DERR-2024-006543

WSP USA Environment & Infrastructure Inc.
10876 South River Front Parkway; Suite 250
South Jordan, Utah 84095
T: [phone]
F: [phone]
wsp.com
March 9, 2023
Mr. Damian Foti
General Electric Company
1 River Road 5-7W
Schenectady, New York 12305
Subject: Groundwater Sampling Results
50 East 1100 North
North Salt Lake, Utah
Dear Mr. Foti:
WSP USA Environment & Infrastructure Inc. (WSP) has prepared this letter report for the
Groundwater Sampling activities conducted at the 3D Storage property, owned by DS
Investments LLC (property owner) located at 50 East 1100 North, North Salt Lake, Utah
(Site) and west of the former General Electric (GE) North Salt Lake facility. WSP personnel
conducted the December 2022 groundwater sampling activities in accordance with the
off-site assessment scope of work provided on August 11, 2022, and accepted by Utah
Department of Environmental Quality (UDEQ), Division of Environmental Response and
Remediation (DERR) on August 18, 2022.
BACKGROUND
The UDEQ DERR requested additional sampling to evaluate the nature and extent of
potential impacts in groundwater by email on March 17, 2022, and the subsequent DERR
letter to GE on March 28, 2022. GE agreed to access with the property owner on a Right of
Entry Agreement signed by Chris Holder on August 18, 2022. On September 8, 2022,
monitoring wells, Offsite A-1 and Offsite A-2, were installed to a depth of 20 feet below
ground surface (bgs) and ground water samples were collected. Well locations are shown
on the site map as Figure 1. Following the initial September 2022 off-site monitoring well
installation and sampling and analysis event, the UDEQ requested that an additional
groundwater sampling event be conducted from the Offsite A-1 and Offsite A-2
monitoring wells in conjunction with the GE North Salt Lake On-Site December 2022
quarterly ground water sampling event.
GROUNDWATER SAMPLING
The water table was measured on December 12, 2022, at 8.39 feet bgs in Offsite A-1 and
9.91 feet bgs in Offsite A-2 Wells. Field data sheets (FDS) were used to record the depth to
water (DTW), total depth, and calculated well casing volume for each well. The FDS are
provided in Appendix A.
Groundwater samples were collected on December 14, 2022 and submitted for laboratory
analysis. The monitoring wells were purged and sampled with a peristaltic pump using
low flow purging and sampling procedures (EPA, 2017), as detailed in the approved SCW.
The water quality parameters of temperature, pH, specific conductivity, dissolved oxygen,
oxidation-reduction potential (ORP), and turbidity were measured during well purging at
five-minute intervals and recorded on the FDS (Appendix A).
Page 2
The groundwater samples were collected into clean, laboratory-provided sample
containers that contain the preservatives required by the analytical procedure and stored
in an ice filled container at approximately 4 degrees Celsius. Except for 1,4-Dioxane and
dissolved hydrogen samples, groundwater samples were delivered under chain-of-
custody documentation to Eurofins Environment Testing America (Eurofins) in Denver,
Colorado via overnight shipping. Groundwater samples for dissolved hydrogen were
delivered under chain-of-custody to Pace Analytical Gulf Coast (PACE) in Baton Rouge,
Louisiana via overnight shipping and groundwater samples for 1,4-Dioxane were hand
delivered under chain-of-custody to Chemtech-Ford Laboratories (CTF) in Sandy, Utah.
ANALYTICAL RESULTS
The analytical results of the groundwater samples were compared to the EPA Maximum
Contaminant Level (MCL) and/or the Tapwater Drinking Water Standard (TDWS) if no
MCL is available and summarized in the following section below. The laboratory analytical
reports are provided in Appendix B.
Volatile Organic Compounds (VOCs)
A summary of VOC results and applicable regulatory standards are provided in Table 1.
Monitored Natural Attenuation Parameters
The groundwater samples from Offsite A-1 and Offsite A-2 wells were also analyzed for
chemical parameters for Monitored Natural Attenuation (MNA) modeling. The list of
analytes and testing results is provided in Table 2.
DATA QUALITY
Quality Assurance (QA) and quality control (QC) measures for groundwater sampling
followed the requirements of the SAP. These measures included standardized procedures
for samples collection, preservation, delivery, and laboratory analysis. Evaluation of the
reliability and usability of data was done by analyzing QC samples.
Field QC samples collected during the groundwater sampling activities included a Trip
Blank, which was prepared by the laboratory and included in the same cooler used for
samples delivery.
QC SAMPLE ANALTYICAL RESULTS
The Trip Blank samples was analyzed for VOCs and 1,4-Dioxane and were included with
the samples collected from the wells located at the GE facility. The analytical results were
below the laboratory detection limits for the analytes.
LABORATORY QA/QC
The groundwater samples were analyzed for VOCs and MNA parameters at Eurofins in
Arvada, Colorado. Due to the method detection limits required for 1,4-dioxine, the
groundwater samples were analyzed for 1,4-dioxane at CTF in Sandy, Utah. The ground
water samples for dissolved hydrogen were analyzed at PACE in Baton Rouge, Louisiana.
Eurofins, CTF, and PACE are Utah Certified Laboratories under Utah Rule R444-14.
Laboratory Quality Assurance/Quality Control (QA/QC) procedures were followed in
accordance with the analytical methods used, and standard laboratory procedures. The
internal laboratory QA/QC for water samples included analysis of method blank,
laboratory control samples, MS/MSD, and surrogates. The laboratory Analytical Reports
(Appendix B) include QC data for the sample analyses, and a project narrative that
summarizes the review of QC parameters and explains any deviation from the analytical
Page 3
methods. Any deviation from established control limits is flagged by the laboratory and
noted in the analytical report by a qualifier letter, as described below.
•Alkalinity was detected in method blank MB 280-597409/110 at a level that was
above the method detection limit but below the reporting limit. Alkalinity was
detected in method blank MB 280-597409/6 at a level that was above the method
detection limit but below the reporting limit. Alkalinity was detected in method
blank MB 280-597409/84 at a level that was above the method detection limit but
below the reporting limit. If the associated sample reported a result above the
MDL and/or RL, the result was flagged.
•Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were received
with less than one shift remaining on a test with a holding time of 48 hours or less.
As such the laboratory had insufficient time analyze within holding time, these
samples were analyzed outside of holding time for nitrate and anion analysis.
•Samples Offsite A-1 (280-170477-1)[20X] and Offsite A-2 (280-170477-2)[20X]
required dilution prior to analysis. The reporting limits have been adjusted
accordingly.
•Sulfate was detected in method blank MB 280-598232/14 at a level that was above
the method detection limit but below the reporting limit. The value should be
considered an estimate and has been flagged. If the associated sample reported a
result above the MDL and/or RL, the result has been flagged.
•Samples Offsite A-1 (280-170477-1)[10X] and Offsite A-2 (280-170477-2)[10X] required
dilution prior to analysis. The reporting limits have been adjusted accordingly.
The quality of the data is acceptable. No data was rejected based on QA/QC parameters
and the analytical data is considered usable for the intended use.
REFERENCES
EPA Regional Screening Level (RSL) Summary Table (TR=1E-06, HQ=1) November 2022
UDEQ DERR Letter RE: General Electric Salt Lake City VCP Site, North Salt Lake, Utah
December 2022 Groundwater Monitoring Report, Former General Electric Facility, 130
East 1100 North, North Salt Lake, Utah, VCP No. C-102
SIGNATURES
If you have any questions, please do not hesitate to contact the undersigned.
Yours sincerely,
WSP USA
Environment & Infrastructure Inc.
Written By: Reviewed by:
Corey Buchanan, PG Bradley K Glisson, CHMM
Project Geologist Project Manager
Page 4
Attachments:
Figure 1 – Monitoring Well Locations
Table 1 – VOC Results
Table 2 – MNA Parameter Results
Appendix A – Field Data Sheets
Appendix B – Laboratory Analytical Reports
ATTACHMENT
FIGURES
© 2022 Microsoft Corporation © 2022 Maxar ©CNES (2022) Distribution Airbus DS
MW-15
MW-18
MW-3
MW-16
MW-17
MW-19
MW-2
MW-1
MW-4
MW-5
MW-6
B-11/MW-7
MW-22
MW-10
MW-11
MW-12
MW-13
MW-14
MW-20
MW-21
MW-8
MW-23
OFFSITE-A1
OFFSITE-A2
WSP USA Environment & Infrastructure, Inc.
10876 SOUTH RIVERFRONT PARKWAY SUITE 250,
SOUTH JORDAN, UTAH 84095
PHONE: [phone]
CHRIS HOLDER3D STORAGE 50 EAST 1100 NORTHNORTH SALT LAKE, UTAH
OFFSITE WELL INSTALLATION & SAMPLING REPORT
FIGURE 1
MONITORING WELL LOCATION MAP
ATTACHMENT
TABLES
December 2022 Groundwater Monitoring Report
Chris Holder, 3D Storage
Well ID Sample ID Sample Date 1,
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OFFSITE A-1 OFFSITE A-1 9/15/2022 <0.36 <0.40 <0.32 1.30 <0.65 74 <0.57 <0.51 NA NA NA NA NA NA NA
OFFSITE A-1 OFFSITE A-1 12/14/2022 <0.36 <0.40 <0.32 1.4 <0.65 67 <0.57 <0.51 NA NA NA NA NA NA NA
OFFSITE A-2 OFFSITE A-2 9/15/2022 <0.36 <0.4 <0.32 0.65 J <0.65 22 <0.57 <0.51 NA NA NA NA NA NA NA
OFFSITE A-2 OFFSITE A-2 12/14/2022 <0.36 <0.40 <0.32 0.87 J <0.65 27 <0.57 <0.51 NA NA NA NA NA NA NA
Notes:
^EPA Regional Screening Level (RSL) (TR=1E-6, HQ=1) MCL, November 2022, Except as noted
† DERR Tier-1 groundwater screening level, 2005
*EPA Regional Screening Level (RSL) (TR=1E-6, HQ=1) for tap water, November 2022
NA - not analyzed
J - analyte was detected below the laboratory reporting limit; value is estimatedBold denotes analyte exceeded the screening criteria
Units
Screening Levels^
TABLE 1: VOLATILE ORGANIC COMPOUNDS ANALYTICAL RESULTS
< Indicates the analyte was not detected at the method detection limit (laboratory reporting limit for 2017-2022 sampling)
Project # WDP0014
Page 1 of 1
December 2022 Groundwater Monitoring Report
Chris Holder, 3D Storage
12/14/2022
Nitrate as N NSL mg/L 2.3 H
Alkalinity NSL mg/L 410 B
Ferric Iron NSL mg/L 2.4
Ferrous Iron NSL mg/L <0.021 HF
Chloride NSL mg/L 350
Sulfate NSL mg/L 230 B
Methane NSL ug/L 4.0 J
Iron 14000 ug/L 2,400
Dissolved Hydrogen NSL nM 28
*EPA Regional Screening Level (RSL) (TR=1E-6, HQ=1) for tap water, November 2022
J - analyte was detected below the laboratory reporting limit; value is estimated
< - indicates the analyte was not detected at the method detection limit
Bold denotes analyte exceeded the screening criteria
NA- Not Analyzed
NSL - No standards listed by EPA RSL, November 2022
H - Sample was prepped or analyzed beyond the specified holding time
B - Compound was found in the black and sample
HF - Field parameter with a holding time of 15 minutes. Test performed by laboratory on request.
30<15<15
0.92 J
990
470 B
0.89
0.10 J HF
420
220 B
OFFSITE A-2OFFSITE A-1
12/14/2022
2.1 H
TABLE 2: GENERAL CHEMISTRY - MNA RESULTS
Parameter Units 9/15/2022 9/15/2022
Screening
Levels*
2.6 2.4
440420
1800 540
1.80 0.5
30.00 6.3
270 240
<0.021 <0.021
400 420
Page 1 of 1
ATTACHMENT
A APPENDIX
Field Data Sheets
Initial Depth to Water (ft):Well Diameter (in):
Total Depth of Well (ft):1 Casing Volume (gal):
Method of Purging:3 Casing Volumes (gal):
Measuring Point (TOC, etc.):Pump Intake Depth (feet):
±3%±10% or
<0.5 mg/L ±10 mV ±10% or <5 NTU
11:50 250.00
11:55 9.71 250 16.98 0.87 75.00 12.10
12:00 10.91 250 16.13 0.81 73.50 7.94
12:05 12.07 250 15.87 0.70 74.90 21.70
12:10 13.86 250 16.44 0.86 72.70 18.90
12:15 15.19 250 16.64 1.19 70.00 37.60
12:20 15.95 250 15.60 2.12 6.79 30.03
12:25 17.04 250 16.90 3.64 71.60 39.00
12:30 18.94 250 16.28 2.36 69.60 47.40
12:35 19.30 250 15.62 5.24 70.10 30.00
15.62 5.24 70.1 30
Sample ID:Method of Sampling:
QA/QC Samples (Yes/No):Sample Date:
Duplicate ID:Sample Collection Time:
Sample Container Type(s):Total Volume Purged (gal):
Preservative(s):Sample Depth (ft):
Analysis/Method(s):Depth to Water After Sampling (ft):
Equipment Calibrated (Y/N):Calibrated Within Criteria (Y/N):
QA/QC’d by:
Groundwater Field Data Sheet
19.3
Offsite A-2
No
NA
4.5
12:45
6 40ml HCL preserved VOA vials
Stability Reached (Y/N):If No, Provide Explanation NA
MNA samples also collected Corey Buchanan
QA/QC Date:
Instruments (Manufacturer, Model, and Serial No.):
Turbidity Meter, Water Quality Meter, Water Level Meter, Peristaltic Pump
Geotech turbidimeter 18021633, YSI 556 MPS 06G2421
Calculations:Signature:
V= 0.0408*(19.53-8.39)*(2.02
= 1.8 gal.
Where:
V = Casing Volume (gallons)
DIA - Well Diameter (inch)
Water Column = DTB-DTW (feet)
Notes:Name (print):
Yes Yes
6.84
VOCs - EPA 8260C,1,4-Dioxane - EPA 8260C-SIM,Arsenic
HNO3, HCL, Ice (4 °C)
Na
Turbidity
(NTU)
2.321.50
6.80
6.78
Stabilization Criteria ±0.1 ±3%
2.26
DO
(mg/L)
Clear
Comments/Observations
During Purging
(color, sediment, odor, etc.)
Flow Rate
(ml/min)
Cum.
Volume
(gal.)
Temp.
(°C)
pH
(SU)Time
1.00
6.69
3.00
2.28
2.00
2.14
Bubbles, limited volume
2.10
Well ID:
Specific
Electrical
Conductance
(mS/cm)
Pump
Water
Level
(feet)
6.70
Project Name: CHRIS HOLDER (3D STORAGE) 50 EAST 1100 NORTHNORTH SALT LAKE, UTAH
8.39
Project Number:WDP0014
6.73
Field Personnel(s): Corey Buchanan
Pumping/Purging Started
12/14/22Date:
5.5
1.8
2.0
ORP
(mV)
2.50
0.50
Project Manager Brad Glisson
Offsite A-1
19.53
Yes
Well casing volume:
6.84
Na
2.29
6.74
2.21
2.18
4.00
3.50 6.78
12/14/22
Pump
Final Values: 2.206
6.78
2.25
Minor bubbles
Top of Casing
4.50
𝑉𝑉=𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶∗𝐷𝐷𝐷𝐷𝐷𝐷2 ∗0.0408
1/6/23CB
Initial Depth to Water (ft):Well Diameter (in):
Total Depth of Well (ft):1 Casing Volume (gal):
Method of Purging:3 Casing Volumes (gal):
Measuring Point (TOC, etc.):Pump Intake Depth (feet):
±3%±10% or
<0.5 mg/L ±10 mV ±10% or <5 NTU
09:35 250.00
09:40 10.61 250 17.21 0.95 142.10 7.77
09:45 11.52 250 17.70 0.91 132.00 5.66
09:50 12.73 250 17.48 1.12 137.20 2.23
09:55 13.81 250 17.02 1.13 126.00 16.40
10:00 14.60 250 17.16 1.11 123.70 17.00
10:05 14.71 250 15.71 1.45 123.80 31.80
10:10 14.81 250 16.35 1.57 123.80 30.10
10:15 14.91 250 16.16 1.53 118.10 23.80
10:20 15.11 250 16.86 1.51 114.20 23.40
10:25 15.74 250 16.80 2.29 101.60 10.90
10:30 15.93 250 16.70 1.79 102.30 12.90
10:35 16.98 250 17.61 2.71 92.60 27.5x
10:40 18.61 250 17.28 2.85 81.20 12.90
10:45 18.70 250 17.11 2.97 80.60 10.30
10:55 18.81 250 15.60 3.66 86.00 8.99
15.6 3.66 86 8.99
Sample ID:Method of Sampling:
QA/QC Samples (Yes/No):Sample Date:
Duplicate ID:Sample Collection Time:
Sample Container Type(s):Total Volume Purged (gal):
Preservative(s):Sample Depth (ft):
Analysis/Method(s):Depth to Water After Sampling (ft):
Equipment Calibrated (Y/N):Calibrated Within Criteria (Y/N):
QA/QC’d by:
Groundwater Field Data Sheet
18.7
Offsite A-2
No
NA
4.70
10:00
6 40ml HCL preserved VOA vials
Stability Reached (Y/N):If No, Provide Explanation NA
MNA samples also collected Corey Buchanan
QA/QC Date:
Instruments (Manufacturer, Model, and Serial No.):
Turbidity Meter, Water Quality Meter, Water Level Meter, Peristaltic Pump
Geotech turbidimeter 18021633, YSI 556 MPS 06G2421
Calculations:Signature:
V= 0.0408*(19.42-9.91)*(2.02
= 1.6 gal.
Where:
V = Casing Volume (gallons)
DIA - Well Diameter (inch)
Water Column = DTB-DTW (feet)
Notes:Name (print):
Yes Yes
6.55
VOCs - EPA 8260C,1,4-Dioxane - EPA 8260C-SIM,Arsenic
HNO3, HCL, Ice (4 °C)
Na
Turbidity
(NTU)
2.331.00
6.74
6.77
Stabilization Criteria ±0.1 ±3%
2.42
DO
(mg/L)
Clear
Comments/Observations
During Purging
(color, sediment, odor, etc.)
Flow Rate
(ml/min)
Cum.
Volume
(gal.)
Temp.
(°C)
pH
(SU)Time
0.50
6.73
2.00
2.41
1.25
2.19
3.50 6.70 2.40
6.74
6.68
2.37
Well ID:
Specific
Electrical
Conductance
(mS/cm)
Pump
Water
Level
(feet)
6.65
3.75
Project Name: CHRIS HOLDER (3D STORAGE) 50 EAST 1100 NORTHNORTH SALT LAKE, UTAH
9.91
Project Number:WDP0014
6.60
Field Personnel(s): Corey Buchanan
Pumping/Purging Started
12/14/22Date:
4.7
1.6
2.0
ORP
(mV)
1.50
0.25
Project Manager Brad Glisson
Offsite A-2
19.42
2.41
Yes
Well casing volume:
2.39
6.57
4.70 6.55 2.42
2.41
Na
2.34
6.55
2.33
2.20
2.50
3.00
2.30 6.49
12/14/22
Pump
Final Values: 2.415
6.56
2.26
3.25
Top of Casing
2.75
6.64 2.40
4.00 6.68
𝑉𝑉=𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝑊𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶𝐶∗𝐷𝐷𝐷𝐷𝐷𝐷2 ∗0.0408
CB 1/6/23
ATTACHMENT

B APPENDIX
Laboratory Analytical Reports
ANALYTICAL REPORT
PREPARED FOR
Attn: Brad Glisson
WSP USA Environment & Infrastructure Inc.
3800 Ezell Rd #100
Nashville TN 37211
Generated 1/3/2023 11:10 AM
JOB DESCRIPTION
Salt Lake City, Utah
JOB NUMBER
280-170477-1
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
Page 1 of 349
Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with any
exceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval of the
laboratory. All questions regarding this report should be directed to the Eurofins TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
1/3/2023 11:10 AM
Authorized for release by
Shelby R Turner, Project Manager I
[e-mail]

Page 2 of 349
Table of Contents
Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Detection Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .9
Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .10
Default Detection Limits . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .14
Surrogate Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .16
QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .17
QC Association . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .25
Chronicle . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .27
Certification Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .28
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .29
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .30
Manual Integration Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .31
Reagent Traceability . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .42
Organic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .62
GC/MS VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .62
8260C . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .62
8260C QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .63
8260C Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .73
Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77
8260C ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .77
8260C CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .183
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .191
8260C Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .191
Page 3 of 349
Table of Contents
8260C LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .193
8260C Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .197
8260C Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .208
GC VOA . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .212
Method RSK-175 . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .212
Method RSK-175 QC Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .213
Method RSK-175 Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .222
Standards Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .224
Method RSK-175 ICAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .224
Method RSK-175 CCAL Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .244
Raw QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .260
Method RSK-175 Blank Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .260
Method RSK-175 LCS/LCSD Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .261
Method RSK-175 Duplicate/Triplicate Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .263
Method RSK-175 Run Logs . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .264
Method RSK-175 Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .267
Inorganic Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .269
Metals Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .269
Met Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .270
Met Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .271
Met QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .273
Met ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .273
Met CRQL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .275
Met Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .276
Met ICSA/ICSAB . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .279
Met LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .281
Page 4 of 349
Table of Contents
Met MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .282
Met Linear Ranges . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .284
Met Preparation Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .285
Met Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .286
Met Internal Standards . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .290
Met Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .294
General Chemistry Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .295
Gen Chem Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .296
Gen Chem Sample Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .297
Gen Chem QC Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .299
Gen Chem ICV/CCV . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .299
Gen Chem Blanks . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .305
Gen Chem Duplicates . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .306
Gen Chem LCS/LCSD . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .307
Gen Chem MDL . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .310
Gen Chem Analysis Run Log . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .321
Gen Chem Prep Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .334
Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . . 342
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .343
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .349
Page 5 of 349
Definitions/Glossary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: GE-Salt Lake City, Utah
Qualifiers
GC/MS VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
GC VOA
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
Metals
Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Qualifier
General Chemistry
Qualifier Description
B Compound was found in the blank and sample.
Qualifier
H Sample was prepped or analyzed beyond the specified holding time
HF Field parameter with a holding time of 15 minutes. Test performed by laboratory at client's request.
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
Page 6 of 349
CASE NARRATIVE
Client: WSP USA Environment & Infrastructure Inc.
Project: Salt Lake City, Utah
Report Number: 280-170477-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received on 12/16/2022 9:15 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperatures of the 4 coolers at receipt time were 0.1º C, 0.4º C, 3.3º C and 3.6º C.
The following samples were received with less than one shift (8 hours) remaining on a test with a holding time of 48 hours or less. As
such, the laboratory had insufficient time to analyze Nitrate by IC within holding time: Offsite A-1 (280-170477-1) and Offsite A-2
(280-170477-2). The client was notified on 12/19/22 and instructed the laboratory to proceed with analysis.
Dissolved Hydrogen analysis was performed by Pace Analytical Gulf Coast. Data is reported separately under SDG 280-170477-2.
VOLATILE ORGANIC COMPOUNDS (GC/MS)
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for volatile organic compounds (GC/MS) in
accordance with 8260C. The samples were analyzed on 12/25/2022.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
DISSOLVED GASES
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for dissolved gases in accordance with RSK_175. The
samples were analyzed on 12/21/2022.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL METALS (ICP/MS)
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for Total Metals (ICP/MS) in accordance with SW846
6020B. The samples were prepared and analyzed on 12/22/2022.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ALKALINITY
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for Alkalinity in accordance with SM20 2320B. The
samples were analyzed on 12/21/2022.
