon is located on the attached COC Confidential Business Jnfom1ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tf ne of this compan) or any member of its staff, or reproduction ofth1s report in conncc11on w1th the advertisement. promotion or so.le of any produc1 or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIE8 Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB-78683 Date Analyzed: Test Code: 200.7-DIS Date Prepared: Calcium < 1.00 Magnesium <0.100 Potassium < 1.00 Sodium < 1.00 Vanadium < 0.00500 Lab Sample ID: MB-78684 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Arsenic < 0.00200 Cadmium <0.000500 Chromium < 0.00200 Cobalt < 0.00400 Copper < 0.00200 Manganese < 0.00200 Molybdenum < 0.00200 Nickel < 0.00200 Selenium < 0.00200 Tin < 0.00400 Zinc < 0.00600 Lab Sample ID: MB-78684 Date Analyzed: Test Code: 200.8-DIS Date Prepared: 3440 South 700 West Salt Lake City, UT 84 I I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Tanner Holliday Dept: ME QC Type: MBLK -------- Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 08/10/2021 1447h 08/02/2021 943h mg/L E200.7 0.0434 1.00 mg/L E200.7 0.0138 0.100 mg/L E200.7 0.177 1.00 mg/L E200 7 0.323 1.00 mg/L E200.7 0.00137 0.00500 08/13/2021 1312h 08/02/2021 943h mg/L E200.8 0.000298 0.00200 mg/L E200.8 0,0000742 0.000500 mg/L E200.8 0.000920 0.00200 mg/L E200_8 0.000300 0.00400 mg/L E200.8 0.00111 0.00200 mg/L E200.8 0.000930 0.00200 mg/L E200.8 0.000884 0.00200 mg/L E200,8 0.000584 0.00200 mg/L E200.8 0.000508 0.00200 mg/L E200.8 0.000968 0.00400 mg/L E20D.8 0.00418 0.00600 08/ I 3/2021 I 526h 08/02/2021 943h -------------- Beryllium < 0.000200 mg/L E20D.8 0.0000198 0.000200 Iron < 0.0100 mg/L E200.8 0.00312 0.0100 Lead < 0.000200 mg/L E20D.8 0.0000588 0.000200 Thallium < 0.000200 mg/L E20D.8 0.0000418 0.000200 Uranium < 0,000200 mg/L E20D.8 0.0000176 0.000200 Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPO Amt % RPO Limit Qual Report Date: 8/24/2021 Page 52 of 72 analyses applrc-Oblo to the CWA. SOWA, and RCRA ar< pcrfom,cd in accordance to NELAC pro1uc:ols. Pcnlnent san1pling infonnai,on is located on the attached COC. Confideniinl Bu,h,ess lnfom1ation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this comp.:m)' or any member of its staff, or r'cproduct1on of this report in connecticn wnh the 3dvcrdscment. promotion or s:ilc of any product or process, or in connection wi1h tht re-publication of this report for any purpose other than for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB-78951 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Silver < 0.00200 Lab Sample ID: MB-78693 Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury < 0.0000900 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Tanner Holliday Units Method 08/16/2021 1005h 08/13/2021 1610h mg/L E200 8 08/03/202 I 111 Oh 08/02/2021 1214h mg/L E245.l Reporting MDL Limit 0.000232 0.00200 0.0000396 0.0000900 Dept: ME QC Type: MBLK ---- Amount Spike Ref. Spiked Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/24/202 I Page 53 of72 analyses applicable to the CWA. SOW A, and RCRA are pcrro1111od in accordcnee to NE LAC protQ<:Ols Pertinent sampling infom1nuon is located on the attached COC. Conridenunl Bw;mess lnfonnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in c:onr~ccuQn with 1hc ndveruscmcnt, promOtlon crs:tle or any product or process, or ln connrctkm with the rc•publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer QC SU~Y REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: MS ------- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 2107791-002EMS Date Analyzed: 08/10/2021 1550h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Calcium 516 mg/L E200.7 0.434 10.0 10.00 505 107 70 -130 Magnesium 168 mg/L E200.7 0.138 1.00 10.00 157 110 70 -130 Sodium 344 mg/L E200,7 3.23 10.0 10.00 334 99.7 70-130 Lab Sample ID: 2107791-00JEMS Date Analyzed: 08/10/2021 1556h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Calcium 411 mg/L E200.7 0.434 10.0 10.00 395 153 70-130 2 Magnesium 194 mg/L E200,7 0.138 1.00 10.00 182 126 70 -130 Sodium 143 mg/L E200.7 3.23 10.0 10.00 132 115 70 -130 Lab Sample ID: 210779l-002EMS Date Analyzed: 08/10/2021 1700h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Potassium 27.0 mg/L E200 7 0.177 1.00 10.00 14.7 123 70 -130 Vanadium 0.210 mg/L E200.7 0.00137 0.00500 0.2000 0 105 70 -130 Lab Sample ID: 2107791-00JEMS Date Analyzed: 08/10/2021 1707h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Potassium 21.5 mg/L E200.7 0.177 1.00 10.00 9.58 119 70-130 Vanadium 0.209 mg/L E200,7 0.00137 0.00500 0.2000 0 105 70 -130 Lab Sample ID: 2107791-002EMS Date Analyzed: 08/13/2021 1330h Test Code: 200.8-DIS Date Prepared: 08/02/2021 943h ------- Arsenic 0.219 mg/L E200.8 0.000298 0.00200 0.2000 0.000334 109 75 -125 Beryllium 0.194 mg/L E200.8 0.000198 0.00200 0.2000 0 96.9 75 -125 Cadmium 0.201 mg/L E200.8 0.0000742 0.000500 0.2000 0.00163 99.9 75 -125 Chromium 0.201 mg/L E200.8 0.000920 0.00200 0.2000 0 IOI 75 -125 Cobalt 0.196 mg/L E200.8 0.000300 0.00400 0.2000 0.00238 96.6 75 -125 Copper 0.197 mg/L E200.8 0.001 II 0.00200 0.2000 0 98.6 75 -125 Report Date: 8/24/2021 Page 54 of 72 analyses apphc.1blc to the CWA, SDWA, and RCRA an: pcrfonncd in accordarn:c lo NEI.AC protocols Penonent sampling inl'onnauon is located on the niu,chcd COC. Conlidcndal Bu.<iness Information: This report is provided (or the exclusive use of the addressee. Privileges of subsequent use of tf ne of this compnny or ~ny member of its staff, or reproduction of 1b1s report in tonncciiori whh the ndvcnt1'('ment, promo11on or~lc of any product or proc.css.. Of ,n conn«J1on wtth tile rr~publication of this report for any purpose othcr than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 841 I 9 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: MS -------- Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample lD: 2107791-002EMS Date Analyzed: 08/13/2021 1330h Test Code: 200.8-DIS Date Prepared: 08/02/2021 943h Iron 1.02 mg/L E200.8 0.0312 0.100 1.000 0 102 75 -125 Lead 0.189 mg/L E200.8 0.000588 0.00200 0.2000 0 94.3 75 -125 Manganese 2.06 mg/L E200 8 0.000930 0.00200 0.2000 1.84 I 13 75 -125 Molybdenum 0.223 mg/L E200.8 0.000884 0.00200 0.2000 0.00523 109 75 -125 Nickel 0.204 mg/L E200.8 0.000584 0.00200 0.2000 0.00453 99.8 75 -125 Selenium 0.200 mg/L E200.8 0.000508 0.00200 0.2000 0 100 75 -125 Thallium 0.187 mg/L E200.8 0.000418 0.00200 0.2000 0 93.7 75 -125 Tin 1.02 mg/L E200.8 0.000968 0.00400 1.000 0 102 75 -125 Uranium 0.257 mg/L E200.8 0.000176 0.00200 0.2000 0.06 98.5 75 -125 Zinc 1.03 mg/L E200.8 0.00418 0.00600 1.000 0.0152 101 75 -125 Lab Sample ID: 2107791-00JEMS Date Analyzed: 08/13/2021 134 I h Test Code: 200.8-DIS Date Prepared: 08/02/202 l 943h Arsenic 0.223 mg/L E200.8 0.000298 0.00200 0.2000 0.000529 Ill 75 -125 Beryllium 0.195 mg/L E200,8 0.000198 0.00200 0.2000 0 97.6 75 -125 Cadmium 0.206 mg/L E200,8 0.0000742 0.000500 0.2000 0.0000755 103 75 -125 Chromium 0.202 mg/L E200.8 0.000920 0.00200 0.2000 0 IOI 75 -125 Cobalt 0.194 mg/L E200.8 0.000300 0.00400 0.2000 0 97.0 75 -125 Copper 0.199 mg/L E200.8 0.00111 0.00200 0.2000 0.00123 98.8 75 -125 Iron 1.03 mg/L E200.8 0.0312 0.100 1.000 0 103 75 -125 Lead 0.191 mg/L E200,8 0.000588 0.00200 0.2000 0 95.7 75 -125 Manganese 0.204 mg/L E200.8 0.000930 0.00200 0.2000 0 102 75 -125 Molybdenum 0.220 mg/L E200.8 0.000884 0.00200 0.2000 0.00367 108 75 -125 Nickel 0.199 mg/L E200.8 0.000584 0.00200 0.2000 0 99.6 75 -125 Selenium 0.290 mg/L E200.8 0.000508 0.00200 0.2000 0.0865 102 75 -125 Thallium 0.190 mg/L E200.8 0.000418 0.00200 0.2000 0 95.2 75 -125 Tin 1.02 mg/L E200.8 0.000968 0.00400 1.000 0 102 75 -125 Report Date: 8/24/2021 Page 55 of72 analyses applicable to the C\VA, SOWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. Conr,dentutl 8u$lncs$ lnforrnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of thls report in c:onr,cc:uon with the advcn1s.cmcnt. promotion or sale of any product or process, or in conn~tiou whh the ~pl1blication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Tanner Holliday ME MS ----------------------- Analyte Result Lab Sample ID: 2107791-00JEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Uranium 0.217 Zinc 1.03 Lab Sample ID: 2107791-00ZEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Manganese 2.09 -Lab Sample ID: 2107791-0llEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Silver 0.186 Lab Sample ID: 2107791-0lZEMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Silver 0.194 Lab Sample ID: 2107791-00IEMS Date Analyzed: Test Code: HG-DW-DIS-245.1 Date Prepared: Mercury 0.00330 Units Method 08/13/2021 1341h 08/02/2021 943h mg/L E200.8 mg/L E200,8 -08/13/2021 1501h 08/02/2021 943h mg/L E200.8 -08/16/2021 1112h 08/13/2021 1610h mg/L E200.8 08/16/2021 1125h 08/13/2021 1610h mg/L E200.8 -08/03/2021 1124h 08/02/2021 1214h mg/L E245,I 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. MDL 0.000176 0.00418 0.00186 0.000232 0.000232 0.0000396 Reporting Limit 0.00200 0.00600 0.00400 0.00200 0.00200 0.0000900 Amount Spiked 0.2000 1.000 0.2000 0.2000 0.2000 0,003330 Spike Ref. Amount 0.02 0 1.84 0 0 0 %REC 98.6 103 126 93.0 96.8 99.1 Limits 75 -125 75 -125 75 -125 75 -125 75 -125 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt % RPO Limit Qua) 7 Report Date: 8/24/2021 Page 56 of 72 analyses applicable to the CWA. SOWA, and RCRA tm: pcrfonncd in accordootc to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business information: This report ls provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or rcproductlon of this report in connec1fon ,vtth the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer C SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2 021 QC Type: MSD --- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2l07791-002EMSD Date Analyzed: 08/10/2021 1552h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Calcium 525 mg/L E200.7 0.434 10.0 10.00 505 201 70 -130 516 1.80 20 Magnesium 171 mg/L E200.7 0.138 1.00 10.00 157 138 70 -130 168 1.65 20 Sodium 350 mg/L E200.7 3.23 10.0 10.00 334 163 70-130 344 1.8 I 20 Lab Sample ID: 2107791-00JEMSD Date Analyzed: 08/10/2021 I 558h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Calcium 413 mg/L E200 7 0.434 10.0 10.00 395 179 70 -130 411 0.640 20 Magnesium 196 mg/L E200.7 0.138 1.00 10.00 182 139 70 -130 194 0.711 20 Sodium 144 mg/L E200.7 3.23 10.0 10.00 132 124 70 -130 143 0.644 20 Lab Sample ID: 2l07791-002EMSD Date Analyzed: 08/10/2021 1703h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Potassium 27.5 mg/L E200.7 0.177 1.00 10.00 14.7 127 70 -130 27 1.66 20 Vanadium 0.209 mg/L E200,7 0.00137 0.00500 0.2000 0 104 70 -130 0.21 0.545 20 Lab Sample ID: 2107791-00JEMSD Date Analyzed: 08/ 10/202 I 1709h Test Code: 200.7-DIS Date Prepared: 08/02/2021 943h Potassium 21.4 mg/L E200.7 0.177 1.00 10.00 9.58 I 19 70 -130 21.5 0.365 20 Vanadium 0.208 mg/L E200.7 0.00137 0.00500 0.2000 0 104 70 -130 0.209 0.863 20 Lab Sample ID: 2107791-002EMSD Date Analyzed: 08/13/2021 1334h Test Code: 200.8-DIS Date Prtpared: 08/02/2021 943h ---- Arsenic 0.215 mg/L E200 8 0.000298 0.00200 0.2000 0.000334 107 75 -125 0.219 1.96 20 Beryllium 0.187 mg/L E200.8 0.000198 0.00200 0.2000 0 93.5 75 -125 0.194 3.55 20 Cadmium 0.200 mg/L E200,8 0.0000742 0.000500 0.2000 0.00163 99,0 75 -125 0.201 0.872 20 Chromium 0.197 mg/L E200,8 0.000920 0.00200 0.2000 0 98.4 75 -125 0.201 2.31 20 Cobalt 0.191 mg/L E200.8 0.000300 0.00400 0.2000 0.00238 94.5 75 -125 0,196 2.19 20 Copper 0.193 mg/L E200.8 0.00111 0.00200 0.2000 0 96.7 75 -125 0.197 1.93 20 Report Date: 8/24/2021 Page 57 of72 analyses appllcoble 10 the CWA. SOWA, and RCRA are pcrformod in accordllnc:o to NELAC p«nocols. Pertinent ,arnpllng infoonauon is located on the attached COC tor,fidcntial Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of 1! ne of this company or any member of its staff, or reproductton or this report in connccuon wnh the ~dvertisement. promolion or sale of any product or process. or in conMC-Jion with tJ,e re-publication of this report for any purpose other than for the addressee will be granted only on contact. This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (80 I) 263-8686, Toll Free: (888) 263-8686, Fax: (80 I) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-Iabs.com Jose Rocha QA Officer QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday LabSetID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: MSD Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2107791-002EMSD Date Analyzed: 08/13/2021 1334h Test Code: 200.8-D!S Date Prepared: 08/02/2021 943h Iron 0.990 mg/L E200.8 0.0312 0.100 1.000 0 99.0 75 -125 1.02 2.93 20 Lead 0.186 mg/L E200.8 0.000588 0.00200 0.2000 0 93.2 75 -125 0.189 1.23 20 Manganese 2.05 mg/L E200.8 0.000930 0.00200 0.2000 1.84 108 75 -125 2.06 0.498 20 Molybdenum 0.222 mg/L E200 8 0.000884 0.00200 0.2000 0.00523 108 75 -125 0.223 0.561 20 Nickel 0.198 mg/L E200.8 0.000584 0.00200 0.2000 0.00453 96.5 75 -125 0.204 3.29 20 Selenium 0.199 mg/L E200 8 0.000508 0.00200 0.2000 0 99.5 75 -125 0.2 0.626 20 Thallium 0.185 mg/L E200.8 0.000418 0.00200 0.2000 0 92.7 75 -125 0.187 1.03 20 Tin 1.02 mg/L E200.8 0.000968 0.00400 1.000 0 102 75 -125 1.02 0.434 20 Uranium 0.255 mg/L E200 8 0.000176 0.00200 0.2000 0.06 97.5 75 -125 0.257 0.708 20 Zinc 1.01 mg/L E200.8 0.00418 0.00600 1.000 0.0152 99.5 75 -125 1.03 1.71 20 Lab Sample ID: 2107791-003EMSD Date Analyzed: 08/13/2021 I 345h Test Code: 200.8-DIS Date Prepared: 08/02/2021 943h Arsenic 0.221 mg/L E200 8 0.000298 0.00200 0.2000 0.000529 110 75 -125 0.223 0.744 20 Beryllium 0.196 mg/L E200.8 0.000198 0.00200 0.2000 0 98.2 75 -125 0.195 0.653 20 Cadmium 0.200 mg/L E200,8 0.0000742 0.000500 0.2000 0.0000755 99.8 75 -125 0.206 2.88 20 Chromium 0.206 mg/L E200.8 0.000920 0.00200 0.2000 0 103 75 -125 0.202 1.56 20 Cobalt 0.194 mg/L E200.8 0.000300 0.00400 0.2000 0 96.9 75 -125 0.194 0.128 20 Copper 0.200 mg/L E200,8 0.00111 0.00200 0.2000 0.00123 99.3 75 -125 0.199 0.485 20 Iron 1.02 mg/L E200.8 0.0312 0.100 1.000 0 102 75 -125 1.03 0.639 20 Lead 0.192 mg/L E200.8 0.000588 0.00200 0.2000 0 96.1 75 -125 0.191 0.397 20 Manganese 0.204 mg/L E200,8 0.000930 0.00200 0.2000 0 102 75 -125 0.204 0.100 20 Molybdenum 0.218 mg/L E200.8 0.000884 0.00200 0.2000 0.00367 107 75 -125 0.22 0.838 20 Nickel 0.201 mg/L E200 8 0.000584 0.00200 0.2000 0 IOI 75 -125 0.199 0.935 20 Selenium 0.288 mg/L E200 8 0.000508 0.00200 0.2000 0.0865 IOI 75 -125 0.29 0.736 20 Thallium 0.192 mg/L E200.8 0.000418 0.00200 0.2000 0 95.8 75 -125 0.19 0.595 20 Tin 1.02 mg/L E200.8 0.000968 0.00400 1.000 0 102 75 -125 1.02 0.0441 20 Report Date: 8/24/2021 Page 58 of72 anaJyses applicable to the CWA, SOWA, and RCRA are perfonncd in accordance 10 NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction Qf 1his report in conm:cuon with the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: ME Project: 3rd Quarter Ground Water 2021 QC Type: MSD --~m------ Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: 2107791-00JEMSD Date Analyzed: 08/13/2021 1345h Test Code: 200.8-DIS Date Prepared: 08/02/2021 94 3 h Uranium 0.219 mg/L E200.8 0.000176 0.00200 0.2000 0.02 99.5 75 -125 0.217 0.793 20 Zinc 1.01 mg/L E200 8 0.00418 0.00600 1.000 0 101 75 -125 1.03 1.76 20 Lab Sample ID: 2107791-002EMSD Date Analyzed: 08/13/202 I 1505h Test Code: 200.8-DIS Date Prepared: 08/02/2021 943h Manganese 2.13 mg/L E200.8 0.00186 0.00400 0.2000 1.84 148 75 -125 2.09 2.05 20 Lab Sample ID: 2107791-0llEMSD Date Analyzed: 08/16/2021 1117h Test Code: 200.8-DIS Date Prepared: 08/13/2021 1610h Silver 0.189 mg/L E200 8 0.000232 0.00200 0.2000 0 94.3 75 -125 0.186 1.39 20 Lab Sample ID: 2107791-012EMSD Date Analyzed: 08/16/2021 1129h Test Code: 200.8-DIS Date Prepared: 08/13/2021 1610h Silver 0.189 mg/L E200.8 0.000232 0.00200 0.2000 0 94.7 75 -125 0.194 2.19 20 Lab Sample ID: 2107791-00lEMSD Date Analyzed: 08/03/2021 1126h Test Code: HG-DW-DIS-245.1 Date Prepared: 08/02/2021 1214h Mercury 0.00348 mg/L E245.I 0.0000396 0.0000900 0.003330 0 104 85 -115 0.0033 5.21 20 2 -Analyte concentration is too high for accurate matrix spike recovery and/or RPD. Report Date: 8/24/2021 Page 59 of 72 analyses applicable to the CWA. SOWA, and RCRA are pcrfom1cd in accord:inc.c-10 NE LAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Information: TI1is report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report ,n conrtec110n with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Method MDL Reporting Limit Contact: Dept: QC Type: Amount Spiked Tanner Holliday WC DUP Spike Ref. Amount %REC Lab Sample ID: 2107791-00lCDUP Date Analyzed: 07/30/2021 1345h Test Code: TDS-W-2540C Total Dissolved Solids 2,710 mg/L SM2540C 16.0 20.0 Lab Sample ID: 2107791-0llCDUP Date Analyzed: 07/30/2021 1345h Test Code: TDS-W-2540C Total Dissolved Solids 4,610 mg/L SM2540C 16.0 20.0 Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual 2680 1.34 5 4490 2.64 5 Report Date: 8/24/2021 Page 60 of 72 analyses appl1coblc l<l ihc CWA, SOWA, and RCRA are pcrlonned m accord.o.nct" to NBL.AC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business lnformntion: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this comp.<my or any member of its staff, or reproductiqn ofth1s report in connection with 1he advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer _QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 210779 l Dept: WC Project: 3rd Quarter Ground Water 2021 QC Type: LCS ---- Reporting Amount Spike Ref. RPDRef. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPD Limit Qual Lab Sample ID: LCS-R155357 Date Analyzed: 08/10/2021 I 948h Test Code: 300.0-W Chloride 5.08 mg/L E300.0 0.0198 0.100 5.000 0 102 90 -110 Fluoride 4.97 mg/L E300.0 0.00260 0.100 5.000 0 99.5 90 -110 Sulfate 5.11 mg/L E300.0 0.0750 0.500 5.000 0 102 90 -110 Lab Sample ID: LCS-Rl54964 Date Analyzed: 08/02/2021 11 00h Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) 249 mg/L SM2320B 0.333 1.00 250.0 0 99.6 90 -110 Lab Sample ID: LCS-78746 Date Analyzed: 08/04/2021 1336h Test Code: NH3-W-350.l Date Prepared: 08/04/2021 1050h Ammonia (as N) 2.17 mg/L E350.1 0.0495 0.0500 2.000 0 109 90 -110 Lab Sample ID: LCS-Rl54940 Date Analyzed: 08/02/2021 1359h Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) 1.02 mg/L E353.2 0.00541 0.0100 1.000 0 102 90 -110 Lab Sample ID: LCS-Rl55201 Date Analyzed: 08/06/2021 1415h Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 1.09 mg/L E353.2 0.00541 0.0100 1.000 0 109 90 -110 Lab Sample ID: LCS-R154924 Date Analyzed: 07 /30/202 I 1345h Test Code: TDS-W-2540C -------------------· ----- Total Dissolved Solids 208 mg/L SM2540C 8.00 10.0 205.0 0 IOI 80 -120 Report Date: 8/24/2021 Page 61 of 72 analyses appl1C11ble 10 the CWA. SOWA, and RC'RA ore pcrfonncd in accordance 10 NELAC protocols. P,•runent samphni; mron11011.,,, is loco1od on the attached COC Confidcnlial llu~iness Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oftf ne of this company or MY member of its staff, or reproduction uf llus report in conncc11on with the :wh·cn,scmcnt, promo1inn of sak of~ny produc1 or process. or in conlll..:Uon whh 1hc re-publication of this report for any purpose other than for the addressee will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB-R155357 Date Analyzed: Test Code: 300.0-W Chloride <0.100 Fluoride < 0.100 Sulfate < 0.500 Lab Sample ID: MB-R154964 Date Analyzed: Test Code: ALK-W-23208-LL Bicarbonate (as CaCO3) < 1.00 Carbonate (as CaC03) < 1.00 Lab Sample ID: MB-78746 Date Analyzed: Test Code: NH3-W-350.l Date Prepared: Ammonia (as N) < 0.0500 Lab Sample ID: MB-R154940 Date Analyzed: Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-R155201 Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-R154924 Date Analyzed: Test Code: TDS-W-2540C ----- Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fmc (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/10/2021 1924h mg/L E300,0 0.0198 0.100 mg/L E300.0 0.00260 0.100 mg/L E300.0 0.0750 0.500 08/02/2021 1100h mg/L SM2320B 0.333 1.00 mg/L SM2320B 0.333 1.00 08/04/2021 1336h 08/04/2021 I 050h mg/L E350.l 0.0495 0.0500 08/02/2021 1357h mg/L E353.2 0.00541 0.0100 08/06/2021 1414h mg/L E353,2 0.00541 0.0100 07/30/2021 I 345h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 8/24/2021 Page 62 of72 analyses applicable to the CWA, SOWA, and RCRA are ptrfonned in accordanrc 10 NEL--\C protocols Pertinent sampling information is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of1h,s report in co,1ncc11on wnh lhc advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107791-00JBMS Date Analyzed: Test Code: 300.0-W Chloride 1,410 Fluoride 979 Sulfate 2,200 Lab Sample ID: 2107791-0UBMS Date Analyzed: Test Code: 300.0-W Chloride 705 Fluoride 489 Sulfate 1,270 Lab Sample ID: 2107791-00IBMS Date Analyzed: Test Code: ALK-W-2320B-LL Alkalinity (as CaCO3) 2,820 Lab Sample ID: 2107791-00IDMS Date Analyzed: Test Code: NH3-W-350.l Date Prepared: Ammonia (as N) 2.39 Lab Sample ID: 2107668-002AMS Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 19.3 Lab Sample ID: 2107791-006DMS Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 9.74 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Tol1 Free: (888) 263-8686, Fmc (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/ I 0/2021 2122h mg/L E300.0 3.96 20.0 1,000 mg/L E300.0 0.520 20.0 1,000 mg/L E300.0 15.0 100 1,000 08/11/2021 1527h mg/L E300.0 1.98 10.0 500.0 mg/L E300.0 0.260 10.0 500.0 mg/L E300 0 7.50 50.0 500.0 08/02/2021 II 00h mg/L SM2320B 0.333 1.00 2,500 08/04/2021 1338h 08/04/2021 1050h mg/L E350.1 0.0495 0.0500 2.000 08/02/2021 1414h mg/L E353.2 0.0541 0.100 l0.00 08/02/2021 1426h mg/L E353.2 0.0541 0.100 10.00 Tanner Holliday WC MS Spike Ref. Amount %REC 391 102 0.623 97.8 1210 99.1 188 103 0.318 97.8 754 104 320 100 0.483 95.2 6,09 132 0 97.4 Limits 90 -110 90 -110 90 -110 90 -110 90 -110 90 -110 80 -120 90 -110 90 -110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/24/2021 Page 63 of72 analyses applicable to the CWA. SDWA, and RCRA are performed in accord3n<:"-C t('II NELAC protocols Pertinent sampling information is located on the attached COC Confidential Buslness Information: This report is provided for the oxclusive use 0(1hc addressee. Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of1h1s report m co11m:ction with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose olhcr lhan for the nddrcs:sc.e will be granted only on contact. This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107791-0lODMS Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 12.0 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday WC MS Spike Ref. Amount %REC 08/06/2021 1445h mg/L E353.2 0.0541 0.100 10.00 0.377 116 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 90-110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer ----- RPD Ref. Amt %RPO RPD Limit Qual Report Date: 8/24/2021 Page 64 of 72 analyses applicable to the CWA, SOWA, and RCRA are pcrfonncd in accordoocc to l\~ELAC protocols Pertinent sampling information is located on the attached COC Confidential Business [nformation: TI1is report is provided for the exclusive use of the addressee. Privileges ofs\lbscquent use oft~ ne of this company or any member of its staff, or reproduction of1h1s report m connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the oddressee will be granted only on coma<it. This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, fa'(: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West OC SUMMARY REPORT ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: WC Project: 3rd Quarter Ground Water 2021 QC Type: MSD ---- Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2107791-00JBMSD Date Analyzed: 08/10/2021 2146h Test Code: 300.0-W Chloride 1,400 mg/L E3000 3.96 20.0 1,000 391 101 90 -110 1410 0.383 20 Fluoride 979 mg/L E300.0 0.520 20.0 1,000 0.623 97.8 90 -110 979 0.00781 20 Sulfate 2,190 mg/L E300.0 15.0 100 1,000 1210 97.9 90 -110 2200 0.544 20 Lab Sample ID: 2107791-012BMSD Date Analyzed: 08/11/2021 1550h Test Code: 300.0-W Chloride 700 mg/L E300.0 1.98 10.0 500.0 188 102 90 -110 705 0.761 20 Fluoride 487 mg/L E300,0 0.260 10.0 500.0 0.318 97.4 90 -110 489 0.392 20 Sulfate 1,260 mg/L E300,0 7.50 50.0 500.0 754 102 90 -110 1270 0.924 20 -Lab Sample JD: 2107791-00lBMSD Date Analyzed: 08/02/2021 11 OOh Test Code: ALK-W-2320B-LL Alkalinity (as CaC03) 2,830 mg/L SM2320B 0.333 1.00 2,500 320 100 80 -120 2830 0.177 10 Lab Sample ID: 2107791-00IDMSD Date Analyzed: 08/04/202 I 1339h Test Code: NH3-W-350.l Date Prepared: 08/04/2021 1050h Ammonia (as N) 2.28 mg/L E350,l 0.0495 0.0500 2.000 0.483 89.8 90 -I 10 2.39 4.61 10 § Lab Sample ID: 2107668-002AMSD Date Analyzed: 08/02/2021 1415h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 16.0 mg/L E353.2 0.0541 0.100 10.00 6.09 99.1 90 -110 19.3 18.7 10 @ Lab Sample ID: 2107791-006DMSD Date Analyzed: 08/02/2021 1427h Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 10.5 mg/L E353.2 0.0541 0.100 10.00 0 105 90 -110 9.74 7.51 10 Report Date: 8/24/2021 Page 65 of 72 analyses applkable lO the. CWA. SOWA, and RCRA arc pcrfom1cd in accordon<:c to NELAC' protocols Pertinent sampling infom1ation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this comp:tny or tu·.y member of its staff, or l'C'product1on of1h1s report 1n 4;'0fln«tion with the advertisement. promotion or sale of any product or process. or in connection with the re•publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Contact: Dept: Tanner Holliday WC Project: 3rd Quarter Ground Water 2021 QC Type: MSD ---------- Reporting Amount Analyte Result Units Method MDL Limit Spiked Lab Sample ID: 2107791-0lODMSD Date Analyzed: 08/06/2021 1446h Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) 15.1 mg/L E353.2 0.0541 0.100 10.00 @ -High RPD due to suspected sample non-homogeneity or matrix inLerference. § -QC limits are set with an accuracy of two significant figures, therefore the recovery rounds lo an acceptable value within the control limits. 