Alkalinity was detected in method blank MB 280-597409/110 at a level that was above the method detection limit but below the reporting
limit. Alkalinity was detected in method blank MB 280-597409/6 at a level that was above the method detection limit but below the
reporting limit. Alkalinity was detected in method blank MB 280-597409/84 at a level that was above the method detection limit but below
the reporting limit. If the associated sample reported a result above the MDL and/or RL, the result has been flagged. Refer to the QC
report for details.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ANIONS (48 HOURS)
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for anions (48 hours) in accordance with EPA Method
300.0 (48 Hours). The samples were analyzed on 12/17/2022.
Page 7 of 349
The following samples were received outside of holding time: Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2).
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
FERRIC IRON
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for ferric iron in accordance with SM19 3500 FE D.
The samples were analyzed on 12/29/2022.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
FERROUS IRON
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for ferrous iron in accordance with SM 3500 FE B.
The samples were analyzed on 12/19/2022.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
TOTAL CHLORIDE
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for total chloride in accordance with SM20 4500 Cl-E.
The samples were analyzed on 12/30/2022.
Samples Offsite A-1 (280-170477-1)[20X] and Offsite A-2 (280-170477-2)[20X] required dilution prior to analysis. The reporting limits
have been adjusted accordingly.
No analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
SULFATE
Samples Offsite A-1 (280-170477-1) and Offsite A-2 (280-170477-2) were analyzed for sulfate in accordance with SM 4500 S04 E. The
samples were analyzed on 12/30/2022.
Sulfate was detected in method blank MB 280-598232/14 at a level that was above the method detection limit but below the reporting
limit. The value should be considered an estimate, and has been flagged. If the associated sample reported a result above the MDL
and/or RL, the result has been flagged. Refer to the QC report for details.
Samples Offsite A-1 (280-170477-1)[10X] and Offsite A-2 (280-170477-2)[10X] required dilution prior to analysis. The reporting limits
have been adjusted accordingly.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Page 8 of 349
Detection Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Client Sample ID: Offsite A-1 Lab Sample ID: 280-170477-1
trans-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA11.4 8260C
Trichloroethene 1.0 ug/L0.30 Total/NA1678260C
cis-1,2-Dichloroethene 1.0 ug/L0.32 Total/NA1168260C
1,1-Dichloroethane 1.0 ug/L0.22 Total/NA12.3 8260C
1,1-Dichloroethene 1.0 ug/L0.23 Total/NA11.1 8260C
Methane 5.0 ug/L0.63 Total/NA14.0 J RSK-175
Iron 50 ug/L22 Total/NA124006020B
Nitrate as N 0.50 mg/L0.090 Total/NA12.3 H 300.0
Alkalinity 10 mg/L3.1 Total/NA1410 B SM 2320B
Ferric Iron 0.20 mg/L0.021 Total/NA12.4 SM 3500
Chloride 40 mg/L14 Total/NA20350SM 4500 Cl- E
Sulfate 50 mg/L7.1 Total/NA10230 B SM 4500 SO4 E
Client Sample ID: Offsite A-2 Lab Sample ID: 280-170477-2
trans-1,2-Dichloroethene
RL
1.0 ug/L
MDL
0.37
Analyte Result Qualifier Unit Dil Fac D Method Prep Type
Total/NA1J0.87 8260C
1,1,1-Trichloroethane 1.0 ug/L0.39 Total/NA10.39 J 8260C
Trichloroethene 1.0 ug/L0.30 Total/NA1278260C
cis-1,2-Dichloroethene 1.0 ug/L0.32 Total/NA15.5 8260C
1,1-Dichloroethane 1.0 ug/L0.22 Total/NA11.9 8260C
1,1-Dichloroethene 1.0 ug/L0.23 Total/NA10.93 J 8260C
Methane 5.0 ug/L0.63 Total/NA10.92 J RSK-175
Iron 50 ug/L22 Total/NA19906020B
Nitrate as N 0.50 mg/L0.090 Total/NA12.1 H 300.0
Alkalinity 10 mg/L3.1 Total/NA1470 B SM 2320B
Ferric Iron 0.20 mg/L0.021 Total/NA10.89 SM 3500
Ferrous Iron 0.20 mg/L0.021 Total/NA10.10 J HF SM 3500 FE B
Chloride 40 mg/L14 Total/NA20420SM 4500 Cl- E
Sulfate 50 mg/L7.1 Total/NA10220 B SM 4500 SO4 E
Eurofins Denver
This Detection Summary does not include radiochemical test results.
Page 9 of 349
Client Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Lab Sample ID: 280-170477-1Client Sample ID: Offsite A-1
Matrix: WaterDate Collected: 12/14/22 12:45
Date Received: 12/16/22 09:15
Method: SW846 8260C - Volatile Organic Compounds by GC/MS
RL MDL
ND 15 6.6 ug/L 12/25/22 14:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Acetone
15 5.9 ug/L 12/25/22 14:43 1ND2-Butanone (MEK)
1.0 0.31 ug/L 12/25/22 14:43 1NDBenzene
1.0 0.42 ug/L 12/25/22 14:43 1NDChlorobenzene
2.0 0.63 ug/L 12/25/22 14:43 1NDCarbon disulfide
1.0 0.57 ug/L 12/25/22 14:43 1NDCarbon tetrachloride
1.0 0.44 ug/L 12/25/22 14:43 1NDCyclohexane
5.0 1.8 ug/L 12/25/22 14:43 1ND1,2-Dibromo-3-Chloropropane
5.0 2.4 ug/L 12/25/22 14:43 1NDBromomethane
2.0 1.2 ug/L 12/25/22 14:43 1NDBromoform
4.0 1.4 ug/L 12/25/22 14:43 1NDChloroethane
1.0 0.36 ug/L 12/25/22 14:43 1NDChloroform
1.0 0.40 ug/L 12/25/22 14:43 1NDChlorobromomethane
1.0 0.39 ug/L 12/25/22 14:43 1NDDichlorobromomethane
2.0 0.62 ug/L 12/25/22 14:43 1NDChlorodibromomethane
1.0 0.36 ug/L 12/25/22 14:43 1NDIsopropylbenzene
5.0 1.7 ug/L 12/25/22 14:43 1NDMethyl n-butyl ketone (MNBK)
2.0 0.75 ug/L 12/25/22 14:43 1NDChloromethane
3.0 0.96 ug/L 12/25/22 14:43 1NDDichlorodifluoromethane
1.0 0.37 ug/L 12/25/22 14:43 11.4trans-1,2-Dichloroethene
2.0 0.65 ug/L 12/25/22 14:43 1NDtrans-1,3-Dichloropropene
2.0 0.94 ug/L 12/25/22 14:43 1NDMethylene Chloride
5.0 1.6 ug/L 12/25/22 14:43 1NDMethyl acetate
5.0 0.25 ug/L 12/25/22 14:43 1NDMethyl tert-butyl ether
5.0 0.98 ug/L 12/25/22 14:43 1ND4-Methyl-2-pentanone (MIBK)
1.0 0.31 ug/L 12/25/22 14:43 1NDMethylcyclohexane
1.0 0.36 ug/L 12/25/22 14:43 1NDStyrene
1.0 0.21 ug/L 12/25/22 14:43 1ND1,1,2,2-Tetrachloroethane
2.0 0.70 ug/L 12/25/22 14:43 1ND1,2,3-Trichlorobenzene
1.0 0.58 ug/L 12/25/22 14:43 1ND1,2,4-Trichlorobenzene
1.0 0.32 ug/L 12/25/22 14:43 1NDToluene
1.0 0.39 ug/L 12/25/22 14:43 1ND1,1,1-Trichloroethane
1.0 0.27 ug/L 12/25/22 14:43 1ND1,1,2-Trichloroethane
1.0 0.30 ug/L 12/25/22 14:43 167Trichloroethene
3.0 0.73 ug/L 12/25/22 14:43 1NDFreon 113
2.0 0.51 ug/L 12/25/22 14:43 1NDVinyl chloride
2.0 0.36 ug/L 12/25/22 14:43 1NDm-Xylene & p-Xylene
1.0 0.33 ug/L 12/25/22 14:43 1NDo-Xylene
1.0 0.40 ug/L 12/25/22 14:43 1NDTetrachloroethene
1.0 0.37 ug/L 12/25/22 14:43 1ND1,2-Dichlorobenzene
1.0 0.33 ug/L 12/25/22 14:43 1ND1,3-Dichlorobenzene
1.0 0.39 ug/L 12/25/22 14:43 1ND1,4-Dichlorobenzene
1.0 0.32 ug/L 12/25/22 14:43 116cis-1,2-Dichloroethene
2.0 0.63 ug/L 12/25/22 14:43 1NDcis-1,3-Dichloropropene
1.0 0.22 ug/L 12/25/22 14:43 12.31,1-Dichloroethane
1.0 0.23 ug/L 12/25/22 14:43 11.11,1-Dichloroethene
1.0 0.54 ug/L 12/25/22 14:43 1ND1,2-Dichloroethane
1.0 0.52 ug/L 12/25/22 14:43 1ND1,2-Dichloropropane
150 19 ug/L 12/25/22 14:43 1ND1,4-Dioxane
Eurofins Denver
Page 10 of 349
Client Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Lab Sample ID: 280-170477-1Client Sample ID: Offsite A-1
Matrix: WaterDate Collected: 12/14/22 12:45
Date Received: 12/16/22 09:15
Method: SW846 8260C - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 1.0 0.30 ug/L 12/25/22 14:43 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Ethylbenzene
1.0 0.40 ug/L 12/25/22 14:43 1ND1,2-Dibromoethane
2.0 0.57 ug/L 12/25/22 14:43 1NDTrichlorofluoromethane
1,2-Dichloroethane-d4 (Surr)89 70 -127 12/25/22 14:43 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr)102 12/25/22 14:43 180-125
4-Bromofluorobenzene (Surr)95 12/25/22 14:43 178-120
Dibromofluoromethane (Surr)97 12/25/22 14:43 177-120
Method: RSK-175 - Dissolved Gases (GC)
RL MDL
4.0 J 5.0 0.63 ug/L 12/21/22 19:34 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Methane
Method: SW846 6020B - Metals (ICP/MS)
RL MDL
2400 50 22 ug/L 12/22/22 07:26 12/22/22 18:46 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Iron
General Chemistry
RL MDL
2.3 H 0.50 0.090 mg/L 12/17/22 04:27 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Nitrate as N (MCAWW 300.0)
10 3.1 mg/L 12/21/22 03:23 1410 BAlkalinity (SM 2320B)
0.20 0.021 mg/L 12/29/22 16:06 12.4Ferric Iron (SM 3500)
0.20 0.021 mg/L 12/19/22 14:09 1ND HFFerrous Iron (SM 3500 FE B)
40 14 mg/L 12/30/22 16:01 20350Chloride (SM 4500 Cl- E)
50 7.1 mg/L 12/30/22 16:07 10230 BSulfate (SM 4500 SO4 E)
Lab Sample ID: 280-170477-2Client Sample ID: Offsite A-2
Matrix: WaterDate Collected: 12/14/22 11:00
Date Received: 12/16/22 09:15
Method: SW846 8260C - Volatile Organic Compounds by GC/MS
RL MDL
ND 15 6.6 ug/L 12/25/22 15:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Acetone
15 5.9 ug/L 12/25/22 15:04 1ND2-Butanone (MEK)
1.0 0.31 ug/L 12/25/22 15:04 1NDBenzene
1.0 0.42 ug/L 12/25/22 15:04 1NDChlorobenzene
2.0 0.63 ug/L 12/25/22 15:04 1NDCarbon disulfide
1.0 0.57 ug/L 12/25/22 15:04 1NDCarbon tetrachloride
1.0 0.44 ug/L 12/25/22 15:04 1NDCyclohexane
5.0 1.8 ug/L 12/25/22 15:04 1ND1,2-Dibromo-3-Chloropropane
5.0 2.4 ug/L 12/25/22 15:04 1NDBromomethane
2.0 1.2 ug/L 12/25/22 15:04 1NDBromoform
4.0 1.4 ug/L 12/25/22 15:04 1NDChloroethane
1.0 0.36 ug/L 12/25/22 15:04 1NDChloroform
1.0 0.40 ug/L 12/25/22 15:04 1NDChlorobromomethane
1.0 0.39 ug/L 12/25/22 15:04 1NDDichlorobromomethane
2.0 0.62 ug/L 12/25/22 15:04 1NDChlorodibromomethane
1.0 0.36 ug/L 12/25/22 15:04 1NDIsopropylbenzene
5.0 1.7 ug/L 12/25/22 15:04 1NDMethyl n-butyl ketone (MNBK)
2.0 0.75 ug/L 12/25/22 15:04 1NDChloromethane
Eurofins Denver
Page 11 of 349
Client Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Lab Sample ID: 280-170477-2Client Sample ID: Offsite A-2
Matrix: WaterDate Collected: 12/14/22 11:00
Date Received: 12/16/22 09:15
Method: SW846 8260C - Volatile Organic Compounds by GC/MS (Continued)
RL MDL
ND 3.0 0.96 ug/L 12/25/22 15:04 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Dichlorodifluoromethane
1.0 0.37 ug/L 12/25/22 15:04 10.87 Jtrans-1,2-Dichloroethene
2.0 0.65 ug/L 12/25/22 15:04 1NDtrans-1,3-Dichloropropene
2.0 0.94 ug/L 12/25/22 15:04 1NDMethylene Chloride
5.0 1.6 ug/L 12/25/22 15:04 1NDMethyl acetate
5.0 0.25 ug/L 12/25/22 15:04 1NDMethyl tert-butyl ether
5.0 0.98 ug/L 12/25/22 15:04 1ND4-Methyl-2-pentanone (MIBK)
1.0 0.31 ug/L 12/25/22 15:04 1NDMethylcyclohexane
1.0 0.36 ug/L 12/25/22 15:04 1NDStyrene
1.0 0.21 ug/L 12/25/22 15:04 1ND1,1,2,2-Tetrachloroethane
2.0 0.70 ug/L 12/25/22 15:04 1ND1,2,3-Trichlorobenzene
1.0 0.58 ug/L 12/25/22 15:04 1ND1,2,4-Trichlorobenzene
1.0 0.32 ug/L 12/25/22 15:04 1NDToluene
1.0 0.39 ug/L 12/25/22 15:04 10.39 J1,1,1-Trichloroethane
1.0 0.27 ug/L 12/25/22 15:04 1ND1,1,2-Trichloroethane
1.0 0.30 ug/L 12/25/22 15:04 127Trichloroethene
3.0 0.73 ug/L 12/25/22 15:04 1NDFreon 113
2.0 0.51 ug/L 12/25/22 15:04 1NDVinyl chloride
2.0 0.36 ug/L 12/25/22 15:04 1NDm-Xylene & p-Xylene
1.0 0.33 ug/L 12/25/22 15:04 1NDo-Xylene
1.0 0.40 ug/L 12/25/22 15:04 1NDTetrachloroethene
1.0 0.37 ug/L 12/25/22 15:04 1ND1,2-Dichlorobenzene
1.0 0.33 ug/L 12/25/22 15:04 1ND1,3-Dichlorobenzene
1.0 0.39 ug/L 12/25/22 15:04 1ND1,4-Dichlorobenzene
1.0 0.32 ug/L 12/25/22 15:04 15.5cis-1,2-Dichloroethene
2.0 0.63 ug/L 12/25/22 15:04 1NDcis-1,3-Dichloropropene
1.0 0.22 ug/L 12/25/22 15:04 11.91,1-Dichloroethane
1.0 0.23 ug/L 12/25/22 15:04 10.93 J1,1-Dichloroethene
1.0 0.54 ug/L 12/25/22 15:04 1ND1,2-Dichloroethane
1.0 0.52 ug/L 12/25/22 15:04 1ND1,2-Dichloropropane
150 19 ug/L 12/25/22 15:04 1ND1,4-Dioxane
1.0 0.30 ug/L 12/25/22 15:04 1NDEthylbenzene
1.0 0.40 ug/L 12/25/22 15:04 1ND1,2-Dibromoethane
2.0 0.57 ug/L 12/25/22 15:04 1NDTrichlorofluoromethane
1,2-Dichloroethane-d4 (Surr)92 70 -127 12/25/22 15:04 1
Surrogate Dil FacAnalyzedPreparedQualifier Limits%Recovery
Toluene-d8 (Surr)106 12/25/22 15:04 180-125
4-Bromofluorobenzene (Surr)95 12/25/22 15:04 178-120
Dibromofluoromethane (Surr)98 12/25/22 15:04 177-120
Method: RSK-175 - Dissolved Gases (GC)
RL MDL
0.92 J 5.0 0.63 ug/L 12/21/22 20:01 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Methane
Method: SW846 6020B - Metals (ICP/MS)
RL MDL
990 50 22 ug/L 12/22/22 07:26 12/22/22 18:48 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Iron
Eurofins Denver
Page 12 of 349
Client Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Lab Sample ID: 280-170477-2Client Sample ID: Offsite A-2
Matrix: WaterDate Collected: 12/14/22 11:00
Date Received: 12/16/22 09:15
General Chemistry
RL MDL
2.1 H 0.50 0.090 mg/L 12/17/22 04:42 1
Analyte Dil FacAnalyzedPreparedUnit DResult Qualifier
Nitrate as N (MCAWW 300.0)
10 3.1 mg/L 12/21/22 03:39 1470 BAlkalinity (SM 2320B)
0.20 0.021 mg/L 12/29/22 16:06 10.89Ferric Iron (SM 3500)
0.20 0.021 mg/L 12/19/22 14:09 10.10 J HFFerrous Iron (SM 3500 FE B)
40 14 mg/L 12/30/22 16:17 20420Chloride (SM 4500 Cl- E)
50 7.1 mg/L 12/30/22 16:08 10220 BSulfate (SM 4500 SO4 E)
Eurofins Denver
Page 13 of 349
Default Detection Limits
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS
1.01,1,1-Trichloroethane ug/L
Analyte UnitsMDLRL
0.39
1.01,1,2,2-Tetrachloroethane ug/L0.21
1.01,1,2-Trichloroethane ug/L0.27
1.01,1-Dichloroethane ug/L0.22
1.01,1-Dichloroethene ug/L0.23
2.01,2,3-Trichlorobenzene ug/L0.70
1.01,2,4-Trichlorobenzene ug/L0.58
5.01,2-Dibromo-3-Chloropropane ug/L1.8
1.01,2-Dibromoethane ug/L0.40
1.01,2-Dichlorobenzene ug/L0.37
1.01,2-Dichloroethane ug/L0.54
1.01,2-Dichloropropane ug/L0.52
1.01,3-Dichlorobenzene ug/L0.33
1.01,4-Dichlorobenzene ug/L0.39
1501,4-Dioxane ug/L19
152-Butanone (MEK)ug/L5.9
5.04-Methyl-2-pentanone (MIBK)ug/L0.98
15Acetone ug/L6.6
1.0Benzene ug/L0.31
2.0Bromoform ug/L1.2
5.0Bromomethane ug/L2.4
2.0Carbon disulfide ug/L0.63
1.0Carbon tetrachloride ug/L0.57
1.0Chlorobenzene ug/L0.42
1.0Chlorobromomethane ug/L0.40
2.0Chlorodibromomethane ug/L0.62
4.0Chloroethane ug/L1.4
1.0Chloroform ug/L0.36
2.0Chloromethane ug/L0.75
1.0cis-1,2-Dichloroethene ug/L0.32
2.0cis-1,3-Dichloropropene ug/L0.63
1.0Cyclohexane ug/L0.44
1.0Dichlorobromomethane ug/L0.39
3.0Dichlorodifluoromethane ug/L0.96
1.0Ethylbenzene ug/L0.30
3.0Freon 113 ug/L0.73
1.0Isopropylbenzene ug/L0.36
5.0Methyl acetate ug/L1.6
5.0Methyl n-butyl ketone (MNBK)ug/L1.7
5.0Methyl tert-butyl ether ug/L0.25
1.0Methylcyclohexane ug/L0.31
2.0Methylene Chloride ug/L0.94
2.0m-Xylene & p-Xylene ug/L0.36
1.0o-Xylene ug/L0.33
1.0Styrene ug/L0.36
1.0Tetrachloroethene ug/L0.40
1.0Toluene ug/L0.32
1.0trans-1,2-Dichloroethene ug/L0.37
2.0trans-1,3-Dichloropropene ug/L0.65
1.0Trichloroethene ug/L0.30
2.0Trichlorofluoromethane ug/L0.57
2.0Vinyl chloride ug/L0.51
Eurofins Denver
Page 14 of 349
Default Detection Limits
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: RSK-175 - Dissolved Gases (GC)
5.0Methane ug/L
Analyte UnitsMDLRL
0.63
Method: 6020B - Metals (ICP/MS)
Prep: 3020A
50Iron ug/L
Analyte UnitsMDLRL
22
General Chemistry
0.50Nitrate as N mg/L
Analyte UnitsMDLRL
0.090
10Alkalinity mg/L3.1
0.20Ferric Iron mg/L0.021
0.20Ferrous Iron mg/L0.021
2.0Chloride mg/L0.68
5.0Sulfate mg/L0.71
Eurofins Denver
Page 15 of 349
Surrogate Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS
Prep Type: Total/NAMatrix: Water
Lab Sample ID Client Sample ID (70-127) (80-125) (78-120) (77-120)
DCA TOL BFB DBFM
89 102 95 97280-170477-1
Percent Surrogate Recovery (Acceptance Limits)
Offsite A-1
92 106 95 98280-170477-2 Offsite A-2
89 107 95 98LCS 280-597688/1002 Lab Control Sample
90 105 96 98LCSD 280-597688/4 Lab Control Sample Dup
90 107 96 97MB 280-597688/7 Method Blank
Surrogate Legend
DCA = 1,2-Dichloroethane-d4 (Surr)
TOL = Toluene-d8 (Surr)
BFB = 4-Bromofluorobenzene (Surr)
DBFM = Dibromofluoromethane (Surr)
Eurofins Denver
Page 16 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS
Client Sample ID: Method BlankLab Sample ID: MB 280-597688/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
RL MDL
Acetone ND 15 6.6 ug/L 12/25/22 10:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 5.915 ug/L 12/25/22 10:55 12-Butanone (MEK)
ND 0.311.0 ug/L 12/25/22 10:55 1Benzene
ND 0.421.0 ug/L 12/25/22 10:55 1Chlorobenzene
ND 0.632.0 ug/L 12/25/22 10:55 1Carbon disulfide
ND 0.571.0 ug/L 12/25/22 10:55 1Carbon tetrachloride
ND 0.441.0 ug/L 12/25/22 10:55 1Cyclohexane
ND 1.85.0 ug/L 12/25/22 10:55 11,2-Dibromo-3-Chloropropane
ND 2.45.0 ug/L 12/25/22 10:55 1Bromomethane
ND 1.22.0 ug/L 12/25/22 10:55 1Bromoform
ND 1.44.0 ug/L 12/25/22 10:55 1Chloroethane
ND 0.361.0 ug/L 12/25/22 10:55 1Chloroform
ND 0.401.0 ug/L 12/25/22 10:55 1Chlorobromomethane
ND 0.391.0 ug/L 12/25/22 10:55 1Dichlorobromomethane
ND 0.622.0 ug/L 12/25/22 10:55 1Chlorodibromomethane
ND 0.361.0 ug/L 12/25/22 10:55 1Isopropylbenzene
ND 1.75.0 ug/L 12/25/22 10:55 1Methyl n-butyl ketone (MNBK)
ND 0.752.0 ug/L 12/25/22 10:55 1Chloromethane
ND 0.963.0 ug/L 12/25/22 10:55 1Dichlorodifluoromethane
ND 0.371.0 ug/L 12/25/22 10:55 1trans-1,2-Dichloroethene
ND 0.652.0 ug/L 12/25/22 10:55 1trans-1,3-Dichloropropene
ND 0.942.0 ug/L 12/25/22 10:55 1Methylene Chloride
ND 1.65.0 ug/L 12/25/22 10:55 1Methyl acetate
ND 0.255.0 ug/L 12/25/22 10:55 1Methyl tert-butyl ether
ND 0.985.0 ug/L 12/25/22 10:55 14-Methyl-2-pentanone (MIBK)
ND 0.311.0 ug/L 12/25/22 10:55 1Methylcyclohexane
ND 0.361.0 ug/L 12/25/22 10:55 1Styrene
ND 0.211.0 ug/L 12/25/22 10:55 11,1,2,2-Tetrachloroethane
ND 0.702.0 ug/L 12/25/22 10:55 11,2,3-Trichlorobenzene
ND 0.581.0 ug/L 12/25/22 10:55 11,2,4-Trichlorobenzene
ND 0.321.0 ug/L 12/25/22 10:55 1Toluene
ND 0.391.0 ug/L 12/25/22 10:55 11,1,1-Trichloroethane
ND 0.271.0 ug/L 12/25/22 10:55 11,1,2-Trichloroethane
ND 0.301.0 ug/L 12/25/22 10:55 1Trichloroethene
ND 0.733.0 ug/L 12/25/22 10:55 1Freon 113
ND 0.512.0 ug/L 12/25/22 10:55 1Vinyl chloride
ND 0.362.0 ug/L 12/25/22 10:55 1m-Xylene & p-Xylene
ND 0.331.0 ug/L 12/25/22 10:55 1o-Xylene
ND 0.401.0 ug/L 12/25/22 10:55 1Tetrachloroethene
ND 0.371.0 ug/L 12/25/22 10:55 11,2-Dichlorobenzene
ND 0.331.0 ug/L 12/25/22 10:55 11,3-Dichlorobenzene
ND 0.391.0 ug/L 12/25/22 10:55 11,4-Dichlorobenzene
ND 0.321.0 ug/L 12/25/22 10:55 1cis-1,2-Dichloroethene
ND 0.632.0 ug/L 12/25/22 10:55 1cis-1,3-Dichloropropene
ND 0.221.0 ug/L 12/25/22 10:55 11,1-Dichloroethane
ND 0.231.0 ug/L 12/25/22 10:55 11,1-Dichloroethene
ND 0.541.0 ug/L 12/25/22 10:55 11,2-Dichloroethane
ND 0.521.0 ug/L 12/25/22 10:55 11,2-Dichloropropane
Eurofins Denver
Page 17 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Method BlankLab Sample ID: MB 280-597688/7
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
RL MDL
1,4-Dioxane ND 150 19 ug/L 12/25/22 10:55 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
ND 0.301.0 ug/L 12/25/22 10:55 1Ethylbenzene
ND 0.401.0 ug/L 12/25/22 10:55 11,2-Dibromoethane
ND 0.572.0 ug/L 12/25/22 10:55 1Trichlorofluoromethane
1,2-Dichloroethane-d4 (Surr)90 70 -127 12/25/22 10:55 1
MB MB
Surrogate Dil FacPrepared AnalyzedQualifier Limits%Recovery
107 12/25/22 10:55 1Toluene-d8 (Surr)80 -125
96 12/25/22 10:55 14-Bromofluorobenzene (Surr)78 -120
97 12/25/22 10:55 1Dibromofluoromethane (Surr)77 -120
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597688/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
Acetone 100 98.1 ug/L 98 50 -137
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
2-Butanone (MEK)100 114 ug/L 114 53 -135
Benzene 25.0 28.2 ug/L 113 69 -126
Chlorobenzene 25.0 27.2 ug/L 109 78 -118
Carbon disulfide 25.0 28.2 ug/L 113 56 -128
Carbon tetrachloride 25.0 23.1 ug/L 92 60 -133
Cyclohexane 25.0 25.5 ug/L 102 57 -134
1,2-Dibromo-3-Chloropropane 25.0 23.5 ug/L 94 58 -122
Bromomethane 25.0 25.0 ug/L 100 25 -163
Bromoform 25.0 24.8 ug/L 99 57 -125
Chloroethane 25.0 27.2 ug/L 109 52 -144
Chloroform 25.0 26.4 ug/L 106 68 -128
Chlorobromomethane 25.0 24.6 ug/L 99 71 -130
Dichlorobromomethane 25.0 24.3 ug/L 97 67 -126
Chlorodibromomethane 25.0 24.9 ug/L 100 71 -122
Isopropylbenzene 25.0 27.7 ug/L 111 70 -127
Methyl n-butyl ketone (MNBK)100 114 ug/L 114 58 -134
Chloromethane 25.0 28.5 ug/L 114 43 -142
Dichlorodifluoromethane 25.0 24.1 ug/L 96 26 -152
trans-1,2-Dichloroethene 25.0 27.7 ug/L 111 66 -129
trans-1,3-Dichloropropene 25.0 24.4 ug/L 97 66 -127
Methylene Chloride 25.0 27.7 ug/L 111 64 -128
Methyl acetate 50.0 54.9 ug/L 110 59 -133
Methyl tert-butyl ether 25.0 27.1 ug/L 108 70 -127
4-Methyl-2-pentanone (MIBK)100 113 ug/L 113 56 -135
Methylcyclohexane 25.0 24.5 ug/L 98 58 -136
Styrene 25.0 27.8 ug/L 111 79 -120
1,1,2,2-Tetrachloroethane 25.0 28.0 ug/L 112 72 -122
1,2,3-Trichlorobenzene 25.0 25.7 ug/L 103 70 -127
1,2,4-Trichlorobenzene 25.0 26.2 ug/L 105 73 -124
Toluene 25.0 28.0 ug/L 112 68 -127
1,1,1-Trichloroethane 25.0 25.0 ug/L 100 62 -132
Eurofins Denver
Page 18 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597688/1002
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
1,1,2-Trichloroethane 25.0 27.2 ug/L 109 72 -128
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Trichloroethene 25.0 27.1 ug/L 109 70 -125
Freon 113 25.0 22.9 ug/L 92 60 -137
Vinyl chloride 25.0 28.7 ug/L 115 53 -141
m-Xylene & p-Xylene 25.0 28.4 ug/L 114 76 -122
o-Xylene 25.0 28.4 ug/L 114 77 -120
Tetrachloroethene 25.0 27.3 ug/L 109 72 -127
1,2-Dichlorobenzene 25.0 26.5 ug/L 106 77 -121
1,3-Dichlorobenzene 25.0 26.8 ug/L 107 76 -121
1,4-Dichlorobenzene 25.0 26.0 ug/L 104 76 -119
cis-1,2-Dichloroethene 25.0 27.1 ug/L 109 69 -126
cis-1,3-Dichloropropene 25.0 26.0 ug/L 104 75 -120
1,1-Dichloroethane 25.0 26.1 ug/L 104 66 -130
1,1-Dichloroethene 25.0 26.1 ug/L 105 62 -130
1,2-Dichloroethane 25.0 23.6 ug/L 94 61 -130
1,2-Dichloropropane 25.0 27.2 ug/L 109 68 -127
1,4-Dioxane 500 547 ug/L 109 59 -134
Ethylbenzene 25.0 28.7 ug/L 115 76 -121
1,2-Dibromoethane 25.0 26.4 ug/L 106 81 -118
Trichlorofluoromethane 25.0 23.7 ug/L 95 57 -144
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
89
LCS LCS
Qualifier Limits%Recovery
107Toluene-d8 (Surr)80 -125
954-Bromofluorobenzene (Surr)78 -120
98Dibromofluoromethane (Surr)77 -120
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-597688/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
Acetone 100 106 ug/L 106 50 -137 8 21
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
2-Butanone (MEK)100 116 ug/L 116 53 -135 2 20
Benzene 25.0 27.7 ug/L 111 69 -126 2 20
Chlorobenzene 25.0 26.5 ug/L 106 78 -118 2 20
Carbon disulfide 25.0 27.7 ug/L 111 56 -128 2 20
Carbon tetrachloride 25.0 23.4 ug/L 94 60 -133 1 20
Cyclohexane 25.0 25.1 ug/L 101 57 -134 1 32
1,2-Dibromo-3-Chloropropane 25.0 23.5 ug/L 94 58 -122 0 21
Bromomethane 25.0 25.0 ug/L 100 25 -163 0 40
Bromoform 25.0 24.4 ug/L 97 57 -125 2 20
Chloroethane 25.0 27.0 ug/L 108 52 -144 1 30
Chloroform 25.0 25.8 ug/L 103 68 -128 2 20
Chlorobromomethane 25.0 25.0 ug/L 100 71 -130 2 20
Dichlorobromomethane 25.0 24.4 ug/L 98 67 -126 1 20
Chlorodibromomethane 25.0 24.3 ug/L 97 71 -122 2 20
Isopropylbenzene 25.0 27.3 ug/L 109 70 -127 1 20
Eurofins Denver
Page 19 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 8260C - Volatile Organic Compounds by GC/MS (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-597688/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597688
Methyl n-butyl ketone (MNBK)100 120 ug/L 120 58 -134 5 21
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Chloromethane 25.0 27.3 ug/L 109 43 -142 4 20
Dichlorodifluoromethane 25.0 24.0 ug/L 96 26 -152 0 21
trans-1,2-Dichloroethene 25.0 27.1 ug/L 108 66 -129 2 20
trans-1,3-Dichloropropene 25.0 23.9 ug/L 96 66 -127 2 20
Methylene Chloride 25.0 27.7 ug/L 111 64 -128 0 20
Methyl acetate 50.0 58.6 ug/L 117 59 -133 6 20
Methyl tert-butyl ether 25.0 26.9 ug/L 108 70 -127 1 20
4-Methyl-2-pentanone (MIBK)100 113 ug/L 113 56 -135 1 20
Methylcyclohexane 25.0 23.8 ug/L 95 58 -136 3 21
Styrene 25.0 27.4 ug/L 110 79 -120 1 20
1,1,2,2-Tetrachloroethane 25.0 27.3 ug/L 109 72 -122 3 20
1,2,3-Trichlorobenzene 25.0 26.5 ug/L 106 70 -127 3 20
1,2,4-Trichlorobenzene 25.0 25.7 ug/L 103 73 -124 2 20
Toluene 25.0 27.3 ug/L 109 68 -127 3 20
1,1,1-Trichloroethane 25.0 25.2 ug/L 101 62 -132 1 20
1,1,2-Trichloroethane 25.0 27.1 ug/L 109 72 -128 0 20
Trichloroethene 25.0 26.4 ug/L 105 70 -125 3 20
Freon 113 25.0 23.6 ug/L 94 60 -137 3 23
Vinyl chloride 25.0 27.5 ug/L 110 53 -141 4 25
m-Xylene & p-Xylene 25.0 27.3 ug/L 109 76 -122 4 20
o-Xylene 25.0 27.8 ug/L 111 77 -120 2 20
Tetrachloroethene 25.0 26.2 ug/L 105 72 -127 4 20
1,2-Dichlorobenzene 25.0 26.2 ug/L 105 77 -121 1 20
1,3-Dichlorobenzene 25.0 26.4 ug/L 106 76 -121 1 20
1,4-Dichlorobenzene 25.0 25.6 ug/L 103 76 -119 1 20
cis-1,2-Dichloroethene 25.0 27.8 ug/L 111 69 -126 2 20
cis-1,3-Dichloropropene 25.0 25.3 ug/L 101 75 -120 3 20
1,1-Dichloroethane 25.0 26.2 ug/L 105 66 -130 0 20
1,1-Dichloroethene 25.0 26.5 ug/L 106 62 -130 1 21
1,2-Dichloroethane 25.0 23.0 ug/L 92 61 -130 2 20
1,2-Dichloropropane 25.0 26.5 ug/L 106 68 -127 3 20
1,4-Dioxane 500 622 ug/L 124 59 -134 13 24
Ethylbenzene 25.0 27.8 ug/L 111 76 -121 3 20
1,2-Dibromoethane 25.0 26.1 ug/L 105 81 -118 1 20
Trichlorofluoromethane 25.0 23.3 ug/L 93 57 -144 2 28
1,2-Dichloroethane-d4 (Surr)70 -127
Surrogate
90
LCSD LCSD
Qualifier Limits%Recovery
105Toluene-d8 (Surr)80 -125
964-Bromofluorobenzene (Surr)78 -120
98Dibromofluoromethane (Surr)77 -120
Eurofins Denver
Page 20 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: RSK-175 - Dissolved Gases (GC)
Client Sample ID: Method BlankLab Sample ID: MB 280-597520/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597520
RL MDL
Methane ND 5.0 0.63 ug/L 12/21/22 16:21 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597520/4
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597520
Methane 65.7 66.1 ug/L 101 75 -125
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-597520/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597520
Methane 65.7 65.2 ug/L 99 75 -125 1 20
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Offsite A-2Lab Sample ID: 280-170477-2 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597520
Methane 0.92 J 0.995 J ug/L 8 20
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: 6020B - Metals (ICP/MS)
Client Sample ID: Method BlankLab Sample ID: MB 280-597451/1-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597704 Prep Batch: 597451
RL MDL
Iron ND 50 22 ug/L 12/22/22 07:26 12/22/22 18:22 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597451/2-A
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597704 Prep Batch: 597451
Iron 800 850 ug/L 106 80 -120
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Method: 300.0 - Anions, Ion Chromatography
Client Sample ID: Method BlankLab Sample ID: MB 280-596980/39
Matrix: Water Prep Type: Total/NA
Analysis Batch: 596980
RL MDL
Nitrate as N ND 0.50 0.090 mg/L 12/17/22 03:12 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Eurofins Denver
Page 21 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: 300.0 - Anions, Ion Chromatography (Continued)
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-596980/37
Matrix: Water Prep Type: Total/NA
Analysis Batch: 596980
Nitrate as N 2.50 2.38 mg/L 95 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-596980/38
Matrix: Water Prep Type: Total/NA
Analysis Batch: 596980
Nitrate as N 2.50 2.40 mg/L 96 90 -110 1 10
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Lab Control SampleLab Sample ID: MRL 280-596980/3
Matrix: Water Prep Type: Total/NA
Analysis Batch: 596980
Nitrate as N 0.250 0.237 J mg/L 95 50 -150
Analyte
MRL MRL
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Method: SM 2320B - Alkalinity
Client Sample ID: Method BlankLab Sample ID: MB 280-597409/110
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
RL MDL
Alkalinity 3.37 J 10 3.1 mg/L 12/21/22 03:15 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Method BlankLab Sample ID: MB 280-597409/6
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
RL MDL
Alkalinity 3.47 J 10 3.1 mg/L 12/20/22 11:52 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Method BlankLab Sample ID: MB 280-597409/84
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
RL MDL
Alkalinity 3.78 J 10 3.1 mg/L 12/20/22 22:51 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597409/109
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
Alkalinity 200 210 mg/L 105 89 -109
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Denver
Page 22 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: SM 2320B - Alkalinity (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-597409/5
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
Alkalinity 200 203 mg/L 102 89 -109 2 10
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Client Sample ID: Offsite A-1Lab Sample ID: 280-170477-1 DU
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597409
Alkalinity 410 B 422 mg/L 2 10
Analyte
DU DU
DUnitResult Qualifier
Sample
Result
Sample
Qualifier LimitRPD
RPD
Method: SM 3500 FE B - Iron, Ferrous and Ferric
Client Sample ID: Method BlankLab Sample ID: MB 280-597184/11
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597184
RL MDL
Ferrous Iron ND 0.20 0.021 mg/L 12/19/22 14:06 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-597184/9
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597184
Ferrous Iron 2.00 1.97 mg/L 99 85 -121
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-597184/10
Matrix: Water Prep Type: Total/NA
Analysis Batch: 597184
Ferrous Iron 2.00 1.99 mg/L 100 85 -121 1 10
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Method: SM 4500 Cl- E - Chloride, Total
Client Sample ID: Method BlankLab Sample ID: MB 280-598240/15
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598240
RL MDL
Chloride ND 2.0 0.68 mg/L 12/30/22 15:43 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-598240/13
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598240
Chloride 20.0 19.9 mg/L 100 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Eurofins Denver
Page 23 of 349
QC Sample Results
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method: SM 4500 Cl- E - Chloride, Total (Continued)
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-598240/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598240
Chloride 20.0 20.0 mg/L 100 90 -110 0 10
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Method: SM 4500 SO4 E - Sulfate, Total
Client Sample ID: Method BlankLab Sample ID: MB 280-598232/14
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598232
RL MDL
Sulfate 0.737 J 5.0 0.71 mg/L 12/30/22 15:39 1
MB MB
Analyte Dil FacAnalyzedPreparedDUnitResult Qualifier
Client Sample ID: Lab Control SampleLab Sample ID: LCS 280-598232/12
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598232
Sulfate 25.0 25.6 mg/L 103 90 -110
Analyte
LCS LCS
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits
Client Sample ID: Lab Control Sample DupLab Sample ID: LCSD 280-598232/13
Matrix: Water Prep Type: Total/NA
Analysis Batch: 598232
Sulfate 25.0 25.7 mg/L 103 90 -110 0 10
Analyte
LCSD LCSD
DUnitResult Qualifier %Rec
Spike
Added
%Rec
Limits LimitRPD
RPD
Eurofins Denver
Page 24 of 349
QC Association Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
GC/MS VOA
Analysis Batch: 597688
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 8260C280-170477-1 Offsite A-1 Total/NA
Water 8260C280-170477-2 Offsite A-2 Total/NA
Water 8260CMB 280-597688/7 Method Blank Total/NA
Water 8260CLCS 280-597688/1002 Lab Control Sample Total/NA
Water 8260CLCSD 280-597688/4 Lab Control Sample Dup Total/NA
GC VOA
Analysis Batch: 597520
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water RSK-175280-170477-1 Offsite A-1 Total/NA
Water RSK-175280-170477-2 Offsite A-2 Total/NA
Water RSK-175MB 280-597520/6 Method Blank Total/NA
Water RSK-175LCS 280-597520/4 Lab Control Sample Total/NA
Water RSK-175LCSD 280-597520/5 Lab Control Sample Dup Total/NA
Water RSK-175280-170477-2 DU Offsite A-2 Total/NA
Metals
Prep Batch: 597451
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 3020A280-170477-1 Offsite A-1 Total/NA
Water 3020A280-170477-2 Offsite A-2 Total/NA
Water 3020AMB 280-597451/1-A Method Blank Total/NA
Water 3020ALCS 280-597451/2-A Lab Control Sample Total/NA
Analysis Batch: 597704
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 6020B 597451280-170477-1 Offsite A-1 Total/NA
Water 6020B 597451280-170477-2 Offsite A-2 Total/NA
Water 6020B 597451MB 280-597451/1-A Method Blank Total/NA
Water 6020B 597451LCS 280-597451/2-A Lab Control Sample Total/NA
General Chemistry
Analysis Batch: 596980
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water 300.0280-170477-1 Offsite A-1 Total/NA
Water 300.0280-170477-2 Offsite A-2 Total/NA
Water 300.0MB 280-596980/39 Method Blank Total/NA
Water 300.0LCS 280-596980/37 Lab Control Sample Total/NA
Water 300.0LCSD 280-596980/38 Lab Control Sample Dup Total/NA
Water 300.0MRL 280-596980/3 Lab Control Sample Total/NA
Analysis Batch: 597184
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 3500 FE B280-170477-1 Offsite A-1 Total/NA
Water SM 3500 FE B280-170477-2 Offsite A-2 Total/NA
Water SM 3500 FE BMB 280-597184/11 Method Blank Total/NA
Water SM 3500 FE BLCS 280-597184/9 Lab Control Sample Total/NA
Water SM 3500 FE BLCSD 280-597184/10 Lab Control Sample Dup Total/NA
Eurofins Denver
Page 25 of 349
QC Association Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
General Chemistry
Analysis Batch: 597409
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 2320B280-170477-1 Offsite A-1 Total/NA
Water SM 2320B280-170477-2 Offsite A-2 Total/NA
Water SM 2320BMB 280-597409/110 Method Blank Total/NA
Water SM 2320BMB 280-597409/6 Method Blank Total/NA
Water SM 2320BMB 280-597409/84 Method Blank Total/NA
Water SM 2320BLCS 280-597409/109 Lab Control Sample Total/NA
Water SM 2320BLCSD 280-597409/5 Lab Control Sample Dup Total/NA
Water SM 2320B280-170477-1 DU Offsite A-1 Total/NA
Analysis Batch: 598094
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 3500280-170477-1 Offsite A-1 Total/NA
Water SM 3500280-170477-2 Offsite A-2 Total/NA
Analysis Batch: 598232
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 4500 SO4 E280-170477-1 Offsite A-1 Total/NA
Water SM 4500 SO4 E280-170477-2 Offsite A-2 Total/NA
Water SM 4500 SO4 EMB 280-598232/14 Method Blank Total/NA
Water SM 4500 SO4 ELCS 280-598232/12 Lab Control Sample Total/NA
Water SM 4500 SO4 ELCSD 280-598232/13 Lab Control Sample Dup Total/NA
Analysis Batch: 598240
Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch
Water SM 4500 Cl- E280-170477-1 Offsite A-1 Total/NA
Water SM 4500 Cl- E280-170477-2 Offsite A-2 Total/NA
Water SM 4500 Cl- EMB 280-598240/15 Method Blank Total/NA
Water SM 4500 Cl- ELCS 280-598240/13 Lab Control Sample Total/NA
Water SM 4500 Cl- ELCSD 280-598240/14 Lab Control Sample Dup Total/NA
Eurofins Denver
Page 26 of 349
Lab Chronicle
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Client Sample ID: Offsite A-1 Lab Sample ID: 280-170477-1
Matrix: WaterDate Collected: 12/14/22 12:45
Date Received: 12/16/22 09:15
Analysis 8260C MD12/25/22 14:431 EET DEN597688
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis RSK-175 1 597520 12/21/22 19:34 JPH EET DENTotal/NA 18 mL 18 mL
Prep 3020A 597451 12/22/22 07:26 LJS EET DENTotal/NA 50 mL 50 mL
Analysis 6020B 1 597704 12/22/22 18:46 LMT EET DENTotal/NA
Analysis 300.0 1 596980 12/17/22 04:27 MEC EET DENTotal/NA 5 mL 5 mL
Analysis SM 2320B 1 597409 12/21/22 03:23 KEG EET DENTotal/NA
Analysis SM 3500 1 598094 12/29/22 16:06 DNM EET DENTotal/NA
Analysis SM 3500 FE B 1 597184 12/19/22 14:09 LRB EET DENTotal/NA 2 mL 2 mL
Analysis SM 4500 Cl- E 20 598240 12/30/22 16:01 LRB EET DENTotal/NA 2 mL 2 mL
Analysis SM 4500 SO4 E 10 598232 12/30/22 16:07 LRB EET DENTotal/NA 2 mL 2 mL
Client Sample ID: Offsite A-2 Lab Sample ID: 280-170477-2
Matrix: WaterDate Collected: 12/14/22 11:00
Date Received: 12/16/22 09:15
Analysis 8260C MD12/25/22 15:041 EET DEN597688
Type
Batch
Method
Batch
Prep Type LabAnalystRun
Prepared
or Analyzed
Initial
Amount Amount
Final Batch
NumberFactor
Dil
Total/NA 5 mL 5 mL
Analysis RSK-175 1 597520 12/21/22 20:01 JPH EET DENTotal/NA 18 mL 18 mL
Prep 3020A 597451 12/22/22 07:26 LJS EET DENTotal/NA 50 mL 50 mL
Analysis 6020B 1 597704 12/22/22 18:48 LMT EET DENTotal/NA
Analysis 300.0 1 596980 12/17/22 04:42 MEC EET DENTotal/NA 5 mL 5 mL
Analysis SM 2320B 1 597409 12/21/22 03:39 KEG EET DENTotal/NA
Analysis SM 3500 1 598094 12/29/22 16:06 DNM EET DENTotal/NA
Analysis SM 3500 FE B 1 597184 12/19/22 14:09 LRB EET DENTotal/NA 2 mL 2 mL
Analysis SM 4500 Cl- E 20 598240 12/30/22 16:17 LRB EET DENTotal/NA 2 mL 2 mL
Analysis SM 4500 SO4 E 10 598232 12/30/22 16:08 LRB EET DENTotal/NA 2 mL 2 mL
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
Page 27 of 349
Accreditation/Certification Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Laboratory: Eurofins Denver
Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below.