1 -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Spike Ref. Amount 0.377 %REC 147 Limits 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPO Amt %RPO Limit 12 22.7 10 Qual '@ Report Date: 8/24/2021 Page 66 of 72 analyses applicable to the CWA. SDWA, and RCRA are pcrfonned in accordoncc IO NEl..i\C protocols Pertinent sampling information is located on the attached COC Confidential Business lnformntion: TI1is report is pl()vidcd for lhe exclusive use of the addressee. Privileges of PJbscqucn1 use of tr ne of this company or any member of its staff, or reproduction of thts report m connccuon with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on con1act, This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer _QC_SUMMARY REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: MSVOA Project: 3rd Quarter Ground Water 2021 QC Type: LCS ------- Reporting Amount Spike Ref. RPO Ref. RPO Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: LCS VOC-2 073021A Date Analyzed: 07/30/2021 702h Test Code: 8260D-W-DEN100 2-Butanone 17.8 µg/L SW8260D 1.22 20.0 20.00 0 89.2 69 -236 Acetone 18. l µg/L SW8260D 2.76 20.0 20.00 0 90.7 36 -198 Benzene 19.8 µg/L SW8260D 0.147 1.00 20.00 0 99.1 78 -125 Carbon tetrachloride 19.4 µg/L SW8260D 0.785 1.00 20.00 0 97.l 66 -143 Chloroform 18.8 µg/L SW8260D 0.360 1.00 20.00 0 94.2 74 -120 Chloromethane 16.8 µg/L SW8260D 0.682 1.00 20.00 0 83.8 30 -149 Methylene chloride 19.4 µg/L SW8260D 0.451 1.00 20.00 0 97.0 65 -154 Naphthalene 13.6 µg/L SW8260D 0.730 1.00 20.00 0 68.0 55 -128 Tetrahydrofuran 18.1 µg/L SW8260D 0.436 1.00 20.00 0 90.7 59-135 Toluene 20.4 µg/L SW8260D 0.277 1.00 20.00 0 102 69 -129 Xylenes, Total 63.3 µg/L SW8260D 0.746 1.00 60.00 0 106 66 -124 Surr: l,2-Dichloroethane-d4 48.7 µg/L SW8260D 50.00 97.4 80 -136 Surr: 4-Bromofluorobenzene 51.4 µg/L SW8260D 50.00 103 85 -121 Surr: Dibromofluoromethane 48.2 µg/L SW8260D 50.00 96.4 78 -132 Surr: Toluene-d8 50.0 µg/L SW8260D 50.00 100 81 -123 Lab Sample ID: LCS VOC-2 080221A Date Analyzed: 08/02/2021 808h Test Code: 8260D-W-DEN100 2-Butanone 18 µg/L SW8260D 1.22 20.0 20.00 0 89.9 69 -236 Acetone 17.4 µg/L SW8260D 2.76 20.0 20.00 0 86.9 36 -198 Benzene 19.6 µg/L SW8260D 0.147 1.00 20.00 0 98.2 78 -125 Carbon tetrachloride 19.1 µg/L SW8260D 0.785 1.00 20.00 0 95.7 66 -143 Chloroform 18.9 µg/L SW8260D 0.360 1.00 20.00 0 94.6 74 -120 Chloromethane 16.3 µg/L SW8260D 0.682 1.00 20.00 0 81.6 30 -149 Methylene chloride 19.2 µg/L SW8260D 0.451 1.00 20.00 0 96.2 65 -154 Naphthalene 14.6 µg/L SW8260D 0.730 1.00 20.00 0 72.9 55 -128 Tetrahydrofuran 18.5 µg/L SW8260D 0.436 1.00 20.00 0 92.6 59 -135 Report Date: 8/24/2021 Page 67 of 72 analyses apphcablc 10 1h• CWA. SOWA, and RCRA are perfom1ed in accordance 10 Ni:LA(' protocols Pertinent sampling information is located on the attached COC Confidential Business Information: TI1is report is provided for the exclusive use of the addressee, Privileges of subsequent use of tf ne of this compomy or any member of its staff, or reproduction of this report in connccuon wnh the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: LCS VOC-2 080221A Date Analyzed: Test Code: 8260D-W-DEN100 Toluene 20.3 Xylenes, Total 62.6 Surr: l,2-Dichloroethane-d4 47.4 Surr: 4-Bromofluorobenzene 48.8 Surr: Dibromofluoromethane 46.9 Surr: Toluene-d8 48.7 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awa1@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 08/02/2021 808h µg/L SW8260D 0.277 1.00 20.00 0 102 µg/L SW8260D 0.746 1.00 60.00 0 104 µg/L SW8260D 50.00 94.9 µg/L SW8260D 50.00 97.7 µg/L SW8260D 50.00 93.8 µg/L SW8260D 50.00 97.4 Limits 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 8/24/2021 Page 68 of 72 analyses applicable to the CWA. SOWA, and RCRA are pcrfom,cd in accor4oncc to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnformt,tion: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection wlth there-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB VOC-2 073021A Date Analyzed: Test Code: 8260D-W-DENIOO 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrahydrofuran < 1.00 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l ,2-Dichloroethane-d4 48.2 Surr: 4-Bromofluorobenzene 52.5 Surr: Dibromofluoromethane 46.6 Surr: Toluene-d8 49.9 Lab Sample ID: MB VOC-2 080221A Date Analyzed: Test Code: 8260D-W-DENIOO 2-Butanone <20.0 Acetone <20.0 Benzene < 1.00 Carbon tetrachloride < 1.00 Chloroform < 1.00 Chloromethane < 1.00 Methylene chloride < 1.00 Naphthalene < 1.00 Tetrahydrofuran < 1.00 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Tanner Holliday Dept: MS VOA QC Type: MBLK ---------- Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 07 /30/202 I 722h µg/L SW8260D 1.22 20.0 µg/L SW8260D 2.76 20.0 µg/L SW8260D 0.147 1.00 µg/L SW8260D 0.785 1.00 µg/L SW8260D 0.360 1.00 µg/L SW8260O 0.682 1.00 µg/L SW8260D 0.451 1.00 µg/L SW8260D 0.730 1.00 µg/L SW8260D 0.436 1.00 µg/L SW8260D 0.277 1.00 µg/L SW8260O 0.746 1.00 µg/L SW8260D 50.00 96.5 µg/L SW8260D 50.00 105 µg/L SW8260D 50.00 93.3 µg/L SW8260D 50.00 99.9 08/02/2021 828h µg/L SW8260D 1.22 20.0 µg/L SW8260D 2.76 20.0 µg/L SW8260D 0.147 1.00 µg/L SW8260O 0.785 1.00 µg/L SW8260O 0.360 1.00 µg/L SW8260D 0.682 1.00 µg/L SW8260D 0.451 1.00 µg/L SW8260O 0.730 1.00 µg/L SW8260D 0.436 1.00 Limits 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPO Limit Qual Report Date: 8/24/2021 Page 69 of 72 analyses applicable to the CWA. SOWA, and RCRA are performed in accordnncc to NELAC pro1ocols Pertinent sampling information is located on the attached COC Confidential Business lnformsttion: TI1is report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of thls report ln connc-c11on \Vllh 1he advertisement. promotion or sale of any product or process, or in connection with the re-pub I ication of this report for any purpose other 1han for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: MB VOC-2 080221A Date Analyzed: Test Code: 8260D-W-DEN100 Toluene < 1.00 Xylenes, Total < 1.00 Surr: l ,2-Dichloroethane-d4 47.2 Surr: 4-Bromofluorobenzene 52.5 Surr: Dibromofluoromethane 45.7 Surr: Toluene-d8 49.3 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: ,vww.awal-labs.com _Q_C_SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 08/02/202 I 828h µg/L SW8260D 0.277 1.00 µg/L SW8260D 0.746 1.00 µg/L SW8260D 50.00 94.4 µg/L SW8260D 50.00 105 µg/L SW8260D 50.00 91.4 µg/L SW8260D 50.00 98.6 Limits 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/24/202 l Page 70 of 72 analyses applicable to the CWA. SOWA, and RCRA are pcrf'ormcd in accordllnc-e fO NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business lnfomiation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction or 1his report in conncctton with the advertisement, promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2107791 Project: 3rd Quarter Ground Water 2021 Analyte Result Lab Sample ID: 2107791-007AMS Date Analyzed: Test Code: 8260D-W-DENlOO 2-Butanone 169 Acetone 183 Benzene 199 Carbon tetrachloride 201 Chloroform 883 Chloromethane 158 Methylene chloride 194 Naphthalene 133 Tetrahydrofuran 176 Toluene 207 Xylenes, Total 640 Surr: l,2-Dichloroethane-d4 478 Surr: 4-Bromotluorobenzene 506 Surr: Dibromofluoromethane 477 Surr: Toluene-d8 498 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MS Spike Ref. Amount %REC 08/02/2021 1043h µg/L SW8260D 12.2 200 200.0 0 84.4 µg/L SW8260D 27.6 200 200.0 0 91.6 µg/L SW8260D 1.47 10.0 200.0 0 99.4 µg/L SW8260D 7.85 10.0 200.0 0 100 µg/L SW8260D 3.60 10.0 200.0 723 79.9 µg/L SW8260D 6.82 10.0 200.0 0 79.0 µg/L SW8260D 4.51 10.0 200.0 0 97.2 µg/L SW8260D 7.30 10.0 200.0 0 66.7 µg/L SW8260D 4.36 10.0 200.0 0 87.8 µg/L SW8260D 2.77 10.0 200.0 0 104 µg/L SW8260D 7.46 10.0 600.0 0 107 µg/L SW8260D 500.0 95.6 µg/L SW8260D 500.0 IOI µg/L SW8260D 500.0 95.4 µg/L SW8260D 500.0 99.6 Limits 69 -236 36 -198 78 -125 66 -143 74 -120 30 -149 65 -154 55 -128 59 -135 69 -129 66 -124 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 8/24/2021 Page 71 of 72 analyses applicable to the CWA. SOWA, and RCRA are pcrfom1M in accord.once to NELAC proto:ols Pertinent sampling inforn1at1on is located on the attached COC' Confidential Business lnform:1tion: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproducuon orth,s report in c:onncc11on with the advertisement~ promotion or sale of any product or process. or in connection with there-publication of this report for any purpose other than for the addressee will be granted only on contact This 3440 South 700 West Salt Lake City, UT 84119 Jennifer Osborn Phone: (801) 263-8686, Toll Free: (888) 263-8686. fax: (801) 263-8687 Laboratory Director e-mail: awal@awal-labs.com, web: www.awal-labs.com Jose Rocha QA Officer American West _QC SUMMARY REPORT ANALYTICAL L4BORATORIE9 Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Lab Set ID: 2107791 Dept: MSVOA Project: 3rd Quarter Ground Water 2021 QC Type: MSD Reporting Amount Spike Ref. RPD Ref. RPD Analyte Result Units Method MDL Limit Spiked Amount %REC Limits Amt %RPO Limit Qual Lab Sample ID: 2107791-007 AMSD Date Analyzed: 08/02/202 I I I 03h Test Code: 8260D-W-DENIOO 2-Butanone 193 µg/L SW8260D 12.2 200 200.0 0 96.7 69 • 236 169 13.6 35 Acetone 182 µg/L SW8260D 27.6 200 200.0 0 91.1 36 -198 183 0.602 35 Benzene 208 µg/L SW8260D 1.47 10.0 200.0 0 104 78 -125 199 4.38 35 Carbon tetrachloride 211 µg/L SW8260D 7.85 10.0 200.0 0 105 66 · 143 201 4.86 35 Chloroform 923 µg/L SW8260D 3.60 10.0 200.0 723 100 74 -120 883 4.45 35 Chloromethane 169 µg/L SW8260D 6.82 10.0 200.0 0 84.4 30 · 149 158 6.67 35 Methylene chloride 201 µg/L SW8260D 4.51 10.0 200.0 0 100 65 • 154 194 3.19 35 Naphthalene 139 µg/L SW8260D 7.30 10.0 200.0 0 69.6 55 -128 133 4.33 35 Tetrahydrofuran 181 µg/L SW8260D 4.36 10.0 200.0 0 90.7 59 · 135 176 3.14 35 Toluene 215 µg/L SW8260D 2.77 10.0 200.0 0 107 69 • 129 207 3.56 35 Xylenes, Total 665 µg/L SW8260D 7.46 10.0 600.0 0 111 66 · 124 640 3.92 35 Surr: l ,2-Dichloroethane-d4 488 µg/L SW8260D 500.0 97.6 80 · 136 Surr: 4-Bromofluorobenzene 507 µg/L SW8260D 500.0 101 85 • 121 Surr: Dibromofluoromethane 485 µg/L SW8260D 500.0 97.0 78 · 132 Surr: Toluene-d8 499 jlg/L SW8260D 500.0 99.8 81 · 123 Report Date: 8/24/2021 Page 72 of 72 analyses applicable to the CWA. SOWA, and RCRA are pC1"f°o,,nt.-d in accordance to NELAC proto:ols Pertinent sampling information is located on the attached COC. Confidential Business Lnfom,f1tion: This report is provided fOf' 1he exclusive use of the addressee. Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any ptlrp(>.SC' othC'f' than for the addressee will be granted only on contact. This American West Analytical Laboratories Rpt Emailed: UL Denison WORK ORDER Summary Client: Client ID: Project: Energy Fuels Resources, Inc. ENE300 3rd Quarter Ground Water 2021 Contact: Tanner Holliday QC Level: III WorkOrder: 2107791 Due Date: 8/13/2021 WO Type: Project Page 1 of9 Comments: QC 3 (no chromatograms). EDD-Denison. Email Group; (USE PROJECT for special DLs). Do not use "*R_" samples as MS/MSD.; ~ Sample ID Client Sample ID 2107791-00lA MW-11_07272021 2107791-0018 2107791-00lC 2107791-00lD 2107791-00lE 210779 l-002A MW-14_07272021 2107791-002B 2107791-002C Printed: 07/30/21 13:01 LABORATORY CHECK: ¾M 0 Collected Date Received Date Test Code Matrix Set Storage 7/27/2021 1125h 7/30/2021 ll00h 8260D-W-DENlO0 Aqueous Test Group: 8260D-W-DEN I 00;_ # of ~nalytes: 11 I# of Surr: 4 300.0-W 3 SEL Analytes: CL F S04 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analt_tes: TDS NH3-W-350.1 1 SEL AnalJ,_tes: NH3N NH3-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Ana/ytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG HG-DW-DIS-PR IONBALANCE VOCFridge elf-we elf-we elf-tds elf• no2/no3 & nh3 elf -no2/no3 & nh3 elf. 002/003 & nh3 df-mct elf-met df-met df-met df-met df-mct df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/27/2021 1450h 7/30/2021 l 100h 8260D-W-DENlO0 Aqueous VOCFridge Test Group: 8260]2-W-DENI 00; # of Anal)J_tes: 11 I# of Surr: 4 300.0-W df. WC 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL df-we 2 SEL Analytes: ALKB ALKC TDS-W-2540C df-tds 1 SEL Analytes: TDS RT 0 CN □ TAT 0 QC □ LUO □ HOK~ HOK __ _ HOK __ _ COG Emailed .... V .., I . 3 3 WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 2107791-002D MW-14_07272021 2107791-002E 2107791-003A MW-31_07272021 2107791-003B 2107791-003C 2107791-003D 2107791-003E WorkOrder: 2107791 Due Date: 8/13/2021 Page2 of9 Collected Date Received Date Test Code Matrix Sel Storage 7/27/2021 1450h 7/27/2021 1255h 7/30/2021 1100h NH3-W-3S0.l Aqueous 1 SEL Analytes: NH3N NH3-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 1100h 8260D-W-DEN100 Aqueous Test Group: 8260D-W-DENJ00; # of Analytes: 11 l #ofSw-r: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NH3-W-3S0.l 1 SEL AnafJ,_tes: NH3N NH3-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL AnafJ,_tes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met --df-met --df-met --df-met --df-mct --df-met --df-met - VOCFridge 3 ---df-wc --df-wc --df-tds -- df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met --df-met -- df-met --df-met --df-met Printed: 07/30/21 13:01 LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed ____ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 2107791-00JE MW-31_07272021 2107791-004A MW-36_07272021 2107791-004B 2107791-004C 2107791-004D 2107791-004E 2107791-00SA MW-65_07272021 2107791-00SB 2107791-00SC 2107791-005D WorkOrder: 2107791 Due Date: 8/13/2021 Page 3 of9 Collected Date Received Date Test Code Matrix Sel Storage 7/27/2021125Sh 7/30/2021 1100h HG-DW-DIS-PR Aqueous 7/27/2021 1425h 7/27/2021 1450h IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 1100h 8260D-W-DEN100 Aqueous Test GrouE_: 8260D-W-DENI00; # of_Analytes: I I I# ofSurr: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NH3-W-350.l I SEL Analytes: NH3N NH3-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS I 7 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Anal}'tes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 1 IO0h 8260D-W-DEN100 Aqueous Test GroUf'_: 8260D-J!-!)ENJ00; # of A11alytl!!_." I I I# of Surr: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-23208-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C I SEL Analytes: TDS NH3-W-350.l I SEL Analytes: NH3N df-met elf-met VOCFridge df-wc elf-we df-Ids df -no2/no3 & nh3 df -no2/no3 & ob3 df -no2/no3 & oh3 df-met df-met df-met df-met elf-met elf-met df-met VOCFridge df-wc df-wc df-Ids df -no2/no3 & nh3 3 3 Printed: 07/30/21 13:01 LABORATORY CHECK: %M □ RT □ CN □ TAT O QC □ LUO □ HOK ___ HOK __ _ HOK___ COC Emailed~---- WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID Collected Date 2107791-005D MW-65_07272021 7/27/20211450h 2107791-00SE 2107791-006A MW-25_07282021 7/28/2021 1000h 2107791-006B 2107791-006C 2107791-006D 2107791-006E WorkOrder: 2107791 Due Date: 8/13/2021 Page4of9 Received Date Test Code Matrix Sel Storage 7/30/2021 ll00h NH3-W-PR Aqueous NO2/NO3-W-353.2 I SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Anaf;,_tes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 I SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 ll00h 8260D-W-DEN100 Aqueous Test Group: 8260D-W-DENJO0; # of Analytes: 11 I# of Surr: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL 2 SEL Ana~tes: ALKB ALKC TDS-W-2540C I SEL Anal)'tes: TDS Nlll-W-350.1 I SEL Analytes: NH3N NH3-W-PR NO2/NO3-W-353.2 I SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NJ SE AG TLSNUZN 200.8-DIS-PR HG-DW-DlS-245.1 I SEL Analytes: HG HG-DW-DIS-PR df -no2/no3 & nh3 df • no2/no3 & nh3 df-met df-met df-met df-met df-met df-met df-met VOCFridgc df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met df-met df-met df-met df-met df-met 2 Printed: 07/30/21 13:01 LABORATORY CHECK: %M □ RT □ CN O TAT O QC O LUO □ HOK ___ HOK __ _ HOK___ COC Emailed ____ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 2107791-006E J\.IW-25_07282021 2107791-007 A J\.IW-26_07282021 2107791-007B 2107791-007C 2107791-007D 2107791-007E 2107791-00SA J\.IW-39_07282021 2107791-008B 2107791-00SC 2107791-008D Work Order: 2107791 Due Date: 8/13/2021 Page 5 of9 Collected Date Received Date Test Code Matrix Sel Storage 7/28/2021 1000h 7/28/2021 1300h 7/28/2021 1450h 7/30/2021 llOOh IONBALANCE Aqueous df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 llOOh 8260D-W-DENIOO Aqueous Test Group_: 8260D-W-DENIO0; # of A11alytes: 11 I # of Surr: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-23208-LL 2 SEL A1111lytes: ALKB ALKC TDS-W-2540C I SEL Analytes: TDS NHJ-W-3S0.1 I SEL Analytes: NH3N NHJ-W-PR NO2/NO3-W-3S3.2 I SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SELAnalytes: ASBECDCRCOCU FE PBMNMONISEAG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 I SEL Analytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 1100h 8260D-W-DENlOO Aqueous Test Group_: 8260D-W-DENJO0; # of Analytes: 11 I # ofSurr: 4 300.0-W 3 SEL AnaQJ_tes: CL F SO4 ALK-W-23208-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C I SEL Analytes: TDS NH3-W-350.1 I SEL Anal)'les: NH3N NH3-W-PR VOCFridge df-wc df-wc df-Ids df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-met df-met df-met df-met df-met df-mct df-met VOCFridge df-wc df-wc df-Ids df -no2/no3 & nh3 df -no2/no3 & nh3 3 3 Printed: 07/30/21 13:01 LABORATORY CHECK: %M □ RT □ CN □ TAT O QC □ LUO 0 HOK ___ HOK __ _ HOK___ COG Emailed~---- WORK ORDER Summary WorkOrder: 2107791 Page 6 of9 Client: Sample ID 2107791-008D 2107791-00SE 2!07791-009A 2107791-0098 2107791-009C 2107791-009D 210779l-009E Printed: 08/02/2 l 08:33 Energy Fuels Resources, Inc. Client Sample ID Collected Date Received Date MW-39 _ 07282021 7/28/2021 1450h 7/30/2021 11 OOh MW-40_07282021 7/28/2021 1040h 7/30/2021 llOOh Due Date: 8/13/2021 Test Code Matrix Sel Storage NO2/NO3-W-353.2 Aqueous ~ __!_§_EL Anafft~: NO3NO2N 200.7-DIS ~ 5 SEL Ana/ytes: CA MG K NA V 200.7-DIS-PR ~ 200.8-DIS [~ 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NJ SE AG TLSNUZN 200.8-DIS-PR ~ HG-DW-DIS-245.t ~ I SEL Ana/ytes: HG HG-DW-D1S-PR ~ -- IONBALANCE ~ 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 8260D-W-DENIO0 Aqueous ~ Test Group: 8260D-W-DEN100; # of Ana/ytes: 11 l#_?f Surr: 4 300.0-W "11 3 SEL Ana/ytes: CL F SO4 ALK-W-23208-LL ~ 2 SEL Analytes: ALKB A~C TDS-W-2540C i;;i I SELAnc_iiJte.s: TD§~._ NH3-W-350.l ~ I SEL Analytes: NHJN NH3-W-PR ~ --NO2/NO3-W-353.2 ~] I SEL Ana/ytes: NO3NO2N 200.7-DIS ~ 5 SEL Ana!ytes: CA MG K NA V 200.7-D1S-PR ~ -- 200.8-DIS ~ 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR df -no2/no3 & nh3 df-met df-met df-met df-met df-met df-met df-met VOCFridge df-wc df-wc df-Ids df -no2/no3 & nh3 df -no2/no3 & nh3 --df -no2/no3 & nh3 df-met df-met df-met df-met HG-DW-D1S-245.1 ~ df-met 3 _______________________________ I_SELAna-<-ly_te_s:_H_G _______________________ _ HG-DW-DIS-PR -df-met IONBALANCE _ df-met ________________________ _________ 5_S_E_'L_Anaf)!_tes: BALANCE Anions Cations TDS-Balance TDS-Ca/c .. LABORATORY CHECK: %M O RT [J CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COC Emailed. ____ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 2107791-0l0A MW-24_07292021 2107791-010B 2107791-0l0C 2107791-010D 2107791-0l0E 2107791-0llA MW-24A_07292021 2107791-01 lB 2107791-01 lC 2107791-0llD WorkOrder: 2107791 Due Date: 8/13/2021 Page 7 of9 Collected Date Received Date Test Code Matrix Sel Storage 7/29/2021 0710h 7/29/2021 0700h 7/30/2021 ll00h 8260D-W-DENIO0 Aqueous Test GrouJJ: 8260D-W-DENJ00; # of Ana_jytes: l lj__jl_ojSurr: 4 300.0-W 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL 2 SEL Analytes: ALKB ALKC 1DS-W-2540C 1 SEL Analytes: TDS NHJ-W-350.1 I SEL Analytes: NH3N NHJ-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Anal),tes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SELAnalytes: AS BECD CR CO CU FE PB MN MON/SE AG TLSNU'ZN 200.8-DIS-PR HG-DW-DIS-245.1 I SEL Analyres: HG HG-DW-DIS-PR IONBALANCE 5 SEL Anal}'tes: BALANCE Anions Cations TDS-Balance TDS-Calc 7/30/2021 1100h 8260D-W-DENIOO Aqueous Test Group: 8260D-W-DENJO0; # of Analyte§: 11 I# o/Surr: 4 300.0-W 3 SEL Ana!J,tes: CL F SO4 ALK-W-2320B-LL 2 SEL A11al}'tes: ALKB ALKC 1DS-W-2540C 1 SEL AnaQtfes: TDS NH3-W-350.l 1 SEL Ana!J,tes: NH3N NH3-W-PR , NO2/NO3-W-353.2 1 SEL Anal),_tes: NO3NO2N VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/oo3 & nh3 df-met df-met df-met df-met df-met df-met df-met VOCFridge df-wc df-wc df-tds df • 002/003 & nh3 df • 002/003 & nh3 df • no2/no3 & oh3 2 2 Printed: 07/30/21 13:01 LABORATORY CHECK: %M □ RT □ CN O TAT □ QC □ LUO □ HOK ___ HOK __ _ HOK___ COG Emailed~---- WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID 2107791-0llE MW-24A_07292021 2107791-012A MW-30_07292021 2107791-012B 2107791-012C 2107791-012D 2107791-012E WorkOrder: 2107791 Due Date: 8/13/2021 Page8of9 Collected Date Received Date Test Code Matrix Set Storage 7/29/2021 0700h 7/29/2021 0950h 7/30/2021 1100h 200.7-DIS Aqueous 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DIS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN df-met df-met df-met 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met I SEL Analytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Ana!Ji_tes: BALA.NC£ Anions Cations TDS-Balance TDS-Calc 7/30/2021 llOOh 8260D-W-DENlOO Aqueous Test Group: 8260D-W-DEN100; # of Analytes: l_l_l # of Surr: 4 300.0-W 3 SEL Ana{ytes: CL F SO4 ALK-W-23208-LL 2 SEL Analytes: ALKB ALKC TDS-W-2540C 1 SEL Analytes: TDS NHl-W-350.1 1 SEL Analytes: NH3N NH3-W-PR NO2/NO3-W-353.2 1 SEL Analytes: NO3NO2N 200.7-DIS 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR 200.8-DlS 17 SEL Analytes: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR HG-DW-DIS-245.1 1 SEL Ana{ytes: HG HG-DW-DIS-PR IONBALANCE 5 SEL AnaQ'(es: BALANCE Anions Cations TDS-Balance TDS-Calc VOCFridge df-wc df-wc df-tds df -no2/no3 & nh3 df -no2/no3 & nh3 df -no2/no3 & nh3 df-mct df-met df-met df-met df-met df-met df-met Printed: 07 /30121 13 :0 I LABORATORY CHECK: %M O RT O CN O TAT O QC O LUO 0 HOK ___ HOK __ _ HOK___ COG Emailed ____ _ WORK ORDER Summary Work Order: 2107791 Page9 of9 Client: Energy Fuels Resources, Inc. Due Date: 8/13/2021 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 2107791-0BA MW-38 _ 07292021 7/29/2021 0800h 7/30/2021 1100h 8260D-W-DEN100 Aqueous VOCFridge 3 Test Group: 8260D-W-DENJO0; # of Analytes: 11 I# of Surr: 4 2107791-013B 300.0-W df-wc 3 SEL Analytes: CL F SO4 ALK-W-2320B-LL df-wc 2 SEL Analytes: ALKB ALKC 2107791-0BC TDS-W-2540C df-tds I SEL Analytes: TDS 2107791-013D NID-W-350.1 df -no2/no3 & nb3 I SEL Analytes: NH3N NH3-W-PR df -no2/no3 & nb3 NO2/NO3-W-353.2 df -no2/no3 & nb3 I SEL Analytes: NO3NO2N 2107791-013£ 200.7-DIS df-met 5 SEL Analytes: CA MG K NA V 200.7-DIS-PR df-met 200.8-DIS df-met 17 SEL Analyt,es: AS BE CD CR CO CU FE PB MN MO NI SE AG TLSNUZN 200.8-DIS-PR df-met HG-DW-DIS-245.1 df-met 1 SELAnalytes: HG HG-DW-DIS-PR df-met IONBALANCE df-met 5 SEL Analytes: BALANCE Anions Cations TDS-Balance TDS-Calc 2107791-014A Trip Blank 7/27/2021 1125h 7/30/2021 1100h 8260D-W-DENlO0 Aqueous VOCFridge 3 Test Group: 8260D-W-DENJ00: # of Analytes: 11 I# o/Surr: 2107791-0lSA MW-32_07282021 7/28/2021 1515h 7/28/2021 1515h 300.0-W Aqueous df -cl 1 SEL Analx_tes: CL Printed: 08/03/21 09:09 LABORATORY CHECK: %M □ RT □ CN □ TAT □ QC □ LUO □ HOK ___ HOK __ _ HOK___ COC Emailed ____ _ American West Analytical Laboratories 463 w. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 L-~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: tholliday@energyfuels.com; KWeiDel@energyfuels.com Project Name: Project#: PO#: Sampler Name: MW-11_07272021 2 MW-14 07272021 • MW-31_07272021 MW-36_07272021 4 5 , MW-65 07272021 6 • MW-25_07282021 MW-26 07282021 : MW-39 07282021 9 1 MW-40_07282021 l MW-24 07292021 3Rd Quarter Ground Water 2021 Tanner Holliday Samele ID: 1 MW-241'._07292021 1 MW-30 07292021 Rslnqu!sh<Mlby.},. --.U.Jl-/ . Sinnat.u,e .......... ....,,,, .. -,. Print Name: Tamer Holl'A-. {J Relinquished by: Signature Print Name: Relinquished by: Sionature PrlntNM\e: Relinquis!>cd by: "'"nalure ""ntNamo: Date Sampled 7/27/2021 7/27/2021 7/27/2021 7/27/2021 7/27/2021 7/28/2021 7/28/2021 7/28/2021 7/28/2021 7/29/2021 7/29/2021 7/29/2021 Date: 7129/2021 Time: 110n Date: Time: Date: Time: Date: Time: Time Samoled 1125 1450 1255 1425 1450 1000 1300 1450 1040 710 700 950 Received by: Signature Print Name: Received by: Signature PrtntName: Received by: Slanal!.re Print Name: Received by: Signature Print.Name: I CHAIN OF CUSTODY All analysis wlfl be conducted using NElAP aa:redlled melhods and all data win be reported U$1ng AWAL's standard analyle lists and reporllng llmlts (POL) unless speelr1CSRy req\Jll'Sled olll8"Wis9 on lllls Chain ol Custody and/or attached do<Umenlallon. QC Level: I Tum Around Time: Unless other arrangemenis have been made, signed reports wfH be emaHed by 5:00 pm on 3 Standard Ille day they are due. X Include EDD: 0 LOCUSUPWAD ~ aj u EXCEL bO oil X Field Rltered For: --.. ;i:: ~ Dissolved Metals .... ci' lfi ~ 'I" ~ C'l .0 c€ ~ p.. z For Compliance With: ci .,-~ 0 NELAP Cl r<, 0 RCRA o' C'l ;:J >-□ CWA ci ;:::- Cl ci (.) ::i' □ SOWA --.. (') 0 0 ELAP/A2LA .... ~ Cl ci .. ~ u ci' 0 0 NLLAP Lt) Cl (/) ~ Cl C'l ,. ,: D Non-Compliance (') Cl (') al u p· f;j ... Lt) ~ ... D other: 0 ::t. II) .a . i D' ~ '2. CJ D' = lil u II) Cl (IJ .g Cl "" Cl Cl IO .£ (') Cl 0 'I" Cl "' .,-" s: C'l .l9 ., 0 Lt) llJ Lt) iil CD P'.l (/) .!I !:£. C ::. l!!: ::t. ~ .!: OS Known Hazards 0 ., -a -0 ,,,-i IQ .. u C. N l'l llJ ~ ., .,: 0 & 'o E 0 = t Q ., s: 0 "' l!!: l!!: f,< 0 iS 0 > Samele Comments .. If) ... 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X \(\(1_\ 7 w X X X X X X X X X X I Vk')(:/ ~ b<o~ 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X 7 w X X X X X X X X X X \ ,rn t, v,o..\ bm\uu,,... 7 w X X X X X X X X X X 1 voe '\l,r1.\ hVl""I\~ 7 w X X X X X X X X X X Dale: Special Instructions: Time: 2la779l AWAL Lab Sample Set# Page 1 of 3 Due D~; h ":) \ 2--l Laboratory Use Only SampiesW~ l}.-f) ~J:5YC<ed 2 Ambient . 3 Temperature ~•c 4 Received Broken/Leaking (Improperly Sealed) : c:A S © ,\J~ 5a:PreseNed y N . albench y N 6 Received Within t)~llmes N "'OC Tape Was: y, N NA ~ton Outer Package t:2:kcn on Outer Package N NA entonSample Q y N 4 UObrokenonSample G> Y N NA Discrepancies Between Sample Labels and COC Record7t) y N Date: Sample containers for metals were field filtered. See the Analytical Scope of Work for Reporting Limits and voe analyte llme: list. Dato: Time: .. ~ l..l.:i> _I 1.-.....::> 0~ 2;0~\ ~-f\\~ a·~ Trne: • / ( '~ eQ . 2 4 6 7 8 9 1C I I 12 ! Address: Contact: Phone#; Email: Project Name: Project#: PO#: Sampler Name: MW-38 07292021 Trip Blank Kel!IIQlliohodlly; American West Analytical Laboratories 463 W. 3600 S. Salt lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 6425 S. Hwy. 191 Blanding, UT 84511 Tanner Holliday (435} 678-2221 Cell#: tholliday@energyfueJs.com; KWeinel@energyfuels.com 3rd Quarter Ground Water 2021 Tanner Holliday Date Sam_1>lelD: Sampled l 7/29/2021 7/27/2021 ate: Slonal!Jre ... ,~ .JJ. u :/_ 1-~.-ta I 7/29.12Q21 '.J nme: Print Name: Tanner Hoffidav 1100 R!lllnqUlsheG by. Date: ~nature ITlme: Prin1~mo: R~lnqutshed by: Dale: SIQnalure Time: PrinlNamo: Relinquished by: Date: S1nM11 re rime: PrinlName: - I Time Sampled 800 1125 Received by: Sic nature PmlNa,ne: Received by: S_l_!j_nature Print Name: "ecelved by: Signature PrintName: ~ Kecelvedby: 'l Signature CHAIN OF CUSTODY All analysis will be conducted using NELAP accredited melhods and all data win be reported using AWAL's slafldard analyte 11515 and reporting limits (PQL) unless specifically requested otherwise on this Chain of Custody and/or attached documentation. 2\01'7°' \ AWAL Lab Sample Set# Page 2 of 3 QC Level: I Tum Around Time: Unlessotherarrangemenlshavebeenmade, 'Due Date; I l 3 Standard --~oo-"~~~"" ');-i?;, '2-i the day they are due, X Include EDD: Laboratory Use Only 0 LOCUS UPLOAD ~ al \).._<c, u EXCEL !Samples Were: bii :i:: bii IX Field Filtered For: 1 ~ddelivered ...._ ~ Dissolved Metals .... i::· l,j ~ :i Amblcolo~ 'II-2 C'l if of ~ z For Compliance With: Temperature 2 · 9 c:i ., ~-0 NElAP 3 'C C) f;t. D RCRA o' C'l I ;{ ;::,.· D CWA 4 Received Broken/Leaking c:i ~ ~~i o\.i:i C) c:i C) ::i 0 SDWA (!:!Jopeny Sealed) ...._ (YJ C) 0 D ELAP/A2lA N .... ... iii' i::· c:i ~ u D NLLAP 0 C) rn ~ It) C) C'l .!l ,.; D Non-Compliance 5~~ (YJ C) (YJ "' u i::· [;i ... It) ~ ... D Other: ked al benth N 0 ::t. "' ,,:j t D' ~ ('2_ D D' ,e :s C) "' C) " >< C) ,t C) or u IO V N C: ~ C? C) 0 'II-iii .., .,-.,-ii C'l ]j 0 It) Cl.I It) "' ~ rn "' ~ Known Hazards 6 Received Wilton C: ::; :z. ::t. ~ .:: .; 0 " ..... rs ..... 0 "' :i IQ .. ~fWJThnCS (.) 0. N !a II) ,e ,. ,( t) & N E 0 ~ .!I s= 0 0 "' ii or ,g Sample Comments ,,. "' :z. ;.!: t) Q > 7 w X X X X X X X X X X 3 w X ICOC Tape Was: e:::::rt on outer Package Y N NA ~f/Sl on O\Jtcr Package N NA J Presentonsample @ V N NA 4 Unbroken on Sample @ Y N NA Discrepancies Between Sample y N Labels and CDC RV !l)ate: Special Instructions: nme: Sample containers for metals were field filtered. See the Date: Analytical Scope of Work for Reporting Limits and VOC analyte ;Time: list. Date: [Tlme: \ n .M' 1..C\" rs.>r.,IJ,---Oa1tl .'7LJ I '"21 IPrfnl Name: ~:"\ok\L½e rc:'.::>'fuiJAA... pmo: I l\~ ~ ~ American West Analytical Laboratories 463 W. 3600 S. Salt Lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Address: Blanding, UT 84511 Contact: Tanneer Holliday f435) 678-2221 Phone#: Cell#: ___________ I Email: tholliday@energyfuels.com; kweinel@energyfuels.com; Project Name: 3rd Quarter Ground Water 2021 Project#: PO#: Sampler Name: Tanner Holliday Sample ID: Date Sampled Time Sampled CHAIN OF CUSTODY 2.lt)7·, '41 All analysis will I><! conducted using NELAP accredlled methods and all data will be reported using AWAL's standard enalyle lists and reporting limits (PQL) unless specifically requested otherwise on this Chain of Custody and/or attached documentation, AWAL Lab Sample Set# Page 3 of 3 .i s ~ ~ 8 -[ o E "" 8l QC Level: 3 ~ ~ !2. C') g ...... N g co ci 0 "' ...... t--ci 0 ti. 31 i i .., .e 0 .. i5 C, c:i 0 "J ... 0 ~ :t. u G' Cl "Si £!. Ill ~ co 0 0 "' ...... t--0 0 ti. I ~ .., ~ ! Turn Around Time: co" c:i Cl "' ~ c:i C, £!. a i J .., .e j fl Standard co" g "' ~ c:i Cl £!. a j r,i .., u .E: 0 ., m i5 o' c:i Cl "' ... 0 t) ~ Cl ~ 'I-~ u ... .: i o' c:i Cl "' .. 0 8 1/) :t. i g J ci ~ ~ s 0 ~ i5 §' • IO ~~ ,l! Ill Unless other arrangements have b<!en made, 11D uc Date: I 1· signed reports will be emalled by 5:00 pm on CY'" i ":2.. _,, the day they are due. D t -.J I!!:.- X Include EDD: LOCUS UPLOAD EXCEL X Field Filtered For: Dissolved Metals For Compliance With: □ NELAP □ RCRA □ CWA □ SDWA □ ELAP/A2LA □ NLLAP □ Non-Compliance □ Other: La.boratory Use Only Samples Were: l.J..._ ~s c9 hand dalivecod l Amblon~ 3 TamJ)<J<llturo tl "C 4 Received Broken/leaking • \, (!Sperty Sealed) N 3 \J\ 0, 9 y N 2 '!L-------------;1 0 .. -0 ~ P,...arvod ed olbonch y N ..: -u -3 .. al u ll g e! Known Hazards & Sample Comments 6 Rec<iived Within ~lngTlmes l.1/ N 1 IMW-32_072,82021 7/28/2021 1515 1 IW X 4 5 6 1 ~ on Outer Package V N NA 2 ~on on Outer Package C'./ N NA 3 Present on Sample y N (!;) 4 Unbroken on Sample r\ V N ~ :1 I I I I I I I I I I I I I I I 1r:~~:~~·=r5 Ro11nqutstte,n,y: ~ 1 /_ //,:./ ls~m1ture ........_ ],1AM£.,,,-,'Ll. ,Oat~ V Timo, (Received by. 7/29/20211slgnal\Jre )Oate: ITimo: Special Instructions: Pllnl Nome: Tanner Holliday . 1100 PrtntName:. I . •1sample containers for metals were field filtered. See the Rollnqulshocl t,y: Data. Received by. !Date. I Analytical Scope of Work for Reporting Limits and VOC analyte Slgnatun, S!gnature I . ~ ~ .~ P_rt11_1Namo: ~od by. ls!Qrulture PrinlNnmo= IRalinqulshed by. Sig.nature Frint Nam,,: !Date: rfi"me: Date: iTime: IPrfnlName: :Received by: S_!gnature P_rtl]_I__Name: ,-.. R.ecoivedby:\,.lfl ,':" , I ,.._ ~ L ' IS_'ll!'_al\Jre ~~ ~"-lf"'" Jc,,,< ~ 'PnnlName: ~~ ~rt.A..UJ\ Date: !Time: Oate:7 l3ol-z1 ITime: 11 f :c§Z:) Analysis Ammonia COD Cyanide Metals NOv'NO3 O&G Phenols Sulfide TKN TPO4 CrVI+ Procedure: Frequency: Preservatioo_Chec_kS_heet s l_e Set Ext, Preservative ~oo\ -odl.--003 --oo'-\ -txJS oH<2H2SO4 \/t'_L.. \I-el:.. -ve~ \J />.?:.. l\1ec; pH<2H2SO4 (, I I I oH>I0NaOH pH<2HNO3 1\/eh \tee.. '\.'~ \, .e_G, i\.i,i?£... oH <2li2SO4 i-tf.f>h i (/t.f:., ,11es ·ll.fh ·Ve,t., oH<2HCL , ,. j j I pH <2 H2SO4 pH >9 NaOH. ZnAC oH<2 H2SO4 pH<2H2SO4 pH >9 <NRi )2SO4 Pour a small amount of sample in the sample lid Pour sample from lid gently over wjde range pH paper Do Not dip the pH paper in the sample bottle or lid ~D~ ve.e; I ..../PC:.. \_'if'.h I duH -~001 -00'6 ~e-c; vec., I I \.Jt'C.... ,Jee, 'r-Jes re.e:; I , I-~ -010 ~ ,,e~ It-I ,lf'_C.. '\le~ ve~ Vee.. f I 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + .. # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH > __ due to the sample matrix interference. ~D\l \le<- ' l\.lc'.4 ..:Jee.. I Lab Set ID: pH Lot#: --o,z -Ot~ ·ve..c.. Vt'C.. I f lvec:.. ves (/~ lie<; I I '2 l 077C\\ (£]_01) rev 10-28-2020 M@• I Laboratories LLc a member of The GEL Group INC PO Box :!0712 Char1eS1on. SC 29417 2040 Savage Road Char1eS1on. SC 29407 P 843 556.8171 F 843.766.1178 August 27, 2021 Ms. Kathy Weinel Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado 80228 Re: White Mesa Mill G W Work Order: 551444 Dear Ms. Weinel: GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on August 02, 2021. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies ofGEL's accreditations and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 4289. Purchase Order: DW16138 Enclosures Sincerely, Julie Robinson Project Manager llll Ul~l 1111 II I II 11111 HJ II gel.com August 27, 2021 Laboratory Identification: GEL Laboratories LLC 2040 Savage Road Charleston, South Carolina 29407 (843) 556-8171 Summary: Receipt Narrative for Energy Fuels Resources (USA), Inc. SDG: 551444 ample receipt: The samples arrived at GEL Laboratories LLC, Charleston, South Carolina on August 02, 2021 for analysis. The samples were delivered with proper chain of custody documentation and signatures. All sample containers arrived without any visible signs of tampering or breakage. There are no additional comments concerning sample receipt. Sample ldentilication: The laboratory received the following samples: Laboratory ID Client ID 551444001 MW-11 07272021 551444002 MW-14 07272021 551444003 MW-31 07272021 551444004 MW-36 07272021 551444005 MW-65 07272021 551444006 MW-25 07282021 551444007 MW-26 07282021 551444008 MW-39 07282021 551444009 MW-40 07282021 551444010 MW-24 07292021 551444011 MW-24A 07292021 551444012 MW-30_07292021 551444013 MW-38_07292021 Case Narrati e: Sample analyses were conducted using methodology as outlined in GEL's Standard Operating Procedures. Any technical or administrative problems during analysis, data review, and reduction are contained in the analytical case narratives in the enclosed data package. Page 3 of 27 SDG: 551444 The enclosed data package contains the following sections: Case Narrative, Chain of Custody, Cooler Receipt Checklist, Data Package Qualifier Definitions and data from the following fractions: Radiochemistry. Page 4 of27 SDG: 551444 Julie Robinson Project Manager r,,8£ I Sheet 1 of 1 ( -r, ~ '1 'S'S l Y. Y l--\ -~ r __ , ENERGY FUELS RESOURCES CHAIN OF CUSTODY Sc mples Shipped to: GEL Laboratories, LLC Contact: Tanner Hollidat 2040 Savage Road Ph: 435 678 2221 Charleston, SC 29407 thol liday@.energyfuels.com (843) 556 8171 Chain of Custody/Sampling Analysis Request Project Samplers Name Samplers Signature C 3 Ground Water 2021 Tanner Holliday L 1nA-1ATr ,d/A// l/ Time Sample ID Date Collected Collected Laboratory Analysis Requested MW-11 07272021 7/27/2021 1125 Gross Alpha MW-14 07272021 7/27/2021 1450 Gross Alpha MW-31 07272021 7/27/2021 1255 Gross Alpha MW-36 07272021 7/27/2021 1425 Gross Alpha MW-65 07272021 7/27/2021 1450 Gross Alpha MW-25 07282021 7/28/2021 1000 Gross Alpha i MW-26 07282021 7/28/2021 1300 Gross Alpha I MW-39 07282021 7/28/2021 1450 Gross Alpha MW-40 07282021 7/28/2021 1040 Gross Aloha I MW-24 07292021 7/29/2021 710 Gross Aloha MW-24A 07292021 7/29/2021 700 Gross Alpha I MW-30 07292021 7/29/2021 950 Gross Aloha MW-38 07292021 7/29/2021 800 Gross Alpha Gi•>mments: Please send report to Kathy Weinel at kweinel!@energyfuels.com Ret:=dtr~jgnpure) ~ Tanner Holliday Rernquished By:(Signature) Page 5 of 7 SDG: 551444 Date/Time Received By:(Signature) 7/29/2021 1100 Date/Time I ~] I La!J~ratories LLC ....--.. SAMPLE RECEIPT & REV$W ;FORM SOG/ARICOC/Wo,·k Octfor: , 5 7> \ <-{ 4 LI Re,: ivcd ;y:TYE Date Received: c.-r:.. [2-\ 'c::;;).-1 1!!:::.:~c.!:l.:..___;__:_ _______ J-=:.==;.;_-_\ , . .:~U..,blc: FedEit ~ltpccss FedEx Oro ... ~ Field Services Courier ••••a•• Othe~ Carrier and Tracking Number Sw cctcd Haw rd Information ~ z •y.Nct Counts> IOOcpm on samples not mllrl:cd "radioactive", contact the Radiation Safety Gtoup for further investigation. A)S_hln""d 115 a DOT Huatdous7 \,i Honro Cl:1.SS Shipped; UN#; If UN29 IO, Is 01c Radioactive Shipment Survey Compliont1 Yes_ No_ , V COC notation or radio:u:tlvc stickers on cont:unccs equal clie,:ir designation. ~ B) bid the client designate the samples are to be rccclivcd 115 rodio:u:tive7 • C)_~id the RSO cl:issify the s~plcs ns radlo:u:tlvc7 V ~:>Xlmum Net Counts Observed• (Observed Counts -Arc• Background Counts); ~ !d.cPM I mMtr / a~~=~1wz~3 , D) id O,e client dcs11?11ates:imolcs 11ro h;izllldous? Iv er 11ot,tion or h:izard labels on cantainm equal client dcsigl)•tlon. I El Did lho RSO ldcntlfv nossiblc b:u:nros7 I, ~ 'If D or E. i.s yes, select H:izordi below. IV PCB's R:immablc Foccign Soil RCRA Asbestos Beryllium Other: Somple Receipt Criteria Commcnts/Qualilicr.f (Required for Non-Conforming Items) J Shipping cc.nlaincrs received intact and I\ . ~--~! • Cir.:la AppUe,blo: Su,ls broken O.un,god conuincr u:•ldnc conulncr O~,c, (dc.icn1>c) I scaled? I v !:!f.~ t--'-+---------------1--~,.<;i'•J"'J--+=-,---,,---------------------------------------1 i Chnin of custody C:ocumcnts included ·\ ~.~ Cltclo· Appltc,bltc: Cln:nt con1cc1cd •nd pro,;Jc~ COC . ;::_c created upon receipt r with shipment'! --·-----1 I~ V r I\ , I -·Mi~--~-.-~-.~ti-on_M_e_m_a_d·-.-W-c_t_l~--1-~-f--~-~--D-ry-k-~+.r.NoN-onn~1e_~,-o-~-.-r:--------'-•. -'--~l-(~.-n-.-0--- 31 Sa.mplr.s rcqt•iring ,,old prcscrvaticn V •nil tcmocr.iiures arc recorded in Celsius '-./. TEMP:~ '--- within (0 ~ r. dcl'. C)'i• • e-,13 f(/31J_) 11 ~::c;:t:~ ~~~rmcci and pas.ed on [R 1t/{~j J::~~:'.;;:-::·:.-~-, :-:c.-~-n-=-:v-:1~-:-::.-, ~-=:-=-~-cc~-=-o 1/-,-(l_f_ App~. li-_¢a_b_i_e)-,-. -,-.,....------------.-•• --.-. ------i, ll --1---~ -•. ~(:Jl~L..-------· ~ i I I ~,.-_ I""""'-" '""'""" "'~•'""""" '"'"''"""'" '""""'"''' " I ~ r. -l.'..amplr. contr.incrs intact ar,d scaled? , ·{: t....-•. ·· · · I i • • • • ,, 't . . . . , . , _ __j ,} ls~C'll!?ic:t •:~quirin~ ci•~r:u.cd prescrvatiou ' , • S«,,rlr II/, ,.nd 1;11nuinc11 A!Tcctcd, • ~ • . • : · · · ·--· -• ·-;s.. • -· I I ,at oJrtlpct J,H? I I 1 · · · · • · • ~ · · ' · · 1 • • • __ :!f~~•En-;illo,. >ddc~~~: • •· •· r • _ . , : I • I f I ~J 1«~,~-•-m ~·ncu:::_s "r5oi! K:rs prr;cnt [ovsalids? Yes · No-• 1-1-A· (lfye,, ,:,kc to·VO?'-o/)c>.""1 .. l : :·-_J + Co any samples require Volatile ~1 :::?o;fquid YOA viw, con1 . .u11 ru:id pn;,scrvation? Y cs No Nl\.._(lf unknown. rc)cct I'{(!). . . i' i Analysis? -~i[t . , l¼Tiquld VO/\ vi:ils ;,cc ofhe:lrlsp:1.~7 Yes_ No_: N"-.,__ • • . ,:; ; :; • · ' /r !I ~4 ..., S•mrlc IC.', •nd cor,uinors •IToctcd: • . · i; · . , . . ' · · I IJl'l'J I !O's and tests effected: .. Snmplc~ received within holding time7 V' ~'6, I : ... . .. Sample !C's on COC match ID's on ~ lO's one co11t~inar; nf-fccted: I bottles? Iv (~: .. 1 ·10 Date & time on COC match date & time ~I/ Citclc App!iC;1ble: Nodltcs on cont.liners No ti<1:1cs an containers COC missing info Othcr(i:lcscri~) f on bottles? v ,_ ~ l Number of containers recci vcd match . , , ~'' C/ircle A_pplicablc: ,_lr-r:n:-urn-:-bc_r_i0nd_i_ca_tc_d..,.o_n_c...,o,.,c_? :--:-,...,..--~ -;t'.• h Ale 5,llllple containers identifiable as '.1.i,_~,. v i GEL orovidcd bv use of GEL lnbels? ~ / '----:;:-7:'--.:;--:--;:---:-,:-:-:-=-:---:--:----:-:--:------------,---------l 11_3 COC form is properly signed in • ~ Circle Applic~blc: Nol relinquished Olhcr (describe) relinquished/received sections? .., c.:l] No cont.liner count on COC Other (describe) ColJl.[Ucnts (Uso Conti.nMation Forni if needed): PM (or PMA) review: Initials _ _.,(-i...::. ):['j...;,.,... ___ D~tc 'J.. / 7., / ;::i I Pagc~or_J_ Page 6 of ~7 SDG: 551444 GL-CHL•SR-001 Rev7 GEL Laboratories LLC -Login Review Report GEL Work Order/SDG: 551444 Client SDG: 551444 Q3 Ground Water 2021 Project Manager: Julie Robinson Project Name: Purchase Order: DNMI00100 White Mesa Mill GW DW16138 Package Level: LEVEL3 EDD Format: EIM_DNMI GELID Client Sample ID Client Sample Desc. 551444001 MW-11_07272021 551444002 MW-14_07272021 551444003 MW-31_07272021 551444004 MW-36_07272021 551444005 MW-65_07272021 551444006 MW-25_07282021 551444007 MW-26_07282021 551444008 MW-39_07282021 551444009 MW-40_07282021 551444010 MW-24_07292021 551444011 MW-24A_07292021 551444012 MW-30_07292021 551444013 MW-38_07292021 Client Sample ID Status Tests/Methods -001 MW-11_07272021 REVW GFPC, Total Alpha Radium, Liquid -002 MW-14_07272021 REVW GFPC, Total Alpha Radium, Liquid -003 MW-31_07272021 REVW GFPC, Total Alpha Radium, Liquid -004 MW-36_07272021 REVW GFPC, Total Alpha Radium, Liquid -005 MW-65_07272021 REVW GFPC, Total Alpha Radium, Liquid -006 MW-25_07282021 REVW GFPC, Total Alpha Radium, Liquid -007 MW-26_07282021 REVW GFPC, Total Alpha Radium, Liquid -008 MW-39_07282021 REVW GFPC, Total Alpha Radium, Liquid -009 MW-40_07282021 REVW GFPC, Total Alpha Radium, Liquid -010 MW-24_07292021 REVW GFPC, Total Alpha Radium, Liquid -011 MW-24A_07292021 REVW GFPC, Total Alpha Radium, Liquid Collect Date& Time 27-JUL-21 11 :25 27-JUL-21 14:50 27-JUL-21 12:55 27-JUL-21 14:25 27-JUL-21 14:50 28-JUL-21 10:00 28-JUL-21 13:00 28-JUL-21 14:50 28-JUL-21 10:40 29-JUL-21 07:10 29-JUL -21 07:00 29-JUL-21 09:50 29-JUL-21 08:00 Product Reference Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Gross Alpha Work Order Due Date: 30-AUG-21 Package Due Date: 28-AUG-21 EDD Due Date: 30-AUG-21 Due Date: 30-AUG-21 NG1 Receive Time #of Lab Date& Time Zone Cont. Matrix 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER 02-AUG-21 09:00 -2 1 GROUND WATER Fax Date PM Comments Report Date: 27-AUG-21 Work Order: 551444 Page 1 of 2 Collector: C Prelogin #: 20190487484 Project Workdef ID: 1294356 SDG Status: Closed Logged by: Fax Days to Prelog Lab Field Due Date Process Cote# 20 20 20 20 20 20 20 20 20 20 20 20 20 Aux Data Group QC QC Receive Codes s::f" s::f" -.:t" ..... V) V) Cl Cl VJ r---N 4-< 0 r--- (l,) ~ A,.. GEL Laboratories LLC -Login Review Report -012 MW-30_07292021 -013 MW-38_07292021 REVW GFPC, Total Alpha Radium, Liquid REVW GFPC, Total Alpha Radium, Liquid Product: GFCTORAL Workdef ID: 1458614 Method: EPA 903.0 Product Description: GFPC, Total Alpha Radium, Liquid Gross Alpha Gross Alpha In Product Group? No Samples: 001 , 002, 003, 004, 005, 006, 007, 008, 009, 010, 011, 012, 013 Parmname Check: All parmnames scheduled properly CAS# Contingent Tests Parmname Gross Radium Alpha Action Product Name Login Requirements: Requirement Description Group Name: Group Reference: Report Date: 27-AUG-21 Work Order: 551444 Page 2 of 2 Path: Drinking Water (903.0 or 9315) Product Reference: Gross Alpha Moisture Correction: "As Received" Client RDL or PQL & Unit Reporting Parm Included Included Custom Units Function in Sample? in QC? List? pCi/L REG y y No Samples Include? Comments Peer Review by: ___________ _ Work Order (SDG#), PO# Checked? ____ _ C of C signed in receiver location? _____ _ "1" "1" "1" ...... lr) lr) d Cl rf)_ r:--N (+-, 0 00 (I) 01) ro p.. Radiochemistry Technical Case Narrative Energy Fuels Resources SDG #: 551444 Product: GFPC, Total Alpha Radium, Liquid Analytical Method: EPA 903.0 Analytical Procedure: GL-RAD-A-044 REV# 10 Analytical Batch: 2157704 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# 551444001 551444002 551444003 551444004 551444005 551444006 551444007 551444008 551444009 551444010 551444011 551444012 551444013 1204877840 1204877841 1204877842 1204877843 1204877844 Client Sample Identification MW-11 07272021 MW-14_07272021 MW-31 07272021 MW-36 07272021 MW-65 07272021 MW-25 07282021 MW-26 07282021 MW-39 07282021 MW-40 07282021 MW-24 07292021 MW-24A 07292021 MW-30 07292021 MW-38 07292021 Method Blank (MB) 551444002(MW-14_07272021) Sample Duplicate (DUP) 551444002(MW-14_07272021) Matrix Spike (MS) 55 l 444002(MW-l 4 _ 07272021) Matrix Spike Duplicate (MSD) Laboratory Control Sample (LCS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Preparation Information Aliquot Reduced 1204877841 (MW-14_07272021DUP), 1204877842 (MW-14_07272021MS), 1204877843 (MW-14_07272021MSD) and 551444002 (MW-14_07272021) Aliquots were reduced due to limited sample volume. Technical In formation Recounts Sample 1204877843 (MW-14_0727202 IMSD) was recounted due to low recovery. The recount is reported. Miscellaneous Information Page 10 of27 SDG: 551444 Additional Comments The matrix spike and matrix spike duplicate, 1204877842 (MW-14_07272021MS) and 1204877843 (MW-14_07272021MSD), aliquots were reduced to conserve sample volume. Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 11 of27 SDG: 551444 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 -(843) 556-8171 -www.gel.com Qualifier Definition Report for DNMIO0l Energy Fuels Resources (USA), Inc. Client SDG: 551444 GEL Work Order: 551444 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the CRDL. ReviewNalidation GEL requires all analytical data to be verified by a qualified data reviewer. In addition, all CLP-like deliverables receive a third level review of the fractional data package. The following data validator verified the information presented in this data report: Signature: j~ ~ Name: Theresa Austin Date: 27 AUG 2021 Title: Group Leader Page 12 of27 SDG: 551444 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summarr Energy Fuels Resources (USA), Inc. 225 Union Boulevard Suite 600 Lakewood, Colorado Contact: Ms. Kathy Weinel Workorder: 551444 ----Parm ~ NOM Rad Gas Flow 3atch 2157704 QCl204877841 551444002 DUP Gross Radium Alpha u 0.941 u Uncertainty +l-0.386 QCl204877844 LCS Gross Radium Alpha 566 Uncertainty QC1204877840 MB Gross Radium Alpha u Uncertainty QC1204877842 551444002 MS Gross Radium Alpha 4470 u 0.941 Uncertainty +l-0.386 QC1204877843 551444002 MSD Gross Radium Alpha 4450 u 0.941 Uncertainty +l-0.386 Notes: Counting Uncertainty is calculated at the 68% confidence level (I-sigma). The Qualifiers in this report are defined as follows: ** < > Analyte is a surrogate compound Result is less than value reported Result is greater than value reported The TIC is a suspected aldol-condensation product Units 0.321 pCi/L +l-0.247 513 pCi/L +l-5.54 -0.00284 pCilL +l-0.135 3390 pCi/L +l-38.6 3360 pCilL +l-36.7 RPO% NIA 0.901 A B BD C D F H K L M For General Chemistry and Organic analysis the target analyte was detected in the associated blank. Results are either below the MDC or tracer recovery is low Analyte has been confirmed by GC/MS analysis Results are reported from a diluted aliquot of the sample Estimated Value Analytical holding time was exceeded Analyte present. Reported value may be biased high. Actual value is expected to be lower. Analyte present. Reported value may be biased low. Actual value is expected to be higher. M if above MDC and less than LLD Page 26 of 27 SDG: 551444 Report Date: August 25, 2021 Page l of REC% Ran e Anlst Date Time ------- NIA JXC9 08/23/21 17 :2 90.8 (75%-125%) 08/23121 17:2 08123/21 16:4· 75.8 (75%-125%) 08123121 17:2 75.4 (0%-20%) 08124/21 15:2 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 -(843) 556-8171 -www.gel.com QC Summary Workorder: 551444 Parmname NOM __ Snmpl!.._Qu_ll_!_ C n its_--'RP'=-'D~0/,-'-o _ REC% _ Ran~e Anlst M Matrix Related Failure NIA RPD or %Recovery limits do not apply. NI ND NJ Q R u UI UJ UL X y h See case narrative Analyte concentration is not detected above the detection limit Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier One or more quality control criteria have not been met. Refer to the applicable narrative or DER. Sample results are rejected Analyte was analyzed for, but not detected above the CRDL. Gamma Spectroscopy--Uncertain identification Gamma Spectroscopy--Uncertain identification Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias. Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier QC Samples were not spiked with this compound RPD of sample and duplicate evaluated using +I-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. Preparation or preservation holding time was exceeded Page 2 of Date Time NIA indicates that spike recovery limits do not apply when sample concentration exceed spike cone. by a factor of 4 or more or %RPO not applicable. /\ The Relative Percent Difference (RPD) obtained from the sample duplicate (DU P) is e aluated against the ace ptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +I-the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been perfonned under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 27 of27 SDG: 551444 TabF Laboratory Analytical Reports -Accelerated Monitoring Tab Fl Laboratory Analytical Reports -Accelerated Monitoring August 2021 3440 South 700 West ~alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2108362-001 Client Sample ID: MW-11_08102021 Collection Date: 8/10/2021 111 Oh Received Date: 8/13/2021 93 8h Analytical Results Date Compound Units Prepared Chloride Sulfate mg/L mg/L Date Analyzed 8/18/2021 038h 8/18/2021 038h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qua) E300.0 10.0 57.0 E300.0 50.0 1,370 Report Date: 8/30/2021 Page 8 of 27 All anabses applicable lo lhe CWA. SDWA. and RCRA are perfom1ed in accordance to NELAC protocols_ Pertinent sampling infornuuion is localed on Lhe attached COC Confidential Business Information: This report is pro,·ided for the exclush·e use of the ~cldressee Pri,·ile~es o_f sub .. seq~1ent ~~e or the ~~e of this _co1~pany or ntl) ~mber or its staff, or reproductio~ ~f this repo~ in _con~1eclion .. " ith the a~Yertise1~e111, P~?molio,n ~r sale of~~~. ~rodL~cl or P~?Cess, ~r in '?°nn:_c~ion \\'!th th~ r~~publicu1ion of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2108362-002 Client Sample ID: MW-26_08102021 Collection Date: 8/10/2021 930h Received Date: 8/13/2021 938h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 8/18/2021 102h 8/16/2021 904h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qual E300.0 5.00 61.4 E353.2 0.100 1.42 ------ Report Date: 8/30/2021 Page 9 of27 All an.ii) ses applicable to the CWA. SDW A. and RCRA me perfom1ed in accordance to NELAC protocols Per1inen1 sampling informetion is locoted on the ouached COC Conlidentiol Business lnronnolion: This repon is pro,·ided for the exclush e use of the ~ddressee Pri, ile~es o_f sub__seq~ent ~~e of the ~~e of this ,con;ipany or M) ~mber of its slnlT, or reproduclio~ ~f this repo~ in ~on?eclion ... \\ith the u~ver1isemen1. P~?mo1io;n ~r sale of !1'!~ ~rodl~ct or p1.ocess. ~' in ~onn~c!ion \\'!th 1h~ r~-p~blico1ion of 1his 1epon ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: August Ground Water 2021 Lab Sample ID: 2108362-002C Client Sample ID: MW-26_08102021 ANA1 vr1cAL LAeoRAToR1Fs Collection Date: 8/10/2021 930h Received Date: Analytical Results 8/13/2021 938h Test Code: 8260D-W-DENl00 VOAs by GC/MS Method 8260D/5030C 3440 South 700 West falt Lake City, UT 84119 Analyzed: 8/16/2021 940h Units: µg/L Compound Chloroform Phone: (80 I) 263-8686 Surrogate Units: µg/L Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com ------- Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: 10 Method: CAS Reporting Number Limit 67-66-3 10.0 CAS Result Amount Spiked %REC 17060-07-0 481 500.0 96.1 460-00-4 542 500.0 108 1868-53-7 491 500.0 98.2 2037-26-5 522 500.0 104 --The reporting limits were raised due to high analyte concentrations. web: www.awal-labs.com Jennifer Osborn Laboratory Director Analyzed: 8/16/2021 821h Units: µg/L Compound Carbon tetrachloride Jose Rocha Methylene chloride QA Officer Surrogate Units: µg/L Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: 1 Method: CAS Reporting Number Limit 56-23-5 1.00 75-09-2 1.00 CAS Result Amount Spiked %REC 17060-07-0 48.3 50.00 96.5 460-00-4 55.0 50.00 110 1868-53-7 49.2 50.00 98.3 2037-26-5 52.5 50.00 105 SW8260D Analytical Result Qual 996 Limits Qual --- 80-136 85-121 78-132 81-123 SW8260D Analytical Result Qual < 1.00 1.25 Limits Qua] 80-136 85-121 78-132 81-123 Report Date: 8/30/2021 Page 13 of27 All nnnl~ ses opplicnble to the (WA. SOWA. Rnd RCRA 01e perfom1ed in accordMce to NELAC protocols Pertinent sampling information is locnted on the euached COC Confidentiol Business lnformotion: This report is pro\'ided for the exclusi\ e use of lhe ~ddressce r,i, ile~es o_f su~seq~1en1 ~•~e of the ~~e of this .co1~pan~ or nny '~'!1bei of ils stnfr, or reproductio~ ~f this repo~ in ~on~1ec1ion .. ,,ith 1he a~,·er1isement, P~?mo1i~n ~r ~ale of?'!~_ ~rodL'.ct or p1:?Cess, ~r in ~onn:c!ion \\'!lh th? r~-publicolion of 1his 1t,port American West ANALYTICAL LABORATORIES 3440 South 700 West falt Lake City, UT 841 19 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2108362-003 Client Sample ID: MW-30_08092021 Collection Date: 8/9/2021 1115h Received Date: 8/13/2021 938h Analytical Results Compound Selenium Uranium Units mg/L rng/L Date Prepared 8/16/2021 856h 8/16/2021 856h Date Analyzed 8/26/2021 708h 8/26/2021 708h Contact: Tanner Holliday DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.00500 0.0561 E200.8 0.000500 0.00938 Report Date: 8/30/2021 Page 5 of27 All anal) ses applicable lo the CWA. SDWA. and RCRA are perfom1ed in m:cordance lo NELAC protocols Pertinent sampling information is loc.11ed on the allached COC Confidential Business Information: This report is pro\·ided for the exclusi\ e use of lhe ~dressee Privile~es o_f sub_seq!1ent !'~ or the ~~e of this _co1~p.1ny or an~ ~mber of its staff. or reproduc1io~ ~(this repo~ in ~•~ecl1on .. with the u~vertisemenl, P~?moli~n or !ale of?'!) ~rodL~ct or p,.ocess, ~r in i;onn~c~ion w!th th~ r~-publicalion of lhis report American West ANAi VTICAI LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax:(801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2 !08362-003 Client Sample ID: MW-30_08092021 Collection Date: 8/9/2021 1115h Received Date: 8/13/2021 938h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 8/18/2021 12 Sh 8/16/2021 914h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qual E300.0 5.00 161 E353.2 0.200 16.5 Report Date: 8/30/2021 Page 10 of27 All analyses applicable 10 lhe CWA. SOWA. and RCRA ;ire perf'om1ecl in accordance to NELAC protocols Pertinent sampling ii1rormn1ion is locoted on lhe nunched COC Conliden1inl Business Information: This repon is p10, ided for lhe exclusi, e use of1he ~ddressee_ P1i, ile~es of sub .. seq~1ent ~1~e or the ~~e of this ,co1~pa11y or rm~ ~7mbel' of its slnlT, or reproduclio~ ~f lhis repo~ in ~on~1ection~ with the o~,·ertisement. p~omoti0!101 sRle or~!~ ~todl!ct or p1,?cess, ~r in ~onn:_c~ion w!th th~ r~-publication of lhis report American West ANALYTICAL I ABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: August Ground Water 2021 Lab Sample ID: 2108362-004 Client Sample ID: MW-3 l _ 08092021 Collection Date: 8/9/2021 1340h Received Date: 8/13/2021 938h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Uranium mg/L 8/16/2021 856h 8/26/2021 712h E200.8 0.000500 0.0193 ------ Report Date: 8/30/2021 Page 6 of27 All anab ses applicable to lhe CWA. SOWA. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is localed on the attached COC Conlidenli:il Business Information: This reporl is provided for theexclusi\'e use of the ~ddressee Pri, ile~es of'sub .. seq~enl ~;e of the ~~e of this _crn~pany or an) ~~ber ofils slaIT. or reproduclio~ ~f lhis repo~ in .con~ection .. with lhe a~\'ertisemenl, P~?motio.n ~r sale of ~!Y ~rOdllCl or p~ocess, ~r in ~1111!.c~ion w~lh th~ n:-publicalion of lhis 1eport INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2108362-004 Client Sample ID: MW-31_08092021 ANALvr,cAL I AD0RAT0R1es Collection Date: 8/9/2021 1340h 3440 South 700 West ;aft Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Received Date: 8/13/2021 938h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Sulfate mg/L Total Dissolved Solids mg/L Date Analyzed 8/18/2021 149h 8/l 6/2021 9 I 2h 8/18/2021 149h 8/13/2021 1250h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qual E300.0 10.0 365 E353.2 0.100 15.7 E300.0 50.0 1,130 SM2540C 20.0 2,600 ----- Report Date: 8/30/2021 Page 11 of27 All anal)ses appliczible lo the CWA. SOWA. and RCRA ore perfom1ed in accordance lo NELAC prolocols Pertinenl sampling information is located on the ntlnched ('OC Confidential Business Information: This 1epon is p10Yided for lhe exdusin use of 1he ~ddressee P1i, ile~es o_f sub .. seq~ent ~•~e of the ~~le or1his _co1~pany or nny 1~~~be1 of ils slnff. or reproductio~ ~f !his repo~ in ~on~1eclion .. with the a~,·erlisement. P~?moti~ ~r ~aJe of~!~ ~1od~cl or p~ocess, ~r in ~m1~c~io11 w!lh 1h~ r1;-publicalio11 of 1his report 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: August Ground Water 2021 Lab Sample ID: 2108362-005 Client Sample ID: MW-65_08092021 Collection Date: 8/9/2021 1115h Received Date: 8/13/2021 93 8h Analytical Results Compound Selenium Uranium Units mg/L mg/L Date Prepared 8/16/2021 856h 8/16/2021 856h Date Analyzed 8/26/202 I 730h 8/26/2021 730h Contact: Tanner Holliday DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.00500 0.0572 E200.8 0.000500 0.00948 Report Date: 8/30/2021 Page 7 of27 All anal~ ses applicable to lhe CWA. SDWA. and RCRA are perfonned in accordance to NELAC prolocols Pertinenl sampling information is localed on Lhe attached COC Confidential Business Information: This report is provided for the exclusi, e use of the ~ddressee Pri, ile~es o.r sub,,seq~enl ~~e or the ~?1,Jl.e of lhis .crn~pany or an~ •~mbe1 of its staff, or reproductio~ ~r this repo~ in ~o~eclion,, with lhe u~, ertisemenl, P~?motio_n ~r sale of~!~. rrod~cl or p1,ocess, ~r in ~onn!c~ion w!lh th! r~-publication of I his report INORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. August Ground Water 2021 2108362-005 Client Sample ID: MW-65 08092021 ANAt vr1cAL LAaoAAroR1Es Collection Date: 8/9/2021 1115h 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Received Date: 8/13/2021 93 8h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Contact: Tanner Holliday Date Method Reporting Analytical Analyzed Used Limit Result Qual 8/1 8/2021 300h E300.0 5.00 181 8/16/2021 916h E353.2 0.200 18.6 Report Date: 8/30/2021 Page 12 of27 All ano\~ses llf)plic::nble lo the CWA. SOWA. and RCRA 01e perlbm1ed in accordance to NELAC protocols Pertinent sampling informnlion is locnted on lhe allnched COC. C'onfidtmtial Business lnformo.lion: This report is pro"ided for the e.\ch1si, e use of the ~ddressee Pli, i le~es o,r su~seq~1cmt ~1~e or lhe ~~~e or this ,c01~1pany or nny 1~1!1ber of ils stnff, or reproduclio~ ~~ this repo~ in ~on~1ection ... with the o~,·ertisement. p~~motio.n or sa1e of~!~. ~roch~ct or p1:ocess, ~r in ~onn~c~ion w~lh th~ r:_-publica.1io11 or I his report ANALYTICAi. LARORATORIE6 3440 South 700 West ;aft Lake City, UT 84119 Phone: (801)263-8686 foll Free: (888) 263-8686 Fax: (80 I) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. August Ground Water 2021 2108362-006A Client Sample ID: Trip Blank Collection Date: 8/10/2021 Received Date: 8/13/2021 Analytical Results Analyzed: 8/16/2021 841h Units: µg/L Compound Carbon tetrachloride Chloroform Methylene chloride 930h 938h Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENlO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 75-09-2 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-dB 17060-07-0 460-00-4 1868-53-7 2037-26-5 48.3 54.3 48.3 52.1 50.00 96.6 80-136 50.00 109 85-121 50.00 96.6 78-132 50.00 104 81-123 Report Date: 8/30/2021 Page 14 of27 All onalyses opplicoble lo the CWA. SDWA. Md RCRA are perfom~d in ru::cordance to NE LAC protocols Pertinent sumpling informatio1\ is located on the nltnched COC C'onlict~nliol Business lnfonnalion: This report is pro\ ided for the exclush e use of the ~ddressee P,i, ile~es o,f su~seq~1ent ~,~e of lhe !~~e of this .co1~pany or any 1~'!1be1 of its stnrr, or reproduclio~! ~f this repo~ in fOn~eclion .. with 1he ;;i~'.. ertisemenl P~?moli~n or sale Clf ?1!~ r•odl)Ct or p~ocess, ~r in ~nn~c!ion w!th 1h~ r~•publication of this r~pon ANALYTICAL LABORATORIES 3440 South 700 West )alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: ( 435) 678-2221 RE: August Ground Water 2021 Dear Tanner Holliday: Lab Set ID: 2108362 American West Analytical Laboratories received sample( s) on 8/13/2021 for the analyses presented in the following report. American West Analytical Laboratories (A WAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Approved by: J G Digitally signed 059 . by Jose G. Rocha Rocha Date: 2021.08.30 15:03: 15 -06100' Laboratory Director or designee Report Date: 8/30/2021 Page I of27 All anal)ses applicable to the C'WA. SOWA. and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling informal ion is located on the nllached COC Confidential Business Information: This re~on is provided ror the exclusi\'e use of the ~ddressee, Pri, ile~es o.f sub~seq~1enl ~~e or the ~~1e of Ibis .con:ipan~· or an) ~mbe1 of ils slaff, or reproductio~ ~f lhis repo~ in ~on~eclion ... wilh the a~vertiseme11l. promotio_n or sa1e of~!~ ~rod~cl or p1,ocesi:, ?r in ~onn:_c~ion ,,·!th th~ r~-publication or !his reporl SAMPLE SUMMARY Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: August Ground Water 2021 Lab Set ID: 2108362 Date Received: 8/13/2021 938h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 2108362-00 IA MW-I I 08102021 8/10/2021 1110h Aqueous Anions, E300.0 ~alt Lake City, UT 841 I 9 21083 62-002A MW-26 08102021 8/10/2021 930h Aqueous Anions, E300.0 2108362-002B MW-26 08102021 8/10/2021 930h Aqueous Nitrite/Nitrate (as N), E353.2 2108362-002C MW-26 08102021 8/10/2021 930h Aqueous VOA by GC/MS Method Phone: (80 I) 263-8686 8260D/5030C 2108362-003A MW-30 08092021 8/9/2021 1115h Aqueous Anions, E300.0 Toll Free: (888) 263-8686 2108362-003B MW-30 08092021 8/9/2021 1115h Aqueous Nitrite/Nitrate (as N), E353.2 Fax: (801) 263-8687 2108362-003C MW-30 08092021 8/9/2021 1115h Aqueous ICPMS Metals, Dissolved !