Authority Program Identification Number Expiration Date
Utah NELAP CO000262019-11 07-31-23
The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which
the agency does not offer certification.
Analysis Method Prep Method Matrix Analyte
8260C Water Methyl acetate
SM 3500 Water Ferric Iron
Eurofins Denver
Page 28 of 349
Method Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Method Method Description LaboratoryProtocol
SW8468260CVolatile Organic Compounds by GC/MS EET DEN
RSKRSK-175 Dissolved Gases (GC)EET DEN
SW8466020BMetals (ICP/MS)EET DEN
MCAWW300.0 Anions, Ion Chromatography EET DEN
SMSM 2320B Alkalinity EET DEN
SMSM 3500 Iron, Ferric EET DEN
SMSM 3500 FE B Iron, Ferrous and Ferric EET DEN
SMSM 4500 Cl- E Chloride, Total EET DEN
SMSM 4500 SO4 E Sulfate, Total EET DEN
SW8463020APreparation, Total Metals EET DEN
SW8465030CPurge and Trap EET DEN
Protocol References:
MCAWW = "Methods For Chemical Analysis Of Water And Wastes", EPA-600/4-79-020, March 1983 And Subsequent Revisions.
RSK = Sample Prep And Calculations For Dissolved Gas Analysis In Water Samples Using A GC Headspace Equilibration Technique, RSKSOP-175,
Rev. 0, 8/11/94, USEPA Research Lab
SM = "Standard Methods For The Examination Of Water And Wastewater"
SW846 = "Test Methods For Evaluating Solid Waste, Physical/Chemical Methods", Third Edition, November 1986 And Its Updates.
Laboratory References:
EET DEN = Eurofins Denver, 4955 Yarrow Street, Arvada, CO 80002, TEL [phone]
Eurofins Denver
Page 29 of 349
Sample Summary
Job ID: 280-170477-1Client: WSP USA Environment & Infrastructure Inc.
Project/Site: Salt Lake City, Utah
Lab Sample ID Client Sample ID Matrix Collected Received
280-170477-1 Offsite A-1 Water 12/14/22 12:45 12/16/22 09:15
280-170477-2 Offsite A-2 Water 12/14/22 11:00 12/16/22 09:15
Eurofins DenverPage 30 of 349
Lab Name:Job No.:
SDG No.:
GC/MS VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VMS_X4 590907
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
STD005 280-590907/13 IC
X43662.D10/22/22 11:33 GC Column:DB-624 (60.25)ID:0.25(mm)
Iodomethane Peak assignment corrected RWB2 10/24/22 10:373.05
2,2-Dichloropropane Peak assignment corrected RWB2 10/24/22 10:374.22
n-Heptane Peak assignment corrected RWB2 10/24/22 10:375.04
1,4-Dioxane Assign Peak RWB2 10/24/22 10:375.59
Toluene Assign Peak RWB2 10/24/22 10:376.37
Hexachlorobutadiene Assign Peak RWB2 10/24/22 10:3811.91
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
STD010 280-590907/14 IC
X43664.D10/22/22 12:14 GC Column:DB-624 (60.25)ID:0.25(mm)
n-Heptane Assign Peak RWB2 10/22/22 13:305.04
8260C
Page 31 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/4
J1044.D11/22/22 16:02 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 16:541.21
Ethane Baseline Smoothing DJQ7 11/22/22 16:531.46
Ethene Baseline Smoothing DJQ7 11/22/22 16:541.75
Propane Assign Peak DJQ7 11/22/22 16:582.51
Acetylene Assign Peak DJQ7 11/22/22 17:044.13
Butane Assign Peak DJQ7 11/22/22 17:054.41
isobutylene Assign Peak DJQ7 11/22/22 17:065.33
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/4
J1044.D11/22/22 16:02 GC Column:HP-Plot Q ID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 17:031.64
Ethene Assign Peak DJQ7 11/22/22 17:012.57
Acetylene Assign Peak DJQ7 11/22/22 17:012.73
Ethane Baseline Smoothing DJQ7 11/22/22 17:022.99
Propane Assign Peak DJQ7 11/22/22 17:004.91
isobutylene Assign Peak DJQ7 11/22/22 17:086.26
Butane Assign Peak DJQ7 11/22/22 17:096.42
RSK-175
Page 32 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/5
J1045.D11/22/22 16:16 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 17:301.21
Ethane Baseline Smoothing DJQ7 11/22/22 17:301.46
Ethene Baseline Smoothing DJQ7 11/22/22 17:311.75
Propane Assign Peak DJQ7 11/22/22 17:332.51
Acetylene Assign Peak DJQ7 11/22/22 17:394.13
Butane Assign Peak DJQ7 11/22/22 17:444.41
isobutylene Assign Peak DJQ7 11/22/22 17:425.33
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/5
J1045.D11/22/22 16:16 GC Column:HP-Plot Q ID:0.53(mm)
Ethene Baseline Smoothing DJQ7 11/22/22 17:312.58
Acetylene Assign Peak DJQ7 11/22/22 17:392.73
Ethane Baseline Smoothing DJQ7 11/22/22 17:323.00
Propane Assign Peak DJQ7 11/22/22 17:344.92
isobutylene Assign Peak DJQ7 11/22/22 17:436.26
Butane Assign Peak DJQ7 11/22/22 17:436.42
RSK-175
Page 33 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/6
J1046.D11/22/22 16:30 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 17:481.21
Ethane Baseline Smoothing DJQ7 11/22/22 17:481.46
Ethene Baseline Smoothing DJQ7 11/22/22 17:481.75
Propane Assign Peak DJQ7 11/22/22 17:492.51
Acetylene Assign Peak DJQ7 11/22/22 17:524.13
Butane Assign Peak DJQ7 11/22/22 18:014.41
isobutylene Assign Peak DJQ7 11/22/22 17:585.33
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/6
J1046.D11/22/22 16:30 GC Column:HP-Plot Q ID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 17:471.65
Acetylene Assign Peak DJQ7 11/22/22 17:522.73
Propane Assign Peak DJQ7 11/22/22 17:514.92
isobutylene Assign Peak DJQ7 11/22/22 17:596.26
Butane Assign Peak DJQ7 11/22/22 18:026.42
RSK-175
Page 34 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/7
J1047.D11/22/22 16:44 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 18:111.21
Ethane Baseline Smoothing DJQ7 11/22/22 18:131.46
Ethene Baseline Smoothing DJQ7 11/22/22 18:141.75
Propane Assign Peak DJQ7 11/22/22 18:152.51
Acetylene Assign Peak DJQ7 11/22/22 18:164.13
Butane Assign Peak DJQ7 11/22/22 18:174.41
isobutylene Assign Peak DJQ7 11/22/22 18:185.33
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/7
J1047.D11/22/22 16:44 GC Column:HP-Plot Q ID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 18:121.64
Acetylene Assign Peak DJQ7 11/22/22 18:162.73
Ethane Baseline Smoothing DJQ7 11/22/22 18:132.99
Propane Assign Peak DJQ7 11/22/22 18:164.91
isobutylene Assign Peak DJQ7 11/22/22 18:196.26
Butane Assign Peak DJQ7 11/22/22 18:186.42
RSK-175
Page 35 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/8
J1048.D11/22/22 16:57 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 19:041.21
Ethane Baseline Smoothing DJQ7 11/22/22 19:051.46
Ethene Baseline Smoothing DJQ7 11/22/22 19:061.75
Propane Assign Peak DJQ7 11/22/22 19:072.51
Acetylene Assign Peak DJQ7 11/22/22 19:104.12
Butane Assign Peak DJQ7 11/22/22 19:114.41
isobutylene Assign Peak DJQ7 11/22/22 19:115.32
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/8
J1048.D11/22/22 16:57 GC Column:HP-Plot Q ID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 19:051.64
Acetylene Assign Peak DJQ7 11/22/22 19:102.72
Ethane Baseline Smoothing DJQ7 11/22/22 19:062.99
Propane Assign Peak DJQ7 11/22/22 19:084.91
isobutylene Assign Peak DJQ7 11/22/22 19:136.26
Butane Assign Peak DJQ7 11/22/22 19:146.42
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/9
J1049.D11/22/22 17:11 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 19:151.21
Ethane Baseline Smoothing DJQ7 11/22/22 19:161.46
Ethene Baseline Smoothing DJQ7 11/22/22 19:171.75
isobutylene Assign Peak DJQ7 11/22/22 19:185.32
RSK-175
Page 36 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 594440
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/9
J1049.D11/22/22 17:11 GC Column:HP-Plot Q ID:0.53(mm)
Propane Split Peak DJQ7 11/22/22 19:174.91
isobutylene Split Peak DJQ7 11/22/22 19:186.26
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/10
J1050.D11/22/22 17:25 GC Column:HP-Plot Q ID:0.53(mm)
Methane Baseline Smoothing DJQ7 11/22/22 18:041.64
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
IC 280-594440/12
J1052.D11/22/22 17:53 GC Column:HP-Plot Q ID:0.53(mm)
Methane Column bleed DJQ7 11/22/22 19:201.64
RSK-175
Page 37 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 597520
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCVRT 280-597520/2
J1982.D12/21/22 15:19 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 12/21/22 15:381.22
Ethane Baseline Smoothing DJQ7 12/21/22 15:391.47
Ethene Baseline Smoothing DJQ7 12/21/22 15:391.74
Butane Assign Peak DJQ7 12/21/22 15:354.37
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCVRT 280-597520/2
J1982.D12/21/22 15:19 GC Column:HP-Plot Q ID:0.53(mm)
isobutylene Split Peak DJQ7 12/21/22 15:366.27
Butane Split Peak DJQ7 12/21/22 15:366.42
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCS 280-597520/4
J1984.D12/21/22 15:54 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 12/21/22 17:471.21
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCSD 280-597520/5
J1985.D12/21/22 16:08 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 12/21/22 17:451.21
RSK-175
Page 38 of 349
Lab Name:Job No.:
SDG No.:
GC VOA MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:VGC_J 597520
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-597520/18
J1998.D12/21/22 19:47 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 12/21/22 20:061.21
Ethane Baseline Smoothing DJQ7 12/21/22 20:061.46
Ethene Baseline Smoothing DJQ7 12/21/22 20:071.75
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-597520/30
J2010.D12/21/22 22:28 GC Column:Rt-Alumina KClID:0.53(mm)
Methane Baseline Smoothing DJQ7 12/21/22 23:581.21
Ethane Baseline Smoothing DJQ7 12/21/22 23:591.46
Ethene Baseline Smoothing DJQ7 12/21/22 23:591.75
Propane Instrument noise DJQ7 12/21/22 23:592.52
Acetylene Sample matrix interference DJQ7 12/22/22 00:004.13
Butane Assign Peak DJQ7 12/22/22 00:014.42
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-597520/30
J2010.D12/21/22 22:28 GC Column:HP-Plot Q ID:0.53(mm)
isobutylene Split Peak DJQ7 12/22/22 00:016.26
Butane Assign Peak DJQ7 12/22/22 00:016.42
RSK-175
Page 39 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:WC_IonChrom10 596980
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
MRL 280-596980/3
Info 2_DENPC179_Anions_20221216-182635.d12/16/22 18:11 GC Column:Metrosepp A SupID:
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:307.44
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-596980/29
Info 2_DENPC179_Anions_20221217-005728.d12/17/22 00:42 GC Column:Metrosepp A SupID:
Nitrite as N Baseline Smoothing LVW8 12/19/22 14:405.30
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:407.37
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCS 280-596980/37
Info 2_DENPC179_Anions_20221217-025750.d12/17/22 02:42 GC Column:Metrosepp A SupID:
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:427.37
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
LCSD 280-596980/38
Info 2_DENPC179_Anions_20221217-031251.d12/17/22 02:57 GC Column:Metrosepp A SupID:
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:437.37
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-596980/41
Info 2_DENPC179_Anions_20221217-035750.d12/17/22 03:42 GC Column:Metrosepp A SupID:
Nitrite as N Baseline Smoothing LVW8 12/19/22 14:445.30
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:447.37
300.0
Page 40 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY MANUAL INTEGRATION SUMMARY
Eurofins Denver 280-170477-1
Instrument ID:Analysis Batch Number:WC_IonChrom10 596980
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
280-170477-1 Offsite A-1
Info 2_DENPC179_Anions_20221217-044244.d12/17/22 04:27 GC Column:Metrosepp A SupID:
Nitrate as N Isomers LVW8 12/19/22 14:457.42
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
280-170477-2 Offsite A-2
Info 2_DENPC179_Anions_20221217-045743.d12/17/22 04:42 GC Column:Metrosepp A SupID:
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:457.43
Lab Sample ID:Client Sample ID:
Date Analyzed:Lab File ID:
COMPOUND NAME RETENTION
TIME
MANUAL INTEGRATION
DATEANALYSTREASON
CCV 280-596980/50
Info 2_DENPC179_Anions_20221217-061234.d12/17/22 05:57 GC Column:Metrosepp A SupID:
Nitrite as N Baseline Smoothing LVW8 12/19/22 14:465.30
Nitrate as N Baseline Smoothing LVW8 12/19/22 14:467.37
300.0
Page 41 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
10/26/22 09/24/22 20 mL MV-568720_00043 1000 uL Acrolein 987.5 ug/mLAcrolein_A_00015 Methanol, Lot 230446
02/28/23 (Purchased Reagent)Acrolein 19750 ug/mLRESTEK, Lot A0175809.MV-568720_00043
12/27/22 12/20/22 1000 mL Alk stk std_00023 4 mL Alkalinity 200 mg/LAlk daily lcs_01070 Di Water, Lot na
10/30/23 (Purchased Reagent)Alkalinity 50 g/LSPEX, Lot 2-106BT.Alk stk std_00023
Acrolein_A_00015 Acrolein 49.375 ug/mL100 uL 5 uL10/26/22 10/22/22Cal Dil Std_00104 P&T Methanol, Lot
ED137-US
Bromomethane 5 ug/mLMV-Gas A_00136 2 uL
Chloroethane 5 ug/mL
Chloromethane 5 ug/mL
Dichlorodifluoromethane 5 ug/mL
Dichlorofluoromethane 5 ug/mL
Trichlorofluoromethane 5 ug/mL
Vinyl chloride 5 ug/mL
2-Chloroethyl vinyl ether 5 ug/mL
2-Butanone (MEK)20 ug/mLMV-MegaMainA_00078 5 uL
4-Methyl-2-pentanone (MIBK)20 ug/mL
Acetone 20 ug/mL
Methyl n-butyl ketone (MNBK)20 ug/mL
Vinyl acetate 10 ug/mL
Cyclohexanone 150 ug/mL
1,1,1,2-Tetrachloroethane 5 ug/mL
1,1,1-Trichloroethane 5 ug/mL
1,1,2,2-Tetrachloroethane 5 ug/mL
1,1,2-Trichloroethane 5 ug/mL
1,1-Dichloroethane 5 ug/mL
1,1-Dichloroethene 5 ug/mL
1,1-Dichloropropene 5 ug/mL
1,2,3-Trichlorobenzene 5 ug/mL
1,2,3-Trichloropropane 5 ug/mL
1,2,4-Trichlorobenzene 5 ug/mL
1,2,4-Trimethylbenzene 5 ug/mL
1,2-Dibromo-3-Chloropropane 5 ug/mL
1,2-Dibromoethane 5 ug/mL
1,2-Dichlorobenzene 5 ug/mL
1,2-Dichloroethane 5 ug/mL
1,2-Dichloropropane 5 ug/mL
1,3,5-Trimethylbenzene 5 ug/mL
1,3-Dichlorobenzene 5 ug/mL
1,3-Dichloropropane 5 ug/mL
1,4-Dichlorobenzene 5 ug/mL
1,4-Dioxane 100 ug/mL
2,2-Dichloropropane 5 ug/mL
2-Chlorotoluene 5 ug/mL
2-Methyl-2-propanol 50 ug/mL
3-Chloro-1-propene 5 ug/mL
4-Chlorotoluene 5 ug/mL
4-Isopropyltoluene 5 ug/mL
Page 42 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Acrylonitrile 50 ug/mL
Benzene 5 ug/mL
Bromobenzene 5 ug/mL
Bromoform 5 ug/mL
Carbon disulfide 5 ug/mL
Carbon tetrachloride 5 ug/mL
Chlorobenzene 5 ug/mL
Chlorobromomethane 5 ug/mL
Chlorodibromomethane 5 ug/mL
Chloroform 5 ug/mL
cis-1,2-Dichloroethene 5 ug/mL
cis-1,3-Dichloropropene 5 ug/mL
Cyclohexane 5 ug/mL
Dibromomethane 5 ug/mL
Dichlorobromomethane 5 ug/mL
Ethyl ether 5 ug/mL
Ethyl methacrylate 5 ug/mL
Ethylbenzene 5 ug/mL
Freon 113 5 ug/mL
Hexachlorobutadiene 5 ug/mL
Hexane 5 ug/mL
Iodomethane 5 ug/mL
Isobutyl alcohol 125 ug/mL
Isopropylbenzene 5 ug/mL
m-Xylene & p-Xylene 5 ug/mL
Methyl acetate 10 ug/mL
Methyl tert-butyl ether 5 ug/mL
Methylcyclohexane 5 ug/mL
Methylene Chloride 5 ug/mL
n-Butylbenzene 5 ug/mL
n-Heptane 5 ug/mL
N-Propylbenzene 5 ug/mL
Naphthalene 5 ug/mL
o-Xylene 5 ug/mL
sec-Butylbenzene 5 ug/mL
Styrene 5 ug/mL
tert-Butylbenzene 5 ug/mL
Tetrachloroethene 5 ug/mL
Tetrahydrofuran 10 ug/mL
Toluene 5 ug/mL
trans-1,2-Dichloroethene 5 ug/mL
trans-1,3-Dichloropropene 5 ug/mL
trans-1,4-Dichloro-2-butene 5 ug/mL
Trichloroethene 5 ug/mL
1-Chlorohexane 4 ug/mL
2-Pentanone 16 ug/mL
sec-Butyl Alcohol 120 ug/mL
10/26/22 09/24/22 20 mL MV-568720_00043 1000 uL Acrolein 987.5 ug/mL.Acrolein_A_00015 Methanol, Lot 230446
Page 43 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
02/28/23 (Purchased Reagent)Acrolein 19750 ug/mLRESTEK, Lot A0175809..MV-568720_00043
MV-569722_00021 Bromomethane 250 ug/mL12.5 mL 1250 uL11/14/22 10/12/22.MV-Gas A_00136 P&T Methanol, Lot
198123
Chloroethane 250 ug/mL
Chloromethane 250 ug/mL
Dichlorodifluoromethane 250 ug/mL
Dichlorofluoromethane 250 ug/mL
Trichlorofluoromethane 250 ug/mL
Vinyl chloride 250 ug/mL
MV-569723_00016 1250 uL 2-Chloroethyl vinyl ether 250 ug/mL
05/31/25 (Purchased Reagent)Bromomethane 2500 ug/mLRESTEK, Lot A0184726..MV-569722_00021
Chloroethane 2500 ug/mL
Chloromethane 2500 ug/mL
Dichlorodifluoromethane 2500 ug/mL
Dichlorofluoromethane 2500 ug/mL
Trichlorofluoromethane 2500 ug/mL
Vinyl chloride 2500 ug/mL
01/31/25 (Purchased Reagent)2-Chloroethyl vinyl ether 2500 ug/mLRESTEK, Lot A0180640..MV-569723_00016
MV-569721_00013 2-Butanone (MEK)400 ug/mL25 mL 800 uL10/31/22 09/27/22.MV-MegaMainA_00078 P&T Methanol, Lot