-mail: awal@awal-labs.com 2108362-004A MW-31 08092021 8/9/202 I 1340h Aqueous Anions, E300.0 2108362-004B MW-31 08092021 8/9/2021 1340h Aqueous Nitrite/Nitrate (as N), E353.2 web: www.awal-labs.com 2108362-004C MW-31 08092021 8/9/2021 1340h Aqueous ICPMS Metals, Dissolved 2108362-004D MW-31 08092021 8/9/2021 1340h Aqueous Total Dissolved Solids, A2540C 2108362-00SA MW-65 08092021 8/9/2021 1115h Aqueous Anions, E300.0 Jennifer Osborn 2108362-00SB MW-65 08092021 8/9/2021 1115h Aqueous Nitrite/Nitrate (as N), E353.2 Laboratory Director 2108362-00SC MW-65 08092021 8/9/2021 1115h Aqueous ICPMS Metals, Dissolved 2108362-006A Trip Blank 8/10/2021 930h Aqueous VOA by GC/MS Method Jose Rocha 8260D/5030C QA Officer Report Date: 8/30/202 I Page 2 of27 All analyses applicable to the CWA. SDW A. and RCRA are performed in accordance to NELAC prolocols Pcrtinenl sampling information is localed on Lhe altached COC Confidential Business Information: This repon is prm·ided for the exclusive use of the ~ddressee P1i\ ile~es o_f su~seq~ent ~~e of the ~~e of this.cmi:ipany or anr ~mbe, of its slaff, or reproduclio~ ~fthis repo~ in ~011~1ec1ion,. ,vith the a~vertisement, P~?motio_n or sale of~!~ rrodl~Cl or p1:oces1:, ~r in ~onn:_c!ion w!1h th~ r~-publication of lhis repon 3440 South 700 West ;alt Lake City, UT 84 I 19 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: August Ground Water 2021 2108362 8/13/2021 8/9-8/10/2021 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 8/30/2021 Page 3 of27 All anal~ ses applicable to the CWA. SDW A. and RCRA are perfom1ed in accordance to NELAC prolocols Pertinent sampling information is localed otl the allached COC Confidential Business Jnfonnalion: This repon is prO\ ided for lhe exclusi,e use of lhe ~ddressee Pri,·ile~es o_f sub~seq~1enl ~~e of lhe ~?1:'1e of this ,co1~pany or atl) 1~mbe1 of ils staff, or reproduclio~ ~f this repo~ in ~011~1ection~ \\ilh the a~, ertisemenl, 1->~?motio~ or sale of?'!~ ~rod~cl or p1,ocess, ~r in 7onn:_c~io11 w!th th~ n~-publica1io11 of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 !-mail: awa1@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: August Ground Water 2021 2108362 8/13/2021 8/9-8/10/2021 Intact None SW-846 8260D/5030C Volatile Organic Compounds General Set Comments: Multiple target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: the MS and MSD percent recoveries for Chloroform were outside of the control limits due to sample matrix interference. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 8/30/2021 Page 4 of27 All anal~ses applicable to the CWA. SDWA. and RCRA are perfom1ed in accordance lo NELAC protocols Pertinenl sampling information is located on the allached COC Confidenlial Business Information: This report is prol'ided for the excll1~,~ U!(! of the ~ddressee Pril ile~es o,f su~seq~enl ~~e of lhe ~~e of lhis .coi~pony or M) •~mber of ils slaff, or reproductio~ ~f !his repo~ in ~on~1eclion .. \\ilh lhe a~;·ertise1'!1enl. P~?motio.n 01 ~aJe of ~!Y. ~roch)cl or P~?cess, ~r in ~nn~c~ion w!th th~ r~-publicahoo o(lhis report ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: LCS-78965 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.192 Uranium 0.190 3440 South 700 West Salt Lake City, UT 84119 Phone: (801 ) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-Iabs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/26/2021 704h 08/16/202 I 856h mg/L E200.8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 Tanner Holliday ME LCS Spike Ref. Amount %REC 0 96.2 0 95.0 Limits 85 -115 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/30/2021 Page 15 of27 analyses applicable to the CW A. SDWA, and RCRA are perfonned in accordance to N ELAC protocols Pertinent samphng mfonnation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement promotion or sale of any product or proce~ or in connection with the re-pubJication of this report for any purpose other than for the addressee wiJI be granted only on contact. This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: MB-78965 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium < 0.000500 Uranium < 0.000500 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT_ Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/26/2021 700h 08/16/2021 856h mg/L E200.8 0.000127 0.000500 mg/L E200.8 0.0000440 0.000500 Tanner Holliday ME MBLK Spike Ref. Amount ¾REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt ¾RPO Limit Qual Report Date: 8/30/2021 Page 16 of27 analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sarnphng infonnation is located on the attached COC. Confidential Business Information: This reJX>n is provided for the exclusive use of the addressee Privileges of subsequent use oftl· ne of this company or any member of its staff, or reproduction of this report in connection with the advertisemenL promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2 I 08362-004CMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.297 Uranium 0.220 3440 South 700 West Salt Lake City, UT 841 I 9 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/26/2021 723h 08/16/2021 856h mg/L E200,8 0.000127 0.000500 0.2000 mg/L E200.8 0.0000440 0.000500 0.2000 Tanner Holliday ME MS Spike Ref. Amount %REC 0.0934 102 0.0193 100 Limits 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 8/30/2021 Page 17 of 27 analyses applicable to the CW A. S DW A, and RC RA are performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its stafT, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-,publication of this report for any purpose other than for the addressee will be granted only on contact. This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Lab Sample ID: 2108362-004CMSD Test Code: Selenium Uranium 200.8-DIS Result Date Analyzed: Date Prepared: 0.302 0.220 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/26/2021 726h 08/16/2021 856h mg/L E200.8 0.000127 0.000500 0.2000 mg/L E200 8 0.0000440 0.000500 0.2000 Tanner Holliday ME MSD Spike Ref. Amount %REC 0.0934 104 0.0193 100 Limits 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit 0.297 1.40 20 0.22 0.0427 20 Qual Report Date: 8/30/2021 Page 18 of27 analyses app1 icable to the CW A. SOW A, and RCRA are perfonned in accordance to N ELAC protocols Pertinent samphng information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process~ or in connection ,Vlth the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2108362-004DDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 2,650 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fa'C: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday WC DUP Spike Ref. Amount %REC 08/13/2021 1250h mg/L SM2540C 16.0 20.0 Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer ·------ RPDRef. RPD Amt %RPO Limit Qual 2600 1.83 5 Report Date: 8/30/2021 Page 19 of27 analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: ll1is report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Method MDL Reporting Limit Contact: Dept: QC Type: Amount Spiked Tanner Holliday WC LCS Spike Ref. Amount %REC Lab Sample ID: LCS-Rl55612 Date Analyzed: 08/17/2021 2153h Test Code: Chloride Sulfate 300.0-W Lab Sample ID: LCS-Rl55493 Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) Lab Sample ID: LCS-Rl55501 Test Code: TDS-W-2540C Total Dissolved Solids 5.34 mg/L E300.0 5.09 mg/L E300 0 Date Analyzed: 08/16/2021 856h 1.01 mg/L E353.2 Date Analyzed: 08/13/2021 1250h 182 mg/L SM2540C 0.0198 0.100 0.0750 0.500 0.00541 0.0100 8.00 10.0 5.000 5.000 1.000 205.0 0 0 0 0 107 102 101 88.8 Limits 90-110 90 -110 90 -110 80 • 120 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt % RPD Limit Qual Report Date: 8/30/2021 Page 20 of 27 analyses applicable to the CWA. SOWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling infomiation is located on the attached COC Confidential Business lnfonnation: Tilis report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its statT, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: MB-R155612 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Sulfate < 0.500 Lab Sample ID: MB-SPLP Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Sulfate <0.500 Lab Sample ID: MB-R155493 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-RISSSOI Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC_SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/17/20212129h mg/L E300.0 0.0198 0.100 mg/L E300.0 0.0750 0.500 08/17 /202 I 2217h mg/L E300.0 0.0198 0.100 mg/L E300.0 0.0750 0.500 08/16/2021 855h mg/L E353 2 0.00541 0.0100 08/13/202 I 1250h mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer --- RPD Ref. Amt ¾RPD RPD Limit Qual Report Date: 8/30/2021 Page 21 of27 analyses applicable to the CWA. SDWA, and RCRA are pcrfonnccl in accordance to NE-LAC prolocols Pertinent sampling information is located on the attached COC Confidential Business Lnformation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the adverti!-ement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted onl y on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2108362-004AMS Date Analyzed: Test Code: 300.0-W Chloride 870 Sulfate 1,610 Lab Sample ID: 2108362-002BMS Date Analyzed: Test Code: NO2/N03-W-353.2 Nitrate/Nitrite (as N) 11.6 3440 South 700 West SaltLakeCity,UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/18/2021 213h mg/L E300,0 1.98 10.0 500.0 mg/L E300.0 7.50 50.0 500.0 08/16/2021 905h mg/L E353.2 0.0541 0.100 10.00 Tanner Holliday WC MS Spike Ref. Amount ¾REC 365 101 1130 96.0 1.42 102 Limits 90 -110 90 -110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt ¾RPD Limit Qual Report Date: 8/30/2021 Page 22 of27 analyses applicable to the CWA. SOWA. and RCRA are performed in accordance to N ELAC protocols Pertinent sampling inforrnation is located on the attached COC Confidential Business Information: TI1is report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff~ or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2108362-004AMSD Date Analyzed: Test Code: 300.0-W Chloride 863 Sulfate 1,590 Lab Sample ID: 2108362-002BMSD Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 11. 7 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 08/18/2021 236h mg/L E300.0 1.98 10.0 500.0 mg/L E300.0 7.50 50.0 500.0 08/16/2021 906h mg/L E353.2 0.0541 0.100 10.00 Tanner Holliday WC MSD Spike Ref. Amount %REC 365 99.7 1130 92.3 1.42 103 Limits 90-110 90 -110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPD Limit 870 0.759 20 1610 1.16 20 11.6 0.819 10 Qual Report Date: 8/30/2021 Page 23 of27 analyses applicable to the CWA. S DW A, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnfom,ation: TI11s report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: LCS VOC-2 081621A Date Analyzed: Test Code: 8260D-W-DENI00 Carbon tetrachloride 22.6 Chloroform 20.9 Methylene chloride 21.5 Surr: l,2-Dichloroethane-d4 48.0 Surr: 4-Bromofluorobenzene 50.3 Surr: Dibromofluoromethane 49.1 Surr: Toluene-d8 51.1 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail : awal@awal-labs.com, web: www.awal-labs.com QLSUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 08/16/2021 709h µg/L SW8260D 0.785 1.00 20.00 0 113 µg/L SW8260D 0.360 1.00 20.00 0 104 µg/L SW8260D 0.451 1.00 20.00 0 108 µg/L SW8260D 50.00 95.9 µg/L SW8260D 50.00 101 µg/L SW8260D 50.00 98.2 µg/L SW8260D 50.00 102 Limits 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/30/2021 Page 24 of27 analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NE LAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any puipose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: MB VOC-2 081621A Date Analyzed: Test Code: 8260D-W-DEN100 Carbon tetrachloride < 1.00 Chlorofonn < 1.00 Methylene chloride < 1.00 Surr: I ,2-Dichloroethane-d4 48.2 Surr: 4-Bromofluorobenzene 53.8 Surr: Dibromofluoromethane 48.1 Surr: Toluene-d8 51.7 Units 3440 South 700 West Salt Lake City, UT 841 19 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com J)C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 08/16/2021 728h µg/L SW8260D 0.785 1.00 µg/L SW8260D 0.360 1.00 µg/L SW8260D 0.451 1.00 µg/L SW8260D 50.00 96.3 µg/L SW8260D 50.00 108 µg/L SW8260D 50.00 96.2 µg/L SW8260D 50.00 103 Limits 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPD Amt %RPD Limit Qual Report Date: 8/30/2021 Page 25 of 27 analyses applicable to 1he CWA. SOWA, and RCRA are perfom1ed. in accordance LO NELAC protocols Pertinent sampling infonnation is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use oftt ne of this company or any member of its staff, or reproduction of thls report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wiJI be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2108362-002CMS Date Analyzed: Test Code: 8260D-W-DENlOO Carbon tetrachloride 223 Chloroform 1,220 Methylene chloride 218 Surr: 1,2-Dichloroethane-d4 479 Surr: 4-Bromofluorobenzene 513 Surr: Dibromofluoromethane 491 Surr: Toluene-d8 515 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Tanner Holliday Dept: MS VOA QC Type: MS Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 08/16/2021 959h µg/L SW8260D 7.85 10.0 200.0 0 112 µg/L SW8260D 3.60 10.0 200.0 1230 -6.55 µg/L SW8260D 4.51 10.0 200.0 1.25 109 µg/L SW8260D 500.0 95.7 µg/L SW8260D 500.0 103 µg/L SW8260D 500.0 98.2 µg/L SW8260D 500.0 103 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 8/30/2021 Page 26 of27 analyses applicable to the CWA. SDWA, and RCRA are perfom1ed in accordanc.e to NE LAC protocols Pertinent sampling information is located on the attached COC Confidential Business Infom1a1ion: This report is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff. or reproduction of this report in connection with the advenisement. promotion or sale of any product or process. or in connection with the re--publ ication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2108362 Project: August Ground Water 2021 Analyte Result Lab Sample ID: 2108362-002CMSD Date Analyzed: Test Code: 8260D-W-DENI00 Carbon tetrachloride 226 Chloroform 1,230 Methylene chloride 221 Surr: l,2-Dichloroethane-d4 485 Surr: 4-Bromofluorobenzene 532 Surr: Dibromofluoromethane 496 Surr: Toluene-d8 521 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MSD Spike Ref. Amount %REC 08/16/2021 1019h µg/L SW8260D 7.85 10.0 200.0 0 113 µg/L SW8260D 3.60 10.0 200.0 1230 0.100 µg/L SW8260D 4.51 10.0 200.0 1.25 110 µg/L SW8260D 500.0 96.9 µg/L SW8260D 500.0 106 µg/L SW8260D 500.0 99.1 µg/L SW8260D 500.0 104 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. Limits 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 223 1.33 35 1220 1.09 35 219 1.14 35 Qual Report Date: 8/30/2021 Page 27 of27 analyses applicable to the CWA. SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC, Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement~ promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West Analytical Laboratories Rpt Emailed: UL Denison WORK ORDER Summary WorkOrder: 2108362 Due Date: 8/27/2021 Page 1 of2 Client: Energy Fuels Resources, Inc. Client ID: ENE300 Contact: Tanner Holliday Project: August Ground Water 2021 QC Level: III WO Type: Project Comments: QC 3 (no chromatograms). EDD-Denison. Email Group; (USE PROJECT for special DLs). Do not use "*R_" samples as MS/MSD.; Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 2108362-00lA MW-l 1_08102021 8/10/2021 1110h 8/13/2021 0938h 300.0-W Aqueous ~I df-wc l SEL Ana/ytes: CLS04 _ -----••·. _ •·-· --- 2108362-002A MW-26_08102021 8/10/2021 0930h 8/13/2021 0938h 300.0-W Aqueous [;,j df-wc _ I SEL A,ialytes: CL --··-·--2108362-002B NO2/NO3-W-353.2 ~ df-no2/no3 -----·•-1 SEL A11a/yres: N03N02N ----·--- 2108362-002C 8260D-W-DENl00 lvrl Purge 3 Test Group: 8260D-W-DENIO0; #of Ana/ytes: 31# o[Surr: 4_ 2108362-00JA MW-30_08092021 8/9/2021 111 Sh 8/13/2021 0938h 300.0-W Aqueous ~] df-wc I SEL Ana/ytes: CL ----· ---· --------------· ---------· 2108362-0038 NO2/NO3-W-353.2 ~] df -no2/no3 I SEL A11aly1es: N03N02N -----~-.. . ·-····---------------------------·----·---2 l08362-003C 200.8-DIS l'(j df -dismelals _________________ l Sl!L A11a/ylf!.!:_ SEU ___ _ 200.8-DIS-PR O df -dismetals 2108362-004A MW-31_08092021 8/9/2021 1340h 8/13/2021 0938h 300.0-W Aqueous [,tj df-wc _______ 2 SEL Analytes: CLS04 _____________ _ 2108362-0048 NO2/NO3-W-353.2 [,ij df -no2/no3 -----------··· ____ I SEL Ana/ytes: NOJN02N ... 2 I08362-004C 200.8-D1S [v'J df -dismetals ----------~---------------------JS_E_L_A_,~~'1:_t_es_:_U ________ _ 200.8-DIS-PR --------------------Q___df-dismetals 2108362-004D TDS-W-2540C [~ df-tds I SEL A7!.aflt~s: TDS 2108362-00SA MW-65_08092021 8/9/2021 ll lSh 8/13/2021 0938h 300.0-W Aqueous i;,J df-wc ___________ J_S_'ELAna/ytes: CL _ ------------------2108362-0058 NO2/NO3-W-353.2 [,iij df -no2/no3 . _ I SE_L Analyles: f!_03N_D_2_f:I _ _ ___ _ ________ _ 2108362-00SC 200.8-DIS I~ df -dismetals ---------·----__ 2 SEL Anal)!!eS: SE U ------------ Printed: 08/30/21 14:00 LABORATORY CHECK: %M [] RT □ CN [] TAT[] QC CJ LUO U HOK ___ HOK __ _ HOK___ COG Emailedc..-___ _ WORK ORDER Summary Client: Energy Fuels Resources, Inc. Sample ID Client Sample ID Collected Date 2108362-00SC MW-65 08092021 8/9/2021 111 Sh 2108362-006A Trip Blank 8/10/2021 0930h Received Date Test Code Matrix 8/13/2021 0938h 200.8-DIS-PR Aqueous WorkOrder: 2108362 Due Date: 8/27/2021 Sel Storage 0 df -<lismetals 8/13/2021 0938h 8260D-W-DENlO0 Aqueous [~j Purge T~1 G.1:!!':'P:___82~~D-W-~ENJOO:' 1±_ of Analytes.-_3 !__# ofSurr: 4 Page2 of2 3 Printed: 08/30/21 14:00 LABORATORY CHECK: %M L.:J RT LI CN O TAT LJ QC [J LUO [J HOK ___ HOK __ _ HOK___ COC Emailed~---- 3 4 5 6 ) I ! I American West Analytical Laboratories 463 W. 3600 S. Salt lake City, UT 84115 Phone# (801) 263-8686 Toll Free# (888) 263-8686 ~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. Address: 6425 S. Hwy. 191 Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: Email: thollida.y@energyfuels.com; kweinel@energyfnels.com; Project Name: August Ground Water 2021 Project#: PO#: Sampler Name: Tanner Holliday Date Samole ID: Samoled MW-11_08102021 ~-r 'i!'l?:,ol-2.\ o-U \. 1-\c.\l,!"'-'I 8/10/2021 MW-26_~1 0'?5 \ OZ.Cl 2-l 8/10/2021 MW-30_08092021 8/9/2021 MW-31_08092021 8/9/2021 MW-65_08092021 8/9/2021 Trip Blank 8/10/2021 Rollnqufohed. ~ JI:. /// Dole, rsignahln!I -. I h ........ .,, ""' -.., 8/13/2021 I Tl<11•: (' J'i '.3 'I( PrfnlN.ame: T onnor Hollldo• Relfnquls/lod by. Dole: Slan11ure Tlme: PrintNomo: R6ilnqulahed by: Oate: Signature ;lime: Print Name: Rollnqulshod by: Date: c:.1nna1ure Time: PrtntName: CHAIN OF CUSTODY i la f3~z..__ All analysis will be conducted using NELAP accrediled methods and all data WIii be reported using AWAL's standard analyte lists and reporting llmlts (PQL) unless specifically requested othervdse on this Chain of Custody and/or attached documentation, AWAL Lab Sample Set# Page 1 of 1 I QC Level: I Tum Around Time: Unless other arrangements have been made, I""' Da<o signed reports ,.;11 be emailed by 5:00 pm on 3 Standard the day they are due, i::: X Include EDD: Laboratory Use Only 0 LOCUS UPLOAD 1 EXCEL lsamples Were: 0 X Field Filtered For: Shippedfanddnlhlon,d ~ G Dissolved Metals 1 i::: 00 OS Ambient~• ci co' co' ,c: 2 0 00 0 0 .... For Compliance With: ci Ill Temperature C} ,. ~ 0c IN C) C) E! □ NELAP ---0 C'I ('I o' 3 t--IN 0 ci ---i;:-i;:-0 .. □ RCRA 0 t--g 0 C) ..5! □ CWA 4 Received Broken/Leaking £!.. ci C) 0) ,,Q □ SDWA 0 Cl (Improperly Sealed) ~ ~ .. a~ II £!.. 0 □ ELAP/A2LA y @ .. II ] E! E! u o' • IC □ NLLAP II o' ::s -a ~ 0 !~ t'i' OS i □ Non-Cornpflance 6 ~ Preseived IIO 0 C) C ~ § § ~ C) 0) ,S II □ Other: t;; N C) l l/) 0) .. ~ I D' .. 'I-0 0 .., ockod al bench I!? ~ .. :;i 0 11.1 ~ .2] ., I') .., 0 C) .., .., .., C) y N C: C) ;J; C) ,,Q -~ 0 Ill ! Ill ! Ill l/) C: ::. IC .l: C) .E: ~ ::t. 0 iJ Known Hazards 6 Received Within l/) ~ 0 ., ..... 0 ::t. 0 0 0 • I? (!)!ding Times Time (.) a. ('I ~ ro • • • 0 .. 0 .... & 0 E g 6 Q • • • ~ 0 0 II N Samoled cu i5 i5 i5 iS ro Samole Comments .. en E-:> f- 1110 1 w X X 930 5 w X X X , Present on Ouler Po~ Y N NA 1115 3 w X X X X 2 Unbroken on Outer Pack~ \ 1340 4 w X X X X X Y N NA , 1115 3 w X X X X 3 Present on Sample c;,, y N 4 Unbroken on Sample (;) 930 w X y N 3 k>iscrepancies Between Semple y N Labels and CCC 0 Rooo1"od by. ---6 Slgnob.rro • ,f _i ~_,, -cA :.,__, , ~~/j-;x.1 Special Instructions: 7~ I/A '"-.J.L./, . / / IT<m«'o/'7 ~ PrintNeme; Sample containers for metals were field filtered. See the Received by: I / Dale: Analytical Scope of Work for Reporting Limits and voe analyte Sionatura lime: list PrintName: Received by: Dale: Signature nme: PrtntNama: Received by: Date: ,Signature Time: Print Name: I Analysis Ammonia COD Cyanide Metals N02/N03 O&G Phenols Sulfide TKN TP04 CrVI+ Procedure: Frequency: Preservatio_n Check Sheet s Je Set E Preservative 2..-~3 L/ 5 pH<2H2S04 pH<2H2S04 pH>lONaOH pH<2HN03 !k{ V~, V .... 5 pH <2 H2.S04 ½> i,,; /·IL) v..e-< pH<2HCL , , y pH<2H2S04 pH >9 NaOH. ZnAC pH<2H2S04 pH<2H2S04 pH >9 (N14hS04 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid d PH 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + ~ # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH > __ due to the sample matrix interference. Lab Set ID: pH Lot#: 2./0~)CJl"L C,70Q rev 10-28-2020 TabF2 Laboratory Analytical Reports -Accelerated Monitoring September 2021 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: September Ground Water 2021 Lab Sample ID: 2109256-001 Client Sample ID: MW-l 1_09072021 Collection Date: 9/7/2021 1320h Received Date: 9/10/2021 1100h Analytical Results Date Compound Units Prepared Chloride Sulfate mg/L mg/L Date Analyzed 9/23/2021 427h 9/23/2021 014h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qual E300.0 2.00 49.6 E300.0 100 1,240 Report Date: 9/24/2021 Page 8 of27 All anal) ses applicable 1o the CWA SOWA. and RCRA are performed in accordance to NELAC prolocols Pertinent sampling information is locu1ed on the all ached COC Confidential Business Information: This repor1 is provided for the exclusi, e use of the ~ddressee Pri,·ile~es o_Fsub__seq~enl ~?e of lhe ~:u:ne of lhis .con_1pany or ml) ~I!1be1 of its stafT, or reproduclio~ ~~this repo~ in _con~eclion-"·ith lhe a~'.'er1isemenL P~?motio,n ~r ~ale of~!). ~rod~cl or P~?cess, ~r in 7onm;c!io11 w~lh th~ r~-publication of this report INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: September Ground Water 2021 Lab Sample ID: 2109256-002 Client Sample ID: MW-26_09092021 LAeoR AToR1Es Collection Date: 9/9/2021 800h 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 :-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Received Date: 9/10/2021 1100h Analytical Results Date Compound Units Prepared Chloride mg/L Nitrate/Nitrite (as N) mg/L Date Analyzed 9/23/2021 221h 9/15/2021 1458h Contact: Tanner Holliday Method Reporting Analytical Used Limit Result Qual E300.0 2.00 59.3 E353.2 0.100 0.710 Report Date: 9/24/2021 Page 9 of27 All anal) ses applicable to the CWA, SOWA. and RCRA are pcrfom1ed in accordance to NELAC prolocols. Pertinent sampling informalion is located on lhe altached COC Confidential Business lnformalion: This report is pro,•ided for the exclusi, e use of the !ddressee Pri, ile~es of sub.:'eq~nl ~~e or the ~~e of I his 0co~pany or .tn) ~mber of its slafT, or reproduclio~ ~f this repo~ in ~o~eclion~ with the ~vertise~nt, P~?molio,n or sale of ~~y ~rodl~Cl or p~ocess, ~r in ~nn~~ion w!th th~ r~-publicalion of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com ORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: September Ground Water 2021 Lab Sample ID: 2109256-002C Client Sample ID: MW-26_09092021 Collection Date: 9/9/2021 800h Received Date: 9/10/2021 1100h Analytical Results Analyzed: 9/15/2021 842h Extracted: Units: µg/L Dilution Factor: Compound Chloroform 10 CAS Contact: Tanner Holliday Test Code: 8260D-W-DENIOO VOAs by GC/MS Method 8260D/5030C Method: SW8260D Reporting Analytical Number Limit Result Qual 67-66-3 10.0 516 _, Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: I ,2-Dichloroethane-d4 17060-07-0 488 500.0 97.6 80-136 Surr: 4-Bromofluorobenzene 460-00-4 485 500.0 97.0 85-121 Surr: Dibromofluoromethane 1868-53-7 467 500.0 93.5 78-132 Surr: Toluene-d8 2037-26-5 479 500.0 95.9 81-123 ' -Malrix spike recove1y indicates malrix inlerference. The method is in control as indicaled by !he LCS. web: www.awal-labs.com ~ -The reporting limits were raised due to high analyle concentrations. Jennifer Osborn Analyzed: 9/15/2021 743h Units: µg/L Laboratory Director Compound Jose Rocha QA Officer Carbon tetrachloride Methylene chloride Surrogate Units: µg/L Surr: 1,2-Dichloroethane-d4 Surr: 4-Bromofluorobenzene Surr: Dibromofluoromethane Surr: Toluene-d8 Extracted: Dilution Factor: Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 56-23-5 1.00 < 1.00 75-09-2 1.00 < 1.00 CAS Result Amount Spiked %REC Limits Qual 17060-07-0 50.7 50,00 101 80-136 460-00-4 49.2 50.00 98.3 85-121 1868-53-7 48.9 50.00 97.8 78-132 2037-26-5 49.6 50.00 99.3 81-123 Report Date: 9/24/2021 Page 13 of27 All analyses applicable to lhe CWA. SOWA. and RCRA are perfom1ed in accordance to NELAC protocols. Pertinenl sampling information is located on the atlached COC Confidential Business Informal ion: This repor1 is pro,·ided for lhe e.xdusi\ e use of 1he ~ddressee Pri\ ile~es o~ sub~seq~1enl ~e or lhe ~~e of lh1s _co':'pany or rm) 1~~1ber of ils slttIT, or reproduclio~ ~f lhis repo~ in ~0t~1eclion~ with the a~"ertisemenl, P~?moti~ or sale of~~ ~rodl~ct or p~ocess, ~r in ~onn~c!ion "!th 1h~ r~-p~blication of this report INORGANIC ANALYTICAL REPORT American West ANALYTICAL LABORATOR I E6 3440 South 700 West Client: Energy Fuels Resources, Inc. Project: September Ground Water 2021 Lab Sample ID: 2109256-003 Client Sample ID: MW-30_09082021 Collection Date: 9/8/2021 1220h Received Date: Analytical Results Compound 9/10/2021 1100h Units Date Prepared Date Analyzed ;;alt Lake City, UT 84119 Selenium mg/L mg/L 9/13/2021 1144h 9/18/2021 1054h 9/13/2021 1144h 9/18/2021 1054h Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Uranium Contact: Method Used £200.8 £200.8 Tanner Holliday DISSOLVED METALS Reporting Limit 0.00500 0.000300 Analytical Result 0.0604 0.00974 Qual Report Date: 9/24/2021 Page 5 of27 All analyses applicable to lhe CWA. SDW A. and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on Ll1e allached COC Confidential Business Information: This report is prm'ided for the c_~IUihc use of the ~ddressee Prfrile~es o~ suh .. seq~enf ~e of the ~?'?1e of lhis .co~~ny or M) ~mber of ils slaff, or reproducrio~ ~f lhis repo~ in ~~eel ion~ ,lilh the a~vertise~ent, P~?moti~n ~r ~aJe of ~!):_~r<xJ~cl or p~~s. ~r in ~nm,:c!ion \\'!lh th~ r~·p~bl.ica.ilan of lhis reJX)n 3440 South 700 West ,alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-Iabs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: September Ground Water 2021 Lab Sample ID: 2109256-003 Client Sample ID: MW-30_09082021 Collection Date: 9/8/2021 1220h Received Date: 9/10/2021 11 00h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 9/23/2021 246h E300.0 5.00 183 Nitrate/Nitrite (as N) mg/L 9/15/202 I 1504h E353.2 0.100 15.4 Report Date: 9/24/2021 Page IO of 27 All analyses applicable to the CWA. SOWA, and RCRA are perfom1ed in accordance to NELAC protocols Pertinenl sampling information is located on Lhe allached COC Confidenlial Business lnfonnation: This report is pro\'ided for 1he exclusi,·e use of the ~ddressee Pri, ile~es oF sub__seq~ent ~~e of the ~~e of this _con:ipany or an) ~mber of its slaff, or reproduclio~ ~f this repo~ in ~0•~1eclion .. with the a~vertise~ent P~?motio_n ~r sale of ?'