181124
4-Methyl-2-pentanone (MIBK)400 ug/mL
Acetone 400 ug/mL
Methyl n-butyl ketone (MNBK)400 ug/mL
Vinyl acetate 200 ug/mLMV-569724_00034 1000 uL
Cyclohexanone 3000 ug/mLMV-569727_00020 3000 uL
1,1,1,2-Tetrachloroethane 100 ug/mLMV-571992_00015 1000 uL
1,1,1-Trichloroethane 100 ug/mL
1,1,2,2-Tetrachloroethane 100 ug/mL
1,1,2-Trichloroethane 100 ug/mL
1,1-Dichloroethane 100 ug/mL
1,1-Dichloroethene 100 ug/mL
1,1-Dichloropropene 100 ug/mL
1,2,3-Trichlorobenzene 100 ug/mL
1,2,3-Trichloropropane 100 ug/mL
1,2,4-Trichlorobenzene 100 ug/mL
1,2,4-Trimethylbenzene 100 ug/mL
1,2-Dibromo-3-Chloropropane 100 ug/mL
1,2-Dibromoethane 100 ug/mL
1,2-Dichlorobenzene 100 ug/mL
1,2-Dichloroethane 100 ug/mL
1,2-Dichloropropane 100 ug/mL
1,3,5-Trimethylbenzene 100 ug/mL
1,3-Dichlorobenzene 100 ug/mL
1,3-Dichloropropane 100 ug/mL
1,4-Dichlorobenzene 100 ug/mL
1,4-Dioxane 2000 ug/mL
2,2-Dichloropropane 100 ug/mL
2-Chlorotoluene 100 ug/mL
Page 44 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
2-Methyl-2-propanol 1000 ug/mL
3-Chloro-1-propene 100 ug/mL
4-Chlorotoluene 100 ug/mL
4-Isopropyltoluene 100 ug/mL
Acrylonitrile 1000 ug/mL
Benzene 100 ug/mL
Bromobenzene 100 ug/mL
Bromoform 100 ug/mL
Carbon disulfide 100 ug/mL
Carbon tetrachloride 100 ug/mL
Chlorobenzene 100 ug/mL
Chlorobromomethane 100 ug/mL
Chlorodibromomethane 100 ug/mL
Chloroform 100 ug/mL
cis-1,2-Dichloroethene 100 ug/mL
cis-1,3-Dichloropropene 100 ug/mL
Cyclohexane 100 ug/mL
Dibromomethane 100 ug/mL
Dichlorobromomethane 100 ug/mL
Ethyl ether 100 ug/mL
Ethyl methacrylate 100 ug/mL
Ethylbenzene 100 ug/mL
Freon 113 100 ug/mL
Hexachlorobutadiene 100 ug/mL
Hexane 100 ug/mL
Iodomethane 100 ug/mL
Isobutyl alcohol 2500 ug/mL
Isopropylbenzene 100 ug/mL
m-Xylene & p-Xylene 100 ug/mL
Methyl acetate 200 ug/mL
Methyl tert-butyl ether 100 ug/mL
Methylcyclohexane 100 ug/mL
Methylene Chloride 100 ug/mL
n-Butylbenzene 100 ug/mL
n-Heptane 100 ug/mL
N-Propylbenzene 100 ug/mL
Naphthalene 100 ug/mL
o-Xylene 100 ug/mL
sec-Butylbenzene 100 ug/mL
Styrene 100 ug/mL
tert-Butylbenzene 100 ug/mL
Tetrachloroethene 100 ug/mL
Tetrahydrofuran 200 ug/mL
Toluene 100 ug/mL
trans-1,2-Dichloroethene 100 ug/mL
trans-1,3-Dichloropropene 100 ug/mL
trans-1,4-Dichloro-2-butene 100 ug/mL
Trichloroethene 100 ug/mL
Page 45 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
1-Chlorohexane 80 ug/mLMV-CUS17739.s_00011 2000 uL
2-Pentanone 320 ug/mL
sec-Butyl Alcohol 2400 ug/mL
01/31/25 (Purchased Reagent)2-Butanone (MEK)12500 ug/mLRESTEK, Lot A0180742..MV-569721_00013
4-Methyl-2-pentanone (MIBK)12500 ug/mL
Acetone 12500 ug/mL
Methyl n-butyl ketone (MNBK)12500 ug/mL
06/30/23 (Purchased Reagent)Vinyl acetate 5000 ug/mLRESTEK, Lot A0179890..MV-569724_00034
03/31/25 (Purchased Reagent)Cyclohexanone 25000 ug/mLRESTEK, Lot A0182677..MV-569727_00020
09/30/24 (Purchased Reagent)1,1,1,2-Tetrachloroethane 2500 ug/mLRESTEK, Lot A0183568..MV-571992_00015
1,1,1-Trichloroethane 2500 ug/mL
1,1,2,2-Tetrachloroethane 2500 ug/mL
1,1,2-Trichloroethane 2500 ug/mL
1,1-Dichloroethane 2500 ug/mL
1,1-Dichloroethene 2500 ug/mL
1,1-Dichloropropene 2500 ug/mL
1,2,3-Trichlorobenzene 2500 ug/mL
1,2,3-Trichloropropane 2500 ug/mL
1,2,4-Trichlorobenzene 2500 ug/mL
1,2,4-Trimethylbenzene 2500 ug/mL
1,2-Dibromo-3-Chloropropane 2500 ug/mL
1,2-Dibromoethane 2500 ug/mL
1,2-Dichlorobenzene 2500 ug/mL
1,2-Dichloroethane 2500 ug/mL
1,2-Dichloropropane 2500 ug/mL
1,3,5-Trimethylbenzene 2500 ug/mL
1,3-Dichlorobenzene 2500 ug/mL
1,3-Dichloropropane 2500 ug/mL
1,4-Dichlorobenzene 2500 ug/mL
1,4-Dioxane 50000 ug/mL
2,2-Dichloropropane 2500 ug/mL
2-Chlorotoluene 2500 ug/mL
2-Methyl-2-propanol 25000 ug/mL
3-Chloro-1-propene 2500 ug/mL
4-Chlorotoluene 2500 ug/mL
4-Isopropyltoluene 2500 ug/mL
Acrylonitrile 25000 ug/mL
Benzene 2500 ug/mL
Bromobenzene 2500 ug/mL
Bromoform 2500 ug/mL
Carbon disulfide 2500 ug/mL
Carbon tetrachloride 2500 ug/mL
Chlorobenzene 2500 ug/mL
Chlorobromomethane 2500 ug/mL
Chlorodibromomethane 2500 ug/mL
Chloroform 2500 ug/mL
cis-1,2-Dichloroethene 2500 ug/mL
cis-1,3-Dichloropropene 2500 ug/mL
Page 46 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Cyclohexane 2500 ug/mL
Dibromomethane 2500 ug/mL
Dichlorobromomethane 2500 ug/mL
Ethyl ether 2500 ug/mL
Ethyl methacrylate 2500 ug/mL
Ethylbenzene 2500 ug/mL
Freon 113 2500 ug/mL
Hexachlorobutadiene 2500 ug/mL
Hexane 2500 ug/mL
Iodomethane 2500 ug/mL
Isobutyl alcohol 62500 ug/mL
Isopropylbenzene 2500 ug/mL
m-Xylene & p-Xylene 2500 ug/mL
Methyl acetate 5000 ug/mL
Methyl tert-butyl ether 2500 ug/mL
Methylcyclohexane 2500 ug/mL
Methylene Chloride 2500 ug/mL
n-Butylbenzene 2500 ug/mL
n-Heptane 2500 ug/mL
N-Propylbenzene 2500 ug/mL
Naphthalene 2500 ug/mL
o-Xylene 2500 ug/mL
sec-Butylbenzene 2500 ug/mL
Styrene 2500 ug/mL
tert-Butylbenzene 2500 ug/mL
Tetrachloroethene 2500 ug/mL
Tetrahydrofuran 5000 ug/mL
Toluene 2500 ug/mL
trans-1,2-Dichloroethene 2500 ug/mL
trans-1,3-Dichloropropene 2500 ug/mL
trans-1,4-Dichloro-2-butene 2500 ug/mL
Trichloroethene 2500 ug/mL
05/31/24 (Purchased Reagent)1-Chlorohexane 1000 ug/mLAgilent, Lot 6676357.sec..MV-CUS17739.s_00011
2-Pentanone 4000 ug/mL
sec-Butyl Alcohol 30000 ug/mL
01/06/23 12/30/22 100 mL Cl Cal Std_00021 20 mL Chloride 199.96 mg/LCl Cal Int_00040 ELGA Water, Lot na
01/12/23 12/30/22 500 mL NaCl for TOX_00003 0.8241 g Chloride 999.798 mg/L.Cl Cal Std_00021 ELGA Water, Lot N/A
01/22/23 (Purchased Reagent)Chloride 0.6066 g/gFisher, Lot 177409..NaCl for TOX_00003
01/06/23 12/30/22 100 mL Cl ICV Std_00005 20 mL Chloride 200 mg/LCl ICV Int_00039 ELGA Water, Lot na
01/08/23 (Purchased Reagent)Chloride 1000 mg/LERA, Lot 080121m.Cl ICV Std_00005
12/20/22 12/19/22 500 mL FE Stock Cal_00005 0.3511 g Ferrous Iron 99.9933 mg/LFE Cal INT_00644 Di Water, Lot na
08/31/23 (Purchased Reagent)Ferrous Iron 0.1424 g/gHach, Lot A9210.FE Stock Cal_00005
12/20/22 12/19/22 500 mL FE Stock ICV_00005 0.3511 g Ferrous Iron 99.9933 mg/LFE ICV INT_00641 Di Water, Lot na
11/03/23 (Purchased Reagent)Ferrous Iron 0.1424 g/gFisher, Lot 187526.FE Stock ICV_00005
12/21/22 12/14/22 100 mL IC N03 cal_00027 2.5 mL Nitrate as N 25 mg/LIC Cal low_00681 Di Water, Lot NA
01/31/23 (Purchased Reagent)Nitrate as N 1000 mg/LRicca, Lot 2108C49.IC N03 cal_00027
Page 47 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
12/14/22 12/07/22 100 mL IC NO3 ICV_00018 2.5 mL Nitrate as N 25 mg/LIC ICV 5_00385 Di Water, Lot na
03/26/23 (Purchased Reagent)Nitrate as N 1000 mg/LERA, Lot 830421m.IC NO3 ICV_00018
12/21/22 12/14/22 200 mL IC Cal low_00681 20 mL Nitrate as N 2.5 mg/L as NIC LCS_01923 Di Water, Lot 27
12/21/22 12/14/22 100 mL IC N03 cal_00027 2.5 mL Nitrate as N 25 mg/L.IC Cal low_00681 Di Water, Lot NA
01/31/23 (Purchased Reagent)Nitrate as N 1000 mg/LRicca, Lot 2108C49..IC N03 cal_00027
12/23/22 12/22/22 250 mL MS CALSTD-2_00103 0.25 mL Iron 2000 ug/Lms 77 cal std_02872 2%HNO3/0.5% HCl, Lot
215109/22c166207
01/26/24 (Purchased Reagent)Iron 2000 mg/LCPI, Lot 1208136-1.MS CALSTD-2_00103
12/23/22 12/22/22 200 mL ms 77 cal std_02872 100 mL Iron 1000 ug/Lms 77 ccv_02880 2%HNO3/0.5% HCl, Lot
222846/221613
12/23/22 12/22/22 250 mL MS CALSTD-2_00103 0.25 mL Iron 2000 ug/L.ms 77 cal std_02872 2%HNO3/0.5% HCl, Lot
215109/22c166207
01/26/24 (Purchased Reagent)Iron 2000 mg/LCPI, Lot 1208136-1..MS CALSTD-2_00103
MS ICSA STOCK_00048 Al 100 mg/L100 mL 5 mL12/28/22 12/21/22ms 77 icsa_00656 2%HNO3/0.5% HCl, Lot
212725/22c66200
Ca 100 mg/L
Iron 100 mg/L
K 100 mg/L
Mg 100 mg/L
Mo 2 mg/L
Na 100 mg/L
Al 100 mg/LMS ICSA STOCK_00050 5 mL
Ca 100 mg/L
Iron 100 mg/L
K 100 mg/L
Mg 100 mg/L
Mo 2 mg/L
Na 100 mg/L
08/08/23 (Purchased Reagent)Al 1000 mg/LCPI, Lot 1208135-1.MS ICSA STOCK_00048
Ca 1000 mg/L
Iron 1000 mg/L
K 1000 mg/L
Mg 1000 mg/L
Mo 20 mg/L
Na 1000 mg/L
08/01/23 (Purchased Reagent)Al 1000 mg/LIV, Lot s2-meb706044.MS ICSA STOCK_00050
Ca 1000 mg/L
Iron 1000 mg/L
K 1000 mg/L
Mg 1000 mg/L
Mo 20 mg/L
Na 1000 mg/L
ICV MIX-1a_00001 As 0.1 mg/L100 mL 0.1 mL12/28/22 12/21/22ms 77 icsab_00652 2%HNO3/0.5% HCl, Lot
222846/221613
Ba 0.1 mg/L
Be 0.1 mg/L
Cd 0.1 mg/L
Page 48 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Co 0.1 mg/L
Cr 0.1 mg/L
Cu 0.1 mg/L
Li 0.2 mg/L
Mn 0.1 mg/L
Ni 0.1 mg/L
Pb 0.1 mg/L
Se 0.1 mg/L
Sr 0.2 mg/L
Tl 0.1 mg/L
V 0.1 mg/L
Mo 2.1 mg/LICV MIX-1B_00001 0.1 mL
Sb 0.1 mg/L
Sn 0.1 mg/L
Al 102 mg/LMS ICSA STOCK_00047 10 mL
Ca 107 mg/L
Iron 102 mg/L
K 107 mg/L
Mg 107 mg/L
Mo 2.1 mg/L
Na 107 mg/L
U 0.1 mg/LMS ICVMIX--3_00005 0.1 mL
Ag 0.1 mg/LMS ICVMIX--5_00002 0.1 mL
B 1 mg/L
Ca 107 mg/L
K 107 mg/L
Li 0.2 mg/L
Mg 107 mg/L
Na 107 mg/L
Sr 0.2 mg/L
Th 0.1 mg/L
Zn 0.1 mg/L
Al 102 mg/LMS ICVMIX-2_00005 0.1 mL
Ca 107 mg/L
Iron 102 mg/L
K 107 mg/L
Mg 107 mg/L
Na 107 mg/L
08/09/23 (Purchased Reagent)As 100 mg/LIV, Lot t2-meb722098.ICV MIX-1a_00001
Ba 100 mg/L
Be 100 mg/L
Cd 100 mg/L
Co 100 mg/L
Cr 100 mg/L
Cu 100 mg/L
Li 100 mg/L
Mn 100 mg/L
Ni 100 mg/L
Page 49 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Pb 100 mg/L
Se 100 mg/L
Sr 100 mg/L
Tl 100 mg/L
V 100 mg/L
08/05/23 (Purchased Reagent)Mo 100 mg/LIV, Lot t2-meb722099.ICV MIX-1B_00001
Sb 100 mg/L
Sn 100 mg/L
06/03/23 (Purchased Reagent)Al 1000 mg/LCPI, Lot 1136841.MS ICSA STOCK_00047
Ca 1000 mg/L
Iron 1000 mg/L
K 1000 mg/L
Mg 1000 mg/L
Mo 20 mg/L
Na 1000 mg/L
03/10/23 (Purchased Reagent)U 100 mg/LCPI, Lot 1072838-1.MS ICVMIX--3_00005
08/01/23 (Purchased Reagent)Ag 100 mg/LIV, Lot t2-meb721663.MS ICVMIX--5_00002
B 1000 mg/L
Ca 5000 mg/L
K 5000 mg/L
Li 100 mg/L
Mg 5000 mg/L
Na 5000 mg/L
Sr 100 mg/L
Th 100 mg/L
Zn 100 mg/L
05/16/23 (Purchased Reagent)Al 2000 mg/LCPI, Lot 1146029-1.MS ICVMIX-2_00005
Ca 2000 mg/L
Iron 2000 mg/L
K 2000 mg/L
Mg 2000 mg/L
Na 2000 mg/L
12/23/22 12/22/22 250 mL MS ICVMIX-2_00005 0.1 mL Iron 800 ug/Lms 77 icv_02882 2%HNO3/0.5% HCl, Lot
215109/22c166207
05/16/23 (Purchased Reagent)Iron 2000 mg/LCPI, Lot 1146029-1.MS ICVMIX-2_00005
12/23/22 12/22/22 100 mL MS LLCCV_00007 1 mL Iron 0.05 mg/LMS 77 LLCCV_02699 2%HNO3/0.5% HCl, Lot
215109/22c166207
09/30/23 (Purchased Reagent)Iron 5 mg/LCPI, Lot 220602.MS LLCCV_00007
CALSTD-1_00002 As 20000 ug/L500 mL 100 mL01/20/23 07/20/22ms spike 1_00014 1% HNO3, Lot 261535
Ba 20000 ug/L
Be 20000 ug/L
Cd 20000 ug/L
Co 20000 ug/L
Cr 20000 ug/L
Cu 20000 ug/L
Li 20000 ug/L
Mn 20000 ug/L
Page 50 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Mo 20000 ug/L
Ni 20000 ug/L
Pb 20000 ug/L
Sb 20000 ug/L
Se 20000 ug/L
Si 200000 ug/L
SiO2 428000 ug/L
Sn 20000 ug/L
Sr 20000 ug/L
Tl 20000 ug/L
V 20000 ug/L
Al 400000 ug/LCALSTD-2_00001 100 mL
Ca 400000 ug/L
Iron 400000 ug/L
K 400000 ug/L
Mg 400000 ug/L
Na 400000 ug/L
08/08/23 (Purchased Reagent)As 100 mg/LCPI, Lot 1148545-1.CALSTD-1_00002
Ba 100 mg/L
Be 100 mg/L
Cd 100 mg/L
Co 100 mg/L
Cr 100 mg/L
Cu 100 mg/L
Li 100 mg/L
Mn 100 mg/L
Mo 100 mg/L
Ni 100 mg/L
Pb 100 mg/L
Sb 100 mg/L
Se 100 mg/L
Si 1000 mg/L
SiO2 2140 mg/L
Sn 100 mg/L
Sr 100 mg/L
Tl 100 mg/L
V 100 mg/L
06/27/23 (Purchased Reagent)Al 2000 mg/LCPI, Lot 1146028-1.CALSTD-2_00001
Ca 2000 mg/L
Iron 2000 mg/L
K 2000 mg/L
Mg 2000 mg/L
Na 2000 mg/L
1000 Ag_00017 Ag 20 mg/L500 mL 10 mL01/01/23 11/24/22MS spike 2_00103 1% HNO3, Lot 275002
Sr 20 mg/L1000 Sr_00015 10 mL
U 20 mg/L1000 U_00043 10 mL
Zn 20 mg/L1000 Zn_00027 10 mL
Page 51 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
10000 Th_00027 1 mL Th 20 mg/L
11/24/22 (Purchased Reagent)Ag 1000 mg/LCPI, Lot 1026960-69.1000 Ag_00017
03/13/23 (Purchased Reagent)Sr 1000 mg/LCPI, Lot 1096004-19.1000 Sr_00015
05/16/23 (Purchased Reagent)U 1000 mg/LCPI, Lot 1062807-9.1000 U_00043
11/24/22 (Purchased Reagent)Zn 1000 mg/LCPI, Lot 1095528-11.1000 Zn_00027
09/24/23 (Purchased Reagent)Th 10000 mg/LCPI, Lot 1161822-1.10000 Th_00027
1,2-Dichloroethene, Totalmv-Cent BFB_00004
1,3-Dichloropropene, Total
Tentatively Identified
Compound
Total BTEX
Trihalomethanes, Total
Xylenes, Total
mv-IS/SS Tune_00001 10 mL BFB 50 ug/mL
11/30/23 (Purchased Reagent)BFB 250 ug/mLRestek, Lot A0143593.mv-IS/SS Tune_00001
MV-569722_00021 Bromomethane 250 ug/mL12.5 mL 1250 uL11/14/22 10/12/22MV-Gas A_00136 P&T Methanol, Lot
198123
Chloroethane 250 ug/mL
Chloromethane 250 ug/mL
Dichlorodifluoromethane 250 ug/mL
Dichlorofluoromethane 250 ug/mL
Trichlorofluoromethane 250 ug/mL
Vinyl chloride 250 ug/mL
MV-569723_00016 1250 uL 2-Chloroethyl vinyl ether 250 ug/mL
05/31/25 (Purchased Reagent)Bromomethane 2500 ug/mLRESTEK, Lot A0184726.MV-569722_00021
Chloroethane 2500 ug/mL
Chloromethane 2500 ug/mL
Dichlorodifluoromethane 2500 ug/mL
Dichlorofluoromethane 2500 ug/mL
Trichlorofluoromethane 2500 ug/mL
Vinyl chloride 2500 ug/mL
01/31/25 (Purchased Reagent)2-Chloroethyl vinyl ether 2500 ug/mLRESTEK, Lot A0180640.MV-569723_00016
MV-569722_00021 Bromomethane 250 ug/mL12.5 mL 1250 uL12/30/22 11/30/22MV-Gas A_00139 P&T Methanol, Lot
198123
Chloroethane 250 ug/mL
Chloromethane 250 ug/mL
Dichlorodifluoromethane 250 ug/mL
Trichlorofluoromethane 250 ug/mL
Vinyl chloride 250 ug/mL
05/31/25 (Purchased Reagent)Bromomethane 2500 ug/mLRESTEK, Lot A0184726.MV-569722_00021
Chloroethane 2500 ug/mL
Chloromethane 2500 ug/mL
Dichlorodifluoromethane 2500 ug/mL
Trichlorofluoromethane 2500 ug/mL
Vinyl chloride 2500 ug/mL
MV-569722.sec_00015 Bromomethane 250 ug/mL12.5 mL 1250 uL11/21/22 10/18/22MV-Gas B_00120 P&T Methanol, Lot
ea1899-us
Page 52 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Chloroethane 250 ug/mL
Chloromethane 250 ug/mL
Dichlorodifluoromethane 250 ug/mL
Trichlorofluoromethane 250 ug/mL
Vinyl chloride 250 ug/mL
02/28/25 (Purchased Reagent)Bromomethane 2500 ug/mLRESTEK, Lot A0182212.MV-569722.sec_00015
Chloroethane 2500 ug/mL
Chloromethane 2500 ug/mL
Dichlorodifluoromethane 2500 ug/mL
Trichlorofluoromethane 2500 ug/mL
Vinyl chloride 2500 ug/mL
mv-30241_00012 1,4-Dichlorobenzene-d4 50 ug/mL50 mL 1000 uL11/21/22 10/07/22mv-IS_SS_00049 P&T Methanol, Lot
198123
Chlorobenzene-d5 50 ug/mL
Fluorobenzene 50 ug/mL
1,2-Dichloroethane-d4 (Surr)50 ug/mLMV-567650_00030 1000 uL
4-Bromofluorobenzene (Surr)50 ug/mL
Dibromofluoromethane (Surr)50 ug/mL
Toluene-d8 (Surr)50 ug/mL
05/31/27 (Purchased Reagent)1,4-Dichlorobenzene-d4 2500 ug/mLRestek, Lot A0185733.mv-30241_00012
Chlorobenzene-d5 2500 ug/mL
Fluorobenzene 2500 ug/mL
05/31/26 (Purchased Reagent)1,2-Dichloroethane-d4 (Surr)2500 ug/mLRestek, Lot A0172587.MV-567650_00030
4-Bromofluorobenzene (Surr)2500 ug/mL
Dibromofluoromethane (Surr)2500 ug/mL
Toluene-d8 (Surr)2500 ug/mL
mv-30241_00012 1,4-Dichlorobenzene-d4 50 ug/mL50 mL 1000 uL01/31/23 12/19/22mv-IS_SS_00053 P&T Methanol, Lot
198123
Chlorobenzene-d5 50 ug/mL
Fluorobenzene 50 ug/mL
05/31/27 (Purchased Reagent)1,4-Dichlorobenzene-d4 2500 ug/mLRestek, Lot A0185733.mv-30241_00012
Chlorobenzene-d5 2500 ug/mL
Fluorobenzene 2500 ug/mL
MV-567650_00030 1,2-Dichloroethane-d4 (Surr)50 ug/mL50 mL 1000 uL01/31/23 12/19/22mv-IS_SS_00053 P&T Methanol, Lot
198123
4-Bromofluorobenzene (Surr)50 ug/mL
Dibromofluoromethane (Surr)50 ug/mL
Toluene-d8 (Surr)50 ug/mL
05/31/26 (Purchased Reagent)1,2-Dichloroethane-d4 (Surr)2500 ug/mLRestek, Lot A0172587.MV-567650_00030
4-Bromofluorobenzene (Surr)2500 ug/mL
Dibromofluoromethane (Surr)2500 ug/mL
Toluene-d8 (Surr)2500 ug/mL
MV-569721.sec_00009 2-Butanone (MEK)400 ug/mL25 mL 800 uL11/21/22 10/18/22MV-MegaMain B_00076 P&T Methanol, Lot
181124
4-Methyl-2-pentanone (MIBK)400 ug/mL
Acetone 400 ug/mL
Methyl n-butyl ketone (MNBK)400 ug/mL
Page 53 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
1,1,1-Trichloroethane 100 ug/mLMV-571992.sec_00007 1000 uL
1,1,2,2-Tetrachloroethane 100 ug/mL
1,1,2-Trichloroethane 100 ug/mL
1,1-Dichloroethane 100 ug/mL
1,1-Dichloroethene 100 ug/mL
1,2,3-Trichlorobenzene 100 ug/mL
1,2,4-Trichlorobenzene 100 ug/mL
1,2-Dibromo-3-Chloropropane 100 ug/mL
1,2-Dibromoethane 100 ug/mL
1,2-Dichlorobenzene 100 ug/mL
1,2-Dichloroethane 100 ug/mL
1,2-Dichloropropane 100 ug/mL