!Y. -~rod~cl or P~?cess, ~r in ~onm;c~ion w!th th~ r:-p~blication of this report American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: September Ground Water 2021 Lab Sample ID: 2109256-004 Client Sample ID: MW-31_0907202 l Collection Date: 9/7/2021 1420h Received Date: 9/10/2021 11 00h Analytical Results DISSOLVED METALS Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Uranium mg/L 9/13/2021 1144h 9/18/2021 1112h E200.8 0.000300 0.0202 ---- Report Date: 9/24/2021 Page 6 of27 All analyses applicable to the CW A. SDWA. and RCRA are perfom1ed in accordance lo NELAC prolocols Pertinent sampling informalion is localed on Lhe al1ached COC Confidenlial Business Jnfonnation: This repon is pro,,ided ror lhe exch.1Sh e use o[the ~cldressee Pri\"ile~es o,r sub .. seq~nt ~?e or the ~?1.11e or lhis ,con;ipany or an) ~mber of ils staff, or reproducli~ ~~ this repo~ in .co1~ection,. ,vith the a~\•ertise1~ent, p~~motio_n ~r ~a1e of ?1!Y._~rod~c1 or P~?ce~s, ~r in ~nn:c~ion \\'!lh lh~ r~-publication of this repon American West ANALYTICAL LABORATORIES 3440 South 700 West ;alt Lake City, UT 84119 Phone:(801)263-8686 foll Free: (888) 263-8686 Fax: (801)263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: September Ground Water 2021 Lab Sample ID: 2109256-004 Client Sample ID: MW-31_09072021 Collection Date: 9/7/2021 1420h Received Date: 9/10/2021 1100h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 9/23/2021 311 h £300.0 10.0 356 Nitrate/Nitrite (as N) mg/L 9/15/2021 1507h £353.2 0.100 16.0 Sulfate mg/L 9/23/2021 31 lh £300.0 50.0 1,130 Total Dissolved Solids mg/L 9/10/2021 1220h SM2540C 20.0 2,870 Report Date: 9/24/2021 Page 11 of27 All wrnlyses applicable to the CWA. SOWA, and RCRA are performed in accordance lo NELAC protocols Pertinenl sampling information is located on the altached COC Confidenlial Business [nfonnalion: This repon is pr0\1ided for the exclusi,·e use of the ~ddressee Pri\ ile~es o_f sub ... seq~enl ~~e of !he ~?1:'1e of lhis _con:ipany or ITTl)' ~mbe1 of ils slaff, or reproductio~ ~f I his repo~ in ~o~ection,. wilh the a~,•ertisemenL, P~?mo1io_n or saJe of ?1!) ~roch~cl or p1:oces1;, ~r in :°nn;:c~ion w!th th~ r~-publicalion or this repon INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Project: September Ground Water 2021 Lab Sample ID: 2109256-005 Client Sample ID: MW-65_09072021 tAooRAToR1es Collection Date: 9/7/2021 1420h 3440 South 700 West ,alt Lake City, UT 84119 Phone:(801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Received Date: 9/10/2021 11 00h Analytical Results Date Compound Units Prepared Uranium mg/L 9/13/2021 II 44h Date Analyzed 9/18/2021 1116h Contact: Tanner Holliday DISSOLVED METALS Method Reporting Analytical Used Limit Result Qual E200.8 0.000300 0.0194 ------ Report Date: 9/24/2021 Page 7 of27 All analyses applicable to lhe CWA. SOW A. and RCRA are performed in accordance lo NELAC protocols Pertinent sampling informa1ion is loca1ed on lhe altached COC Confidential Business Jnformalion: This repon is pro,,ided for the culumt' use orthe ~ddressee Pri, ile~es o! sub,.seq~ent ~:'e or lhe ~~e of I his _con,1pany or M) ~mber of its slaIT, or reproducli~ ~f this repo~ in ~M?eclion,. \\•ith lhe a~vertisemenl, P~?motio_n ~r ~ale of ?1!Y. ~rod~ct or p~~cess. ~r in ~onn~c~ion w~th lh~ r~-pubhr.nuon or this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801)263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer INORGANIC ANALYTICAL REPORT Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday Project: September Ground Water 2021 Lab Sample ID: 2109256-005 Client Sample ID: MW-65_09072021 Collection Date: 9/7/2021 1420h Received Date: 9/10/2021 1100h Analytical Results Date Date Method Reporting Analytical Compound Units Prepared Analyzed Used Limit Result Qual Chloride mg/L 9/23/2021 453h E300.0 1.00 356 Nitrate/Nitrite (as N) mg/L 9/15/2021 1508h E353.2 0.100 16.5 Sulfate mg/L 9/23/202 I 337h E300.0 100 1,130 Total Dissolved Solids mg/L 9/10/2021 1220h SM2540C 20.0 3,640 ------ Report Date: 9/24/2021 Page 12 of27 All anal)ses applicable to lhe CWA SDWA. and RCRA are perfom1ed in accordance lo NELAC protocols Per1inenl sampling information is located on the attached COC Confidential Business Information: This repon is provided for 1hc(\.,cl.lffl,·c-use of the !ddressee Privile~es o_f sub,.seq~enl ~1~e of the ~?':'1e of this _cm~pw1y or anr ~mber of its slaJT, or reproductio~ ~f this repo~ in ~on~1ection .. ,\i1.h the a~vertise~I P~?motio;n ~r ~a1e of ~!Y. ~rodl~ct or P~?cess, ~r in ~nn:c~ion \\'!lh II~ ~•pubticmion or this report 3440 South 700 West ~alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (80 I) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer ORGANIC ANALYTICAL REPORT Client: Project: Lab Sample ID: Energy Fuels Resources, Inc. September Ground Water 2021 2109256-006A Client Sample ID: Trip Blank Collection Date: 9/9/2021 800h Received Date: 9/10/2021 11 00h Analytical Results Analyzed: 9/15/2021 941h Units: µg/L Compound Carbon tetrachloride Chloroform Methylene chloride Extracted: Dilution Factor: Contact: Tanner Holliday Test Code: 8260D-W-DENIO0 VOAs by GC/MS Method 8260D/5030C Method: SW8260D CAS Reporting Analytical Number Limit Result Qual 56-23-5 1.00 < 1.00 67-66-3 1.00 < 1.00 75-09-2 1.00 < 1.00 Surrogate Units: µg/L CAS Result Amount Spiked %REC Limits Qual Surr: l ,2-Dichloroethane-d4 Surr: 4-Bromofluorohenzene Surr: Dibromofluoromethane Surr: Toluene-d8 17060-07-0 460-00-4 1868-53-7 2037-26-5 50.1 49.8 47.5 49.1 50.00 JOO 80-136 50.00 99.6 85-121 50.00 95.1 78-132 50.00 98.2 81-123 Report Date: 9/24/2021 Page 14 of27 All analyses applicable to lhe CWA. SOWA. and RCRA are perfom1ed in RCcordance 10 NELAC protocols, Pertinent sampling information is locnled on lhe allached COC Confidenlial Business Jnformalion: This repon is pro,•ided for lhe exclusi, e use of lhe ~dressee P1i, ile~es o! su~seq~ent ~e or the ~~e of this .co";pany or any 1~mber of its st:uf. or reproduc(io~ ~~ 1his repo~ in ~on~ecfion ... \\~th the a~vertisemenL p~~moli~ ~r sale of~!) ~rod~cl or p~ocess, ~r in ~onn~c~ion w!lh lh~ r~-publicalion of this repor1 3440 South 700 West ,alt Lake City, UT 84119 Phone: (80 I) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osbom Laboratory Director Jose Rocha QA Officer Tanner Holliday Energy Fuels Resources, Inc. 6425 South Hwy 191 Blanding, UT 84511 TEL: (435) 678-2221 RE: September Ground Water 2021 Dear Tanner Holliday: Lab Set ID: 2109256 American West Analytical Laboratories received sample(s) on 9/10/2021 for the analyses presented in the following report. American West Analytical Laboratories (AWAL) is accredited by The National Environmental Laboratory Accreditation Program (NELAP) in Utah and Texas; and is state accredited in Colorado, Idaho, New Mexico, Wyoming, and Missouri. All analyses were performed in accordance to the NELAP protocols unless noted otherwise. Accreditation scope documents are available upon request. If you have any questions or concerns regarding this report please feel free to call. The abbreviation "Surr" found in organic reports indicates a surrogate compound that is intentionally added by the laboratory to determine sample injection, extraction, and/or purging efficiency. The "Reporting Limit" found on the report is equivalent to the practical quantitation limit (PQL). This is the minimum concentration that can be reported by the method referenced and the sample matrix. The reporting limit must not be confused with any regulatory limit. Analytical results are reported to three significant figures for quality control and calculation purposes. Thank You, Digitally signed by J • f Jennifer Osborn e n n I e r DN: cn=Jennifer Osborn, o=AWAL, ou=Organics, 0 b email=jenn@awal-labs. S Orn com, c=US Date: 202"1 .09.24 Approved by: 11:5259-os·oo· Laboratory Director or designee Report Date: 9/24/202 I Page I of27 All analyses applicable lo lhe CWA. SOWA. and RCRA are performed in accordance to NELAC protocols. Pertinent s&npli.ria,inforrnation is localed on the attached COC. Conlidentiul Business Information: This repon is provided for the ti'(dush·,e UIC of the '!'1dressee Prl\·ile~es o! sub .. seq~enl ~~e of the ~?':"e of this .con:ipany or an) ~mhe1 of ils s1aIT. or reproducli~ ~f this ~ iii .con~eclion~ wilh the n~~•ertise~enl. P~?molio,n o_r ~ale of ~Y. ~rodl~Cl or p~~cess. ~r in ~nn:c!ion w!th lh~ r:-p~bhtmtQn or this report SAMPLE SUMMARY American West Client: Energy Fuels Resources, Inc. Contact: Tanner Holliday ANALYTICAL LABORATORIES Project: September Ground Water 2021 Lab Set ID: 2109256 Date Received: 9/10/2021 1100h Lab Sample ID Client Sample ID Date Collected Matrix Analysis 3440 South 700 West 2109256-001 A MW-11 09072021 9/7/2021 1320h Aqueous Anions, E300.0 ~alt Lake City, UT 84119 2109256-002A MW-26 09092021 9/9/2021 800h Aqueous Nitrite/Nitrate (as N), E353.2 2109256-002B MW-26 09092021 9/9/2021 800h Aqueous Anions, E300.0 2109256-002C MW-26 09092021 9/9/2021 800h Aqueous VOA by GC/MS Method Phone: (801) 263-8686 8260D/5030C 2109256-003A MW-30 09082021 9/8/2021 1220h Aqueous Nitrite/Nitrate (as N), E353.2 Toll Free: (888) 263-8686 2109256-003 B MW-30 09082021 9/8/2021 1220h Aqueous Anions, E300.0 Fax: (801) 263-8687 2109256-003C MW-30 09082021 9/8/2021 1220h Aqueous ICPMS Metals, Dissolved !-mail: awal@awal-labs.com 2109256-004A MW-31 09072021 9/7/2021 1420h Aqueous Nitrite/Nitrate (as N), E353.2 2109256-004B MW-31 09072021 9/7/2021 1420h Aqueous Anions, E300.0 web: www.awal-labs.com 2109256-004C MW-31 09072021 9/7/2021 1420h Aqueous Total Dissolved Solids, A2540C 2109256-004 D MW-31 09072021 9/7/2021 1420h Aqueous ICPMS Metals, Dissolved 2109256-005A MW-65 09072021 9/7/2021 1420h Aqueous Nitrite/Nitrate (as N), E353.2 Jennifer Osborn 2109256-005B MW-65 09072021 9/7/2021 1420h Aqueous Anions, E300.0 Laboratory Director 2109256-005C MW-65 09072021 9/7/2021 1420h Aqueous Total Dissolved Solids, A2540C 2109256-005D MW-65 09072021 9/7/2021 1420h Aqueous ICPMS Metals, Dissolved Jose Rocha 2109256-006A Trip Blank 9/9/2021 800h Aqueous VOA by GC/MS Method QA Officer 8260D/5030C Report Date: 9/24/2021 Page 2 of27 All anal)ses applicable to the CWA. SDW A. and RCRA are performed in accordance 10 NELAC protocols Per1inenl sampling infommtion is located on the auached COC. Confidential Business Jnfonnution: This repon is pro,·ided ror the exclusirn use of lhe ~ddressee Pri, ile~es o_f sub__seq~ent ~1~e or the ~?':'1e of this _co~pany or an)' ,~mber of its staff, or reproductio~ ~~this repo~ in ~o~echon~ "~th the a~,•enisement, P~?motio,n or sale of ~!Y ~rod~ct or P~?cess, ~r in ~nn~c!ion w~lh th~ r~-publication of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 ~-mail: awal@awal-labs.com web: www.awal-labs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Inorganic Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: September Ground Water 2021 2109256 9/10/2021 9/7-9/9/2021 Intact None Holding Time and Preservation Requirements: The analysis and preparation of all samples were performed within the method holding times. All samples were properly preserved. Preparation and Analysis Requirements: The samples were analyzed following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD: Method Blanks (MB): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Samples (LCS): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike / Matrix Spike Duplicates (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, indicating no apparent matrix interferences. Duplicate (DUP): The parameters that required a duplicate analysis had RPDs within the control limits. Corrective Action: None required. Report Date: 9/24/2021 Page 3 of 27 All analyses applicable lo lhe CWA. SOWA. and RCRA are perfom1ed in accordance lo NELAC prolocols Pcr1inenl sampling informalion is located on Lhe attached COC Coniidentinl Business Information: This repon is provided for the exclusi\"e use of1he ~ddressee Pri\ ile~es of sub~seq~enl ~~e of the ~'.1',11e or this _con_ipany or rul) ~t;~ber of ils stalT, or reproductio~ ~f this repo~ in ~on~eclion .. \\ilh Lhe °'!vertise~ent. P~?moti~n or ~ale of ?1!Y. ~rod~cl or P~?cess, ~r in ~nn:c~ion w~lh lh~ r:-p~blication of this report 3440 South 700 West ;alt Lake City, UT 84119 Phone: (801) 263-8686 Toll Free: (888) 263-8686 Fax: (801) 263-8687 !-mail: awal@awal-labs.com web: www.awal-Iabs.com Jennifer Osborn Laboratory Director Jose Rocha QA Officer Volatile Case Narrative Client: Contact: Energy Fuels Resources, Inc. Tanner Holliday Project: Lab Set ID: Sample Receipt Information: Date of Receipt: Date of Collection: Sample Condition: C-O-C Discrepancies: Method: Analysis: September Ground Water 2021 2109256 9/10/2021 9/7-9/9/2021 Intact None SW-846 8260D/5030C Volatile Organic Compounds General Set Comments: One or more target analytes were observed above reporting limits. Holding Time and Preservation Requirements: All samples were received in appropriate containers and properly preserved. The analysis and preparation of all samples were performed within the method holding times following the methods stated on the analytical reports. Analytical QC Requirements: All instrument calibration and calibration check requirements were met. All internal standard recoveries met method criterion. Batch QC Requirements: MB, LCS, MS, MSD, RPD, and Surrogates: Method Blanks (MBs): No target analytes were detected above reporting limits, indicating that the procedure was free from contamination. Laboratory Control Sample (LCSs): All LCS recoveries were within control limits, indicating that the preparation and analysis were in control. Matrix Spike/ Matrix Spike Duplicate (MS/MSD): All percent recoveries and RPDs (Relative Percent Differences) were inside established limits, with the following exceptions: the MSD percent recovery for Chloroform on sample 2109256-002C were outside of the control limits due to sample matrix interference. Surrogates: All surrogate recoveries were within established limits. Corrective Action: None required. Report Date: 9/24/2021 Page 4 of27 All analyses applicable to lhe CW A. SDWA0 and RCRA are performed in accordance to NE LAC protocols. Per1inent samplin£ information is located on Lhe attached COC. Confidenllal Business Information: This repon is pro,•ided for the extll.1$1\e U1oe of the !ddressee. Pri\ ile~es a:sub ... seq~ent ~~e of the ~~e of I his _con:1pany or any ~~ber of its staff, or reproductio~ ~f I his repory in ~on?eclion ... wilh lhe ~,,ertise~enl, P~?motio_n or saJe of~!~ ~rodL~cl or p~ocess, ~r in :onn:c~ion '''!lh th~ r1;-publiC1Ulon or1his repon ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: LCS-79537 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.197 Uranium 0.192 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/18/2021 I 050h 09/ 13/202 I 1144h -- mg/L E200,8 0.000508 0.00200 0.2000 mg/L E200.8 0.000176 0.00200 0.2000 Tanner Holliday ME LCS Spike Ref. Amount %REC 0 98.6 0 96.0 Limits 85 -115 85 -115 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 9/24/2021 Page 15 of 27 analyses applicable to the CW A. SOW A, and RCRA are perfom1ed in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. Confidential Business Information: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection with the re•publication of this report for any purpose other than for the addressee will be granted only on contacL This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: MB-79537 Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium < 0.000200 Uranium < 0.000200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-Iabs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/18/202 I 104 7h 09/13/2021 1144h mg/L E200.8 0.0000508 0.000200 mg/L E200.8 0.0000176 0.000200 Tanner Holliday ME MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director. Jose Rocha QA Officer RPO Ref. - RPO - Amt %RPO Limit Qual Report Date: 9/24/2021 Page 16 of27 analyses applicable to the CWA. SOWA, and RCRA. are performed in accordance to NE LAC protocols Pertinent sampling infoTTTiation is located on the attached COC Confidential Business lnfonnation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use of tt ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 202 l Analyte Result Lab Sample ID: 2109256-00JCMS Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.252 Uranium 0.203 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/18/2021 1130h 09/13/2021 1144h ----- mg/L E200 8 0.000508 0.00200 0.2000 mg/L E200,8 0.000176 0.00200 0.2000 Tanner Holliday ME MS Spike Ref. Amount %REC 0.0604 95.6 0.00974 96.4 Limits 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. RPO Amt %RPO Limit Qual Report Date: 9/24/2021 Page 17 of27 analyses applicable to the CWA, SDWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent samphng information is located on the attached COC Confidential Business Information: This repon is provided for the exclusive use of the addressee Privileges of subsequent use of ti- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee wiJI be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256-00JCMSD Date Analyzed: Test Code: 200.8-DIS Date Prepared: Selenium 0.254 Uranium 0.204 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/18/2021 1134h 09/13/2021 1144h mg/L E200 8 0.000508 0.00200 0.2000 mg/L E200,8 0.000176 0.00200 0.2000 Tanner Holliday ME MSD Spike Ref. Amount %REC 0.0604 96.6 0.00974 97.1 Limits 75 -125 75 -125 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt ¾RPD Limit 0.252 0.801 20 0.203 0.697 20 Qual Report Date: 9/24/2021 Page 18 of27 analyses applicable to the CWA. SD\VA, and RCRA are performed in accordance to NELAC protocols Pertinenl sampling information is located on the attached COC Confidential Business Jnfom,ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt- ne of this company or any member of itS staff~ or reproduction of this report in connection with the advenisement, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256-004CDUP Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 2,860 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday WC DUP Spike Rd. Amount %REC 09/10/2021 1220h ----- mg/L SM2540C 16.0 20.0 Limits -- - Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual - 2870 0.559 5 ----- Report Date: 9/24/2021 Page 19 of27 analyses applicable to the CWA. SDWA, and RCRA are performed in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business lnfom1ation: This report is provided for the exclusive use of the addressee. Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement, promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact, This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: LCS-Rl56998 Date Analyzed: Test Code: 300.0-W Chloride 4.65 Sulfate 4.69 Lab Sample ID: LCS-Rl56682 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) 1.01 Lab Sample ID: LCS-R156557 Date Analyzed: Test Code: TDS-W-2540C Total Dissolved Solids 200 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: Tanner Holliday WC QC Type: LCS Reporting Amount Spike Ref. Units Method MDL Limit Spiked Amount %REC 09/22/2021 2116h ---- mg/L E300.0 0.0198 0.100 5.000 0 93.0 mg/L E300 0 O.Q750 0.500 5.000 0 93.7 09/15/2021 1436h --~ mg/L E353.2 0.00541 0.0100 1.000 0 IOI 09/10/2021 1220h Limits 90-110 90 -110 -- 90-110 -------- mg/L SM2540C 8.00 10.0 205.0 0 97.6 80 -120 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Rer. RPD Amt %RPO Limit Qual Report Date: 9/24/2021 Page 20 of27 analyses applicable to the CWA. SDWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling infom1ation is located on the attached COC Confidential Business Jnfom1ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tJ- ne of this company or any member of it3 staff, or reproduction of this report in connection wlth the advertlsement_ promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: MB-R156998 Date Analyzed: Test Code: 300.0-W Chloride < 0.100 Sulfate < 0.500 Lab Sample ID: MB-R156682 Date Analyzed: Test Code: N02/N03-W-353.2 Nitrate/Nitrite (as N) < 0.0100 Lab Sample ID: MB-R156557 Date Analyzed: Test Code: TDS-W-2540C -- Total Dissolved Solids < 10.0 3440 South 700 West Salt Lake City, UT &4 I 19 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/22/2021 2051 h mg/L E300.0 0.0198 0.100 mg/L E300.0 0.0750 0.500 09/15/2021 1435h mg/L E353 2 0.00541 0.0100 09/10/2021 1220h ------- mg/L SM2540C 8.00 10.0 Tanner Holliday WC MBLK Spike Ref. Amount %REC Limits Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual -----~~---------------- Report Date: 9/24/2021 Page 21 of27 analyses applicable to the CWA, SDWA, and RCRA are perfom1ed in accordance to NE LAC protocols Pertinent sampling information is located on the attached COC, Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LIIBORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256-00lAMS Date Analyzed: Test Code: 300.0-W - Chloride 2,450 Sulfate 3,670 Lab Sample ID: 2109256-00JAMS Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 36.4 Lab Sample ID: 2109256-002AMS Date Analyzed: Test Code: NO2/NO3-W-353.2 Nitrate/Nitrite (as N) 10.3 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal @awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Units Method MDL Limit Spiked 09/23/2021 039h ----- mg/L E300,0 9.90 50.0 2,500 mg/L E300,0 37.5 250 2,500 -09/15/20211517h ---- mg/L E353,2 0.108 0.200 20.00 09/15/2021 1459h ---- mg/L E353.2 0.0541 0.100 10.00 Tanner Holliday WC MS Spike Ref. Amount %REC 49.6 95.9 1240 96.9 15.4 105 - 0.71 95.8 Limits 90 -110 90 -110 90 -110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRef. Amt %RPO ----- RPD Limit Qual Report Date: 9/24/2021 Page 22 of27 analyses applicable to the CWA. SDWA, and RCRA are perfom,ed in accordance to NELAC protocols Pertinent sampling inforrnat1on is located on the attached COC, Confidential Business [nforrnation: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process. or in connection with the re•publ ication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256-00IAMSD Date Analyzed: Test Code: 300.0-W Chloride 2,450 Sulfate 3,670 Lab Sample ID: 2109256-00JAMSD Date Analyzed: Test Code: N02/NO3-W-353.2 Nitrate/Nitrite (as N) 36.4 Lab Sample ID: 2 l09256-002AMSD Date Analyzed: Test Code: NO2/NO3-W-353.2 -- Nitrate/Nitrite (as N) 10.1 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Units Method 09/23/2021 155h mg/L mg/L E300.0 E300.0 09/15/2021 1518h mg/L E353.2 09/15/202 I 1500h mg/L E353,2 MDL 9.90 37.5 0.108 0.0541 Reporting Limit 50.0 250 0.200 0.100 Contact: Dept: QC Type: Amount Spiked 2,500 2,500 20.00 10.00 Tanner Holliday WC MSD Spike Ref. Amount 49.6 1240 15.4 0.71 %REC 96.0 97.2 105 93.9 Limits 90-I 10 90 -110 90-110 90 -110 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPDRer. RPO Amt % RPD Limit Qual 2450 3670 36.4 10.3 0.114 0.168 0.0689 1.90 20 20 10 10 Report Date: 9/24/2021 Page 23 of27 analyses applicable to the CWA. SDWA, and RCRA are perfonned in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisement. promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: LCS VOC-2 091521A Date Analyzed: Test Code: 8260D-W-DENIOO Carbon tetrachloride 23.9 Chloroform 20.9 Methylene chloride 20.5 Surr: l,2-Dichloroethane-d4 51.6 Surr: 4-Bromofluorobenzene 48.4 Surr: Dibromofluoromethane 50.0 Surr: Toluene-d8 50.3 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax: (801) 263-8687 e-mail : awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA LCS Spike Ref. Amount %REC 09/15/202 I 629h ------ µg/L SW8260D 0.785 1.00 20.00 0 119 µg/L SW8260D 0.360 1.00 20.00 0 105 µg/L SW8260D 0.451 1.00 20.00 0 102 µg/L SW8260D 50.00 103 µg/L SW8260D 50.00 96.7 µg/L SW8260D 50.00 100 µg/L SW8260D 50.00 IOI -- Limits - 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPD Ref. RPD Amt %RPO Limit Qual Report Date: 9/24/2021 Page 24 of 27 analyses applical;ilie to the CWA. SUWA, and RCRA are pcrfomied in accordance to NELAC protocols Pertinent sampling infonnation is located on the attached COC. Confidential Business lnfom1ation: This report is provided for the exclusive use of the addressee Privileges of subsequent use of tt ne of this compnny ar nny member of its staff, or reproduction of this report in connection with the advertisement~ promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: MB VOC-2 091521A Date Analyzed: Test Code: 8260D-W-DENlOO - Carbon tetrachloride < 1.00 Chloroform < 1.00 Methylene chloride < 1.00 Surr: l ,2-Dichloroethane-d4 50.5 Surr: 4-Bromofluorobenzene 49.1 Surr: Dibromofluoromethane 47.0 Surr: Toluene-d8 50.2 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, fax: (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com C SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MBLK Spike Ref. Amount %REC 09/15/2021 649h µg/L SW8260D 0.785 1.00 µg/L SW8260D 0.360 1.00 µg/L SW8260D 0.451 1.00 µg/L SW8260D 50.00 IOI µg/L SW8260D 50.00 98.3 µg/L SW8260D 50.00 94.0 µg/L SW8260D 50.00 100 Limits 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPD Amt %RPO Limit Qual --------- Report Date: 9/24/2021 Page 25 of27 analyses applicable to the CWA. SOWA, and RCRA are performed. in accordance to NELAC protocols Pertinent sampling information is located on the attached COC Confidential Business Information; This report is provided for the exclusive use of the addressee Privileges of subsequent use of tl- ne of this company or any member of iB staff, or reproduction of this report in connection with the advertisement promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This ANALYTICAL LABORATORIES Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256-002CMS Date Analyzed: Test Code: 8260D-W-DENIOO Carbon tetrachloride 225 Chloroform 725 Methylene chloride 192 Surr: 1,2-Dichloroethane-<14 505 Surr: 4-Bromofluorobenzene 472 Surr: Dibromofluoromethane 486 Surr: Toluene-d8 491 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686, Fax : (801) 263-8687 e-mail: awal@awal-labs.com, web: www.awal-labs.com QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MS Spike Ref. Amount %REC 09/15/2021 902h µg/L SW8260D 7.85 10.0 200.0 0 113 µg/L SW8260D 3.60 10.0 200.0 516 104 µg/L SW8260D 4.51 10.0 200.0 0 95.9 µg/L SW8260D 500.0 IOI µg/L SW8260D 500.0 94.3 µg/L SW8260D 500.0 97.2 µg/L SW8260D 500.0 98.2 2109256-002CMS: The reporting limits were raised due to high analyle concentrations. Limits 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit Qual Report Date: 9/24/2021 Page 26 of27 analyses applicable to the CWA, SOWA, and RCRA are performed in accordance to NELAC protocols Pertinent samphng infom1ation is located on the attached COC. Confidential Business lnformation: This report is provided for the exclusive use of the addressee Privileges of subsequent use oft~ ne of this company or any member of its staff, or reproduction of this report in connection with the advertisemenl promotion or sale of any product or process, or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This Client: Energy Fuels Resources, Inc. Lab Set ID: 2109256 Project: September Ground Water 2021 Analyte Result Lab Sample ID: 2109256--002CMSD Date Analyzed: Test Code: 8260D-W-DEN100 Carbon tetrachloride 257 Chloroform 775 Methylene chloride 221 Surr: l,2-Dichloroethane-d4 512 Surr: 4-Bromofluorobenzene 484 Surr: Dibromofluoromethane 502 Surr: Toluene-d8 501 Units 3440 South 700 West Salt Lake City, UT 84119 Phone: (801) 263-8686, Toll Free: (888) 263-8686. fax: (801) 263-8687 e-mail : awal@awal-labs.com, web: www.awal-labs.com _QC SUMMARY REPORT Contact: Dept: QC Type: Reporting Amount Method MDL Limit Spiked Tanner Holliday MSVOA MSD Spike Ref. Amount %REC 09/15/2021 922h µg/L SW8260D 7.85 10.0 200.0 0 129 µg/L SW8260D 3.60 10.0 200.0 516 129 µg/L SW8260D 4.51 10.0 200.0 0 110 µg/L SW8260D 500.0 102 µg/L SW8260D 500.0 96.8 µg/L SW8260D 500.0 100 µg/L SW8260D 500.0 100 ' -Matrix spike recovery indicates matrix interference. The method is in control as indicated by the LCS. 2109256-002CMSD: The reporting limits were raised due to high analyte concentrations. Limits 66 -143 74 -120 65 -154 80 -136 85 -121 78 -132 81 -123 Jennifer Osborn Laboratory Director Jose Rocha QA Officer RPO Ref. RPO Amt %RPO Limit 225 13.2 35 725 6.70 35 192 14.0 35 Qual Report Date: 9/24/2021 Page 27 of27 analyses applicable to the CWA, SD\.\1A, and RCRA are performed in accordance to NELAC protocols. Pertinent sampling information is located on the attached COC Confidential Business Information: TI,is report is provided for the exclusive use of the addressee Privileges of subsequent use oftJ- ne of this company or any member of its staff, or reproduction of this report in connection with the advertisemenl promotion or sale of any product or process. or in connection with the re-publication of this report for any purpose other than for the addressee will be granted only on contact This American West Analytical Laboratories WORK ORDER Summary Client: Energy Fuels Resources, Inc. Client ID: ENE300 Contact: Tanner Holliday Project: September Ground Water 2021 QC Level: III Comments: QC 3 (no chromatograms). EDD-Denison. Email Group. Do not use "*R_" samples as MS/MSD.; Sample ID Client Sample ID Collected Date Received Date Test Code 2109256-00lA MW-11_09072021 9nfl021 1320h 9/10/2021 l lO0h 300.0-W 2 SEL Analftes: CL SO4 2109256-002A MW-26_09092021 9/9/2021 0800h 9/10/2021 ll00h NO2/NO3-W-353.2 I SEL Anal;i_tes: NO3NO2N 21092S6-0028 300.0-W I SEL Analytes: CL 21092S6-002C 8260D-W-DEN100 Rpt Emailed: Matrix Aqueous Aqueous WorkOrder: 2109256 Due Date: 9/24/2021 WO Type: Project Set Storage df-cl/so4 df-no2/no3 df-cl VOCFridge Test Group: 8260D-W-DENI00; # of Analytes: 3 /_JI_ ofSurr: 4 2109256-003A MW-30_09082021 9/8/2021 1220h 9/10/2021 1100h NO2/NO3-W-353.2 Aqueous df-no2/no3 1 SEL Ana/.),_tes: NO3NO2N 21092S6-0038 300.0-W df. cl 1 SEL Analytes: CL 2109256-003C 200.8-DIS df. dis met 2 SEL Analytes: SE U 200.&-DIS-PR df-dismet 2109256-004A MW-31_09072021 9n/2021 1420h 9/10/2021 1100h NO2/NO3-W-353.2 Aqueous df-no2/no3 1 SEL Ana1l_tes: NO3NO2N 2109256-0048 300.0-W df-cl/so4 2 SEL Analytes: CL SO4 2109256-004C TDS-W-2540C df-tds 1 SEL Analytes: TDS 2109256-004D 200.&-DIS df-dismet 1 SEL Analytes: U 200.&-DIS-PR df-dismet 2109256-005A MW-65_09072021 9n/2021 1420h 9/10/2021 l lOOh NO2/NO3-W-353.2 Aqueous df-no2/no3 1 SEL Analytes: NO3NO2N 2109256-0058 300.0-W df-cl/so4 2 SEL Analytes: CL SO4 2109256-005C '. TDS-W-25llOC df-tds 1 SEL Analytes: TDS UL Denison Pagel of2 ~ 3 Printed: 09/14/21 11:23 LABORATORY CHECK: %M O RT □ CN □ TAT O QC □ LUO 0 HOK __ HOK __ HOK___ COC Emailed'------ WORK ORDER Summary WorkOrder: 2109256 Page 2 of2 Client: Energy Fuels Resources, Inc. Due Date: 9/24/2021 Sample ID Client Sample ID Collected Date Received Date Test Code Matrix Sel Storage 2109256-005D MW-65_09072021 9/7/20211420h 9/10/2021 1100h 200.8-DIS Aqueous df-dismet I SEL Analytes: U 200.8-DIS-PR df-dis met 2109256-006A Trip Blank 9/9/2021 0800h 9/10/2021 1100h 8260D-W-DENIOO Aqueous VOCFridge 3 Test Group: 8260D-W-DENI00; # of Analytes: 31 # of Su": 4 Printed: 09/14/21 11 :23 LABORATORY CHECK: %M □ RT O CN O TAT □ QC O LUO □ HOK ___ HOK __ _ HOK___ COC Emailed'------ \ ) American West Analytical Laboratories CHAIN OF CUSTODY 463 W. 3600 S. Salt Lake City, UT 841 15 Phone# (801) 263-8686 Toll Free# (888) 263-8686 All analysis wlll be conducted using NELAP accredited methods and all dsla will be reported using AWAL'e standard analyl.e llsls and reporting llmits (PCL} unless specifically requested oth8fWise on this Chain of Custody and/or attached documentation, 2-\ cfrz.. s~ AWAL lab Sample Set# Page of ~ Fax# (801) 263-8687 Email awal@awal-labs.com www.awal-labs.com Client: Energy Fuels Resources, Inc. 6425 S. Hwy. 191 Address: Blanding, UT 84511 Contact: Tanner Holliday Phone#: (435) 678-2221 Cell#: -----------Email: tholliday@eneqyfu.els.com; kweinel@energyfuels.com; Project Name: September Ground Water 2021 Project#: -------------- PO#: 1 Sampler Name: ~Tfaa;n~n;e;r;iHio~Wu.id~a~y~---------------------1 j ~ I I . c: :E 8 -! Sample ID: MW-11_09072021 Date Sampled 9/7/2021 Time Sampled 1320 0 ~ ~ (JJ l IW QC Level: 3 ~ ~ !2. g ..... N g 00 0 0 N ---t--0 0 ~ 3: J ~ I MW-26_09092021 9/9/2021 800 5 IW IX MW-30_09082021 9/8/2021 1220 3 w X MW-31_09072021 9/7/2021 1420 4 w X MW-65_09072021 9/7/2021 1420 4 w X Trip Blank 9/9/2021 800 3 IW c c:i 0 O") ... 0 ~ ~ a X X X X X G' 0 ;Ji ~ ! X X 00 0 0 N ---t--: 0 0 ~ I ~ ~ II s X X X Turn Around Time: ~ c:i 0 ~ ;:::-g ~ e .: a .., ~ ~ 1 0 = lS Standard ~ g ~ ;:::- c:i 0 ~ e i j ~ i lS X c c:i 0 O") .... 0 \.) ~ 0 ::g '1-:5. GI ~ l c c:i 0 O") .... 0 0 0 Ill ~ 0 Ill X X X = 0 J ,; ~ .i: ... GI e j 'ff Q @' -10 a~ .. !!2_ ,2 GI Unless other arrangements have been made, IIDue Date: j signed reports will be emailed by 5:00 pm on 9 \ 4 \ ~ ' the day they am due. 2. , ~ X Include EDD: LOCUS UPLOAD EXCEL Ix Field FIitered For: Dissolved Metals For Compliance With: □ NELAP □ RCRA □ CWA □ SDWA □ ELAPIA2LA □ NLLAP □ Non-Compliance □ Other: Laboratory Use Only lsompllkS Woce: tJJ> 7 1e handdolllta<ed 2 An\blMtore 3 Temporalut'o .(), Z ·c 4 Received Broken/Leaklng (Improperly Sealed.tr.\ y ~ o ~ L---------------.1 .. -0 .. -0 S~y Preserved N Checked et bench y N .i: -t) 11 .. " t) .. 0 ~ >f-'. X X Known Hazards & Sample Comments 6 Received Within ~g Timos '-J N r u.s-\df.1v~\ 1 ~I on Outer Plrckage C-,J N NA 2~~ken on Outer Package l_,) N . NA 3 Present on Sample C\ y N V 4 Unlxoio,n on Samplo ~ Y N 1. NA) ::1 I I I I I I I I I I I I I I I 11~!:~pi~~·==gs 12 13 ls1tinat\no ......._ \altiU~ ~ / ~ -1Ro1ttiquTshc<I by;-\ )h / ~ Orfnl Nami~:_ RollnqulJINld by: ls!!t_naluro IPrintN11nu,: jR<tllnqulohod by: IS_!g_nahmt IPdnlNa111_~: Rellnqul•had by: ls1nna1ure PrtntName: T_!_Onfll" Homda.,y I Date: iTJmo: Dato: ·runo: Date: rn,no, Date: fnme: ~eceived by. 9/9/2021lsignalure 1100IP.r!nt Name: Received by: ISi!1_nature IPrfntName: jRecelved by: :Signature .E_rlntName: Received by: $~nature PrlnlN"!lle: A (· l)A,t ,·J...r-.~J_,{_j ~ 7r2 AC\L~. t::::ll'L.tLAi'O Oete: Time: Cate: [Time: Cate: ITime: Date: 7 I iD~' ITime: \ : ..:;,, I • {.A. - Special Instructions: Sample containers for metals were field filtered. See the Analytical Scope of Work for Reporting Limits and voe analyte list. Analysis Ammonia COD Cyanide Metals NOz/NO3 O&G Phenols Sulfide TKN TPO4 CrVI+ Procedure: Frequency: Preserva_1ion Check Sheet s le Set E Preservative -O'Ol -oo-:S -coif -ei,15 pH<2 H2SO4 oH<2H2SO4 pH>l0NaOH pH<2 HNO3 I --1-e~ "'-'·e.s 1--... e.c.,, oH<2H2SO4 ~.~ <J-eh Je..s ,;J e..~ pH<2HCL I I I pH <2 H2SO4 pH >9 NaOH, ZnAC pH<2 H2SO4 pH<2 H2SO4 pH >9 CNRi )2804 Pour a small amount of sample in the sample lid Pour sample from lid gently over wide range pH paper Do Not dip the pH paper in the sample bottle or lid doH - 1) 2) 3) 4) 5) 6) 7) If sample is not preserved, properly list its extension and receiving pH in the appropriate column above Flag COC, notify client if requested Place client conversation on COC Samples may be adjusted All samples requiring preservation * + • # • The sample required additional preservative upon receipt. The sample was received unpreserved. The sample was received unpreserved and therefore preserved upon receipt. The sample pH was unadjustable to a pH < 2 due to the sample matrix. The sample pH was unadjustable to a pH > __ due to the sample matrix interference. Lab Set ID: pH Lot#: 21092..-5\o (pJm rev 1~28-2020 TabG Quality Assurance and Data Validation Tables G-1 A: Quarter!, Field QA/QC Evaluation 1x Casing 2x Casing Location Volume Volume Pumped Volume Volume Check Conductivity RPO pH RPO Temperature RPO Redox RPO Turbidity RPO MW-11 29.20 58.59 58.4 okay 3253 3254 0.03 7.14 7.15 0.14 15.01 14.99 0.13 495 494 0.20 913.5 920.6 0.77 MW-12 13.58 28.21 27.16 okay 4168 4165 0.07 6.61 6.62 0.15 16.29 16.27 0.12 451 449 0.44 0.0 0.0 0.00 MW-14 17.55 36.89 35.1 okay 3715 3710 0.13 7.08 7.06 0.28 15.18 15.20 0.13 484 484 0.00 0 0 0.00 MW-24 6.39 13,00 1'2.78 Pumped Ory 4427 4431 0.09 5.90 6 .. 85 o._es 16.95 16.~ 0.65 NM NG NM NC MW-24A 7.01 14.-40 14.02 Pump,«t Dry 4412 4413 0.02-5.25 5.27. 0:38 15.28 15.22 ~39 NM NC NM NC MW-25 21.97 45.57 43.94 okay 3162 3170 0.25 6.90 6.88 0.29 15.05 15.00 0.33 497 497 0.00 9.1 9.0 1.10 MW-26 NA Continuously Pumped well --3344 NC 7.15 NC 18.03 NC 475 NC 0 NC MW-27 24.16 49.91 48.32 okay 1159 1159 0.00 7.17 7.18 0.14 15.34 15.31 0.20 470 470 0.00 0 0 0.00 MW-28 23.10 46.65 46.2 okay 4187 4196 0.21 6.54 6.53 0.15 16.36 16.32 0.24 506 505 0.20 0 0 0.00 MW-29 18.14 39.06 36.28 okay 4575 4578 0.07 6.78 6.77 0.15 15.01 15.01 0.00 400 394 1.51 5.3 5.4 1.87 MW-30 22.67 45.57 45.34 okay 2204 2207 0.14 6.97 6.98 0.14 14.97 14.98 0.07 497 496 0.20 0 0 0.00 MW-31 39.60 80.29 79.2 okay 3335 3315 0.60 7.11 7.10 0.14 15.45 15.40 0.32 491 491 0.00 0 0 0.00 MW-32 31.53 65.10 63.06 okay 3721 3720 0.03 6.98 6.95 0.43 15.41 15.36 0.32 257 254 1.17 14.3 14.5 1.39 MW-36 7.27 16.27 14.54 okay 3890 3908 0.46 7.20 7.19 0.14 15.38 15.34 0.26 486 486 0.00 0 0 0.00 MW:.38 2.59 5.00 5.18 Pumped Orv· 4373 4370 0 .. 07 6.2-5 6,23 0.32 16.75 16.70 0.30 NM NC NM Ne MW-39 24.63 49.91 49.26 okay 4770 4773 0.06 5.45 5.43 0.37 15.80 15.78 0.13 389 392 0.77 1.1 1. 1 0.00 MW-40 26.17 53.16 52.34 okay 3835 3837 0.05 7.09 7.08 0.14 15.18 15.13 0.33 494 494 0.00 0 0 0.00 MW-26, 1s a continual!,'. pumped well. MW-24 MW-24A MW-38 were um ed d!Y and sam led after recove ---NM == Not Measured. The QAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO == Relative Percent Difference The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The OAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. Dissolved Oxygen RPO 7.3 7.0 4.20 21 .7 22.0 1.37 5.8 6.0 3.39 NM NQ NM NO 5.9 5.8 1.71 28.5 NC 103.3 103.2 0.10 30.5 30.0 1.65 3.1 3.1 0.00 57.0 57.0 0.00 118.0 118.0 0.00 32.0 31 .8 0.63 81.0 80.0 1.24 NM NC 8.1 8.1 0.00 117.0 117.0 0.00 G-18: Accelerated Field QA/QC Evaluation Au9ust 1x Casing 2x Casing Volume Location Volume Volume Pumped Volume Check Conductivity RPD pH MW-11 29.24 58.59 58.48 okay 3116 I 3114 0.06 7.30 I 7.29 MW,26 NA Continuously Pumped well --3402 NC 6.94 MW-30 22.77 45.57 45.54 okay 2209 I 2213 0.18 6.82 I 6.84 MW-31 39.66 80.29 79.32 okay 3250 I 3260 0.31 7.13 I 7.13 September MW-11 29.20 58.59 58.4 okay 3129 I 3123 0.19 6.95 I MW-26 NA Continuously Pumped well -3487 NC 6.54 MW-30 22.71 45.57 45.42 okay 2243 I 2240 0.13 6.67 I MW-31 39.56 80.29 79.12 okay 3399 I 3399 0.00 6.61 I MW-26 1s a continually pumped well. iTlni e are no ehs t at we e ed d ar;id sam led after l'i ova . NM= Not Measured. The OAP does not require the measurement of redox potential or turbidity in wells that were purged to dryness. RPO = Relative Percent Difference 7.00 6.70 6.62 RPO 0.14 NC 0.29 0.00 0.72 NC 0.45 0.15 Dissolved Temperature RPO Redox RPD Turbidity RPO Oxygen 15.01 I 15.04 0.20 326 I 326 0.00 4.0 I 4.0 0.00 6.0 I 5.9 16.37 NC 507 NC 1.0 NC 34.5 15.11 I 15.10 0.07 532 I 530 0.38 0 I 0 0.00 55.o I 55.0 15.43 I 15.45 0.13 504 I 504 0.00 13.0 I 13.0 0.00 116.0 I 116.0 15.10 I 15.08 0.13 476 I 474 0.42 92.0 I 94.0 2.15 7.6 I 7.6 15.95 NC 488 NC 0 NC 27.0 15.00 I 15.00 0.00 466 I 465 0.21 0 I 0 0.00 55.3 I 55.5 15.13 I 15.13 0.00 460 I 459 0.22 4.8 I 4.8 0.00 114.o I 114.o The OAP states that turbidity should be less than 5 Nephelometric Turbidity Units ("NTU") prior to sampling unless the well is characterized by water that has a higher turbidity. The OAP does not require that turbidity measurements be less than 5 NTU prior to sampling. As such, the noted observations regarding turbidity measurements less than 5 NTU are included for information purposes only. RPO 1.68 NC 0.00 0.00 0.00 NC 0.36 0.00 G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check Trip Blank Acetone 7/27/2021 7/30/2021 3 14 OK Trip Blank Benzene 7/27/2021 7/30/2021 3 14 OK Trip Blank Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK Trip Blank Chloroform 7/27/2021 7/30/2021 3 14 OK Trip Blank Chloromethane 7/27/202 I 7/30/2021 3 14 OK Trip Blank Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK Trip Blank Methylene chloride 7/27/2021 7/30/2021 3 14 OK Trip Blank Naphthalene 7/27/2021 7/30/2021 3 14 OK Trip Blank Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK Trip Blank Toluene 7/27/2021 7/30/2021 3 14 OK Trip Blank Xylenes, Total 7/27/2021 7/30/2021 3 14 OK MW-11 Acetone 7/27/2021 7/30/2021 3 14 OK MW-11 Arsenic 7/27/2021 8/13/2021 17 180 OK MW-11 Benzene 7/27/2021 7/30/2021 3 14 OK MW-11 Beryllium 7/27/2021 8/13/2021 17 180 OK MW-11 Bicarbonate as CaCO3 7/27/2021 8/2/2021 6 14 OK MW-11 Cadmium 7/27/2021 8/13/2021 17 180 OK MW-11 Calcium 7/27/2021 8/10/2021 14 180 OK MW-11 Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK MW-11 Carbonate as CO3 7/27/2021 8/2/2021 6 14 OK MW-11 Chloride 7/27/2021 8/10/2021 14 28 OK MW-11 Chloroform 7/27/2021 7/30/2021 3 14 OK MW-11 Chloromethane 7/27/2021 7/30/2021 3 14 OK MW-11 Chromium 7/27/2021 8/13/2021 17 180 OK MW-11 Cobalt 7/27/2021 8/13/2021 17 180 OK MW-11 Copper 7/27/2021 8/13/2021 17 180 OK MW-11 Fluoride 7/27/2021 8/11/2021 15 28 OK MW-11 Gross Radium Alpha 7/27/2021 8/23/2021 27 180 OK MW-11 Iron 7/27/2021 8/13/2021 17 180 OK MW-11 Lead 7/27/2021 8/13/2021 17 180 OK MW-11 Magnesium 7/27/2021 8/10/2021 14 180 OK MW-11 Manganese 7/27/2021 8/13/2021 17 180 OK MW-11 Mercury 7/27/2021 8/3/2021 7 180 OK MW-11 Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK MW-11 Methylene chloride 7/27/2021 7/30/2021 3 14 OK MW-11 Molybdenum 7/27/2021 8/13/2021 17 180 OK MW-11 Naphthalene 7/27/2021 7/30/2021 3 14 OK MW-11 Nickel 7/27/2021 8/13/2021 17 180 OK MW-11 Nitrate + Nitrite as N 7/27/2021 8/2/2021 6 28 OK MW-11 Nitrogen, Ammonia as N 7/27/2021 8/4/2021 8 28 OK MW-11 Potassium 7/27/2021 8/10/2021 14 180 OK MW-11 Selenium 7/27/2021 8/13/2021 17 180 OK MW-11 Silver 7/27/2021 8/16/2021 20 180 OK MW-11 Sodium 7/27/2021 8/10/2021 14 180 OK MW-11 Sulfate 7/27/2021 8/10/2021 14 28 OK MW-11 Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK MW-11 Thallium 7/27/2021 8/13/2021 17 180 OK MW-11 Tin 7/27/2021 8/13/2021 17 180 OK MW-11 Toluene 7/27/2021 7/30/2021 3 14 OK MW-11 Total Dissolved Solids 7/27/2021 7/30/2021 3 7 OK MW-11 Uranium 7/27/2021 8/13/2021 17 180 OK MW-11 Vanadium 7/27/2021 8/10/2021 14 180 OK MW-11 Xylenes, Total 7/27/2021 7/30/2021 3 14 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-11 Zinc 7/27/2021 8/13/2021 17 180 OK MW-12 Selenium 7/21/2021 8/2/2021 12 180 OK MW-12 Uranium 7/21/2021 8/2/2021 12 180 OK MW-14 Acetone 7/27/2021 7/30/2021 3 14 OK MW-14 Arsenic 7/27/2021 8/13/2021 17 180 OK MW-14 Benzene 7/27/2021 7/30/2021 3 14 OK MW-14 Beryllium 7/27/2021 8/13/2021 17 180 OK MW-14 Bicarbonate as CaCO3 7/27/2021 8/2/2021 6 14 OK MW-14 Cadmium 7/27/2021 8/13/2021 17 180 OK MW-14 Calcium 7/27/2021 8/10/2021 14 180 OK MW-14 Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK MW-14 Carbonate as CO3 7/27/2021 8/2/2021 6 14 OK MW-14 Chloride 7/27/2021 8/10/2021 14 28 OK MW-14 Chloroform 7/27/2021 7/30/2021 3 14 OK MW-14 Chloromethane 7/27/2021 7/30/2021 3 14 OK MW-14 Chromium 7/27/2021 8/13/2021 17 180 OK MW-14 Cobalt 7/27/2021 8/13/2021 17 180 OK MW-14 Copper 7/27/2021 8/13/2021 17 180 OK MW-14 Fluoride 7/27/2021 8/11/2021 15 28 OK MW-14 Gross Radium Alpha 7/27/2021 8/23/2021 27 180 OK MW-14 Iron 7/27/2021 8/13/2021 17 180 OK MW-14 Lead 7/27/2021 8/13/2021 17 180 OK MW-14 Magnesium 7/27/2021 8/10/2021 14 180 OK MW-14 Manganese 7/27/2021 8/13/2021 17 180 OK MW-14 Mercury 7/27/2021 8/3/2021 7 180 OK MW-14 Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK MW-14 Methylene chloride 7/27/2021 7/30/2021 3 14 OK MW-14 Molybdenum 7/27/2021 8/13/2021 17 180 OK MW-14 Naphthalene 7/27/2021 7/30/2021 3 14 OK MW-14 Nickel 7/27/2021 8/13/2021 17 180 OK MW-14 Nitrate + Nitrite as N 7/27/2021 8/2/2021 6 28 OK MW-14 Nitrogen, Ammonia as N 7/27/2021 8/4/2021 8 28 OK MW-14 Potassium 7/27/2021 8/10/2021 14 180 OK MW-14 Selenium 7/27/2021 8/13/2021 17 180 OK MW-14 Silver 7/27/2021 8/16/2021 20 180 OK MW-14 Sodium 7/27/2021 8/10/2021 14 180 OK MW-14 Sulfate 7/27/2021 8/10/2021 14 28 OK MW-14 Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK MW-14 Thallium 7/27/2021 8/13/2021 17 180 OK MW-14 Tin 7/27/2021 8/13/2021 17 180 OK MW-14 Toluene 7/27/2021 7/30/2021 3 14 OK MW-14 Total Dissolved Solids 7/27/2021 7/30/2021 3 7 OK MW-14 Uranium 7/27/2021 8/13/2021 17 180 OK MW-14 Vanadium 7/27/2021 8/10/2021 14 180 OK MW-14 Xylenes, Total 7/27/2021 7/30/2021 3 14 OK MW-14 Zinc 7/27/2021 8/13/2021 17 180 OK MW-24 Acetone 7/29/2021 7/30/2021 1 14 OK MW-24 Arsenic 7/29/2021 8/13/2021 15 180 OK MW-24 Benzene 7/29/2021 7/30/2021 1 14 OK MW-24 Beryllium 7/29/2021 8/13/2021 15 180 OK MW-24 Bicarbonate as CaCO3 7/29/2021 8/2/2021 4 14 OK MW-24 Cadmium 7/29/2021 8/13/2021 15 180 OK MW-24 Calcium 7/29/2021 8/10/2021 12 180 OK G-2A: Quarterly Holding Time Evaluation I Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-24 Carbon tetrachloride 7/29/2021 7/30/2021 1 14 OK MW-24 Carbonate as CO3 7/29/2021 8/2/2021 4 14 OK MW-24 Chloride 7/29/2021 8/11/2021 13 28 OK MW-24 Chloroform 7/29/2021 7/30/2021 1 14 OK MW-24 Chloromethane 7/29/2021 7/30/2021 1 14 OK MW-24 Chromium 7/29/2021 8/13/2021 15 180 OK MW-24 Cobalt 7/29/2021 8/13/2021 15 180 OK MW-24 Coooer 7/29/2021 8/13/2021 15 180 OK MW-24 Fluoride 7/29/2021 8/11/2021 13 28 OK MW-24 Gross Radium Alpha 7/29/2021 8/23/2021 25 180 OK MW-24 Iron 7/29/2021 8/13/2021 15 180 OK MW-24 Lead 7/29/2021 8/13/2021 15 180 OK MW-24 Magnesium 7/29/2021 8/10/2021 12 180 OK MW-24 Manganese 7/29/2021 8/13/2021 15 180 OK MW-24 Mercury 7/29/2021 8/3/2021 5 180 OK MW-24 Methyl ethyl ketone 7/29/2021 7/30/2021 l 14 OK MW-24 Methylene chloride 7/29/2021 7/30/2021 1 14 OK MW-24 Molybdenum 7/29/2021 8/13/2021 15 180 OK MW-24 Naphthalene 7/29/2021 7/30/2021 1 14 OK MW-24 Nickel 7/29/2021 8/13/2021 15 180 OK MW-24 Nitrate + Nitrite as N 7/29/2021 8/6/2021 8 28 OK MW-24 Nitrogen, Ammonia as N 7/29/2021 8/4/2021 6 28 OK MW-24 Potassium 7/29/2021 8/12/2021 14 180 OK MW-24 Selenium 7/29/2021 8/13/2021 15 180 OK MW-24 Silver 7/29/2021 8/16/2021 18 180 OK MW-24 Sodium 7/29/2021 8/10/2021 12 180 OK MW-24 Sulfate 7/29/2021 8/11/2021 13 28 OK MW-24 Tetrahydrofuran 7/29/2021 7/30/2021 1 14 OK MW-24 Thallium 7/29/2021 8/13/2021 15 180 OK MW-24 Tin 7/29/2021 8/13/2021 15 180 OK MW-24 Toluene 7/29/2021 7/30/2021 1 14 OK MW-24 Total Dissolved Solids 7/29/2021 7/30/2021 1 7 OK MW-24 Uranium 7/29/2021 8/13/2021 15 180 OK MW-24 Vanadium 7/29/2021 8/11/2021 13 180 OK MW-24 Xylenes, Total 7/29/2021 7/30/2021 1 14 OK MW-24 Zinc 7/29/2021 8/13/2021 15 180 OK MW-24A Acetone 7/29/2021 7/30/2021 1 14 OK MW-24A Arsenic 7/29/2021 8/16/2021 18 180 OK MW-24A Benzene 7/29/2021 7/30/2021 1 14 OK MW-24A Beryllium 7/29/2021 8/16/2021 18 180 OK MW-24A Bicarbonate as CaCO3 7/29/2021 8/2/2021 4 14 OK MW-24A Cadmium 7/29/2021 8/13/2021 15 180 OK MW-24A Calcium 7/29/2021 8/10/2021 12 180 OK MW-24A Carbon tetrachloride 7/29/2021 7/30/2021 1 14 OK MW-24A Carbonate as CO3 7/29/2021 8/2/2021 4 14 OK MW-24A Chloride 7/29/2021 8/11/2021 13 28 OK MW-24A Chloroform 7/29/2021 7/30/2021 1 14 OK MW-24A Chloromethane 7/29/2021 7/30/2021 1 14 OK MW-24A Chromium 7/29/2021 8/13/2021 15 180 OK MW-24A Cobalt 7/29/2021 8/13/2021 15 180 OK MW-24A Copper 7/29/2021 8/13/2021 15 180 OK MW-24A Fluoride 7/29/2021 8/11/2021 13 28 OK MW-24A Gross Radium Alpha 7/29/2021 8/23/2021 25 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-24A Iron 7/29/2021 8/13/2021 15 180 OK MW-24A Lead 7/29/2021 8/13/2021 15 180 OK MW-24A Ma_gnesium 7/29/2021 8/10/2021 12 180 OK MW-24A Man_ganese 7/29/2021 8/13/2021 15 180 OK MW-24A Mercury 7/29/2021 8/3/2021 5 180 OK MW-24A Methyl ethyl ketone 7/29/2021 7/30/2021 1 14 OK MW-24A Methylene chloride 7/29/2021 7/30/2021 1 14 OK MW-24A Molybdenum 7/29/2021 8/13/2021 15 180 OK MW-24A Naphthalene 7/29/2021 7/30/2021 1 14 OK MW-24A Nickel 7/29/2021 8/13/2021 15 180 OK MW-24A Nitrate + Nitrite as N 7/29/2021 8/6/2021 8 28 OK MW-24A Nitrogen, Ammonia as N 7/29/2021 8/4/2021 6 28 OK MW-24A Potassium 7/29/2021 8/12/2021 14 180 OK MW-24A Selenium 7/29/2021 8/13/2021 15 180 OK MW-24A Silver 7/29/2021 8/16/2021 18 180 OK MW-24A Sodium 7/29/2021 8/10/2021 12 180 OK MW-24A Sulfate 7/29/2021 8/11/2021 13 28 OK MW-24A Tetrahydrofuran 7/29/2021 7/30/2021 1 14 OK MW-24A Thallium 7/29/2021 8/13/2021 15 180 OK MW-24A Tin 7/29/2021 8/13/2021 15 180 OK MW-24A Toluene 7/29/2021 7/30/2021 1 14 OK MW-24A Total Dissolved Solids 7/29/2021 7/30/2021 1 7 OK MW-24A Uranium 7/29/2021 8/13/2021 15 180 OK MW-24A Vanadium 7/29/2021 8/11/2021 13 180 OK MW-24A Xylenes, Total 7/29/2021 7/30/2021 1 14 OK MW-24A Zinc 7/29/2021 8/13/2021 15 180 OK MW-25 Acetone 7/28/2021 7/30/2021 2 14 OK MW-25 Arsenic 7/28/2021 8/16/2021 19 180 OK MW-25 Benzene 7/28/2021 7/30/2021 2 14 OK MW-25 Beryllium 7/28/2021 8/16/2021 19 180 OK MW-25 Bicarbonate as CaCO3 7/28/2021 8/2/2021 5 14 OK MW-25 Cadmium 7/28/2021 8/13/2021 16 180 OK MW-25 Calcium 7/28/2021 8/10/2021 13 180 OK MW-25 Carbon tetrachloride 7/28/2021 7/30/2021 2 14 OK MW-25 Carbonate as CO3 7/28/2021 8/2/2021 5 14 OK MW-25 Chloride 7/28/2021 8/10/2021 13 28 OK MW-25 Chloroform 7/28/2021 7/30/2021 2 14 OK MW-25 Chloromethane 7/28/2021 7/30/2021 2 14 OK MW-25 Chromium 7/28/2021 8/13/2021 16 180 OK MW-25 Cobalt 7/28/2021 8/13/2021 16 180 OK MW-25 Cooner 7/28/2021 8/13/2021 16 180 OK MW-25 Fluoride 7/28/2021 8/11/2021 14 28 OK MW-25 Gross Radium Alpha 7/28/2021 8/23/2021 26 180 OK MW-25 Iron 7/28/2021 8/16/2021 19 180 OK MW-25 Lead 7/28/2021 8/16/2021 19 180 OK MW-25 Ma_gnesium 7/28/2021 8/10/2021 13 180 OK MW-25 Man_ganese 7/28/2021 8/13/2021 16 180 OK MW-25 Mercury 7/28/2021 8/3/2021 6 180 OK MW-25 Methyl ethyl ketone 7/28/2021 7/30/2021 2 14 OK MW-25 Methylene chloride 7/28/2021 7/30/2021 2 14 OK MW-25 Molybdenum 7/28/2021 8/13/2021 16 180 OK MW-25 Naphthalene 7/28/2021 7/30/2021 2 14 OK MW-25 Nickel 7/28/2021 8/13/2021 16 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-25 Nitrate + Nitrite as N 7/28/2021 8/2/2021 5 28 OK MW-25 Nitrogen, Ammonia as N 7/28/2021 8/4/2021 7 28 OK MW-25 Potassium 7/28/2021 8/12/2021 15 180 OK MW-25 Selenium 7/28/2021 8/13/2021 16 180 OK MW-25 Silver 7/28/2021 8/16/2021 19 180 OK MW-25 Sodium 7/28/2021 8/10/2021 13 180 OK MW-25 Sulfate 7/28/2021 8/10/2021 13 28 OK MW-25 Tetrahydrofuran 7/28/2021 7/30/2021 2 14 OK MW-25 Thallium 7/28/2021 8/16/2021 19 180 OK MW-25 Tin 7/28/2021 8/13/2021 16 180 OK MW-25 Toluene 7/28/2021 7/30/2021 2 14 OK MW-25 Total Dissolved Solids 7/28/2021 7/30/2021 2 7 OK MW-25 Uranium 7/28/2021 8/16/2021 19 180 OK MW-25 Vanadium 7/28/2021 8/10/2021 13 180 OK MW-25 Xylenes, Total 7/28/2021 7/30/2021 2 14 OK MW-25 Zinc 7/28/2021 8/13/2021 16 180 OK MW-26 Acetone 7/28/2021 7/30/2021 2 14 OK MW-26 Arsenic 7/28/2021 8/13/2021 16 180 OK MW-26 Benzene 7/28/2021 7/30/2021 2 14 OK MW-26 Beryllium 7/28/2021 8/13/2021 16 180 OK MW-26 Bicarbonate as CaCO3 7/28/2021 8/2/2021 5 14 OK MW-26 Cadmium 7/28/2021 8/13/2021 16 180 OK MW-26 Calcium 7/28/2021 8/10/2021 13 180 OK MW-26 Carbon tetrachloride 7/28/2021 7/30/2021 2 14 OK MW-26 Carbonate as CO3 7/28/2021 8/2/2021 5 14 OK MW-26 Chloride 7/28/2021 8/11/2021 14 28 OK MW-26 Chloroform 7/28/2021 8/2/2021 5 14 OK MW-26 Chloromethane 7/28/2021 7/30/2021 2 14 OK MW-26 Chromium 7/28/2021 8/13/2021 16 180 OK MW-26 Cobalt 7/28/2021 8/13/2021 16 180 OK MW-26 Coooer 7/28/2021 8/13/2021 16 180 OK MW-26 Fluoride 7/28/2021 8/11/2021 14 28 OK MW-26 Gross Radium Alpha 7/28/2021 8/23/2021 26 180 OK MW-26 Iron 7/28/2021 8/13/2021 16 180 OK MW-26 Lead 7/28/2021 8/13/2021 16 180 OK MW-26 Magnesium 7/28/2021 8/10/2021 13 180 OK MW-26 Manganese 7/28/2021 8/13/2021 16 180 OK MW-26 Mercury 7/28/2021 8/3/2021 6 180 OK MW-26 Methyl ethyl ketone 7/28/2021 7/30/2021 2 14 OK MW-26 Methylene chloride 7/28/2021 7/30/2021 2 14 OK MW-26 Molybdenum 7/28/2021 8/13/2021 16 180 OK MW-26 Naphthalene 7/28/2021 7/30/2021 2 14 OK MW-26 Nickel 7/28/2021 8/13/2021 16 180 OK MW-26 Nitrate + Nitrite as N 7/28/2021 8/2/2021 5 28 OK MW-26 Nitrogen, Ammonia as N 7/28/2021 8/4/2021 7 28 OK MW-26 Potassium 7/28/2021 8/12/2021 15 180 OK MW-26 Selenium 7/28/2021 8/13/2021 16 180 OK MW-26 Silver 7/28/2021 8/16/2021 19 180 OK MW-26 Sodium 7/28/2021 8/10/2021 13 180 OK MW-26 Sulfate 7/28/2021 8/11/2021 14 28 OK MW-26 Tetrah ydrofuran 7/28/2021 7/30/2021 2 14 OK MW-26 Thallium 7/28/2021 8/13/2021 16 180 OK MW-26 Tin 7/28/2021 8/13/2021 16 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-26 Toluene 7/28/2021 7/30/2021 2 14 OK MW-26 Total Dissolved Solids 7/28/2021 7/30/2021 2 7 OK MW-26 Uranium 7/28/2021 8/13/2021 16 180 OK MW-26 Vanadium 7/28/2021 8/10/2021 13 180 OK MW-26 Xylenes, Total 7/28/2021 7/30/2021 2 14 OK MW-26 Zinc 7/28/2021 8/13/2021 16 180 OK MW-27 Nitrate + Nitrite as N 7/22/2021 8/2/2021 11 28 OK MW-28 Chloride 7/23/2021 8/3/2021 11 28 OK MW-28 Nitrate + Nitrite as N 7/23/2021 8/2/2021 10 28 OK MW-28 Selenium 7/23/2021 8/2/2021 10 180 OK MW-28 Uranium 7/23/2021 8/2/2021 10 180 OK MW-29 Uranium 7/22/2021 8/2/2021 11 180 OK MW-30 Acetone 7/29/2021 7/30/2021 1 14 OK MW-30 Arsenic 7/29/2021 8/16/2021 18 180 OK MW-30 Benzene 7/29/2021 7/30/2021 1 14 OK MW-30 Beryllium 7/29/2021 8/13/2021 15 180 OK MW-30 Bicarbonate as CaCO3 7/29/2021 8/2/2021 4 14 OK MW-30 Cadmium 7/29/2021 8/13/2021 15 180 OK MW-30 Calcium 7/29/2021 8/10/2021 12 180 OK MW-30 Carbon tetrachloride 7/29/2021 7/30/2021 1 14 OK MW-30 Carbonate as CO3 7/29/2021 8/2/2021 4 14 OK MW-30 Chloride 7/29/2021 8/11/2021 13 28 OK MW-30 Chloroform 7/29/2021 7/30/2021 1 14 OK MW-30 Chloromethane 7/29/2021 7/30/2021 1 14 OK MW-30 Chromium 7/29/2021 8/13/2021 15 180 OK MW-30 Cobalt 7/29/2021 8/13/2021 15 180 OK MW-30 Copper 7/29/2021 8/13/2021 15 180 OK MW-30 Fluoride 7/29/2021 8/11/2021 13 28 OK MW-30 Gross Radium Alpha 7/29/2021 8/23/2021 25 180 OK MW-30 Iron 7/29/2021 8/13/2021 15 180 OK MW-30 Lead 7/29/2021 8/13/2021 15 180 OK MW-30 Magnesium 7/29/2021 8/10/2021 12 180 OK MW-30 Manganese 7/29/2021 8/13/2021 15 180 OK MW-30 Mercury 7/29/2021 8/3/2021 5 180 OK MW-30 Methyl eU1yl ketone 7/29/2021 7/30/2021 1 14 OK MW-30 Methylene chloride 7/29/2021 7/30/2021 1 14 OK MW-30 Molybdenum 7/29/2021 8/13/2021 15 180 OK MW-30 Naphthalene 7/29/2021 7/30/2021 l 14 OK MW-30 Nickel 7/29/2021 8/13/2021 15 180 OK MW-30 Nitrate + Nitrite as N 7/29/2021 8/2/2021 4 28 OK MW-30 Nitrogen, Ammonia as N 7/29/2021 8/4/2021 6 28 OK MW-30 Potassium 7/29/2021 8/12/2021 14 180 OK MW-30 Selenium 7/29/2021 8/13/2021 15 180 OK MW-30 Silver 7/29/2021 8/16/2021 18 180 OK MW-30 Sodium 7/29/2021 8/10/2021 12 180 OK MW-30 Sulfate 7/29/2021 8/11/2021 13 28 OK MW-30 Tetrahvdrofuran 7/29/2021 7/30/2021 1 14 OK MW-30 Thallium 7/29/2021 8/13/2021 15 180 OK MW-30 Tin 7/29/2021 8/13/2021 15 180 OK MW-30 Toluene 7/29/2021 7/30/2021 1 14 OK MW-30 Total Dissolved Solids 7/29/2021 7/30/2021 1 7 OK MW-30 Uranium 7/29/2021 8/13/2021 15 180 OK MW-30 Vanadium 7/29/2021 8/10/2021 12 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Davs) Time (Days) Check MW-30 Xylenes, Total 7/29/2021 7/30/2021 1 14 OK MW-30 Zinc 7/29/2021 8/13/2021 15 180 OK MW-31 Acetone 7/27/2021 7/30/2021 3 14 OK MW-31 Arsenic 7/27/2021 8/13/2021 17 180 OK MW-31 Benzene 7/27/2021 7/30/2021 3 14 OK MW-31 Beryllium 7/27/2021 8/13/2021 17 180 OK MW-31 Bicarbonate as CaCO3 7/27/2021 8/2/2021 6 14 OK MW-31 Cadmium 7/27/2021 8/13/2021 17 180 OK MW-31 Calcium 7/27/2021 8/10/2021 14 180 OK MW-31 Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK MW-31 Carbonate as CO3 7/27/2021 8/2/2021 6 14 OK MW-31 Chloride 7/27/2021 8/10/2021 14 28 OK MW-31 Chloroform 7/27/2021 7/30/2021 3 14 OK MW-31 Chloromethane 7/27/2021 7/30/2021 3 14 OK MW-31 Chromium 7/27/2021 8/13/2021 17 180 OK MW-31 Cobalt 7/27/2021 8/13/2021 17 180 OK MW-31 Copper 7/27/2021 8/13/2021 17 180 OK MW-31 Fluoride 7/27/2021 8/11/2021 15 28 OK MW-31 Gross Radium Alpha 7/27/2021 8/23/2021 27 180 OK MW-31 Iron 7/27/2021 8/13/2021 17 180 OK MW-31 Lead 7/27/2021 8/13/2021 17 180 OK MW-31 Magnesium 7/27/2021 8/10/2021 14 180 OK MW-31 Manganese 7/27/2021 8/13/2021 17 180 OK MW-31 Mercury 7/27/2021 8/3/2021 7 180 OK MW-31 Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK MW-31 Methylene chloride 7/27/2021 7/30/2021 3 14 OK MW-31 Molybdenum 7/27/2021 8/13/2021 17 180 OK MW-31 Naphthalene 7/27/2021 7/30/2021 3 14 OK MW-31 Nickel 7/27/2021 8/13/2021 17 180 OK MW-31 Nitrate + Nitrite as N 7/27/2021 8/2/2021 6 28 OK MW-31 Nitrogen, Ammonia as N 7/27/2021 8/4/2021 8 28 OK MW-31 Potassium 7/27/2021 8/10/2021 14 180 OK MW-31 Selenium 7/27/2021 8/13/2021 17 180 OK MW-31 Silver 7/27/2021 8/16/2021 20 180 OK MW-31 Sodium 7/27/2021 8/10/2021 14 180 OK MW-31 Sulfate 7/27/2021 8/10/2021 14 28 OK MW-31 Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK MW-31 Thallium 7/27/2021 8/13/2021 17 180 OK MW-31 Tin 7/27/2021 8/13/2021 17 180 OK MW-31 Toluene 7/27/2021 7/30/2021 3 14 OK MW-31 Total Dissolved Solids 7/27/2021 7/30/2021 3 7 OK MW-31 Uranium 7/27/2021 8/13/2021 17 180 OK MW-31 Vanadium 7/27/2021 8/10/2021 14 180 OK MW-31 Xylenes, Total 7/27/2021 7/30/2021 3 14 OK MW-31 Zinc 7/27/2021 8/13/2021 17 180 OK MW-32 Chloride 7/28/2021 8/11/2021 14 28 OK MW-36 Acetone 7/27/2021 7/30/2021 3 14 OK MW-36 Arsenic 7/27/2021 8/13/2021 17 180 OK MW-36 Benzene 7/27/2021 7/30/2021 3 14 OK MW-36 Beryllium 7/27/2021 8/13/2021 17 180 OK MW-36 Bicarbonate as CaCO3 7/27/2021 8/2/2021 6 14 OK MW-36 Cadmium 7/27/2021 8/13/2021 17 180 OK MW-36 Calcium 7/27/2021 8/10/2021 14 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-36 Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK MW-36 Carbonate as CO3 7/27/2021 8/2/2021 6 14 OK MW-36 Chloride 7/27/2021 8/10/2021 14 28 OK MW-36 Chloroform 7/27/2021 7/30/2021 3 14 OK MW-36 Chloromethane 7/27/2021 7/30/2021 3 14 OK MW-36 Chromium 7/27/2021 8/13/2021 17 180 OK MW-36 Cobalt 7/27/2021 8/13/2021 17 180 OK MW-36 Copper 7/27/2021 8/13/2021 17 180 OK MW-36 Fluoride 7/27/2021 8/11/2021 15 28 OK MW-36 Gross Radium Alpha 7/27/2021 8/23/2021 27 180 OK MW-36 Iron 7/27/2021 8/13/2021 17 180 OK MW-36 Lead 7/27/2021 8/13/2021 17 180 OK MW-36 Magnesium 7/27/2021 8/10/2021 14 180 OK MW-36 Manganese 7/27/2021 8/13/2021 17 180 OK MW-36 Mercury 7/27/2021 8/3/2021 7 180 OK MW-36 Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK MW-36 Methylene chloride 7/27/2021 7/30/2021 3 14 OK MW-36 Molybdenum 7/27/2021 8/13/2021 17 180 OK MW-36 Naphthalene 7/27/2021 7/30/2021 3 14 OK MW-36 Nickel 7/27/2021 8/13/2021 17 180 OK MW-36 Nitrate + Nitrite as N 7/27/2021 8/2/2021 6 28 OK MW-36 Nitrogen, Ammonia as N 7/27/2021 8/4/2021 8 28 OK MW-36 Potassium 7/27/2021 8/10/2021 14 180 OK MW-36 Selenium 7/27/2021 8/13/2021 17 180 OK MW-36 Silver 7/27/2021 8/16/2021 20 180 OK MW-36 Sodium 7/27/2021 8/10/2021 14 180 OK MW-36 Sulfate 7/27/2021 8/10/2021 14 28 OK MW-36 Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK MW-36 Thallium 7/27/2021 8/13/2021 17 180 OK MW-36 Tin 7/27/2021 8/13/2021 17 180 OK MW-36 Toluene 7/27/2021 7/30/2021 3 14 OK MW-36 Total Dissolved Solids 7/27/2021 7/30/2021 3 7 OK MW-36 Uranium 7/27/2021 8/13/2021 17 180 OK MW-36 Vanadium 7/27/2021 8/10/2021 14 180 OK MW-36 Xylenes, Total 7/27/2021 7/30/2021 3 14 OK MW-36 Zinc 7/27/2021 8/13/2021 17 180 OK MW-38 Acetone 7/29/2021 8/2/2021 4 14 OK MW-38 Arsenic 7/29/2021 8/13/2021 15 180 OK MW-38 Benzene 7/29/2021 8/2/2021 4 14 OK MW-38 Beryllium 7/29/2021 8/13/2021 15 180 OK MW-38 Bicarbonate as CaCO3 7/29/2021 8/2/2021 4 14 OK MW-38 Cadmium 7/29/2021 8/13/2021 15 180 OK MW-38 Calcium 7/29/2021 8/10/2021 12 180 OK MW-38 Carbon tetrachloride 7/29/2021 8/2/2021 4 14 OK MW-38 Carbonate as CO3 7/29/2021 8/2/2021 4 14 OK MW-38 Chloride 7/29/2021 8/11/2021 13 28 OK MW-38 Chloroform 7/29/2021 8/2/2021 4 14 OK MW-38 Chloromethane 7/29/2021 8/2/2021 4 14 OK MW-38 Chromium 7/29/2021 8/13/2021 15 180 OK MW-38 Cobalt 7/29/2021 8/13/2021 15 180 OK MW-38 Cooner 7/29/2021 8/13/2021 15 180 OK MW-38 Fluoride 7/29/2021 8/11/2021 13 28 OK MW-38 Gross Radium Alpha 7/29/2021 8/23/2021 25 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-38 Iron 7/29/2021 8/13/2021 15 180 OK MW-38 Lead 7/29/2021 8/13/2021 15 180 OK MW-38 Magnesium 7/29/2021 8/10/2021 12 180 OK MW-38 Manganese 7/29/2021 8/13/2021 15 180 OK MW-38 Mercury 7/29/2021 8/3/2021 5 180 OK MW-38 Methyl ethyl ketone 7/29/2021 8/2/2021 4 14 OK MW-38 Methylene chloride 7/29/2021 8/2/2021 4 14 OK MW-38 Molybdenum 7/29/2021 8/13/2021 15 180 OK MW-38 Naphthalene 7/29/2021 8/2/2021 4 14 OK MW-38 Nickel 7/29/2021 8/13/2021 15 180 OK MW-38 Nitrate+ Nitrite as N 7/29/2021 8/6/2021 8 28 OK MW-38 Nitrogen, Ammonia as N 7/29/2021 8/4/2021 6 28 OK MW-38 Potassium 7/29/2021 8/12/2021 14 180 OK MW-38 Selenium 7/29/2021 8/13/2021 15 180 OK MW-38 Silver 7/29/2021 8/16/2021 18 180 OK MW-38 Sodium 7/29/2021 8/10/2021 12 180 OK MW-38 Sulfate 7/29/2021 8/11/2021 13 28 OK MW-38 Tetrahydrofuran 7/29/2021 8/2/2021 4 14 OK MW-38 Thallium 7/29/2021 8/13/2021 15 180 OK MW-38 Tin 7/29/2021 8/13/2021 15 180 OK MW-38 Toluene 7/29/2021 8/2/2021 4 14 OK MW-38 Total Dissolved Solids 7/29/2021 7/30/2021 1 7 OK MW-38 Uranium 7/29/2021 8/13/2021 15 180 OK MW-38 Vanadium 7/29/2021 8/10/2021 12 180 OK MW-38 Xylenes, Total 7/29/2021 8/2/2021 4 14 OK MW-38 Zinc 