1,3-Dichlorobenzene 100 ug/mL
1,4-Dichlorobenzene 100 ug/mL
1,4-Dioxane 2000 ug/mL
Benzene 100 ug/mL
Bromoform 100 ug/mL
Carbon disulfide 100 ug/mL
Carbon tetrachloride 100 ug/mL
Chlorobenzene 100 ug/mL
Chlorobromomethane 100 ug/mL
Chlorodibromomethane 100 ug/mL
Chloroform 100 ug/mL
cis-1,2-Dichloroethene 100 ug/mL
cis-1,3-Dichloropropene 100 ug/mL
Cyclohexane 100 ug/mL
Dichlorobromomethane 100 ug/mL
Ethylbenzene 100 ug/mL
Freon 113 100 ug/mL
Isopropylbenzene 100 ug/mL
m-Xylene & p-Xylene 100 ug/mL
Methyl acetate 200 ug/mL
Methyl tert-butyl ether 100 ug/mL
Methylcyclohexane 100 ug/mL
Methylene Chloride 100 ug/mL
o-Xylene 100 ug/mL
Styrene 100 ug/mL
Tetrachloroethene 100 ug/mL
Toluene 100 ug/mL
trans-1,2-Dichloroethene 100 ug/mL
trans-1,3-Dichloropropene 100 ug/mL
Trichloroethene 100 ug/mL
11/30/24 (Purchased Reagent)2-Butanone (MEK)12500 ug/mLRESTEK, Lot A0178490.MV-569721.sec_00009
4-Methyl-2-pentanone (MIBK)12500 ug/mL
Acetone 12500 ug/mL
Methyl n-butyl ketone (MNBK)12500 ug/mL
06/30/23 (Purchased Reagent)1,1,1-Trichloroethane 2500 ug/mLRESTEK, Lot A0167172.MV-571992.sec_00007
1,1,2,2-Tetrachloroethane 2500 ug/mL
Page 54 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
1,1,2-Trichloroethane 2500 ug/mL
1,1-Dichloroethane 2500 ug/mL
1,1-Dichloroethene 2500 ug/mL
1,2,3-Trichlorobenzene 2500 ug/mL
1,2,4-Trichlorobenzene 2500 ug/mL
1,2-Dibromo-3-Chloropropane 2500 ug/mL
1,2-Dibromoethane 2500 ug/mL
1,2-Dichlorobenzene 2500 ug/mL
1,2-Dichloroethane 2500 ug/mL
1,2-Dichloropropane 2500 ug/mL
1,3-Dichlorobenzene 2500 ug/mL
1,4-Dichlorobenzene 2500 ug/mL
1,4-Dioxane 50000 ug/mL
Benzene 2500 ug/mL
Bromoform 2500 ug/mL
Carbon disulfide 2500 ug/mL
Carbon tetrachloride 2500 ug/mL
Chlorobenzene 2500 ug/mL
Chlorobromomethane 2500 ug/mL
Chlorodibromomethane 2500 ug/mL
Chloroform 2500 ug/mL
cis-1,2-Dichloroethene 2500 ug/mL
cis-1,3-Dichloropropene 2500 ug/mL
Cyclohexane 2500 ug/mL
Dichlorobromomethane 2500 ug/mL
Ethylbenzene 2500 ug/mL
Freon 113 2500 ug/mL
Isopropylbenzene 2500 ug/mL
m-Xylene & p-Xylene 2500 ug/mL
Methyl acetate 5000 ug/mL
Methyl tert-butyl ether 2500 ug/mL
Methylcyclohexane 2500 ug/mL
Methylene Chloride 2500 ug/mL
o-Xylene 2500 ug/mL
Styrene 2500 ug/mL
Tetrachloroethene 2500 ug/mL
Toluene 2500 ug/mL
trans-1,2-Dichloroethene 2500 ug/mL
trans-1,3-Dichloropropene 2500 ug/mL
Trichloroethene 2500 ug/mL
MV-569721_00013 2-Butanone (MEK)400 ug/mL25 mL 800 uL10/31/22 09/27/22MV-MegaMainA_00078 P&T Methanol, Lot
181124
4-Methyl-2-pentanone (MIBK)400 ug/mL
Acetone 400 ug/mL
Methyl n-butyl ketone (MNBK)400 ug/mL
Vinyl acetate 200 ug/mLMV-569724_00034 1000 uL
Cyclohexanone 3000 ug/mLMV-569727_00020 3000 uL
1,1,1,2-Tetrachloroethane 100 ug/mLMV-571992_00015 1000 uL
Page 55 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
1,1,1-Trichloroethane 100 ug/mL
1,1,2,2-Tetrachloroethane 100 ug/mL
1,1,2-Trichloroethane 100 ug/mL
1,1-Dichloroethane 100 ug/mL
1,1-Dichloroethene 100 ug/mL
1,1-Dichloropropene 100 ug/mL
1,2,3-Trichlorobenzene 100 ug/mL
1,2,3-Trichloropropane 100 ug/mL
1,2,4-Trichlorobenzene 100 ug/mL
1,2,4-Trimethylbenzene 100 ug/mL
1,2-Dibromo-3-Chloropropane 100 ug/mL
1,2-Dibromoethane 100 ug/mL
1,2-Dichlorobenzene 100 ug/mL
1,2-Dichloroethane 100 ug/mL
1,2-Dichloropropane 100 ug/mL
1,3,5-Trimethylbenzene 100 ug/mL
1,3-Dichlorobenzene 100 ug/mL
1,3-Dichloropropane 100 ug/mL
1,4-Dichlorobenzene 100 ug/mL
1,4-Dioxane 2000 ug/mL
2,2-Dichloropropane 100 ug/mL
2-Chlorotoluene 100 ug/mL
2-Methyl-2-propanol 1000 ug/mL
3-Chloro-1-propene 100 ug/mL
4-Chlorotoluene 100 ug/mL
4-Isopropyltoluene 100 ug/mL
Acrylonitrile 1000 ug/mL
Benzene 100 ug/mL
Bromobenzene 100 ug/mL
Bromoform 100 ug/mL
Carbon disulfide 100 ug/mL
Carbon tetrachloride 100 ug/mL
Chlorobenzene 100 ug/mL
Chlorobromomethane 100 ug/mL
Chlorodibromomethane 100 ug/mL
Chloroform 100 ug/mL
cis-1,2-Dichloroethene 100 ug/mL
cis-1,3-Dichloropropene 100 ug/mL
Cyclohexane 100 ug/mL
Dibromomethane 100 ug/mL
Dichlorobromomethane 100 ug/mL
Ethyl ether 100 ug/mL
Ethyl methacrylate 100 ug/mL
Ethylbenzene 100 ug/mL
Freon 113 100 ug/mL
Hexachlorobutadiene 100 ug/mL
Hexane 100 ug/mL
Iodomethane 100 ug/mL
Page 56 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Isobutyl alcohol 2500 ug/mL
Isopropylbenzene 100 ug/mL
m-Xylene & p-Xylene 100 ug/mL
Methyl acetate 200 ug/mL
Methyl tert-butyl ether 100 ug/mL
Methylcyclohexane 100 ug/mL
Methylene Chloride 100 ug/mL
n-Butylbenzene 100 ug/mL
n-Heptane 100 ug/mL
N-Propylbenzene 100 ug/mL
Naphthalene 100 ug/mL
o-Xylene 100 ug/mL
sec-Butylbenzene 100 ug/mL
Styrene 100 ug/mL
tert-Butylbenzene 100 ug/mL
Tetrachloroethene 100 ug/mL
Tetrahydrofuran 200 ug/mL
Toluene 100 ug/mL
trans-1,2-Dichloroethene 100 ug/mL
trans-1,3-Dichloropropene 100 ug/mL
trans-1,4-Dichloro-2-butene 100 ug/mL
Trichloroethene 100 ug/mL
1-Chlorohexane 80 ug/mLMV-CUS17739.s_00011 2000 uL
2-Pentanone 320 ug/mL
sec-Butyl Alcohol 2400 ug/mL
01/31/25 (Purchased Reagent)2-Butanone (MEK)12500 ug/mLRESTEK, Lot A0180742.MV-569721_00013
4-Methyl-2-pentanone (MIBK)12500 ug/mL
Acetone 12500 ug/mL
Methyl n-butyl ketone (MNBK)12500 ug/mL
06/30/23 (Purchased Reagent)Vinyl acetate 5000 ug/mLRESTEK, Lot A0179890.MV-569724_00034
03/31/25 (Purchased Reagent)Cyclohexanone 25000 ug/mLRESTEK, Lot A0182677.MV-569727_00020
09/30/24 (Purchased Reagent)1,1,1,2-Tetrachloroethane 2500 ug/mLRESTEK, Lot A0183568.MV-571992_00015
1,1,1-Trichloroethane 2500 ug/mL
1,1,2,2-Tetrachloroethane 2500 ug/mL
1,1,2-Trichloroethane 2500 ug/mL
1,1-Dichloroethane 2500 ug/mL
1,1-Dichloroethene 2500 ug/mL
1,1-Dichloropropene 2500 ug/mL
1,2,3-Trichlorobenzene 2500 ug/mL
1,2,3-Trichloropropane 2500 ug/mL
1,2,4-Trichlorobenzene 2500 ug/mL
1,2,4-Trimethylbenzene 2500 ug/mL
1,2-Dibromo-3-Chloropropane 2500 ug/mL
1,2-Dibromoethane 2500 ug/mL
1,2-Dichlorobenzene 2500 ug/mL
1,2-Dichloroethane 2500 ug/mL
1,2-Dichloropropane 2500 ug/mL
1,3,5-Trimethylbenzene 2500 ug/mL
Page 57 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
1,3-Dichlorobenzene 2500 ug/mL
1,3-Dichloropropane 2500 ug/mL
1,4-Dichlorobenzene 2500 ug/mL
1,4-Dioxane 50000 ug/mL
2,2-Dichloropropane 2500 ug/mL
2-Chlorotoluene 2500 ug/mL
2-Methyl-2-propanol 25000 ug/mL
3-Chloro-1-propene 2500 ug/mL
4-Chlorotoluene 2500 ug/mL
4-Isopropyltoluene 2500 ug/mL
Acrylonitrile 25000 ug/mL
Benzene 2500 ug/mL
Bromobenzene 2500 ug/mL
Bromoform 2500 ug/mL
Carbon disulfide 2500 ug/mL
Carbon tetrachloride 2500 ug/mL
Chlorobenzene 2500 ug/mL
Chlorobromomethane 2500 ug/mL
Chlorodibromomethane 2500 ug/mL
Chloroform 2500 ug/mL
cis-1,2-Dichloroethene 2500 ug/mL
cis-1,3-Dichloropropene 2500 ug/mL
Cyclohexane 2500 ug/mL
Dibromomethane 2500 ug/mL
Dichlorobromomethane 2500 ug/mL
Ethyl ether 2500 ug/mL
Ethyl methacrylate 2500 ug/mL
Ethylbenzene 2500 ug/mL
Freon 113 2500 ug/mL
Hexachlorobutadiene 2500 ug/mL
Hexane 2500 ug/mL
Iodomethane 2500 ug/mL
Isobutyl alcohol 62500 ug/mL
Isopropylbenzene 2500 ug/mL
m-Xylene & p-Xylene 2500 ug/mL
Methyl acetate 5000 ug/mL
Methyl tert-butyl ether 2500 ug/mL
Methylcyclohexane 2500 ug/mL
Methylene Chloride 2500 ug/mL
n-Butylbenzene 2500 ug/mL
n-Heptane 2500 ug/mL
N-Propylbenzene 2500 ug/mL
Naphthalene 2500 ug/mL
o-Xylene 2500 ug/mL
sec-Butylbenzene 2500 ug/mL
Styrene 2500 ug/mL
tert-Butylbenzene 2500 ug/mL
Tetrachloroethene 2500 ug/mL
Page 58 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Tetrahydrofuran 5000 ug/mL
Toluene 2500 ug/mL
trans-1,2-Dichloroethene 2500 ug/mL
trans-1,3-Dichloropropene 2500 ug/mL
trans-1,4-Dichloro-2-butene 2500 ug/mL
Trichloroethene 2500 ug/mL
05/31/24 (Purchased Reagent)1-Chlorohexane 1000 ug/mLAgilent, Lot 6676357.sec.MV-CUS17739.s_00011
2-Pentanone 4000 ug/mL
sec-Butyl Alcohol 30000 ug/mL
MV-569721_00013 2-Butanone (MEK)400 ug/mL25 mL 800 uL01/23/23 12/13/22MV-MegaMainA_00082 P&T Methanol, Lot
181124
4-Methyl-2-pentanone (MIBK)400 ug/mL
Acetone 400 ug/mL
Methyl n-butyl ketone (MNBK)400 ug/mL
1,1,1-Trichloroethane 100 ug/mLMV-571992_00015 1000 uL
1,1,2,2-Tetrachloroethane 100 ug/mL
1,1,2-Trichloroethane 100 ug/mL
1,1-Dichloroethane 100 ug/mL
1,1-Dichloroethene 100 ug/mL
1,2,3-Trichlorobenzene 100 ug/mL
1,2,4-Trichlorobenzene 100 ug/mL
1,2-Dibromo-3-Chloropropane 100 ug/mL
1,2-Dibromoethane 100 ug/mL
1,2-Dichlorobenzene 100 ug/mL
1,2-Dichloroethane 100 ug/mL
1,2-Dichloropropane 100 ug/mL
1,3-Dichlorobenzene 100 ug/mL
1,4-Dichlorobenzene 100 ug/mL
1,4-Dioxane 2000 ug/mL
Benzene 100 ug/mL
Bromoform 100 ug/mL
Carbon disulfide 100 ug/mL
Carbon tetrachloride 100 ug/mL
Chlorobenzene 100 ug/mL
Chlorobromomethane 100 ug/mL
Chlorodibromomethane 100 ug/mL
Chloroform 100 ug/mL
cis-1,2-Dichloroethene 100 ug/mL
cis-1,3-Dichloropropene 100 ug/mL
Cyclohexane 100 ug/mL
Dichlorobromomethane 100 ug/mL
Ethylbenzene 100 ug/mL
Freon 113 100 ug/mL
Isopropylbenzene 100 ug/mL
m-Xylene & p-Xylene 100 ug/mL
Methyl acetate 200 ug/mL
Methyl tert-butyl ether 100 ug/mL
Methylcyclohexane 100 ug/mL
Page 59 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Methylene Chloride 100 ug/mL
o-Xylene 100 ug/mL
Styrene 100 ug/mL
Tetrachloroethene 100 ug/mL
Toluene 100 ug/mL
trans-1,2-Dichloroethene 100 ug/mL
trans-1,3-Dichloropropene 100 ug/mL
Trichloroethene 100 ug/mL
01/31/25 (Purchased Reagent)2-Butanone (MEK)12500 ug/mLRESTEK, Lot A0180742.MV-569721_00013
4-Methyl-2-pentanone (MIBK)12500 ug/mL
Acetone 12500 ug/mL
Methyl n-butyl ketone (MNBK)12500 ug/mL
09/30/24 (Purchased Reagent)1,1,1-Trichloroethane 2500 ug/mLRESTEK, Lot A0183568.MV-571992_00015
1,1,2,2-Tetrachloroethane 2500 ug/mL
1,1,2-Trichloroethane 2500 ug/mL
1,1-Dichloroethane 2500 ug/mL
1,1-Dichloroethene 2500 ug/mL
1,2,3-Trichlorobenzene 2500 ug/mL
1,2,4-Trichlorobenzene 2500 ug/mL
1,2-Dibromo-3-Chloropropane 2500 ug/mL
1,2-Dibromoethane 2500 ug/mL
1,2-Dichlorobenzene 2500 ug/mL
1,2-Dichloroethane 2500 ug/mL
1,2-Dichloropropane 2500 ug/mL
1,3-Dichlorobenzene 2500 ug/mL
1,4-Dichlorobenzene 2500 ug/mL
1,4-Dioxane 50000 ug/mL
Benzene 2500 ug/mL
Bromoform 2500 ug/mL
Carbon disulfide 2500 ug/mL
Carbon tetrachloride 2500 ug/mL
Chlorobenzene 2500 ug/mL
Chlorobromomethane 2500 ug/mL
Chlorodibromomethane 2500 ug/mL
Chloroform 2500 ug/mL
cis-1,2-Dichloroethene 2500 ug/mL
cis-1,3-Dichloropropene 2500 ug/mL
Cyclohexane 2500 ug/mL
Dichlorobromomethane 2500 ug/mL
Ethylbenzene 2500 ug/mL
Freon 113 2500 ug/mL
Isopropylbenzene 2500 ug/mL
m-Xylene & p-Xylene 2500 ug/mL
Methyl acetate 5000 ug/mL
Methyl tert-butyl ether 2500 ug/mL
Methylcyclohexane 2500 ug/mL
Methylene Chloride 2500 ug/mL
o-Xylene 2500 ug/mL
Page 60 of 349
REAGENT TRACEABILITY SUMMARY
Lab Name:
SDG No.:
Job No.:280-170477-1Eurofins Denver
Reagent ID
Exp
Date Date
Prep Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Reagent ID
Volume
Added ConcentrationAnalyte
Styrene 2500 ug/mL
Tetrachloroethene 2500 ug/mL
Toluene 2500 ug/mL
trans-1,2-Dichloroethene 2500 ug/mL
trans-1,3-Dichloropropene 2500 ug/mL
Trichloroethene 2500 ug/mL
08/08/25 (Purchased Reagent)Methane 650500 ug/LSupelco Analytical, Lot 160-402514174-1RSK175methane_00011
03/22/23 (Purchased Reagent)Methane 6570.3 ug/LMatheson, Lot 9301615705RSK7gasMathes_00034
05/27/23 (Purchased Reagent)Acetylene 10667 ug/LMatheson, Lot 9301816642RSK7gasMathes_00035
Butane 23807 ug/L
Ethane 12317 ug/L
Ethylene 11490 ug/L
isobutylene 22984 ug/L
Methane 6570.3 ug/L
Propane 18064 ug/L
01/06/23 12/30/22 50 mL SO4 Cal_00009 5 mL Sulfate 100 mg/LSO4 Cal Int_00042 water, Lot N/A
07/13/24 (Purchased Reagent)Sulfate 1000 mg/LERA, Lot 080722m.SO4 Cal_00009
01/06/23 12/30/22 50 mL SO4 ICV_00007 5 mL Sulfate 100 mg/LSO4 ICV Int_00042 water, Lot N/A
05/31/23 (Purchased Reagent)Sulfate 1000 mg/LSPEX CertiPrep, Lot 5-16so4-2x.SO4 ICV_00007
Page 61 of 349
8260C
Volatile Organic Compounds by GC/MS
Page 62 of 349
FORM II
GC/MS VOA SURROGATE RECOVERY
Lab Name:Job No.:280-170477-1
SDG No.:
Matrix:Water Level:Low
Eurofins Denver
GC Column (1):DB-624 (60.25)ID:0.25(mm)
#Lab Sample IDClient Sample ID ###DBFM DCA TOL BFB
280-170477-1Offsite A-1 97 89 102 95
280-170477-2Offsite A-2 98 92 106 95
MB 280-597688/7 97 90 107 96
LCS
280-597688/1002
98 89 107 95
LCSD
280-597688/4
98 90 105 96
QC LIMITS
DBFM = Dibromofluoromethane (Surr)77-120
DCA = 1,2-Dichloroethane-d4 (Surr)70-127
TOL = Toluene-d8 (Surr)80-125
BFB = 4-Bromofluorobenzene (Surr)78-120
FORM II 8260C
# Column to be used to flag recovery values
Page 63 of 349
GC/MS VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:-X46337-LCS.dWater
Lab ID:LCS 280-597688/1002 Client ID:
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/L)
SPIKE
ADDED
(ug/L)
#
LCS LCS
COMPOUND
Acetone 100 98.1 50-13798
2-Butanone (MEK)100 114 53-135114
Benzene 25.0 28.2 69-126113
Chlorobenzene 25.0 27.2 78-118109
Carbon disulfide 25.0 28.2 56-128113
Carbon tetrachloride 25.0 23.1 60-13392
Cyclohexane 25.0 25.5 57-134102
1,2-Dibromo-3-Chloropropane 25.0 23.5 58-12294
Bromomethane 25.0 25.0 25-163100
Bromoform 25.0 24.8 57-12599
Chloroethane 25.0 27.2 52-144109
Chloroform 25.0 26.4 68-128106
Chlorobromomethane 25.0 24.6 71-13099
Dichlorobromomethane 25.0 24.3 67-12697
Chlorodibromomethane 25.0 24.9 71-122100
Isopropylbenzene 25.0 27.7 70-127111
Methyl n-butyl ketone (MNBK)100 114 58-134114
Chloromethane 25.0 28.5 43-142114
Dichlorodifluoromethane 25.0 24.1 26-15296
trans-1,2-Dichloroethene 25.0 27.7 66-129111
trans-1,3-Dichloropropene 25.0 24.4 66-12797
Methylene Chloride 25.0 27.7 64-128111
Methyl acetate 50.0 54.9 59-133110
Methyl tert-butyl ether 25.0 27.1 70-127108
4-Methyl-2-pentanone (MIBK)100 113 56-135113
Methylcyclohexane 25.0 24.5 58-13698
Styrene 25.0 27.8 79-120111
1,1,2,2-Tetrachloroethane 25.0 28.0 72-122112
1,2,3-Trichlorobenzene 25.0 25.7 70-127103
1,2,4-Trichlorobenzene 25.0 26.2 73-124105
Toluene 25.0 28.0 68-127112
1,1,1-Trichloroethane 25.0 25.0 62-132100
1,1,2-Trichloroethane 25.0 27.2 72-128109
Trichloroethene 25.0 27.1 70-125109
Freon 113 25.0 22.9 60-13792
Vinyl chloride 25.0 28.7 53-141115
m-Xylene & p-Xylene 25.0 28.4 76-122114
o-Xylene 25.0 28.4 77-120114
Tetrachloroethene 25.0 27.3 72-127109
1,2-Dichlorobenzene 25.0 26.5 77-121106
1,3-Dichlorobenzene 25.0 26.8 76-121107
1,4-Dichlorobenzene 25.0 26.0 76-119104
FORM III 8260C
# Column to be used to flag recovery and RPD values
Page 64 of 349
GC/MS VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:-X46337-LCS.dWater
Lab ID:LCS 280-597688/1002 Client ID:
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/L)
SPIKE
ADDED
(ug/L)
#
LCS LCS
COMPOUND
cis-1,2-Dichloroethene 25.0 27.1 69-126109
cis-1,3-Dichloropropene 25.0 26.0 75-120104
1,1-Dichloroethane 25.0 26.1 66-130104
1,1-Dichloroethene 25.0 26.1 62-130105
1,2-Dichloroethane 25.0 23.6 61-13094
1,2-Dichloropropane 25.0 27.2 68-127109
1,4-Dioxane 500 547 59-134109
Ethylbenzene 25.0 28.7 76-121115
1,2-Dibromoethane 25.0 26.4 81-118106
Trichlorofluoromethane 25.0 23.7 57-14495
FORM III 8260C
# Column to be used to flag recovery and RPD values
Page 65 of 349
GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:X46338.DWater
Lab ID:LCSD 280-597688/4 Client ID:
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/L)(ug/L)
#
LCSD LCSD
100 106 21 50-137Acetone8106
100 116 20 53-1352-Butanone (MEK)2116
25.0 27.7 20 69-126Benzene2111
25.0 26.5 20 78-118Chlorobenzene2106
25.0 27.7 20 56-128Carbon disulfide 2111
25.0 23.4 20 60-133Carbon tetrachloride 194
25.0 25.1 32 57-134Cyclohexane1101
25.0 23.5 21 58-1221,2-Dibromo-3-Chloropropane 094
25.0 25.0 40 25-163Bromomethane0100
25.0 24.4 20 57-125Bromoform297
25.0 27.0 30 52-144Chloroethane1108
25.0 25.8 20 68-128Chloroform2103
25.0 25.0 20 71-130Chlorobromomethane2100
25.0 24.4 20 67-126Dichlorobromomethane198
25.0 24.3 20 71-122Chlorodibromomethane297
25.0 27.3 20 70-127Isopropylbenzene1109
100 120 21 58-134Methyl n-butyl ketone (MNBK)5120
25.0 27.3 20 43-142Chloromethane4109
25.0 24.0 21 26-152Dichlorodifluoromethane096
25.0 27.1 20 66-129trans-1,2-Dichloroethene 2108