7/29/2021 8/13/2021 15 180 OK MW-39 Acetone 7/28/2021 7/30/2021 2 14 OK MW-39 Arsenic 7/28/2021 8/16/2021 19 180 OK MW-39 Benzene 7/28/2021 7/30/2021 2 14 OK MW-39 Beryllium 7/28/2021 8/13/2021 16 180 OK MW-39 Bicarbonate as CaCO3 7/28/2021 8/2/2021 5 14 OK MW-39 Cadmium 7/28/2021 8/13/2021 16 180 OK MW-39 Calcium 7/28/2021 8/10/2021 13 180 OK MW-39 Carbon tetrachloride 7/28/2021 7/30/2021 2 14 OK MW-39 Carbonate as CO3 7/28/2021 8/2/2021 5 14 OK MW-39 Chloride 7/28/2021 8/11/2021 14 28 OK MW-39 Chloroform 7/28/2021 7/30/2021 2 14 OK MW-39 Chloromethane 7/28/2021 7/30/2021 2 14 OK MW-39 Chromium 7/28/2021 8/13/2021 16 180 OK MW-39 Cobalt 7/28/2021 8/13/2021 16 180 OK MW-39 Copper 7/28/2021 8/13/2021 16 180 OK MW-39 Fluoride 7/28/2021 8/11/2021 14 28 OK MW-39 Gross Radium Alpha 7/28/2021 8/23/2021 26 180 OK MW-39 Iron 7/28/2021 8/13/2021 16 180 OK MW-39 Lead 7/28/2021 8/13/2021 16 180 OK MW-39 Magnesium 7/28/2021 8/10/2021 13 180 OK MW-39 Manganese 7/28/2021 8/13/2021 16 180 OK MW-39 Mercury 7/28/2021 8/3/2021 6 180 OK MW-39 Methyl ethyl ketone 7/28/2021 7/30/2021 2 14 OK MW-39 Methylene chloride 7/28/2021 7/30/2021 2 14 OK MW-39 Molybdenum 7/28/2021 8/13/2021 16 180 OK MW-39 Naphthalene 7/28/2021 7/30/2021 2 14 OK MW-39 Nickel 7/28/2021 8/13/2021 16 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-39 Nitrate + Nitrite as N 7/28/2021 8/2/2021 5 28 OK MW-39 Nitrogen, Ammonia as N 7/28/2021 8/4/2021 7 28 OK MW-39 Potassium 7/28/2021 8/12/2021 15 180 OK MW-39 Selenium 7/28/2021 8/13/2021 16 180 OK MW-39 Silver 7/28/2021 8/16/2021 19 180 OK MW-39 Sodium 7/28/2021 8/10/2021 13 180 OK MW-39 Sulfate 7/28/2021 8/11/2021 14 28 OK MW-39 Tetrahydrofuran 7/28/2021 7/30/2021 2 14 OK MW-39 Thallium 7/28/2021 8/13/2021 16 180 OK MW-39 Tin 7/28/2021 8/13/2021 16 180 OK MW-39 Toluene 7/28/2021 7/30/2021 2 14 OK MW-39 Total Dissolved Solids 7/28/2021 7/30/2021 2 7 OK MW-39 Uranium 7/28/2021 8/13/2021 16 180 OK MW-39 Vanadium 7/28/2021 8/11/2021 14 180 OK MW-39 Xylenes, Total 7/28/2021 7/30/2021 2 14 OK MW-39 Zinc 7/28/2021 8/13/2021 16 180 OK MW-40 Acetone 7/28/2021 7/30/2021 2 14 OK MW-40 Arsenic 7/28/2021 8/13/2021 16 180 OK MW-40 Benzene 7/28/2021 7/30/2021 2 14 OK MW-40 Beryllium 7/28/2021 8/13/2021 16 180 OK MW-40 Bicarbonate as CaCO3 7/28/2021 8/2/2021 5 14 OK MW-40 Cadmium 7/28/2021 8/13/2021 16 180 OK MW-40 Calcium 7/28/2021 8/10/2021 13 180 OK MW-40 Carbon tetrachloride 7/28/2021 7/30/2021 2 14 OK MW-40 Carbonate as CO3 7/28/2021 8/2/2021 5 14 OK MW-40 Chloride 7/28/2021 8/11/2021 14 28 OK MW-40 Chloroform 7/28/2021 7/30/2021 2 14 OK MW-40 Chloromethane 7/28/2021 7/30/2021 2 14 OK MW-40 Chromium 7/28/2021 8/13/2021 16 180 OK MW-40 Cobalt 7/28/2021 8/13/2021 16 180 OK MW-40 Coooer 7/28/2021 8/13/2021 16 180 OK MW-40 Fluoride 7/28/2021 8/11/2021 14 28 OK MW-40 Gross Radium Alpha 7/28/2021 8/23/2021 26 180 OK MW-40 Iron 7/28/2021 8/13/2021 16 180 OK MW-40 Lead 7/28/2021 8/13/2021 16 180 OK MW-40 Magnesium 7/28/2021 8/10/2021 13 180 OK MW-40 Manganese 7/28/2021 8/13/2021 16 180 OK MW-40 Mercury 7/28/2021 8/3/2021 6 180 OK MW-40 Methyl ethyl ketone 7/28/2021 7/30/2021 2 14 OK MW-40 Methylene chloride 7/28/2021 7/30/2021 2 14 OK MW-40 Molybdenum 7/28/2021 8/13/2021 16 180 OK MW-40 Naphthalene 7/28/2021 7/30/2021 2 14 OK MW-40 Nickel 7/28/2021 8/13/2021 16 180 OK MW-40 Nitrate + Nitrite as N 7/28/2021 8/2/2021 5 28 OK MW-40 Nitrogen, Ammonia as N 7/28/2021 8/4/2021 7 28 OK MW-40 Potassium 7/28/2021 8/12/2021 15 180 OK MW-40 Selenium 7/28/2021 8/13/2021 16 180 OK MW-40 Silver 7/28/2021 8/16/2021 19 180 OK MW-40 Sodium 7/28/2021 8/10/2021 13 180 OK MW-40 Sulfate 7/28/2021 8/11/2021 14 28 OK MW-40 Tetrahydrofuran 7/28/2021 7/30/2021 2 14 OK MW-40 Thallium 7/28/2021 8/13/2021 16 180 OK MW-40 Tin 7/28/2021 8/13/2021 16 180 OK G-2A: Quarterly Holding Time Evaluation Hold Time Allowed Hold Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) Time (Days) Check MW-40 Toluene 7/28/2021 7/30/2021 2 14 OK MW-40 Total Dissolved Solids 7/28/2021 7/30/2021 2 7 OK MW-40 Uranium 7/28/2021 8/13/2021 16 180 OK MW-40 Vanadium 7/28/2021 8/10/2021 13 180 OK MW-40 Xylenes, Total 7/28/2021 7/30/2021 2 14 OK MW-40 Zinc 7/28/2021 8/13/2021 16 180 OK MW-65 Acetone 7/27/2021 7/30/2021 3 14 OK MW-65 Arsenic 7/27/2021 8/16/2021 20 180 OK MW-65 Benzene 7/27/2021 7/30/2021 3 14 OK MW-65 Beryllium 7/27/2021 8/16/2021 20 180 OK MW-65 Bicarbonate as CaCO3 7/27/2021 8/2/2021 6 14 OK MW-65 Cadmium 7/27/2021 8/13/2021 17 180 OK MW-65 Calcium 7/27/2021 8/10/2021 14 180 OK MW-65 Carbon tetrachloride 7/27/2021 7/30/2021 3 14 OK MW-65 Carbonate as CO3 7/27/2021 8/2/2021 6 14 OK MW-65 Chloride 7/27/2021 8/10/2021 14 28 OK MW-65 Chloroform 7/27/2021 7/30/2021 3 14 OK MW-65 Chloromethane 7/27/2021 7/30/2021 3 14 OK MW-65 Chromium 7/27/2021 8/13/2021 17 180 OK MW-65 Cobalt 7/27/2021 8/13/2021 17 180 OK MW-65 Copper 7/27/2021 8/13/2021 17 180 OK MW-65 Fluoride 7/27/2021 8/11/2021 15 28 OK MW-65 Gross Radium Alpha 7/27/2021 8/23/2021 27 180 OK MW-65 Iron 7/27/2021 8/16/2021 20 180 OK MW-65 Lead 7/27/2021 8/16/2021 20 180 OK MW-65 Magnesium 7/27/2021 8/10/2021 14 180 OK MW-65 Manganese 7/27/2021 8/13/2021 17 180 OK MW-65 Mercury 7/27/2021 8/3/2021 7 180 OK MW-65 Methyl ethyl ketone 7/27/2021 7/30/2021 3 14 OK MW-65 Methylene chloride 7/27/2021 7/30/2021 3 14 OK MW-65 Molybdenum 7/27/2021 8/13/2021 17 180 OK MW-65 Naphthalene 7/27/2021 7/30/2021 3 14 OK MW-65 Nickel 7/27/2021 8/13/2021 17 180 OK MW-65 Nitrate + Nitrite as N 7/27/2021 8/2/2021 6 28 OK MW-65 Nitrogen, Ammonia as N 7/27/2021 8/4/2021 8 28 OK MW-65 Potassium 7/27/2021 8/12/2021 16 180 OK MW-65 Selenium 7/27/2021 8/13/2021 17 180 OK MW-65 Silver 7/27/2021 8/16/2021 20 180 OK MW-65 Sodium 7/27/2021 8/10/2021 14 180 OK MW-65 Sulfate 7/27/2021 8/10/2021 14 28 OK MW-65 Tetrahydrofuran 7/27/2021 7/30/2021 3 14 OK MW-65 Thallium 7/27/2021 8/16/2021 20 180 OK MW-65 Tin 7/27/2021 8/13/2021 17 180 OK MW-65 Toluene 7/27/2021 7/30/2021 3 14 OK MW-65 Total Dissolved Solids 7/27/2021 7/30/2021 3 7 OK MW-65 Uranium 7/27/2021 8/16/2021 20 180 OK MW-65 Vanadium 7/27/2021 8/10/2021 14 180 OK MW-65 Xylenes, Total 7/27/2021 7/30/2021 3 14 OK MW-65 Zinc 7/27/2021 8/13/2021 17 180 OK G-2B: Accelerated Holding Time Evaluation Allowed I Hold Time Hold Time Hold Time Location ID Parameter Name Sample Date Analysis Date (Days) (Davs) Check Trip Blank Carbon tetrachloride 8/10/2021 8/16/2021 6 14 OK Trip Blank Chloroform 8/10/2021 8/16/2021 6 14 OK Trip Blank Methylene chloride 8/10/2021 8/16/2021 6 14 OK Trip Blank Carbon tetrachloride 9/9/2021 9/15/2021 6 14 OK Trip Blank Chloroform 9/9/2021 9/15/2021 6 14 OK Trip Blank Methylene chloride 9/9/2021 9/15/2021 6 14 OK MW-11 Sulfate 8/10/2021 8/18/2021 8 28 OK MW-11 Chloride 8/10/2021 8/18/2021 8 28 OK MW-11 Sulfate . 9/7/2021 9/23/2021 16 28 OK MW-11 Chloride 9/7/2021 9/23/2021 16 28 OK MW-26 Chloride 8/10/2021 8/18/2021 8 28 OK MW-26 Carbon tetrachloride 8/10/2021 8/16/2021 6 14 OK MW-26 Chloroform 8/10/2021 8/16/2021 6 14 OK MW-26 Methylene chloride 8/10/2021 8/16/2021 6 14 OK MW-26 Nitrate + Nitrite as N 8/10/2021 8/16/2021 6 28 OK MW-26 Chloride 9/9/2021 9/23/2021 14 28 OK MW-26 Carbon tetrachloride 9/9/2021 9/15/2021 6 14 OK MW-26 Chloroform 9/9/2021 9/15/2021 6 14 OK MW-26 Methylene chloride 9/9/2021 9/15/2021 6 14 OK MW-26 Nitrate + Nitrite as N 9/9/2021 9/15/2021 6 28 OK MW-30 Chloride 8/9/2021 8/18/2021 9 28 OK MW-30 Uranium 8/9/2021 8/26/2021 17 180 OK MW-30 Selenium 8/9/2021 8/26/2021 17 180 OK MW-30 Nitrate + Nitrite as N 8/9/2021 8/16/2021 7 28 OK MW-30 Chloride 9/8/2021 9/23/2021 15 28 OK MW-30 Uranium 9/8/2021 9/18/2021 10 180 OK MW-30 Selenium 9/8/2021 9/18/2021 10 180 OK MW-30 Nitrate + Nitrite as N 9/8/2021 9/15/2021 7 28 OK MW-31 Sulfate 8/9/2021 8/18/2021 9 28 OK MW-31 Chloride 8/9/2021 8/18/2021 9 28 OK MW-31 Uranium 8/9/2021 8/26/2021 17 180 OK MW-31 Nitrate + Nitrite as N 8/9/2021 8/16/2021 7 28 OK MW-31 Total Dissolved Solids 8/9/2021 8/13/2021 4 7 OK MW-31 Sulfate 9/7/2021 9/23/2021 16 28 OK MW-31 Chloride 9/7/2021 9/23/2021 16 28 OK MW-31 Uranium 9/7/2021 9/18/2021 11 180 OK MW-31 Nitrate + Nitrite as N 9/7/2021 9/15/2021 8 28 OK MW-31 Total Dissolved Solids 9/7/2021 9/10/2021 3 7 OK MW-65 Chloride 8/9/2021 8/18/2021 9 28 OK MW-65 Uranium 8/9/2021 8/26/2021 17 180 OK MW-65 Selenium 8/9/2021 8/26/2021 17 180 OK MW-65 Nitrate + Nitrite as N 8/9/2021 8/16/2021 7 28 OK MW-65 Sulfate 9/7/2021 9/23/2021 16 28 OK MW-65 Chloride 9/7/2021 9/23/2021 16 28 OK MW-65 Uranium 9/7/2021 9/18/2021 11 180 OK MW-65 Nitrate + Nitrite as N 9/7/2021 9/15/2021 8 28 OK MW-65 Total Dissolved Solids 9/7/2021 9/10/2021 3 7 OK G-3A: Quarterly Sample Laboratory Receipt Temperature Check Ii' Sample Batch Wells in Batch Temperature GEL 551444 MW-11,MW-14,MW-24,MW-24A,MW-25,MW-26,MW-NA 30, MW-31, MW-36, MW-38, MW-39, MW-40, MW-65 AWAL 2107637 MW-12 NA AWAL 2107668 MW-27,MW-28,MW-29 1.8 °C MW-11, MW-14, MW-24, MW-24A, MW-25, MW-26, MW AWAL2107791 30,MW-31,MW-32,MW-36,MW-38,MW-39,MW-40, 2.9 °C MW-65, Trip Blank NIA= These shipments contained samples for the analysis of gross alpha or metals only. Per Table 1 in the approved QAP, samples submitted for gross alpha or metals analyses do not have a sample temperature requirement. G-3B: Accelerated Sample Laboratory Receipt Temperature Check Sample Batch Wells in Batch Temperature AWAL 2108362-August MW-11, 5, MW-26, MW-30, MW-31, MW-65, Trip Blank 0.2 °C AW AL 21092564 -September MW-11, MW-26, MW-30, MW-31, MW-65, Trip Blank 0.2 °C G-4A: Quarterly Sample Analytical Method Check Parameter QAPMethod Method Used by Lab Ammonia (as N) A4500-NH3 G or E350.l E350.l Nitrate+ Nitrite (as N) E353. l or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 and E200.8 Gross Alpha E900.0 or E900. l or E903.0 E903.0 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-CI B or A4500-Cl E or E300.0 SM4500-CI-E and 300.0 Fluoride A4500-F C or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540C A2540 C Carbonate as CO3, Bicarbonate as HCO3 A2320 B A2320 B Mercury E245.l orE200.7 orE200.8 E245. l Calcium, Magnesium, Potassium, Sodium E200.7 E200.7 G-4B: Accelerated Sample Analytical Method Check Parameter QAPMethod Method Used ty Lab Nitrate+ Nitrite (as N) E353. l or E353.2 E353.2 Metals E200.7 or E200.8 E200.7 or E200.8 voes SW8260B or SW8260C or SW8260D SW8260D Chloride A4500-Cl B or A4500-Cl E or E300.0 E300.0 Sulfate A4500-SO4 E or E300.0 E300.0 TDS A2540C A2540C G-5A Quarterly Sample Reaorting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check Trip Blank Acetone 20 ug/L u 1 20 OK Trip Blank Benzene 1 ug/L u 1 I OK Trip Blank Carbon tetrachloride I ug/L u I I OK Trip Blank Chloroform 1 ug/L u I 1 OK Trip Blank Chloromethane 1 ug/L u 1 1 OK Trip Blank Methyl ethyl ketone 20 ug/L u 1 20 OK Trip Blank Methylene chloride 1 ug/L u 1 1 OK Trip Blank Naphtbalene 1 ug/L u I 1 OK Trip Blank Tetrahvdrofuran 1 ug/L u I 1 OK Trip Blank Toluene 1 u_g/L u I 1 OK Trip Blank Xylenes, Total 1 ug/L u 1 1 OK MW-11 Acetone 20 ug/L u I 20 OK MW-11 Arsenic 5 ug/L u 5 5 OK MW-11 Benzene 1 ug/L u I 1 OK MW-11 Beryllium 0.5 ug/L u 5 0.5 OK MW-11 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-11 Cadmium 0.5 ug/L u 20 0.5 OK MW-11 Calcium 10 mg/L 10 0.5 OK MW-11 Carbon tetrachloride I ug/L u I 1 OK MW-11 Carbonate as CO3 I mg/L u I 1 OK MW-JI Chloride 5 mg/L 50 1 OK MW-11 Chloroform 1 ug/L u I 1 OK MW-11 Chloromethane 1 ug/L u 1 1 OK -MW-11 Chromium 25 ug/L u 20 25 OK MW-11 Cobalt 10 ug/L u 20 10 OK MW-11 Coooer 10 ug/L u 20 10 OK MW-11 Fluoride 0.2 mg/L 2 0.1 OK MW-11 Gross Radium Alpha 0.556 pCi/L u I I OK MW-11 Iron 30 ug/L u 5 30 OK MW-11 Lead 1 ug/L u 5 1 OK MW-11 Magnesium 0.1 mg/L 1 0.5 OK MW-11 Mani!,anese 10 ug/L 20 10 OK MW-11 Mercury 0.5 ug/L u I 0.5 OK MW-11 Melhyl ethyl ketone 20 ug/L u 1 20 OK MW-11 Methylene chloride I ug/L u 1 I OK MW-11 Molybdenum 10 ug/L u 20 10 OK MW-11 Naphlhalene I ug/L u 1 1 OK MW-11 Nickel 20 ug/L u 20 20 OK MW-11 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-11 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-11 Potassium 1 mg/L 1 0.5 OK MW-11 Selenium 5 ug/L u 20 5 OK MW-11 Silver 10 ug/L u 20 10 OK MW-11 Sodium 10 mg/L 10 0.5 OK MW-11 Sulfate 25 mg/L 50 1 OK MW-11 Tetrahydrofuran 1 ug/L 1 1 OK MW-11 Thallium 0.5 ug/L u 5 0.5 OK MW-11 Tin 100 ug/L u 20 100 OK MW-11 Toluene I ug/L u I I OK MW-11 Total Dissolved Solids 20 MG/L 2 10 OK MW-11 Uranium 0.5 ug/L 5 0.3 OK MW-11 Vanadium 15 ug/L u 1 15 OK MW-11 Xylenes, Total 1 ug/L u 1 1 OK MW-11 Zinc 10 u!!IL u 20 10 OK G5AQ -uarter1y amp: e I S I R eporun_g 1m1t ec L .. Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-12 Selenium 5 ug/L 20 5 OK MW-12 Uranium 0.3 ug/L 2 0.3 OK MW-14 Acetone 20 ug/L u 1 20 OK MW-14 Arsenic 5 ug/L u 20 5 OK MW-14 Benzene 1 ug/L u 1 1 OK MW-14 Beryllium 0.5 ug/L u 5 0.5 OK MW-14 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-14 Cadmium 0.5 ug/L 20 0.5 OK MW-14 Calcium 10 mg/L 10 0.5 OK MW-14 Carbon tetrachloride 1 ug/L u 1 1 OK MW-14 Carbonate as CO3 1 mg/L u 1 1 OK MW-14 Chloride 10 mg/L 100 1 OK MW-14 Chloroform 1 ug/L u 1 1 OK MW-14 Chloromethane 1 ug/L u I I OK MW-14 Chromium 25 ug/L u 20 25 OK MW-14 Cobalt 10 ug/L u 20 10 OK MW-14 Copper 10 ug/L u 20 10 OK MW-14 Fluoride 0.1 mg/L 1 0.1 OK MW-14 Gross Radium Alpha 0.935 pCi/L u I I OK MW-14 Iron 30 ug/L u 5 30 OK MW-14 Lead I ug/L u 5 I OK MW-14 Magnesium 1 mg/L 10 0.5 OK MW-14 Manganese 10 ug/L 20 10 OK MW-14 Mercury 0.5 ug/L u I 0.5 OK MW-14 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-14 Methylene chloride I ug/L u 1 I OK MW-14 Molybdenum 10 ug/L u 20 10 OK MW-14 Naphthalene 1 ug/L u 1 1 OK MW-14 Nickel 20 ug/L u 20 20 OK MW-14 Nitrate + Nitrite as N 0.1 mg/L u 10 0.1 OK MW-14 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-14 Potassium I mg/L 1 0.5 OK MW-14 Selenium 5 ug/L u 20 5 OK MW-14 Silver 10 ug/L u 20 10 OK MW-14 Sodium 10 mg/L 10 0.5 OK MW-14 Sulfate 50 mg/L 100 1 OK MW-14 Tetrahydrofuran 1 ug/L u 1 1 OK MW-14 Thallium 0.5 ug/L u 5 0.5 OK MW-14 Tin 100 ug/L u 20 100 OK MW-14 Toluene 1 ug/L u 1 1 OK MW-14 Total Dissolved Solids 20 MG/L 2 10 OK MW-14 Uranium 0.5 ug/L 5 0.3 OK MW-14 Vanadium 15 ug/L u 1 15 OK MW-14 Xylenes, Total 1 ug/L u I 1 OK MW-14 Zinc 10 ug/L 20 10 OK MW-24 Acetone 20 ug/L u I 20 OK MW-24 Arsenic 5 ug/L u 5 5 OK MW-24 Benzene I ug/L u 1 I OK MW-24 Beryllium 0.5 ug/L 5 0.5 OK MW-24 Bicarbonate as CaCO3 1 mg/L u I I OK MW-24 Cadmium 0.5 ug/L 20 0.5 OK MW-24 Calcium 10 mg/L 10 0.5 OK MW-24 Carbon tetrachloride I ug/L u I I OK MW-24 Carbonate as CO3 I mg/L u I I OK G5AQ -1 S I R uarter1y amp: e eportmg 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24 Chloride 20 mg/L 200 1 OK MW-24 Chloroform I uwl, u 1 1 OK MW-24 Chloromethane 1 ug/L u 1 1 OK MW-24 Chromium 25 ug/L u 20 25 OK MW-24 Cobalt 10 ug/L 20 10 OK MW-24 Copper 10 ug/L 20 10 OK MW-24 Fluoride 0.5 mg/L 5 0.1 OK MW-24 Gross Radium Alpha 0.594 pCi/L 1 1 OK MW-24 Iron 30 ug/L u 5 30 OK MW-24 Lead 1 ug/L 5 1 OK MW-24 Magnesium 1 mg/L 10 0.5 OK MW-24 Manganese 10 ug/L 100 10 OK MW-24 Mercury 0.5 ug/L u 1 0.5 OK MW-24 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-24 Methylene chloride I ug/L u I 1 OK MW-24 Molybdenum 10 ug/L u 20 10 OK MW-24 Naphthalene 1 ug/L u 1 1 OK MW-24 Nickel 20 ug/L 20 20 OK MW-24 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-24 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-24 Potassium 2 mg/L 2 0.5 OK MW-24 Selenium 5 ug/L 20 5 OK MW-24 Silver 10 ug/L u 20 10 OK MW-24 Sodium 10 mg/L 10 0.5 OK MW-24 Sulfate 100 mg/L 200 1 OK MW-24 Tetrahydrofuran 1 ug/L u 1 1 OK MW-24 Thallium 0.5 ug/L 5 0.5 OK MW-24 Tin 100 ug/L u 20 100 OK MW-24 Toluene 1 ug/L u 1 1 OK MW-24 Total Dissolved Solids 20 MG/L 2 10 OK MW-24 Uranium 0.5 ug/L 5 0.3 OK MW-24 Vanadium 15 ug/L u 2 15 OK MW-24 Xylenes, Total 1 ug/L u 1 1 OK MW-24 Zinc 10 ug/L 20 10 OK MW-24A Acetone 20 uwl, u 1 20 OK MW-24A Arsenic 5 ug/L u 20 5 OK MW-24A Benzene 1 ug/L u 1 1 OK MW-24A Beryllium 0.5 ug/L 5 0.5 OK MW-24A Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-24A Cadmium 0.5 ug/L 20 0.5 OK MW-24A Calcium 10 mg/L 10 0.5 OK MW-24A Carbon tetrachloride 1 ug/L u I I OK MW-24A Carbonate as CO3 1 mg/L u I 1 OK MW-24A Chloride 20 mg/L 200 1 OK MW-24A Chloroform 1 ug/L u 1 1 OK MW-24A Chloromethane 1 ug/L u 1 1 OK MW-24A Chromium 25 ug/L u 20 25 OK MW-24A Cobalt 10 ug/L 20 10 OK MW-24A Cooner 10 ug/L 20 10 OK MW-24A Fluoride 0.5 mg/L 5 0.1 OK MW-24A Gross Radium Alpha 0.751 pCi/L 1 1 OK MW-24A Iron 30 ug/L u 5 30 OK MW-24A Lead 1 ug/L u 5 1 OK MW-24A Magnesium I mg/L 10 0.5 OK G 5AQ -I S l R uarter1y amp e eporung 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-24A Manganese 10 ug/L 100 10 OK MW-24A Mercury 0.5 ug/L u 1 0.5 OK MW-24A Methyl eth yl ketone 20 ug/L u 1 20 OK MW-24A Methylene chloride 1 ug/L u 1 1 OK MW-24A Molybdenum 10 ug/L u 20 10 OK MW-24A Naphthalene 1 ug/L u 1 1 OK MW-24A Nickel 20 ug/L 20 20 OK MW-24A Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-24A Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-24A Potassium 2 mg/L 2 0.5 OK MW-24A Selenium 5 ug/L 20 5 OK MW-24A Silver 10 ug/L u 20 10 OK MW-24A Sodium 10 mg/L 10 0.5 OK MW-24A Sulfate 100 mg/L 200 I OK MW-24A Telrahydrofuran 1 ug/L u 1 1 OK MW-24A Thallium 0.5 ug/L 5 0.5 OK MW-24A Tin 100 ug/L u 20 100 OK MW-24A Toluene 1 ug/L u 1 1 OK MW-24A Total Dissolved Solids 20 MG/L 2 10 OK MW-24A Uranium 0.5 ug/L 5 0.3 OK MW-24A Vanadium 15 ug/L u 2 15 OK MW-24A Xylenes, Total 1 ug/L u 1 1 OK MW-24A Zinc 10 ug/L 20 10 OK MW-25 Acetone 20 ug/L u 1 20 OK MW-25 Arsenic 5 ug/L u 20 5 OK MW-25 Benzene 1 ug/L u 1 1 OK MW-25 Beryllium 0.5 ug/L u 5 0.5 OK MW-25 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-25 Cadmium 0.5 ug/L 20 0.5 OK MW-25 Calcium 10 mg/L 10 0.5 OK MW-25 Carbon tetrachloride 1 ug/L u 1 1 OK MW-25 Carbonate as CO3 1 mg/L u 1 1 OK MW-25 Chloride 10 mg/L 100 l OK MW-25 Chloroform 1 ug/L u I 1 OK MW-25 Chloromethane I ug/L u 1 I OK MW-25 Chromium 25 ug/L u 20 25 OK MW-25 Cobalt 10 ug/L u 20 10 OK MW-25 Cooner 10 ug/L u 20 10 OK MW-25 Fluoride 0.2 mg/L 2 0.1 OK MW-25 Gross Radium Alpha 0.526 pCi/L u 1 1 OK MW-25 Iron 30 ug/L u 5 30 OK MW-25 Lead 1 ug/L u 5 I OK MW-25 Magnesium 1 mg/L 10 0.5 OK MW-25 Manganese 10 ug/L 20 10 OK MW-25 Mercury 0.5 ug/L u 1 0.5 OK MW-25 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-25 Methylene chloride 1 ug/L u 1 1 OK MW-25 Molybdenum 10 ug/L 20 10 OK MW-25 Napluhalene 1 ug/L u 1 1 OK MW-25 Nickel 20 ug/L u 20 20 OK MW-25 Nitrate + Nitrite as N 0.1 mg/L u 10 0.1 OK MW-25 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-25 Potassium 1 mg/L I 0.5 OK MW-25 Selenium 5 ug/L u 20 5 OK G 5AQ -I S I R uarler1y amp, e eporting 1m1t ec L ' . Ch k - Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-25 Silver 10 ug/L u 20 10 OK MW-25 Sodium 10 mg/L 10 0.5 OK MW-25 Sulfate 50 mg/L 100 1 OK MW-25 Tetrahydrofuran I ug/L u I 1 OK MW-25 Thallium 0.5 ug/L 5 0.5 OK MW-25 Tin 100 ug/L u 20 100 OK MW-25 Toluene 1 ug/L u 1 1 OK MW-25 Total Dissolved Solids 20 MG/L 2 10 OK MW-25 Uranium 0.5 ug/L 5 0.3 OK MW-25 Vanadium 15 ug/L u 1 15 OK MW-25 Xylenes, Total 1 ug/L u 1 1 OK MW-25 Zinc 10 ug/L u 20 10 OK MW-26 Acetone 20 ug/L u 1 20 OK MW-26 Arsenic 5 ug/L u 5 5 OK MW-26 Benzene 1 ug/L u 1 1 OK MW-26 Beryllium 0.5 ug/L u 5 0.5 OK MW-26 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-26 Cadmium 0.5 ug/L 20 0.5 OK MW-26 Calcium 10 mg/L 10 0.5 OK MW-26 Carbon tetrachloride 1 ug/L u 1 1 OK MW-26 Carbonate as CO3 I mg/L u 1 1 OK MW-26 Chloride 10 mg/L 100 I OK MW-26 Chloroform 10 ug/L 10 1 OK MW-26 Chloromethane 1 ug/L u 1 1 OK MW-26 Chromium 25 ug/L u 20 25 OK MW-26 Cobalt 10 ug/L u 20 10 OK MW-26 Copper 10 ug/L u 20 10 OK MW-26 Fluoride 0.2 mg/L 2 0.1 OK MW-26 Gross Radium Alpha 0.591 "pCi/L 1 1 OK MW-26 Iron 100 ug/L 20 30 OK MW-26 Lead 1 ug/L u 5 1 OK MW-26 Magnesium 1 mg/L 10 0.5 OK MW-26 Manganese 10 ug/L 20 10 OK MW-26 Mercury 0.5 ug/L u 1 0.5 OK MW-26 MerJ1yl ethyl ketone 20 ug/L u 1 20 OK MW-26 Methylene chloride 1 ug/L u 1 1 OK MW-26 Molybdenum 10 ug/L u 20 10 OK MW-26 Naphthalene 1 ug/L u 1 1 OK MW-26 Nickel 20 ug/L u 20 20 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-26 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-26 Potassium I mg/L 1 0.5 OK MW-26 Selenium 5 ug/L u 20 5 OK MW-26 Silver 10 ug/L u 20 10 OK MW-26 Sodium 10 mg/L 10 0.5 OK MW-26 Sulfate 50 mg/L 100 1 OK MW-26 Tetrahydrofuran 1 ug/L u 1 1 OK MW-26 Thallium 0.5 ug/L u 5 0.5 OK MW-26 Tin 100 ug/L u 20 100 OK MW-26 Toluene 1 ug/L u 1 1 OK MW-26 Total Dissolved Solids 20 MG/L 2 10 OK MW-26 Uranium 0.5 ug/L 5 0.3 OK MW-26 Vanadium 15 ug/L u 1 15 OK MW-26 Xvlenes, Total 1 ug/L u 1 1 OK G5AQ -uarter1y amp e epol'lml!: I S I Ri 1ml t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-26 Zinc 10 ug/L u 20 10 OK MW-27 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-28 Chloride 10 mg/L 100 1 OK MW-28 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-28 Selenium 5 ug/L 20 5 OK MW-28 Uranium 2 ug/L 20 0.3 OK MW-29 Uranium 0.3 ug/L 2 0.3 OK MW-30 Acetone 20 ug/L u I 20 OK MW-30 Arsenic 5 ug/L u 20 5 OK MW-30 Benzene 1 ug/L u 1 1 OK MW-30 Beryllium 0.5 ug/L u 5 0.5 OK MW-30 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-30 Cadmium 0.5 ug/L u 20 0.5 OK MW-30 Calcium 10 mg/L 10 0.5 OK MW-30 Carbon tetrachloride 1 ug/L u 1 1 OK MW-30 Carbonate as CO3 1 mg/L u I 1 OK MW-30 Chloride 5 mg/L 50 1 OK MW-30 Chloroform 1 ug/L u 1 1 OK MW-30 Chloromethane 1 ug/L u I 1 OK MW-30 Chromium 25 ug/L u 20 25 OK MW-30 Cobalt 10 ug/L u 20 10 OK MW-30 Copper 10 ug/L u 20 10 OK MW-30 Fluoride 0.1 mg/L 1 0.1 OK MW-30 Gross Radium Alpha 0.659 pCi/L u 1 1 OK MW-30 Iron 30 ug/L u 5 30 OK MW-30 Lead 1 ug/L u 5 I OK MW-30 Magnesium 1 mg/L 10 0.5 OK MW-30 Manganese 10 ug/L u 20 10 OK MW-30 Mercury 0.5 ug/L u 1 0.5 OK MW-30 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-30 Methylene chloride 1 ug/L u 1 1 OK MW-30 Molybdenum 10 ug/L u 20 10 OK MW-30 Naphthalene 1 ug/L u 1 1 OK MW-30 Nickel 20 ug/L u 20 20 OK MW-30 Nitrate+ Nitrite as N 0.5 mg/L 50 0.1 OK MW-30 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-30 Potassium 1 mg/L 1 0.5 OK MW-30 Selenium 5 ug/L 20 5 OK MW-30 Silver 10 ug/L u 20 10 OK MW-30 Sodium 10 mg/L 10 0.5 OK MW-30 Sulfate 25 mg/L 50 1 OK MW-30 Tetrahydrofuran 1 ug/L u 1 1 OK MW-30 Thallium 0.5 ug/L u 5 0.5 OK MW-30 Tin 100 ug/L u 20 100 OK MW-30 Toluene 1 ug/L u 1 1 OK MW-30 Total Dissolved Solids 20 MG/L 2 10 OK MW-30 Uranium 0.5 ug/L 5 0.3 OK MW-30 Vanadium 15 ug/L u 1 15 OK MW-30 Xylenes, Total I ug/L u 1 1 OK MW-30 Zinc 10 ug/L u 20 10 OK MW-31 Acetone 20 ug/L u 1 20 OK MW-31 Arsenic 5 ug/L u 20 5 OK MW-31 Benzene 1 ug/L u 1 1 OK MW-31 Beryllium 0.5 ug/L u 5 0.5 OK G-5A Q uarterly amp e eportmg Limit C ec S I R h k Lab Required Reporting Dilution Reporting RL Location Analvte Limit Units Qualifier Factor Limit Check MW-31 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-31 Cadmium 0.5 ug/L u 20 0.5 OK MW-31 Calcium 10 mg/L 10 0.5 OK MW-31 Carbon tetrachloride 1 ug/L u 1 I OK MW-31 Carbonate as CO3 1 mg/L u 1 1 OK MW-31 Chloride 10 mg/L 100 l OK MW-31 Chloroform 1 ug/L u 1 1 OK MW-31 Chloromethane 1 ug/L u 1 1 OK MW-31 Chromium 25 ug/L u 20 25 OK MW-31 Cobalt 10 ug/L u 20 10 OK MW-31 Copper 10 ug/L u 20 10 OK MW-31 Fluoride 0.2 mg/L 2 0.1 OK MW-31 Gross Radium Alpha 0.568 pCi/L u 1 1 OK MW-31 Iron 30 ug/L u 5 30 OK MW-31 Lead 1 ug/L u 5 1 OK MW-31 Magnesium 1 mg/L 10 0.5 OK MW-31 Manganese 10 ug/L u 20 10 OK MW-31 Mercury 0.5 ug/L u 1 0.5 OK MW-31 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-31 Methylene chloride 1 ug/L u 1 I OK MW-31 Molybdenum 10 ug/L u 20 10 OK MW-31 Naphthalene 1 ug/L u 1 1 OK MW-31 Nickel 20 ug/L u 20 20 OK MW-31 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-31 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-31 Potassium 1 mg/L 1 0.5 OK MW-31 Selenium 5 ug/L 20 5 OK MW-31 Silver 10 ug/L u 20 10 OK MW-31 Sodium 10 mg/L 10 0.5 OK MW-31 Sulfate 50 mg/L 100 1 OK MW-31 Tetrahydrofuran 1 ug/L u 1 1 OK MW-31 Thallium 0.5 ug/L u 5 0.5 OK MW-31 Tin 100 ug/L u 20 100 OK MW-31 Toluene 1 ug/L u 1 1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Uranium 0.5 ug/L 5 0.3 OK MW-31 Vanadium 15 ug/L u 1 15 OK MW-31 Xylenes, Total 1 ug/L u 1 1 OK MW-31 Zinc 10 ug/L u 20 10 OK MW-32 Chloride 2 mg/L 20 1 OK MW-36 Acetone 20 ug/L u 1 20 OK MW-36 Arsenic 5 ug/L u 20 5 OK MW-36 Benzene 1 ug/L u 1 1 OK MW-36 Beryllium 0.5 ug/L u 5 0.5 OK MW-36 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-36 Cadmium 0.5 ug/L u 20 0.5 OK MW-36 Calcium 10 mg/L 10 0.5 OK MW-36 Carbon tetrachloride 1 ug/L u 1 1 OK MW-36 Carbonate as CO3 1 mg/L u 1 1 OK MW-36 Chloride 20 mg/L 200 1 OK MW-36 Chloroform 1 ug/L u 1 1 OK MW-36 Chloromethane 1 ug/L u 1 1 OK MW-36 Chromium 25 ug/L u 20 25 OK MW-36 Cobalt 10 ug/L u 20 JO OK G5AQ -I S I R uarteny amp e eporl111g 1m1t ec L' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-36 Coooer 10 ug/L u 20 10 OK MW-36 Fluoride 0.1 mg/L 1 0.1 OK MW-36 Gross Radium Alpha 0.59 pCi/L u 1 1 OK MW-36 Iron 30 ug/L u 5 30 OK MW-36 Lead 1 ug/L u 5 1 OK MW-36 Magnesium 1 mg/L IO 0.5 OK MW-36 Manganese 10 ug/L u 20 10 OK MW-36 Mercury 0.5 ug/L u I 0.5 OK MW-36 Methyl ethyl ketone 20 ug/L u I 20 OK MW-36 Methylene chloride I ug/L u 1 1 OK MW-36 Molybdenum IO ug/L u 20 10 OK MW-36 Naphthalene 1 ug/L u 1 1 OK MW-36 Nickel 20 ug/L u 20 20 OK MW-36 Nitrate + Nitrite as N 0.1 mg/L IO 0.1 OK MW-36 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-36 Potassium 1 mg/L 1 0.5 OK MW-36 Selenium 5 ug/L 20 5 OK MW-36 Silver 10 ug/L u 20 IO OK MW-36 Sodium IO mg/L IO 0.5 OK MW-36 Sulfate 100 mg/L 200 1 OK MW-36 Tetrahydrofuran 1 ug/L u 1 1 OK MW-36 Thallium 0.5 ug/L 5 0.5 OK MW-36 Tin 100 ug/L u 20 100 OK MW-36 Toluene 1 ug/L u I 1 OK MW-36 Total Dissolved Solids 20 MG/L 2 10 OK MW-36 Uranium 0.5 ug/L 5 0.3 OK MW-36 Vanadium 15 ug/L u 1 15 OK MW-36 Xylenes, Total 1 ug/L u 1 1 OK MW-36 Zinc IO ug/L u 20 10 OK MW-38 Acetone 20 ug/L u 1 20 OK MW-38 Arsenic 5 ug/L u 5 5 OK MW-38 Benzene 1 ug/L u 1 1 OK MW-38 Beryllium 0.5 ug/L u 5 0.5 OK MW-38 Bicarbonate as CaCO3 1 mg/L 1 1 OK MW-38 Cadmium 0.5 ug/L u 20 0.5 OK MW-38 Calcium 10 mg/L IO 0.5 OK MW-38 Carbon tetrachloride 1 ug/L u l 1 OK MW-38 Carbonate as CO3 1 mg/L u 1 1 OK MW-38 Chloride 20 mg/L 200 1 OK MW-38 Chloroform 1 ug/L u I 1 OK MW-38 Chloromethane 1 ug/L u 1 1 OK MW-38 Chromium 25 ug/L u 20 25 OK MW-38 Cobalt IO ug/L u 20 10 OK MW-38 Coooer IO ug/L u 20 10 OK MW-38 Fluoride 0.5 mg/L 5 0.1 OK MW-38 Gross Radium Alpha 0.528 pCi/L u 1 1 OK MW-38 Iron 30 ug/L u 5 30 OK MW-38 Lead l ug/L u 5 1 OK MW-38 Magnesium l mg/L IO 0.5 OK MW-38 Manganese IO ug/L u 20 IO OK MW-38 Mercury 0.5 ug/L u 1 0.5 OK MW-38 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-38 Methylene chloride l ug/L u 1 1 OK MW-38 Molybdenum IO ug/L u 20 10 OK G-5A Quarterly Sample Reporting Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-38 Naphthalene 1 ug/L u 1 1 OK MW-38 Nickel 20 ug/L u 20 20 OK MW-38 Nitrate + Nitrite as N 0.2 mg/L 20 0.1 OK MW-38 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-38 Potassium 1 mg/L 1 0.5 OK MW-38 Selenium 5 ug/L 20 5 OK MW-38 Silver 10 ug/L u 20 10 OK MW-38 Sodium 10 mg/L 10 0.5 OK MW-38 Sulfate 100 mg/L 200 1 OK MW-38 Tetrahydrofuran 1 ug/L u 1 1 OK MW-38 Thallium 0.5 ug/L u 5 0.5 OK MW-38 Tin 100 ug/L u 20 100 OK MW-38 Toluene 1 ug/L u 1 1 OK MW-38 Total Dissolved Solids 20 MG/L 2 10 OK MW-38 Uranium 0.5 ug/L 5 0.3 OK MW-38 Vanadium 15 ug/L u 1 15 OK MW-38 Xylenes, Total 1 ug/L u 1 1 OK MW-38 Zinc 10 ug/L u 20 10 OK MW-39 Acetone 20 ug/L u 1 20 OK MW-39 Arsenic 5 ug/L u 20 5 OK MW-39 Benzene 1 ug/L u 1 1 OK MW-39 Beryllium 0.5 ug/L 5 0.5 OK MW-39 Bicarbonate as CaCO3 1 mg/L u 1 1 OK MW-39 Cadmium 0.5 ug/L 20 0.5 OK MW-39 Calcium 10 mg/L 10 0.5 OK MW-39 Carbon tetrachloride 1 ug/L u 1 1 OK MW-39 Carbonate as CO3 1 mg/L u 1 1 OK MW-39 Chloride 20 mg/L 200 1 OK MW-39 Chloroform 1 ug/L u 1 1 OK MW-39 Chloromethane 1 ug/L u 1 1 OK MW-39 Chromium 25 ug/L u 20 25 OK MW-39 Cobalt 10 ug/L 20 10 OK MW-39 Copper 10 ug/L 20 10 OK MW-39 Fluoride 0.5 mg/L 5 0.1 OK MW-39 Gross Radium Alpha 0.573 pCi/L 1 1 OK MW-39 Iron 1000 ug/L 200 30 OK MW-39 Lead 1 ug/L u 5 1 OK MW-39 Magnesium 1 mg/L 10 0.5 OK MW-39 Manganese 20 ug/L 200 10 OK MW-39 Mercury 0.5 ug/L u 1 0.5 OK MW-39 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-39 Methylene chloride 1 ug/L u 1 1 OK MW-39 Molybdenum 10 ug/L u 20 10 OK MW-39 Naphthalene 1 ug/L u 1 1 OK MW-39 Nickel 20 ug/L 20 20 OK MW-39 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-39 Nitrogen, Ammonia as N 0.05 mg/L 1 0.05 OK MW-39 Potassium 2 mg/L 2 0.5 OK MW-39 Selenium 5 ug/L u 20 5 OK MW-39 Silver 10 ug/L u 20 10 OK MW-39 Sodium 10 mg/L 10 0.5 OK MW-39 Sulfate 100 mg/L 200 1 OK MW-39 Tetrahydrofuran 1 ug/L u 1 1 OK MW-39 Thallium 0.5 ug/L 5 0.5 OK G-5A Quarterly Sample Reponin~ Limit Check Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-39 Tin 100 ug/L u 20 100 OK MW-39 Toluene 1 ug/L u 1 1 OK MW-39 Total Dissolved Solids 20 MG/L 2 10 OK MW-39 Uranium 0.5 ug/L 5 0.3 OK MW-39 Vanadium 15 ug/L u 2 15 OK MW-39 Xylenes, Total 1 ug/L u 1 1 OK MW-39 Zinc 10 ug/L 20 10 OK MW-40 Acetone 20 ug/L u 1 20 OK MW-40 Arsenic 5 ug/L u 5 5 OK MW-40 Benzene 1 ug/L u 1 1 OK MW-40 Beryllium 0.5 ug/L u 5 0.5 OK MW-40 Bicarbonate as CaCO3 1 mg/L 1 I OK MW-40 Cadmium 0.5 ug/L u 20 0.5 OK MW-40 Calcium 10 mg/L 10 0.5 OK MW-40 Carbon tetrachloride 1 ug/L u 1 1 OK MW-40 Carbonate as CO3 1 mg/L u 1 1 OK MW-40 Chloride 10 mg/L 100 1 OK MW-40 ' Chloroform 1 ug/L u 1 1 OK MW-40 Chloromethane I ug/L u 1 1 OK MW-40 Chromium 25 ug/L u 20 25 OK MW-40 Cobalt 10 ug/L u 20 10 OK MW-40 Copper 10 ug/L 20 10 OK MW-40 Fluoride 0.5 mg/L 5 0.1 OK MW-40 Gross Radium Alpha 0.416 pCi/L u I 1 OK MW-40 Iron 30 ug/L u 5 30 OK MW-40 Lead 1 ug/L u 5 1 OK MW-40 Magnesium 1 mg/L 10 0.5 OK MW-40 Manganese 10 ug/L 20 10 OK MW-40 Mercury 0.5 ug/L u 1 0.5 OK MW-40 Methyl ethyl ketone 20 ug/L u 1 20 OK MW-40 Methylene chloride 1 ug/L u 1 1 OK MW-40 Molybdenum 10 ug/L u 20 10 OK MW-40 Naphthalene 1 ug/L u 1 1 OK MW-40 Nickel 20 ug/L u 20 20 OK MW-40 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-40 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-40 Potassium 1 mg/L 1 0.5 OK MW-40 Selenium 5 ug/L 20 5 OK MW-40 Silver 10 ug/L u 20 10 OK MW-40 Sodium 10 mg/L 10 0.5 OK MW-40 Sulfate 50 mg/L 100 1 OK MW-40 Tetrahydrofuran 1 ug/L u 1 1 OK MW-40 Thallium 0.5 ug/L u 5 0.5 OK MW-40 Tin 100 ug/L u 20 100 OK MW-40 Toluene 1 ug/L u 1 1 OK MW-40 Total Dissolved Solids 20 MG/L 2 10 OK MW-40 Uranium 0.5 ug/L 5 0.3 OK MW-40 Vanadium 15 ug/L u 1 15 OK MW-40 Xylenes, Total 1 ug/L u 1 1 OK MW-40 Zinc 10 ug/L u 5 10 OK MW-65 Acetone 20 ug/L u 1 20 OK MW-65 Arsenic 5 ug/L u 20 5 OK MW-65 Benzene 1 ug/L u 1 1 OK MW-65 Beryllium 0.5 ug/L u 5 0.5 OK G 5AQ -I S I R uarter1y amp e eporllng 1m1t ec L ' . Ch k Lab Required Reporting Dilution Reporting RL Location Analyte Limit Units Qualifier Factor Limit Check MW-65 Bicarbonate as CaCO3 1 mg/L 1 I OK MW-65 Cadmium 0.5 ug/L 20 0.5 OK MW-65 Calcium 10 mg/L IO 0.5 OK MW-65 Carbon tetrachloride 1 ug/L u 1 1 OK MW-65 Carbonate as CO3 1 mg/L u 1 1 OK MW-65 Chloride 10 mg/L 100 l OK MW-65 Chloroform 1 ug/L u 1 1 OK MW-65 Chloromethane l ug/L u l 1 OK MW-65 Chromium 25 ug/L u 20 25 OK MW-65 Cobalt IO ug/L u 20 IO OK MW-65 Coooer IO ug/L u 20 IO OK MW-65 Fluoride 0.1 mg/L 1 0.1 OK MW-65 Gross Radium Alpha 0.523 oCi/L u l l OK MW-65 Iron 30 ug/L u 5 30 OK MW-65 Lead 1 ug/L u 5 1 OK MW-65 Magnesium l mg/L IO 0.5 OK MW-65 Manganese IO ug/L 20 IO OK MW-65 Mercury 0.5 ug/L u l 0.5 OK MW-65 Methyl ethyl ketone 20 ug/L u l 20 OK MW-65 Methylene chloride 1 ug/L u 1 1 OK MW-65 Molybdenum IO ug/L u 20 10 OK MW-65 Naphthalene l ug/L u l 1 OK MW-65 Nickel 20 ug/L u 20 20 OK MW-65 Nitrate + Nitrite as N 0.1 mg/L u IO 0.1 OK MW-65 Nitrogen, Ammonia as N 0.05 mg/L u 1 0.05 OK MW-65 Potassium l mg/L 1 0.5 OK MW-65 Selenium 5 ug/L u 20 5 OK MW-65 Silver 10 ug/L u 20 IO OK MW-65 Sodium 10 mg/L IO 0.5 OK MW-65 Sulfate 50 mg/L 100 1 OK MW-65 Tetrahydrofuran 1 ug/L u l 1 OK MW-65 Thallium 0.5 ug/L u 5 0.5 OK MW-65 Tin 100 ug/L u 20 100 OK MW-65 Toluene 1 ug/L u l 1 OK MW-65 Total Dissolved Solids 20 MG/L 2 IO OK MW-65 Uranium 0.5 ug/L 5 0.3 OK MW-65 Vanadium 15 ug/L u 1 15 OK MW-65 Xylenes, Total 1 ug/L u l l OK MW-65 Zinc 10 ug/L 20 IO OK G SBA -cce erate dS amp e . eportmg I R 1m1t ec L .. Ch k '. I Lab Required Reporting Dilution Reporting Location Analyte Limit Units Qualifier Factor Limit RLCheck Trip Blank Carbon tetrachloride 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Methylene chloride 1 ug/L u 1 1 OK Trip Blank Carbon tetrachloride 1 ug/L u 1 1 OK Trip Blank Chloroform 1 ug/L u 1 1 OK Trip Blank Methylene chloride 1 ug/L u 1 1 OK MW-11 Sulfate 50 mJ;!,/L 100 1 OK MW-11 Chloride 10 mg/L 100 1 OK MW-11 Sulfate 100 mg/L 200 1 OK MW-11 Chloride 2 mg/L 20 1 OK MW-26 Chloride 5 mg/L 50 1 OK MW-26 Carbon tetrachloride 1 ug/L u 1 1 OK MW-26 Chloroform 10 ug/L 10 1 OK MW-26 Methylene chloride 1 ug/L 1 1 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-26 Chloride 2 mg/L 20 1 OK MW-26 Carbon tetrachloride 1 ug/L u 1 1 OK MW-26 Chloroform 10 ug/L 10 1 OK MW-26 Methylene chloride 1 ug/L u 1 1 OK MW-26 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-30 Chloride 5 mg/L 50 1 OK MW-30 Uranium 0.5 ug/L 5 0.3 OK MW-30 Selenium 5 ug/L 5 5 OK MW-30 Nitrate + Nitrite as N 0.2 mg/L 20 0.1 OK MW-30 Chloride 5 mg/L 50 1 OK MW-30 Uranium 0.3 ug/L 2 0.3 OK MW-30 Selenium 5 ug/L 2 5 OK MW-30 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-31 Sulfate 50 mg/L 100 1 OK MW-31 Chloride 10 mg/L 100 1 OK MW-31 Uranium 0.5 ug/L 5 0.3 OK MW-31 Nitrate+ Nitrite as N 0.1 mg/L 10 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-31 Sulfate 50 mg/L 100 1 OK MW-31 Chloride 10 mg/L 100 1 OK MW-31 Uranium 0.3 ug/L 2 0.3 OK MW-31 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-31 Total Dissolved Solids 20 MG/L 2 10 OK MW-65 Chloride 5 mg/L 50 1 OK MW-65 Uranium 0.5 ug!L 5 0.3 OK MW-65 Selenium 5 ug/L 5 5 OK MW-65 Nitrate + Nitrite as N 0.2 mg/L 20 0.1 OK MW-65 Sulfate 100 mg/L 200 1 OK MW-65 Chloride 1 mg/L 10 1 OK MW-65 Uranium 0.3 ug/L 2 0.3 OK MW-65 Nitrate + Nitrite as N 0.1 mg/L 10 0.1 OK MW-65 Total Dissolved Solids 20 MG/L 2 10 OK G-6A: Quarterly Sample Trip Blank Evaluation ,. Lab Report ·constituent Result 2-Butanone ND Acetone ND Benzene ND Carbon Tetrachloride ND Chloroform ND AWAL 2107791 Chloromethane ND Methylene Chloride ND Naphthalene ND Tetrahydrofuran ND Toluene ND Xvlenes, Total ND G-6B: Accelerated Sample Trip Blank Evaluation All trip blanks for the Accelerated samples were non detect. Blm$ ·~~D.m 11111l:'b:m:ator, AWAL 2108362 8/10/2021 AWAL A WAL 2109256 9/9/2021 AWAL G 7A QA/Q E I -II.,; va uatlon or ~ Q I S uarteny amp e up 1cates I D I" onstitu~nt MW-14 7/,27/21 MW-65 7/27/21 %·RPO Bicarbonate as CaCO3 (mg/L) 355 415 15.58 Cadmium (mg/L) 0.00163 0.00130 22.53 Calcium (mg/L) sos 508 0.59 Chloride (mg/L) 19.0 19.2 I.OS Fluoride (mg/L) 0.109 0.103 5.66 Magnesium (mg/L) 157 160 1.89 Manga nese (mg/L) 1.84 1.85 0.54 Potassium (m!!.IL) 14.7 14.3 2.76 Sodium (mg/L) 334 338 1.19 Sulfate (mg/L) 2200 2190 0.46 TDS (mg/L) 3810 4230 10.45 Uranium (mg/L) 0.0600 0.0573 4.60 Zinc 0.0152 0.0211 32.51 Pc::r the approved QAP, an RPO greater than 20% is acceptable if the reported result are less than S times the RL. These results are provided for information only. ~ NI A -The duplicate test was not performed because both results were not greater than the RL. G 7B QA/QC E 1 -va uat10n or ~ A cce erate amp e up 1cates dS I D r MW-30 MW-65. C.ons:tituenf 8/9/21 8/9/21 %RPD* Nitrate + Nitrite (as N) (mg/L) 16.5 18.6 11.97 Selenium (mg/L) 0.0561 0.0572 1.94 Uranium (mg/L) 0.00938 0.00948 1.06 Chloride (mg/L) 161 181 11.70 MW-3J. MW-65 Consti.tuent 9/7/t},1 9/7/2-1 .%RPO Nitrate + Nitrite (as N) 16.0 16.5 3.08 Sulfate (mg/L) 1130 1130 0.00 Total Dissolved Solids (mg/L) 2870 3640 23.66 Uranium (mg/L) 0.0202 0.01940 4.04 Chloride (mg/L) 356 356 0.00 RPD exceeds the QAP limit of 20%. G-8A: Quarterly Sample Radiologies Counting Error Gross Alpha Counting Gross Alpha minus Rn & minus Rn and U Error~ Within Well u Precision ( +/-) 20% GWCL GWCL? MW-11 l.00U 0.188 NC 3.75 NC MW-14 l .00U 0.386 NC 7.5 NC MW-24 1.92 0.359 y 7.5 NIA MW-24A 2.77 0.475 y - MW-25 1.00U 0.213 NC 7.5 NC MW-26 1.71 0.339 y 4.69 NIA MW-30 l .00U 0.208 NC 3.75 NC MW-31 l.00U 0.190 NC 7.5 NC MW-36 1.00 U 0.205 NC 7.5 NC MW-38 1.00U 0.236 NC - MW-39 2.50 0.412 y - MW-40 1.00U 0.202 NC - MW-65 l.00U 0.143 NC 7.5 NC NIA -the counting error is less than 20% of the activity as required by the GWDP and this check column is not applicable. NC = Not calculated. The sample results are nondetect and the check is not applicable. G-8B: Radiologies Counting Error for Accelerated Samples There are no accelerated samples collected for Gross Alpha. G-9A: Quarterly Sample Laboratory Matrix QC Matrix Spike % Recovery Comparison RPO Lab Report WeU Analyte MS %REC MSD %REC REC Range RPO Range 2107668 MW-28 Nitrate 132 99.1 90-110 18.7 10 2107791 MW-31 Calcium* NC NC 70-130 NC 20 2107791 MW-31 Manganese* NC NC 70-130 NC 20 2107791 MW-14 Sodium* NC NC 70-130 NC 20 2107791 MW-14 Manganese* NC NC 70-130 NC 20 2107791 MW-14 Calcium* NC NC 70-130 NC 20 2107791 MW-28 Nitrate 132 99.1 90-110 18.7 10 2107791 MW-24 Nitrate 116 147 90-110 22.7 10 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount Method Blank Detections All Method Blanks for the quarter were non-detect. Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. Laboratory Duplicate % Recovery Comparison All Laboratory Duplicate samples were within acceptance limits for the quarter. G-9B: Accelerated Laboratory Matrix QC Matrix Spike % Recovery Comparison Lab,RtMrt 2108362 -August Monthly 2109256 -September Monthly W~ll MW-26 MW-26 --- Aoalyte Chloroform Chloroform -- ~$oime MSD%.REC -6.55 0.1 104 129 * Recovery was not calculated as the analyte level in the sample was greater than 4 times the spike amount Laboratory Duplicate % Recovery Comparison All Laboratory Duplicates were within acceptance limits for the quarter. Method Blank Detections All Method Blanks for the quarter were non-detect Laboratory Control Sample All Laboratory Control Samples were within acceptance limits for the quarter. RPDR:ange RECRang-e. RPO% %.. 74-120 1.09 35 74-120 6.7 35 TabH Kriged Current Quarterly Groundwater Contour Map ..... ,_ @ TWN-20 C 5565 TW4-42 ¢5525 MW-38 -Q-5463 TW4-40 ♦5525 estimated dry area temporary perched nitrate monitoring well installed April, 2021showing elevation in feet amsl temporary perched monitoring well installed April, 2019 showing elevation in feet amsl perched monitoring well installed February, 2018 showing elevation in feet amsl temporary perched monitoring well installed February, 2018 showing elevation in feet amsl M;'55 504 perched monitoring well showing elevation in feet amsl TW4-12 . . 0 5568 temporary perched momtonng well showing elevation in feet amsl TWN-7 hed . . . <> temporary perc nitrate momtonng 5569 well showing elevation in feet amsl PIEZ-1 perched piezometer showing '-5588 elevation in feet amsl RUIN SPRING o 5380 seep or spring showing elevation in feet amsl DR-10 • ~ DR-11 , . llR•U-• ' ' ' ... ... ... ~~ llWN-o9 "i;1l PIU;01 ,~ .. .. ,II""' • . , ;/· TWl,(-11 : ··'11"·'" l'WN'12' '·o TWtM NOTES: MW-4, MW-26, TW4-1, TW4-2, TW4-4, TW4-11, TW4-19, TW4-21, TW4-37, TW4-39, TW4-40 and TW4-41 are chloroform pumping wens; TW4-22, TW4-24, TW4-25 and TWN-2 are nitrate pumping wells; TW4-11 water level is below the base of the Burro Canyon Formation HYDRO GEO CHEM, INC. KRIGED 3rd QUARTER, 2021 WATER LEVELS WHITE MESA SITE APPROVED DATE REFERENCE FIGURE H:/718000/nov21 /WUUwl0921 srf H-1 Tab I Groundwater Time Concentration Plots Time concentration plots for MW-01 0.4 ~ .5. GI 0.3 '0 ·c: 0 :::, Li: ~sS~NTERA Chloride in MW-01 Sample Date Fluoride in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-01 5000 4500 4000 3500 ::;-3000 -.. E "; 2500 i Jl 2000 1500 1000 500 G) J --· - I ~9.slNTERA ■ I - Sulfate in MW-01 A. ------~-----~ -- Sample Date Uranium in MW-01 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ---~~ Detected Values ■ Non-Detected Values Time concentration plots for MW-02 Chloride in MW-02 Sample Date Fluoride in MW-02 0.9 0.8 0.7 0.6 ::r -l o.s QI :2 ~ 0.4 :::, ii: 0.3 0.2 0.1 0 r::"°' # 0 ... ~<:' Sample Date ~¾slNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-02 Sulfate in MW-02 0 -1-....... -~---~--~---~--~---~------~----1 e;"°' 0 20 18 16 14 ::l' 12 } E 10 :::, ·2 I!! 8 :::, 6 4 2 0 --._o, C: 0 ~ ... ~<:' ... J£e~NTERA Sample Date Uranium in MW-02 /''b ,:,'\-~ ~o_,. Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-OJA Chloride in MW-03A Sample Date Fluoride in MW-03A 1.8 1.6 1.4 1.2 ~ 'bi! 1 .s a, -a ·g 0.8 :::, il: 0.6 0.4 0.2 0 s:i<-> s5' ~ if ..,-s ~ Sample Date ~cilNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-03A Sulfate in MW-03A 4500 4000 3500 3000 ~ i 2500 a, .... ~ 2000 :::, VI 1500 1000 500 0 I)., ~s::," fJ'b ~ 'l,(; ..,~ ~'I, <;) Sample Date Uranium in MW-03A -25 -H--lt-1---------------~---------------1 -' l § 20 1t-t------t-7 ... -.~-:-,L--7r,--r-r,--.-----::::::::::;;~-t("-Jf ·2 ~ ::::, 15 +-11-1--------------------------------t ~sSINTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values 140 120 100 ::;- "oo 80 E. cu "Cl -~ 60 :E u 40 20 1.8 1.6 1.4 1.2 ::;- "oo 1 -E. cu "Cl -~ 0.8 :I i:i: 0.6 0.4 0.2 0 !:i .x'IJ ~'I> {J~ ~~ Time concentration plots for MW-05 Chloride in MW-OS Sample Date Fluoride in MW-OS Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-05 9000 8000 7000 6000 ::l' 15000 fl ~ 4000 ::, "' 3000 2000 ' -I.. I.. -1000 0 ' 160 140 120 _ 100 ... -~ E 80 ::, ·2 ~ ::::, 60 40 20 --0 -- ~islNTERA Sulfate in MW-05 -A -• -- Sample Date Uranium in MW-05 -~ -• --.. Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ----~-..a...1 .. - G' ' ~ ' ~ Detected Values ■ Non-Detected Values Time concentration plots for MW-11 Chloride in MW-11 80 70 60 _ 50 ...I 'iio !. a, 40 "C ·c: 0 :E I.I 30 20 10 0 r.:'b'\, <:f i:'b' "(-q Sample Date Fluoride in MW-11 Sample Date ~4-s lNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-11 Sulfate in MW-11 Sample Date Uranium in MW-11 ::. } 2.5 -1--------------j~-----~---------------l E :::, ·c 2 +-------------------111-+------------------1 f ::J ~is~NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 O Detected Values ■ Non-Detected Values Time concentration plots for MW-12 0.4 0.35 0.3 -0.25 -' "iio .s 111 0.2 "tJ "§ :::, U:: 0.15 0.1 0.05 0 ~silNTERA Chloride in MW-12 Sample Date Fluoride in MW-12 - '\ J ~ --'\ .. \j I - Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 --r~l • t r, I I u l Detected Values ■ Non-Detected Values Time concentration plots for MW-12 Sulfate in MW-12 ::i-i 5000 +---11------------------------------i J!! J!! 4000 1---..-.-------------------------------1 :i "' 2000 Sample Date Uranium in MW-12 20 ::.-} E 15 :I ·2 I!! ::I 10 Sample Date Detected Values ~rilNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values -::;-~ E. Qj :2 5 :c u Time concentration plots for MW-14 Chloride in MW-14 20 15 10 o -1---~---~-----.----~---~--~---.----.-----1 ,¥q,OJ ~o Sample Date Fluoride in MW-14 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-14 Sulfate in MW-14 Sample Date Uranium in MW-14 80 ::;- } E 60 :I c I! ::, 40 Sample Date ~¼INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values ::; ~ .§. QJ -0 ·c 0 :E u Time concentration plots for MW-15 Chloride in MW-15 40 30 20 0 +-----.-----...-----,-----.----,-------.-----,------,--------! ,i:<o°' ~o fo ¢!OJ 0 Sample Date Fluoride in MW-15 Sample Date Detected Values ~½INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-15 Sulfate in MW-15 0 +-------.-----,-------,-----,------.-----...---------r----.,.....-----1 ~<o°' ❖o Sample Date Uranium in MW-15 } 40 +--I---U--fl---1,f--Mll+-f--lt----------;I----H-----ff---..._----='---1 E :::, c ~ 30 +-----'ll-41-1-------------------------------; :::, 0 +-----,-----r------r-----.-------.-----.----...-------.--------1 ,l°' 0 ~rilNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values Time concentration plots for MW-17 Chloride in MW-17 0 -t-----,.-----r------,,----,----,-----.----r-----.--------, ~"' .... ~o ~¾slNTERA Sample Date Fluoride in MW-17 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values Time concentration plots for MW-17 Sulfate in MW-17 ~ 2000 -·11----wi-------------------~-----=-=------=~~ .5. ! :i 1500 +--llt--..... +-------------------------~--t Ill 0 -t------,----~-----,-----,--------r----,---------,----..----t i:°'"' ~,,, 50 45 40 35 ~ 30 } E 25 :I 'i: "' ... 20 • ::::, 15 10 5 0 i:°'"' ~,,, Sample Date Uranium in MW-17 ~ ~Oj ~,,, Sample Date Detected Values ~4.INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values 80 70 60 _ 50 ... GO .§. a, 40 "Cl ·;:: 0 :E V 30 20 10 0 5:°'"' ~~ ::; GO .§_ 0.25 a, "Cl Time concentration plots for MW-18 Chloride in MW-18 ro -x"" ~~ Sample Date Fluoride in MW-18 -~ 0.2 +---------------+~#-'W-~r--,F--------11--~=----+--t---i ::I u:: ~4-s lNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-18 Sulfate in MW-18 ~ 1500 -t-:a:-11---------,-~r-----------------11-t----------1 "oa .§. ! ] 1000 -1--------------------------------1 0-1---------------------~--~-------1 i:°'"' ~'Ii Sample Date Uranium in MW-18 0-1-------~--~---~------~---~---------1 i:°'"' ~'Ii Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 9 Detected Values ■ Non-Detected Values Time concentration plots for MW-19 Chloride in MW-19 100 90 80 70 ::::;-60 "oa .§. GJ 50 -a -~ :E 40 u 30 20 10 0 ~"'"' ro !'l°' ~'l, ~<, -XOJ ~ ~"" </'~ ~'Ii ~'Ii '>" 'I" Sample Date Fluoride in MW-19 ::::;-i t---"711,;;;;;;:::--~l-------ttr-."'t-""'~---~F"1.,...-"'1F~"t-__,, "oa E "; 0.8 "f<'-----------------IIJ----------------------1 -a ·c: 0 :::, U:: 0.6 +------------------------------------1 Sample Date Detected Values ~4-INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values ::; -a E ::, ·c f ::::, Time concentration plots for MW-19 Sulfate in MW-19 0-1--------~------~------~--~---~---1 l'"' ~,,, 20 15 10 Sample Date Uranium in MW-19 0-1----~---~------~---~--~---~--~---1 !:o,"> ~,,, Sample Date Detected Values ~silNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-20 Chloride in MW-20 80 70 60 _ 50 ... -1111 .§. GJ 40 "Cl -~ :c u 30 20 10 0 9,'0o .¥°'" .: Qe; ~o Sample Date Fluoride in MW-20 Sample Date ~rffilNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-20 Sulfate in MW-20 4500 4000 3500 3000 :::;-1: 2500 .2l '" 2000 ~ ~ Ill 1500 1000 500 0 9J~ ,i' <f Q"' ~o Sample Date Uranium in MW-20 40 35 30 :::;-25 } E 20 ~ ·2 f ::J 15 10 5 0 r.:°'~ Q"' /J-~o Sample Date ~¼INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values 80 70 60 _ 50 ... tio .5. QI 40 :2 l5 :E u 30 20 10 0 ,:;°',;. ~e; 20 ::; tio .5. QI 15 "0 ·c: 0 :::, ii: 10 ,i'' ~o Time concentration plots for MW-22 Chloride in MW-22 Sample Date Fluoride in MW-22 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-22 Sulfate in MW-22 8000 7000 6000 5000 ::;--.. E "; 4000 ... ~ :I .,, 3000 2000 1000 0 9i'Oo ~OJ" <J Qe; ~o Sample Date Uranium in MW-22 40 ::;- } E 30 :I ·c I!! ::::, 20 Sample Date ~sf~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-23 Chloride in MW-23 -::;-bD 20 -t-----------11a--------------------------1 .§.. cu -a ·c: o 15 +--------~11----------------------------l a Sample Date Fluoride in MW-23 0.9 0.8 0.7 0.6 -::;- b'.a .§_ 0.5 cu -a ~ 0.4 ::I ii: 0.3 0.2 0.1 0 s:,'> ... ~~ ~ 'i'-~' Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values 90 80 70 60 ~ } 50 E :::, ·2 40 "' .. ::::, 30 20 10 0 !:)., {;( -,-i ~ ~,§ Time concentration plots for MW-23 Sulfate in MW-23 Sample Date Uranium in MW-23 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-24 Chloride in MW-24 80 70 60 _ 50 ... ..... "° .s QI 40 -0 ·5 :E u 30 20 10 0 5)"> ~ -..v<;< ~-"r-q Sample Date Fluoride in MW-24 1.6 1.4 1.2 ::;-1 ... .s QI 0.8 -0 ·c: 0 :::, U: 0.6 0.4 0.2 0 5)., ~ -..v<;< sf \" Sample Date ~¾elNTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-24 Sulfate in MW-24 ~ 2000 +-------------------------------------1 .§. ! ~ 1500 +----------------------------------1 "' 250 200 :J" 150 l E ~ 'i: [!! :::> 100 so 0 ...... Sample Date Uranium in MW-24 A --- Sample Date Detected Values ..J!e~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-24A Chloride in MW-24A Sample Date Fluoride in MW-24A Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values 4000 3500 3000 1000 500 0 10 9 8 7 :::; 6 } E 5 :, ·c "' ::> 4 2 1 0 c,-...,___ Time concentration plots for MW-24A Sulfate in MW-24A ---__,,-,,-" -----~ "-. -.....,..- Sample Date Uranium in MW-24A - ~ --~ / Sample Date ~¼INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 _..., / Detected Values ■ Non-Detected Values Time concentration plots for MW-25 Chloride in MW-25 40 35 30 _ 25 ... ~ .§. a, 20 "Cl ·c 0 ::c V 15 10 5 0 5)., ~ ,_,(' SI\ 'I" Sample Date Fluoride in MW-25 0.6 ~------------------------------~ 0.5 -1--------------------------------------1 0.2 -t--------------------,._------1---------t 0.1 '1-----------------------------------t 0 -t-------.-----,-----,----,----~--""T"'---~---r-------t ~ai~NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-25 Sulfate in MW-25 2000 -r-----------------------------------, ::;-1200 +------------------------------------1 "iio E '"aj" 1000 +------------------------------------1 ... J!! :i VI 800 +----------------------------------1 600 +----------------------------------1 400 -1------------------------------------1 200 +------------------------------------1 0 +------,------.---,------,-----.-----,-----,------,--------1 Sample Date Uranium in MW-25 i E 6 ::, c f :) 111!!-¼~NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values 100 90 80 70 ::;-60 "iio !. a, so "0 ·;:: 0 :E 40 I.I 30 · 20 10 0 s:i"' ',q,<:J. ~ 0.6 !. Time concentration plots for MW-26 Chloride in MW-26 ~ s:i"' 0 ~q,C Sample Date Fluoride in MW-26 a, 0.5 +-, _______________ __.. ______________ ---I "0 ·;:: 0 ~ 0.4 -----------------------------+-----1-11--l ~ailNTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 • Detected Values ■ Non-Detected Values Time concentration plots for MW-26 Sulfate in MW-26 ::; 1500 +---------------------IIF-------=------------1 tia .s ! ~ ~ 1000 +-------------------------------------1 Sample Date Uranium in MW-26 140 120 100 ::; ...... 80 11: E ::, ·c 60 ra ... ::::, 40 Sample Date Detected Values ~◄~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-27 Chloride in MW-27 40 -:;-'.a .§. cu 30 :2 ~ :E u 20 Sample Date Fluoride in MW-27 Sample Date ~¼~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-27 Sulfate in MW-27 Sample Date Uranium in MW-27 35 30 25 ::; l 20 E :I ·2 15 I'!! ::, 10 5 Sample Date ~ci~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-28 Chloride in MW-28 180 160 140 120 ::; ...... "° 100 E. QI "O ·c: 80 0 :E u 60 40 20 0 !:)<, ~ ~ 'l'<f \.,j Sample Date Fluoride in MW-28 0.8 ..-----------------------------------, 0.2 4-----------------------------------1 0.1 -t----------------------------------1 0 4-----,.---~-----.----~------,.-----.-----,-----,,----1 Sample Date Detected Values ~ri~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-28 70 60 50 -::;- } 40 E :::, c I! 30 :::, 20 10 0 !' ~ Sl°' •l ... ~~ ..,-s ►--¾s~NTERA Sulfate in MW-28 Sample Date Uranium in MW-28 <:) g:,'Y' b, ~...,,ro e;"> ,,. .. 0 't-,s ~-,; ~~ Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ~ c Qe; °' ~,,.... r;~ 0 ..,-s Detected Values ■ Non-Detected Values Time concentration plots for MW-29 Chloride in MW-29 -.:;- ~ 25 .s cu :2 l5 20 :E u 15 10 5 0 S')., ~ S')'b :,<:i '>°"<:' ~,f ,,,c .,,,,q <J Sample Date Fluoride in MW-29 0.8 -.:;-~ .s cu 0.6 ,:, ·~ :i ii: 0.4 Sample Date ~¾s ~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-29 Sulfate in MW-29 3500 -..----------------------------------, ~ 2000 +-----------------11--------------------1 .E.. ! '3 1500 +----------------U--------------------1 VI 1000 +-----------------------------------1 500 +------------------------------------1 0 .....-----.------.------,-------.----.----,-----r----.------1 Sample Date Uranium in MW-29 60 so 40 ::;--1 E 30 :::, "i: ~ :::::, 20 -~ ---- 10 -... ---------IT -- • 0 Sample Date • Detected Values ~-INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-30 Chloride in MW-30 Sample Date Fluoride in MW-30 ::. "iio 0.4 ~-_.-~-----&------------1--1--6---iJ---ll----l .§. cu -0 'g 0.3 +----------------------+-----------------;:;: Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-30 Sulfate in MW-30 800 ~ -;. E. 600 l!l J! :i VI 400 Sample Date Uranium in MW-30 14 12 10 ~ } 8 E :I ·c 6 I! :::, 4 2 Sample Date ~¾e~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-31 Chloride in MW-31 450 400 350 300 -.:;- "iio 250 .§. QI "C -~ 200 :E u 150 100 so D s:i"> ~ t:I ,_q~ ..,-:s Sample Date Fluoride in MW-31 -.:;-"iio 0.8 -+-------+---t-----...;;.:;::,,._---1,:=------,~ft--e--------... --1+-c:::---a--1 .§. QI "C ·c: g 0.6 -1---------11-1------------..... ----------1.t--==--....!f li: ~+.~NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values 1400 1200 1000 ::. -800 ..., .§. ~ ~ 600 ::, "' 400 200 Time concentration plots for MW-31 Sulfate in MW-31 Sample Date Uranium in MW-31 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 e Detected Values ■ Non-Detected Values Time concentration plots for MW-32 0 $:,'\, ? ft .,,,,q 0 ~o 0 .,,,,<!''\, ? <:)~ rf 0 0 ~¼~NTERA Chloride in MW-32 $:J'b ❖ ~..,,,,, }' .,c :<$ <:) '<e; ~'I> ~Q Sample Date Fluoride in MW-32 $:J'b (f..,,<:) ~ ~ ~o.:i; ~ «efJ <:)e; ..... Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ~ ~..,, ~'I> ~ «efJ ~ ~,..,... ~ '>" '>" ~~ ~'I> !.',..,... ~Q 0 Detected Values ■ Non-Detected Values Time concentration plots for MW-32 Sulfate in MW-32 Sample Date Uranium in MW-32 i4 --~~~---------------------------~ E :I l3 ~-f~~~~~-------------------------~ :) Sample Date Detected Values ~is ~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-35 Chloride in MW-35 Sample Date Fluoride in MW-35 ::.-'iio 0.4 'l---:a:,-----:=,-----lk------------------ll---'t-------.11.-="'l-----+--l .§. GI "Cl 'g 0.3 -t-------------H ....... r---#-------"~-l----t-------#----+-1------"1 ..: 0 +-----,----~----,---~----,-----.-----,------r------1 (J...,c::. Q,r; Sample Date Detected Values White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-35 Sulfate in MW-35 0-1----~---~---~--~---~---~--~---~----1 ~..,<::, c;J& Sample Date Uranium in MW-35 } 20 -tt--f-l~r----4~11--F'-----~--=----___:_ov--..:=.:::...---.:at~,:,.'--------'"-c:::~c:;__---i E :::, 'i: f 15 +-.----------------------------------, ::::, Sample Date Detected Values EWsi~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-36 ~¼~NTERA Chloride in MW-36 Sample Date Fluoride in MW-36 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-36 Sulfate in MW-36 ~ 2000 +-------------------------------------; .§. ! ~ 1500 +-------------------------------------1 Ill Sample Date Uranium in MW-36 20 ~ } E 15 ~ ·2 .. ... ::J 10 Sample Date Detected Values ~is~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-37 Chloride in MW-37 Sample Date Fluoride in MW-37 Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-37 Sulfate in MW-37 Sample Date Uranium in MW-37 20 18 16 14 ::i' 12 -l E 10 :::, ·c f! 8 ::::, 6 4 2 0 ..,, !'>'\, ((,..,, ~-:s c.,efl Sample Date ~4-s ~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-38 Chloride in MW-38 so 45 40 ~ ..A.... _._ __.... "/ ~ -V 35 ~ 30 OD .§. a, 25 -a -~ :c 20 u 15 10 5 0 Sample Date Fluoride in MW-38 0.8 ::. tia .§. a, 0.6 -a ·;:: 0 :I ·u:: 0.4 Sample Date .... J£s ~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ~ Detected Values ■ Non-Detected Values Time concentration plots for MW-38 Sulfate in MW-38 3500 3000 2500 .A ~ ~ '~ ~ ~ ~ ---..--- ~ 2000 .§. .l!! "' ... 1500 :j VI 1000 500 0 Sample Date Uranium in MW-38 ::;- } 6.4 E ::, ·2 ~ 6.2 ----+-_._-----------+------------------l :) ~¼~NTERA Sample Date White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-39 Chloride in MW-39 44 43 42 41 ::. ....... .§'. 40 QI "C -~ 39 ::c u 38 37 36 35 'b :-,,'b ~ ~ ,(..., c.,e':/. ..,,,,~ ~ ~,,, ..,-s Sample Date Fluoride in MW-39 0.8 ::. .;a E. QI 0.6 "C ·c: 0 :::, i.: 0.4 Sample Date ~◄INTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values ::. 'iio E 4000 3500 3000 2500 "; 2000 ... ~ :I Ill 1500 1000 500 0 11,,. " Time concentration plots for MW-39 _.>.... 'V" Sulfate in MW-39 '-ti" --/ {') tf 0 .--.... -......... Sample Date Uranium in MW-39 ~ ------ ___. -10 +-------------------------------------1 } E a +-------------------------------------1 :I ·c I'!! ~ 6 +-------------------------------------1 Sample Date Detected Values •.. ih,~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Time concentration plots for MW-40 Chloride in MW-40 40 ::. ~ E. QJ 30 :2 l::i :c u 20 Sample Date Fluoride in MW-40 0.9 0.8 0.7 0.6 ::. ~ E, 0.5 QJ "ti ·;:: 0.4 0 :::, ;:;: 0.3 0.2 0.1 0 'I, :-,.'I> !',,°' ~ ,i:_"> c,"'q § § ~,,, ..,,,, ..,-1$ Sample Date ~ri~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for MW-40 Sulfate in MW-40 Sample Date Uranium in MW-40 20 ::;- 1 E 15 ::, ·c I! ::) 10 Sample Date ~¼~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration plots for TW4-24 Chloride in TW4-24 1400 1200 1000 -::;- ~ 800 £ QI :2 ~ 600 ::c u 400 • 200 Sample Date Fluoride in TW4-24 0.45 0.4 0.35 0.3 -::;-~ £ 0.25 QI "D -~ 0.2 :, ii: 0.15 0.1 0.05 0 'b ~'b ~ ... ~'Ii c,e<:i Sample Date •··~9hs ~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 Detected Values ■ Non-Detected Values Time concentration pl~ts for TW4-24 Sulfate in TW4-24 ~ 2000 --------------------------------- £ ! ~ :i 1500 +---------------------------------1 Ill Sample Date Uranium in TW4-24 900 · 800 700 600 -::;- } 500 E :I ·2 400 I! :::> 300 200 100 0 'b :-,,'b ;/I(. ... ~'Ii c.,eq Sample Date Detected Values ~¾a~NTERA White Mesa Uranium Mill Groundwater Monitoring Report 3rd Quarter 2021 ■ Non-Detected Values Tab J CSV Transmittal Letter Kathy Weinel From: Sent: To: Cc: Subject: Attachments: Dear Mr. Goble, Kathy Weinel Tuesday, November 2, 2021 12:09 PM Phillip Goble Thomas Rushing; David Frydenlund; Logan Shumway; Garrin Palmer; Scott Bakken Transmittal of CSV Files White Mesa Mill 2021 Q3 Groundwater Monitoring Q3 2021 DTW all programs.csv; Q3 2021 GW Analytical Data.csv; Q3 2021 GW Field Data.csv Attached to this e-mail is an electronic copy of laboratory results for groundwater monitoring conducted at the White Mesa Mill during the third quarter of 2021, in Comma Separated Value (CSV) format. Please contact me at 303-389-4134 if you have any questions on this transmittal. Yours Truly Kathy Weinel f ' gf Energy Fuels Resources (USA) Inc. Kathy Weinel Quality Assurance Manager t:303.389.4134 I c: I t:303.389.4125 KWeinel@energyfuels.com 225 Union Blvd., Suite 600 Lakewood, CO 80228 http://www.energyfuels.com This e-mail is intended for the exclusive use of person(s) mentioned as the recipient(s). This message and any attached files with it are confidential and may contain privileged or proprietary information. If you are not the intended recipient(s) please delete this message and notify the sender. You may not use, distribute print or copy this message if you are not the intended recipient(s). 1