25.0 23.9 20 66-127trans-1,3-Dichloropropene 296
25.0 27.7 20 64-128Methylene Chloride 0111
50.0 58.6 20 59-133Methyl acetate 6117
25.0 26.9 20 70-127Methyl tert-butyl ether 1108
100 113 20 56-1354-Methyl-2-pentanone (MIBK)1113
25.0 23.8 21 58-136Methylcyclohexane395
25.0 27.4 20 79-120Styrene1110
25.0 27.3 20 72-1221,1,2,2-Tetrachloroethane 3109
25.0 26.5 20 70-1271,2,3-Trichlorobenzene 3106
25.0 25.7 20 73-1241,2,4-Trichlorobenzene 2103
25.0 27.3 20 68-127Toluene3109
25.0 25.2 20 62-1321,1,1-Trichloroethane 1101
25.0 27.1 20 72-1281,1,2-Trichloroethane 0109
25.0 26.4 20 70-125Trichloroethene3105
25.0 23.6 23 60-137Freon 113 394
25.0 27.5 25 53-141Vinyl chloride 4110
25.0 27.3 20 76-122m-Xylene & p-Xylene 4109
25.0 27.8 20 77-120o-Xylene 2111
25.0 26.2 20 72-127Tetrachloroethene4105
25.0 26.2 20 77-1211,2-Dichlorobenzene 1105
25.0 26.4 20 76-1211,3-Dichlorobenzene 1106
25.0 25.6 20 76-1191,4-Dichlorobenzene 1103
FORM III 8260C
# Column to be used to flag recovery and RPD values
Page 66 of 349
GC/MS VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:X46338.DWater
Lab ID:LCSD 280-597688/4 Client ID:
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/L)(ug/L)
#
LCSD LCSD
25.0 27.8 20 69-126cis-1,2-Dichloroethene 2111
25.0 25.3 20 75-120cis-1,3-Dichloropropene 3101
25.0 26.2 20 66-1301,1-Dichloroethane 0105
25.0 26.5 21 62-1301,1-Dichloroethene 1106
25.0 23.0 20 61-1301,2-Dichloroethane 292
25.0 26.5 20 68-1271,2-Dichloropropane 3106
500 622 24 59-1341,4-Dioxane 13124
25.0 27.8 20 76-121Ethylbenzene3111
25.0 26.1 20 81-1181,2-Dibromoethane 1105
25.0 23.3 28 57-144Trichlorofluoromethane293
FORM III 8260C
# Column to be used to flag recovery and RPD values
Page 67 of 349
FORM IV
GC/MS VOA METHOD BLANK SUMMARY
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Date Analyzed:
GC Column:ID:
Instrument ID:12/25/2022 10:55
DB-624 (60.25)
NHeated Purge:(Y/N)
VMS_X4
X46342.DLab File ID:Lab Sample ID:MB 280-597688/7
WaterMatrix:
0.25(mm)
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
LAB SAMPLE ID
LAB
FILE ID DATE ANALYZEDCLIENT SAMPLE ID
12/25/2022 09:04-X46337-LCS
.d
LCS 280-597688/1002
12/25/2022 09:32X46338.DLCSD 280-597688/4
12/25/2022 14:43X46353.D280-170477-1Offsite A-1
12/25/2022 15:04X46354.D280-170477-2Offsite A-2
FORM IV 8260C
Page 68 of 349
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Job No.:
Lab File ID:
Instrument ID:
X43661.D
VMS_X4
10/22/2022
11:07
BFB Injection Date:
BFB Injection Time:
M/E ION ABUNDANCE CRITERIA % RELATIVE
ABUNDANCE
Analysis Batch No.:590907
50 15.0 - 40.0 % of mass 95 18.0
75 30.0 - 60.0 % of mass 95 50.7
95 Base Peak, 100% relative abundance 100.0
96 5.0 - 9.0 % of mass 95 6.7
173 Less than 2.0 % of mass 174 0.0 (0.0)1
174 Greater than 50% of mass 95 73.1
175 5.0 - 9.0 % of mass 174 6.1 (8.4)1
176 95.0 - 101.0 % of mass 174 70.6 (96.6)1
177 5.0 - 9.0 % of mass 176 4.6 (6.5)2
1-Value is % mass 174
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
2-Value is % mass 176
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
Eurofins Denver 280-170477-1
CLIENT SAMPLE ID LAB
FILE IDLAB SAMPLE ID DATE
ANALYZED
TIME
ANALYZED
STD005 280-590907/13 X43662.D 10/22/2022 11:33
ICIS 280-590907/18 X43663.D 10/22/2022 11:54
STD010 280-590907/14 X43664.D 10/22/2022 12:14
STD020 280-590907/15 X43665.D 10/22/2022 12:35
STD050 280-590907/16 X43666.D 10/22/2022 12:55
STD10 280-590907/17 X43667.D 10/22/2022 13:16
STD75 280-590907/19 X43668.D 10/22/2022 13:36
STD100 280-590907/20 X43669.D 10/22/2022 13:57
STD200 280-590907/21 X43670.D 10/22/2022 14:18
ICV 280-590907/22 X43672.D 10/22/2022 14:59
FORM V 8260C Page 69 of 349
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Job No.:
Lab File ID:
Instrument ID:
X43682.D
VMS_X4
10/23/2022
12:37
BFB Injection Date:
BFB Injection Time:
M/E ION ABUNDANCE CRITERIA % RELATIVE
ABUNDANCE
Analysis Batch No.:590924
50 15.0 - 40.0 % of mass 95 18.1
75 30.0 - 60.0 % of mass 95 51.0
95 Base Peak, 100% relative abundance 100.0
96 5.0 - 9.0 % of mass 95 6.4
173 Less than 2.0 % of mass 174 0.0 (0.0)1
174 Greater than 50% of mass 95 71.7
175 5.0 - 9.0 % of mass 174 6.0 (8.4)1
176 95.0 - 101.0 % of mass 174 71.1 (99.2)1
177 5.0 - 9.0 % of mass 176 4.6 (6.5)2
1-Value is % mass 174
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
2-Value is % mass 176
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
Eurofins Denver 280-170477-1
CLIENT SAMPLE ID LAB
FILE IDLAB SAMPLE ID DATE
ANALYZED
TIME
ANALYZED
ICV 280-590924/12 X43688.D 10/23/2022 15:09
FORM V 8260C Page 70 of 349
FORM V
BROMOFLUOROBENZENE (BFB)
Lab Name:
SDG No.:
Job No.:
Lab File ID:
Instrument ID:
X46337A.D
VMS_X4
12/25/2022
09:04
BFB Injection Date:
BFB Injection Time:
M/E ION ABUNDANCE CRITERIA % RELATIVE
ABUNDANCE
Analysis Batch No.:597688
50 15.0 - 40.0 % of mass 95 17.5
75 30.0 - 60.0 % of mass 95 50.5
95 Base Peak, 100% relative abundance 100.0
96 5.0 - 9.0 % of mass 95 6.9
173 Less than 2.0 % of mass 174 0.0 (0.0)1
174 Greater than 50% of mass 95 72.4
175 5.0 - 9.0 % of mass 174 6.0 (8.2)1
176 95.0 - 101.0 % of mass 174 71.2 (98.4)1
177 5.0 - 9.0 % of mass 176 4.7 (6.7)2
1-Value is % mass 174
THIS CHECK APPLIES TO THE FOLLOWING SAMPLES, MS, MSD, BLANKS AND STANDARDS:
2-Value is % mass 176
GC/MS VOA INSTRUMENT PERFORMANCE CHECK
Eurofins Denver 280-170477-1
CLIENT SAMPLE ID LAB
FILE IDLAB SAMPLE ID DATE
ANALYZED
TIME
ANALYZED
CCV 280-597688/2 X46337.D 12/25/2022 9:04
LCS 280-597688/1002 -X46337-LCS.d 12/25/2022 9:04
LCSD 280-597688/4 X46338.D 12/25/2022 9:32
MB 280-597688/7 X46342.D 12/25/2022 10:55
Offsite A-1 280-170477-1 X46353.D 12/25/2022 14:43
Offsite A-2 280-170477-2 X46354.D 12/25/2022 15:04
FORM V 8260C Page 71 of 349
GC/MS VOA INTERNAL STANDARD AREA AND RETENTION TIME SUMMARY
Lab Name:Job No.:
FORM VIII
Eurofins Denver 280-170477-1
SDG No.:
Sample No.:ICIS 280-590907/18 Date Analyzed:10/22/2022 11:54
Lab File ID (Standard):X43663.D
Instrument ID:VMS_X4 GC Column:DB-624 (60.25)ID:0.25(mm)
Heated Purge: (Y/N)N
Calibration ID:72173
#RT #RT ##RT ##
FB CBNZd5 DCBd4
AREA AREA AREA
UPPER LIMIT
LOWER LIMIT
2687648
671912 153333
613330
241283
965130
5.06 7.57 9.79INITIAL CALIBRATION MID-POINT
5.56
4.56
8.07
7.07
10.29
9.29
1343824 306665 482565
LAB SAMPLE ID CLIENT SAMPLE ID
ICV 280-590907/22 1291679 296668 481127 5.06 7.57 9.79
CCV 280-597688/2 1319687 296442 472113 5.06 7.57 9.79
LCS
280-597688/1002
1319687 296442 472113 5.06 7.57 9.79
LCSD 280-597688/4 1278429 291046 474409 5.06 7.57 9.79
MB 280-597688/7 1319652 295400 473011 5.06 7.57 9.79
280-170477-1 Offsite A-1 1238236 284546 449331 5.06 7.57 9.79
280-170477-2 Offsite A-2 1259557 283418 457981 5.06 7.57 9.79
FB = Fluorobenzene
CBNZd5 = Chlorobenzene-d5
DCBd4 = 1,4-Dichlorobenzene-d4
FORM VIII 8260C
# Column used to flag values outside QC limits
Area Limit = 50%-200% of internal standard area
RT Limit = ± 0.5 minutes of internal standard RT
Page 72 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-1 Lab Sample ID:280-170477-1
Matrix:X46353.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
12/14/2022 12:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 14:43
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
15 6.667-64-1 Acetone ND
15 5.978-93-3 2-Butanone (MEK)ND
1.0 0.3171-43-2 Benzene ND
1.0 0.42108-90-7 Chlorobenzene ND
2.0 0.6375-15-0 Carbon disulfide ND
1.0 0.5756-23-5 Carbon tetrachloride ND
1.0 0.44110-82-7 Cyclohexane ND
5.0 1.896-12-8 1,2-Dibromo-3-Chloropropane ND
5.0 2.474-83-9 Bromomethane ND
2.0 1.275-25-2 Bromoform ND
4.0 1.475-00-3 Chloroethane ND
1.0 0.3667-66-3 Chloroform ND
1.0 0.4074-97-5 Chlorobromomethane ND
1.0 0.3975-27-4 Dichlorobromomethane ND
2.0 0.62124-48-1 Chlorodibromomethane ND
1.0 0.3698-82-8 Isopropylbenzene ND
5.0 1.7591-78-6 Methyl n-butyl ketone (MNBK)ND
2.0 0.7574-87-3 Chloromethane ND
3.0 0.9675-71-8 Dichlorodifluoromethane ND
1.0 0.37156-60-5 trans-1,2-Dichloroethene 1.4
2.0 0.6510061-02-6 trans-1,3-Dichloropropene ND
2.0 0.9475-09-2 Methylene Chloride ND
5.0 1.679-20-9 Methyl acetate ND
5.0 0.251634-04-4 Methyl tert-butyl ether ND
5.0 0.98108-10-1 4-Methyl-2-pentanone (MIBK)ND
1.0 0.31108-87-2 Methylcyclohexane ND
1.0 0.36100-42-5 Styrene ND
1.0 0.2179-34-5 1,1,2,2-Tetrachloroethane ND
2.0 0.7087-61-6 1,2,3-Trichlorobenzene ND
1.0 0.58120-82-1 1,2,4-Trichlorobenzene ND
1.0 0.32108-88-3 Toluene ND
1.0 0.3971-55-6 1,1,1-Trichloroethane ND
1.0 0.2779-00-5 1,1,2-Trichloroethane ND
1.0 0.3079-01-6 Trichloroethene 67
FORM I 8260C
Page 73 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-1 Lab Sample ID:280-170477-1
Matrix:X46353.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
12/14/2022 12:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 14:43
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
3.0 0.7376-13-1 Freon 113 ND
2.0 0.5175-01-4 Vinyl chloride ND
2.0 0.36179601-23-1 m-Xylene & p-Xylene ND
1.0 0.3395-47-6 o-Xylene ND
1.0 0.40127-18-4 Tetrachloroethene ND
1.0 0.3795-50-1 1,2-Dichlorobenzene ND
1.0 0.33541-73-1 1,3-Dichlorobenzene ND
1.0 0.39106-46-7 1,4-Dichlorobenzene ND
1.0 0.32156-59-2 cis-1,2-Dichloroethene 16
2.0 0.6310061-01-5 cis-1,3-Dichloropropene ND
1.0 0.2275-34-3 1,1-Dichloroethane 2.3
1.0 0.2375-35-4 1,1-Dichloroethene 1.1
1.0 0.54107-06-2 1,2-Dichloroethane ND
1.0 0.5278-87-5 1,2-Dichloropropane ND
150 19123-91-1 1,4-Dioxane ND
1.0 0.30100-41-4 Ethylbenzene ND
1.0 0.40106-93-4 1,2-Dibromoethane ND
2.0 0.5775-69-4 Trichlorofluoromethane ND
%RECCAS NO.LIMITSQSURROGATE
89 70-12717060-07-0 1,2-Dichloroethane-d4 (Surr)
102 80-1252037-26-5 Toluene-d8 (Surr)
95 78-120460-00-4 4-Bromofluorobenzene (Surr)
97 77-1201868-53-7 Dibromofluoromethane (Surr)
FORM I 8260C
Page 74 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-2 Lab Sample ID:280-170477-2
Matrix:X46354.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
12/14/2022 11:00
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 15:04
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
15 6.667-64-1 Acetone ND
15 5.978-93-3 2-Butanone (MEK)ND
1.0 0.3171-43-2 Benzene ND
1.0 0.42108-90-7 Chlorobenzene ND
2.0 0.6375-15-0 Carbon disulfide ND
1.0 0.5756-23-5 Carbon tetrachloride ND
1.0 0.44110-82-7 Cyclohexane ND
5.0 1.896-12-8 1,2-Dibromo-3-Chloropropane ND
5.0 2.474-83-9 Bromomethane ND
2.0 1.275-25-2 Bromoform ND
4.0 1.475-00-3 Chloroethane ND
1.0 0.3667-66-3 Chloroform ND
1.0 0.4074-97-5 Chlorobromomethane ND
1.0 0.3975-27-4 Dichlorobromomethane ND
2.0 0.62124-48-1 Chlorodibromomethane ND
1.0 0.3698-82-8 Isopropylbenzene ND
5.0 1.7591-78-6 Methyl n-butyl ketone (MNBK)ND
2.0 0.7574-87-3 Chloromethane ND
3.0 0.9675-71-8 Dichlorodifluoromethane ND
1.0 0.37J156-60-5 trans-1,2-Dichloroethene 0.87
2.0 0.6510061-02-6 trans-1,3-Dichloropropene ND
2.0 0.9475-09-2 Methylene Chloride ND
5.0 1.679-20-9 Methyl acetate ND
5.0 0.251634-04-4 Methyl tert-butyl ether ND
5.0 0.98108-10-1 4-Methyl-2-pentanone (MIBK)ND
1.0 0.31108-87-2 Methylcyclohexane ND
1.0 0.36100-42-5 Styrene ND
1.0 0.2179-34-5 1,1,2,2-Tetrachloroethane ND
2.0 0.7087-61-6 1,2,3-Trichlorobenzene ND
1.0 0.58120-82-1 1,2,4-Trichlorobenzene ND
1.0 0.32108-88-3 Toluene ND
1.0 0.39J71-55-6 1,1,1-Trichloroethane 0.39
1.0 0.2779-00-5 1,1,2-Trichloroethane ND
1.0 0.3079-01-6 Trichloroethene 27
FORM I 8260C
Page 75 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-2 Lab Sample ID:280-170477-2
Matrix:X46354.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
12/14/2022 11:00
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 15:04
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
3.0 0.7376-13-1 Freon 113 ND
2.0 0.5175-01-4 Vinyl chloride ND
2.0 0.36179601-23-1 m-Xylene & p-Xylene ND
1.0 0.3395-47-6 o-Xylene ND
1.0 0.40127-18-4 Tetrachloroethene ND
1.0 0.3795-50-1 1,2-Dichlorobenzene ND
1.0 0.33541-73-1 1,3-Dichlorobenzene ND
1.0 0.39106-46-7 1,4-Dichlorobenzene ND
1.0 0.32156-59-2 cis-1,2-Dichloroethene 5.5
2.0 0.6310061-01-5 cis-1,3-Dichloropropene ND
1.0 0.2275-34-3 1,1-Dichloroethane 1.9
1.0 0.23J75-35-4 1,1-Dichloroethene 0.93
1.0 0.54107-06-2 1,2-Dichloroethane ND
1.0 0.5278-87-5 1,2-Dichloropropane ND
150 19123-91-1 1,4-Dioxane ND
1.0 0.30100-41-4 Ethylbenzene ND
1.0 0.40106-93-4 1,2-Dibromoethane ND
2.0 0.5775-69-4 Trichlorofluoromethane ND
%RECCAS NO.LIMITSQSURROGATE
92 70-12717060-07-0 1,2-Dichloroethane-d4 (Surr)
106 80-1252037-26-5 Toluene-d8 (Surr)
95 78-120460-00-4 4-Bromofluorobenzene (Surr)
98 77-1201868-53-7 Dibromofluoromethane (Surr)
FORM I 8260C
Page 76 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
1Level STD005 280-590907/13 X43662.D
2Level STD010 280-590907/14 X43664.D
3Level STD020 280-590907/15 X43665.D
4Level STD050 280-590907/16 X43666.D
5Level STD10 280-590907/17 X43667.D
6Level ICIS 280-590907/18 X43663.D
7Level STD75 280-590907/19 X43668.D
8Level STD100 280-590907/20 X43669.D
9Level STD200 280-590907/21 X43670.D
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
Dichlorodifluoromethane 0.2359 +++++0.1901 0.2559 0.1737 Ave 12.5
0.2437 0.2281 0.2222 0.2376
15.00.223
4
Chloromethane 0.2543 +++++0.2250 0.2322 0.1902 Ave 8.8
0.2120 0.2086 0.2072 0.2153
0.1000 15.00.218
1
Vinyl chloride 0.2129 +++++0.2009 0.2272 0.1668 Ave 8.6
0.2139 0.2046 0.2020 0.2124
30.00.205
1
Bromomethane ++++++++++0.1335 0.1409 0.1024 Lin1 0.9950
0.0877 0.1033 0.1055 0.1071
0.99000.068
3
0.103
2
Chloroethane 0.1760 +++++0.1262 0.1503 0.1142 Ave 13.3
0.1384 0.1337 0.1320 0.1337
15.00.138
0
Dichlorofluoromethane 0.4031 +++++0.3644 0.3844 0.3228 Ave 6.6
0.3674 0.3533 0.3500 0.3574
15.00.362
9
Trichlorofluoromethane 0.3488 +++++0.3123 0.3352 0.2374 Ave 11.0
0.3184 0.2981 0.2940 0.3217
15.00.308
2
Ethyl ether 0.1992 +++++0.1555 0.1635 0.1651 Ave 7.6
0.1657 0.1711 0.1692 0.1653
15.00.169
3
Acrolein 0.0167 +++++0.0108 0.0122 0.0114 Ave 14.8
0.0118 0.0115 0.0124 0.0121
15.00.012
3
Freon 113 0.1233 +++++0.1463 0.1479 0.1200 Ave 10.2
0.1563 0.1514 0.1279 0.1514
15.00.140
6
1,1-Dichloroethene 0.1636 +++++0.1626 0.1929 0.1597 Ave 8.6
0.1920 0.1892 0.1645 0.1899
30.00.176
8
Acetone ++++++++++0.0714 0.0612 0.0571 Ave 8.3
0.0578 0.0582 0.0594 0.0577
15.00.060
4
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 77 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
Iodomethane 0.0980 +++++0.1395 0.1644 0.1710 Lin1 0.9960
0.2468 0.2683 0.2450 0.2602
0.9900-0.15
9
0.255
6
Carbon disulfide 0.6224 +++++0.5579 0.5806 0.5024 Ave 7.3
0.5948 0.5770 0.5084 0.5709
15.00.564
3
Methyl acetate 0.1939 +++++0.1282 0.1409 0.1292 Ave 14.9
0.1343 0.1372 0.1418 0.1356
15.00.142
7
3-Chloro-1-propene 0.3623 +++++0.3023 0.3003 0.2800 Ave 8.4
0.3160 0.3096 0.2842 0.2958
15.00.306
3
Methylene Chloride 0.4302 +++++0.2662 0.2488 0.2241 Lin2 0.9990
0.2226 0.2228 0.2125 0.2175
0.99000.106
0
0.217
9
2-Methyl-2-propanol 0.0285 +++++0.0207 0.0209 0.0205 Ave 11.9
0.0237 0.0222 0.0251 0.0248
15.00.023
3
Acrylonitrile 0.0835 +++++0.0690 0.0743 0.0710 Ave 5.8
0.0748 0.0733 0.0767 0.0733
15.00.074
5
Methyl tert-butyl ether 0.6773 +++++0.6193 0.6484 0.6275 Ave 2.9
0.6400 0.6567 0.6505 0.6302
15.00.643
7
trans-1,2-Dichloroethene 0.2114 +++++0.2183 0.2110 0.1900 Ave 4.9
0.2150 0.2155 0.1949 0.2123
15.00.208
5
Hexane 1.0561 +++++1.1305 1.1271 0.9549 Ave 10.3
1.3127 1.2301 1.0355 1.2086
15.01.131
9
Vinyl acetate 0.5058 +++++0.4012 0.4226 0.4111 Ave 7.3
0.4355 0.4394 0.4426 0.4263
15.00.435
6
1,1-Dichloroethane 0.4218 +++++0.3858 0.3915 0.3668 Ave 4.7
0.4025 0.3988 0.3666 0.3923
0.1000 15.00.390
8
2-Butanone (MEK)0.0994 +++++0.0771 0.0838 0.0835 Ave 7.6
0.0885 0.0868 0.0930 0.0891
15.00.087
7
cis-1,2-Dichloroethene 0.2087 +++++0.2472 0.2508 0.2305 Ave 5.9
0.2458 0.2469 0.2319 0.2424
15.00.238
0
2,2-Dichloropropane 0.3987 +++++0.3712 0.3858 0.3283 Ave 6.6
0.3911 0.3877 0.3432 0.3806
15.00.373
3
sec-Butyl Alcohol ++++++++++0.0142 0.0146 0.0141 Lin1 0.9980
0.0170 0.0158 0.0178 0.0174
0.9900-0.27
4
0.017
2
Chlorobromomethane 0.1226 +++++0.1128 0.1128 0.1148 Ave 5.5
0.1109 0.1104 0.1046 0.1027
15.00.111
5
Tetrahydrofuran 0.0622 +++++0.0584 0.0586 0.0556 Ave 3.7
0.0586 0.0569 0.0614 0.0594
15.00.058
9
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 78 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
Chloroform 0.3773 +++++0.3922 0.4064 0.3790 Ave 3.2
0.4035 0.4091 0.3831 0.3999
30.00.393
8
1,1,1-Trichloroethane 0.3069 +++++0.3596 0.3586 0.3163 Ave 7.2
0.3653 0.3663 0.3242 0.3626
15.00.345
0
Cyclohexane 0.3378 +++++0.3606 0.3500 0.2858 Ave 9.3
0.3756 0.3578 0.3026 0.3642
15.00.341
8
1,1-Dichloropropene 0.2591 +++++0.2975 0.3062 0.2684 Ave 8.6
0.3242 0.3233 0.2828 0.3225
15.00.298
0
Carbon tetrachloride 0.2865 +++++0.3149 0.3114 0.2573 Ave 7.3
0.3061 0.3073 0.2697 0.3071
15.00.295
0
Isobutyl alcohol 0.0090 +++++0.0062 0.0069 0.0057 Ave 14.4
0.0073 0.0067 0.0077 0.0075
15.00.007
1
Benzene 0.9325 +++++0.8892 0.9132 0.8249 Ave 4.2
0.9125 0.9122 0.8421 0.8841
15.00.888
9
1,2-Dichloroethane 0.3686 +++++0.3346 0.3270 0.3184 Ave 5.1
0.3194 0.3272 0.3194 0.3191
15.00.329
2
n-Heptane 0.2788 +++++0.2121 0.2115 0.1882 Ave 12.5
0.2370 0.2299 0.1993 0.2299
15.00.223
3
Trichloroethene 1.0369 +++++0.9446 0.9832 0.9072 Ave 5.3
1.0501 1.0285 0.9362 1.0042
15.00.986
4
2-Pentanone 0.1163 +++++0.1278 0.1284 0.1280 Ave 8.3
0.1430 0.1391 0.1491 0.1447
15.00.134
6
Methylcyclohexane 0.2592 +++++0.2803 0.2652 0.2132 Ave 9.9
0.2877 0.2784 0.2401 0.2874
15.00.263
9
1,2-Dichloropropane 0.2363 +++++0.2039 0.2333 0.2149 Ave 4.7
0.2285 0.2291 0.2207 0.2269
30.00.224
2
1,4-Dioxane 0.0025 +++++0.0030 0.0029 0.0027 Ave 8.1
0.0031 0.0028 0.0032 0.0031
15.00.002
9
Dibromomethane 0.1435 +++++0.1376 0.1417 0.1368 Ave 1.8
0.1367 0.1400 0.1391 0.1377
15.00.139
1
Dichlorobromomethane 0.3179 +++++0.3283 0.3276 0.3049 Ave 2.4
0.3186 0.3229 0.3141 0.3186
15.00.319
1
2-Chloroethyl vinyl ether 0.1697 +++++0.1329 0.1541 0.1380 Ave 8.2
0.1392 0.1385 0.1463 0.1406
15.00.144
9
cis-1,3-Dichloropropene 1.7725 +++++1.6482 1.6664 1.6295 Ave 3.0
1.7290 1.7418 1.6677 1.6661
15.01.690
1
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 79 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
4-Methyl-2-pentanone (MIBK)0.1840 +++++0.1699 0.1798 0.1719 Ave 4.4
0.1870 0.1836 0.1934 0.1872
15.00.182
1
Toluene 0.9694 +++++0.9735 0.9945 0.9159 Ave 3.5
1.0120 1.0075 0.9338 0.9804
30.00.973
4
trans-1,3-Dichloropropene 0.3651 +++++0.3494 0.3564 0.3489 Ave 2.8
0.3678 0.3739 0.3706 0.3729
15.00.363
1
Ethyl methacrylate 1.1673 +++++1.0515 1.2013 1.2084 Ave 6.1
1.2660 1.2600 1.2789 1.2245
15.01.207
2
1,1,2-Trichloroethane 0.1930 +++++0.1907 0.1822 0.1977 Ave 2.9
0.1961 0.1971 0.1989 0.1973
15.00.194
1
Tetrachloroethene 0.6689 +++++0.7490 0.7394 0.6675 Ave 6.5
0.7798 0.7753 0.6801 0.7491
15.00.726
2
1,3-Dichloropropane 1.5828 +++++1.4623 1.5000 1.4775 Ave 2.7
1.5245 1.5410 1.5152 1.4697
15.01.509
1
Methyl n-butyl ketone (MNBK)0.5092 +++++0.5130 0.5468 0.5206 Ave 5.2
0.5739 0.5557 0.5856 0.5536
15.00.544
8
Chlorodibromomethane 1.0899 +++++0.9141 0.9923 0.9529 Ave 5.0
0.9868 0.9931 0.9820 0.9810
15.00.986
5
1,2-Dibromoethane 0.9243 +++++0.8963 0.8992 0.8581 Ave 2.3
0.8931 0.9050 0.8952 0.8684
15.00.892
5
1-Chlorohexane 2.0684 +++++1.5081 1.3748 1.1855 Lin2 0.9960
1.3900 1.3630 1.1980 1.3420
0.99000.311
5
1.290
1
Chlorobenzene 2.9870 +++++2.7435 2.7541 2.5613 Ave 5.3
2.7252 2.7203 2.5422 2.5858
0.3000 15.02.702
4
1,1,1,2-Tetrachloroethane 0.9523 +++++0.9687 0.9661 0.9214 Ave 2.2
0.9525 0.9582 0.9183 0.9216
15.00.944
9
Ethylbenzene 1.4712 +++++1.3958 1.5162 1.3833 Ave 4.5
1.5453 1.5301 1.3933 1.4664
30.01.462
7
m-Xylene & p-Xylene 1.8697 +++++1.8792 1.8781 1.6885 Ave 4.5
1.9300 1.8911 1.7386 1.8060
15.01.835
2
o-Xylene 1.6101 +++++1.8138 1.8661 1.7514 Ave 4.9
1.8596 1.8555 1.7312 1.7715
15.01.782
4
Styrene 2.9147 +++++2.9560 3.0906 2.9707 Ave 3.3
3.1834 3.1548 2.9755 2.9816
15.03.028
4
Bromoform 0.5833 +++++0.5533 0.6212 0.5989 Ave 5.9
0.6433 0.6522 0.6552 0.6386
0.1000 15.00.618
2
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 80 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
Isopropylbenzene 2.6509 +++++2.8337 2.9791 2.5597 Ave 6.4
3.0429 2.9962 2.6615 2.8670
15.02.823
9
Cyclohexanone 0.0400 +++++0.0350 0.0344 0.0360 Ave 7.0
0.0407 0.0356 0.0406 0.0370
15.00.037
4
1,1,2,2-Tetrachloroethane 0.7808 +++++0.6590 0.7065 0.6866 Ave 4.9
0.7215 0.7200 0.7271 0.7038
0.3000 15.00.713
2
Bromobenzene 0.7074 +++++0.6563 0.6944 0.6517 Ave 3.4
0.6993 0.7016 0.6579 0.6726
15.00.680
2
trans-1,4-Dichloro-2-butene 0.2136 +++++0.2194 0.2242 0.2038 Ave 6.4
0.2382 0.2351 0.2433 0.2432
15.00.227
6
1,2,3-Trichloropropane ++++++++++0.2373 0.2131 0.2118 Ave 3.9
0.2253 0.2176 0.2231 0.2198
15.00.221
1
N-Propylbenzene 0.7773 +++++0.8068 0.8341 0.7064 Ave 6.2
0.8417 0.8378 0.7422 0.8053
15.00.793
9
2-Chlorotoluene 0.6208 +++++0.6930 0.7258 0.6311 Ave 5.7
0.7032 0.6996 0.6418 0.6781
15.00.674
2
1,3,5-Trimethylbenzene 2.3472 +++++2.5577 2.5727 2.3301 Ave 5.2
2.6420 2.6431 2.3691 2.4738
15.02.492
0
4-Chlorotoluene 0.7001 +++++0.7227 0.7050 0.6500 Ave 3.8
0.7220 0.7285 0.6730 0.7043
15.00.700
7
tert-Butylbenzene 1.9177 +++++2.0870 2.0883 1.8603 Ave 5.8
2.1709 2.1491 1.9117 2.0383
15.02.027
9
1,2,4-Trimethylbenzene 2.8405 +++++2.5476 2.6957 2.4579 Ave 5.2
2.7475 2.7056 2.4931 2.5393
15.02.628
4
sec-Butylbenzene 0.5677 +++++0.5762 0.5953 0.5282 Ave 5.6
0.6286 0.6123 0.5512 0.5949
15.00.581
8
1,3-Dichlorobenzene 1.2253 +++++1.2479 1.3350 1.2573 Ave 4.2
1.3677 1.3610 1.2648 1.2794
15.01.292
3
4-Isopropyltoluene 2.3019 +++++2.5500 2.5820 2.3176 Ave 6.0
2.6812 2.6701 2.3775 2.4913
15.02.496
4
1,4-Dichlorobenzene 1.4721 +++++1.3802 1.3264 1.2770 Ave 4.8
1.3632 1.3669 1.2931 1.2905
15.01.346
2
n-Butylbenzene 2.0020 +++++2.2571 2.2552 2.0203 Ave 7.1
2.4275 2.3972 2.1355 2.2537
15.02.218
5
1,2-Dichlorobenzene 1.1542 +++++1.1952 1.2793 1.1960 Ave 3.8
1.2627 1.2809 1.2094 1.2025
15.01.222
5
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 81 of 349
FORM VI
Lab Name:Job No.:
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:590907
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VMS_X4
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
0.25(mm)DB-624 (60.25)ID:
ANALYTE RRF
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CURVE
TYPE
COEFFICIENT
B M1 M2
#%RSD #MAX
%RSD R^2
OR COD
#MIN R^2
OR COD
MIN RRF
/RSE /RSE
LVL 6 LVL 7 LVL 8 LVL 9
1,2-Dibromo-3-Chloropropane ++++++++++0.1560 0.1590 0.1521 Ave 3.2
0.1591 0.1553 0.1685 0.1595
15.00.158
5
1,2,4-Trichlorobenzene 0.6070 +++++0.7271 0.7001 0.6741 Ave 5.8
0.7229 0.7269 0.7124 0.6930
15.00.695
4
Hexachlorobutadiene 0.0925 +++++0.2503 0.2808 0.2491 Lin2 0.9960
0.2898 0.2840 0.2585 0.2588
0.9900-0.09
0
0.277
4
Naphthalene 1.6030 +++++2.3078 2.0365 1.8998 Ave 10.1
1.9498 1.9037 2.0321 1.8941
15.01.953
4
1,2,3-Trichlorobenzene 0.5072 +++++0.6606 0.6011 0.5460 Ave 7.6
0.5861 0.5923 0.6008 0.5793
15.00.584
2
Dibromofluoromethane (Surr)0.2361 +++++0.2394 0.2351 0.2364 Ave 1.0
0.2318 0.2361 0.2365 0.2382
15.00.236
2
1,2-Dichloroethane-d4 (Surr)0.2914 +++++0.2882 0.2866 0.2891 Ave 1.7
0.2757 0.2843 0.2894 0.2902
15.00.286
8
Toluene-d8 (Surr)4.2000 +++++4.1785 4.1863 4.1631 Ave 0.9
4.2463 4.2010 4.1757 4.1196
15.04.183
8
4-Bromofluorobenzene (Surr)1.0002 +++++0.9950 1.0097 0.9900 Ave 0.9
1.0150 1.0151 1.0104 1.0079
15.01.005
4
FORM VI 8260C
Note: The M1 coefficient is the same as Ave RRF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 82 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
Level 1 STD005 280-590907/13 X43662.D
Level 2 STD010 280-590907/14 X43664.D
Level 3 STD020 280-590907/15 X43665.D
Level 4 STD050 280-590907/16 X43666.D
Level 5 STD10 280-590907/17 X43667.D
Level 6 ICIS 280-590907/18 X43663.D
Level 7 STD75 280-590907/19 X43668.D
Level 8 STD100 280-590907/20 X43669.D
Level 9 STD200 280-590907/21 X43670.D
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
Dichlorodifluoromethane AveFB 3149 +++++9730 32850 45528 0.500 +++++2.00 5.00 10.0
327543 20010075.050.01297647594262452938
Chloromethane AveFB 3394 +++++11514 29802 49860 0.500 +++++2.00 5.00 10.0
284890 20010075.050.01175589554315414249
Vinyl chloride AveFB 2842 +++++10282 29168 43713 0.500 +++++2.00 5.00 10.0
287446 20010075.050.01159565540222406303
Bromomethane Lin1FB ++++++++++6832 18088 26832 ++++++++++2.00 5.00 10.0
117888 20010075.050.0584699282328205032
Chloroethane AveFB 2349 +++++6457 19293 29927 0.500 +++++2.00 5.00 10.0
185953 20010075.050.0729805353209265407
Dichlorofluoromethane AveFB 5381 +++++18649 49341 84611 0.500 +++++2.00 5.00 10.0
493762 20010075.050.01951675936150701515
Trichlorofluoromethane AveFB 4656 +++++15981 43032 62226 0.500 +++++2.00 5.00 10.0
427834 20010075.050.01756645786296591811
Ethyl ether AveFB 2659 +++++7955 20984 43279 0.500 +++++2.00 5.00 10.0
222614 20010075.050.0902768452555339813
Acrolein AveFB 2198 +++++5439 15425 29387 4.94 +++++19.8 49.4 98.8
155930 1975988741494651706328523226132
Freon 113 AveFB 1646 +++++7484 18991 31461 0.500 +++++2.00 5.00 10.0
210021 20010075.050.0826474342142300583
1,1-Dichloroethene AveFB 2184 +++++8318 24755 41872 0.500 +++++2.00 5.00 10.0
258010 20010075.050.01037153440109375561
Acetone AveFB ++++++++++14614 31437 59892 ++++++++++8.00 20.0 40.0
310891 8004003002001260608635569462126
Iodomethane Lin1FB 1308 +++++7136 21099 44830 0.500 +++++2.00 5.00 10.0
FORM VI 8260C Page 83 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
331608 20010075.050.01420575655306532695
Carbon disulfide AveFB 8309 +++++28550 74527 131702 0.500 +++++2.00 5.00 10.0
799301 20010075.050.0311756313599631145691
Methyl acetate AveFB 5178 +++++13122 36166 67752 1.00 +++++4.00 10.0 20.0
361084 4002001501001480607758549545016
3-Chloro-1-propene AveFB 4836 +++++15470 38548 73390 0.500 +++++2.00 5.00 10.0
424642 20010075.050.01615159760069614634
Methylene Chloride Lin2FB 5743 +++++13623 31943 58739 0.500 +++++2.00 5.00 10.0
299173 20010075.050.01187492568294442431
2-Methyl-2-propanol AveFB 3798 +++++10602 26887 53816 5.00 +++++20.0 50.0 100
317875 200010007505001352529672491440262
Acrylonitrile AveFB 11146 +++++35304 95316 186159 5.00 +++++20.0 50.0 100
1005804 20001000750500400153120511471455944
Methyl tert-butyl ether AveFB 9041 +++++31689 83227 164496 0.500 +++++2.00 5.00 10.0
859988 20010075.050.0344101017399391303806
trans-1,2-Dichloroethene AveFB 2822 +++++11171 27080 49816 0.500 +++++2.00 5.00 10.0
288912 20010075.050.01159149521265427820
Hexane AveCBNZ
d5
3246 +++++13259 33194 57207 0.500 +++++2.00 5.00 10.0
402552 20010075.050.01567173644639564195
Vinyl acetate AveFB 13505 +++++41062 108496 215506 1.00 +++++4.00 10.0 20.0
1170432 400200150100465596123679631744901
1,1-Dichloroethane AveFB 5630 +++++19741 50260 96149 0.500 +++++2.00 5.00 10.0
540826 20010075.050.02142141980517791891
2-Butanone (MEK)AveFB 5309 +++++15783 43020 87553 2.00 +++++8.00 20.0 40.0
475831 8004003002001946964994679689506
cis-1,2-Dichloroethene AveFB 2786 +++++12648 32192 60419 0.500 +++++2.00 5.00 10.0
330270 20010075.050.01323328620209490204
2,2-Dichloropropane AveFB 5322 +++++18997 49526 86054 0.500 +++++2.00 5.00 10.0
525572 20010075.050.02078208918075769749
sec-Butyl Alcohol Lin1FB ++++++++++17446 44874 88946 ++++++++++48.0 120 240
549406 480024001800120022767091144800753236
Chlorobromomethane AveFB 1636 +++++5773 14483 30099 0.500 +++++2.00 5.00 10.0
149033 20010075.050.0560671279742219259
Tetrahydrofuran AveFB 1660 +++++5972 15055 29155 1.00 +++++4.00 10.0 20.0
157544 400200150100648746328280225905
FORM VI 8260C Page 84 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
Chloroform AveFB 5036 +++++20069 52167 99354 0.500 +++++2.00 5.00 10.0
542298 20010075.050.021836271024688812320
1,1,1-Trichloroethane AveFB 4097 +++++18402 46037 82919 0.500 +++++2.00 5.00 10.0
490873 20010075.050.01980185867316727268
Cyclohexane AveFB 4509 +++++18450 44921 74913 0.500 +++++2.00 5.00 10.0
504763 20010075.050.01988845809531710424
1,1-Dichloropropene AveFB 3459 +++++15221 39309 70363 0.500 +++++2.00 5.00 10.0
435703 20010075.050.01760836756390641999
Carbon tetrachloride AveFB 3825 +++++16116 39973 67451 0.500 +++++2.00 5.00 10.0
411383 20010075.050.01676922721291610127
Isobutyl alcohol AveFB 3010 +++++7875 22229 37096 12.5 +++++50.0 125 250
246665 50002500187512501022732512778333099
Benzene AveFB 12448 +++++45503 117220 216244 0.500 +++++2.00 5.00 10.0
1226181 20010075.050.0482769822526101811187
1,2-Dichloroethane AveFB 4921 +++++17120 41976 83451 0.500 +++++2.00 5.00 10.0
429248 20010075.050.01742530854482649751
n-Heptane AveFB 3722 +++++10853 27155 49323 0.500 +++++2.00 5.00 10.0
318545 20010075.050.01255273533048456556
Trichloroethene AveCBNZ
d5
3187 +++++11078 28955 54352 0.500 +++++2.00 5.00 10.0
322028 20010075.050.01302212582827471719
2-Pentanone AveFB 4967 +++++20933 52752 107375 1.60 +++++6.40 16.0 32.0
615014 64032024016025290811275939884082
Methylcyclohexane AveFB 3460 +++++14341 34040 55891 0.500 +++++2.00 5.00 10.0
386649 20010075.050.01569092642275552839
1,2-Dichloropropane AveFB 3154 +++++10434 29944 56325 0.500 +++++2.00 5.00 10.0
307064 20010075.050.01239102590282454879
1,4-Dioxane AveFB 655 +++++3026 7570 14286 10.0 +++++40.0 100 200
82479 4000200015001000334132171240111391
Dibromomethane AveFB 1915 +++++7042 18189 35856 0.500 +++++2.00 5.00 10.0
183723 20010075.050.0751984372034278055
Dichlorobromomethane AveFB 4243 +++++16800 42048 79912 0.500 +++++2.00 5.00 10.0
428110 20010075.050.01739598840200641184
2-Chloroethyl vinyl ether AveFB 2265 +++++6801 19779 36170 0.500 +++++2.00 5.00 10.0
187017 20010075.050.0767775391264274943
FORM VI 8260C Page 85 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
cis-1,3-Dichloropropene AveCBNZ
d5
5448 +++++19330 49076 97623 0.500 +++++2.00 5.00 10.0
530222 20010075.050.021604891038158798866
4-Methyl-2-pentanone (MIBK)AveFB 9823 +++++34771 92320 180211 2.00 +++++8.00 20.0 40.0
1005373 800400300200408877720689601457952
Toluene AveFB 12941 +++++49814 127657 240074 0.500 +++++2.00 5.00 10.0
1359890 20010075.050.0535346324978442000351
trans-1,3-Dichloropropene AveFB 4874 +++++17879 45749 91451 0.500 +++++2.00 5.00 10.0
494203 20010075.050.02036089991365742440
Ethyl methacrylate AveCBNZ
d5
3588 +++++12332 35378 72396 0.500 +++++2.00 5.00 10.0
388233 20010075.050.01587892796156577884
1,1,2-Trichloroethane AveFB 2576 +++++9758 23387 51829 0.500 +++++2.00 5.00 10.0
263570 20010075.050.01077513532097391254
Tetrachloroethene AveCBNZ
d5
2056 +++++8784 21776 39991 0.500 +++++2.00 5.00 10.0
239150 20010075.050.0971403423400355597
1,3-Dichloropropane AveCBNZ
d5
4865 +++++17150 44175 88515 0.500 +++++2.00 5.00 10.0
467509 20010075.050.01905730943238706770
Methyl n-butyl ketone (MNBK)AveCBNZ
d5
6260 +++++24065 64416 124762 2.00 +++++8.00 20.0 40.0
703938 800400300200287146414582781019444
Chlorodibromomethane AveCBNZ
d5
3350 +++++10721 29222 57089 0.500 +++++2.00 5.00 10.0
302604 20010075.050.01272030611330455466
1,2-Dibromoethane AveCBNZ
d5
2841 +++++10512 26482 51411 0.500 +++++2.00 5.00 10.0
273883 20010075.050.01126034557308415075
1-Chlorohexane Lin2CBNZ
d5
5086 +++++14150 32390 56819 0.400 +++++1.60 4.00 8.00
341004 16080.060.040.01392117596610500110
Chlorobenzene AveCBNZ
d5
9181 +++++32176 81107 153450 0.500 +++++2.00 5.00 10.0
835728 20010075.050.0335301415825921247664
FORM VI 8260C Page 86 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
1,1,1,2-Tetrachloroethane AveCBNZ
d5
2927 +++++11361 28450 55202 0.500 +++++2.00 5.00 10.0
292087 20010075.050.01195088571688439494
Ethylbenzene AveCBNZ
d5
4522 +++++16370 44652 82875 0.500 +++++2.00 5.00 10.0
473901 20010075.050.01901563867337701771
m-Xylene & p-Xylene AveCBNZ
d5
5747 +++++22040 55309 101158 0.500 +++++2.00 5.00 10.0
591868 20010075.050.023418961082337867333
o-Xylene AveCBNZ
d5
4949 +++++21272 54957 104926 0.500 +++++2.00 5.00 10.0
570287 20010075.050.022971721077688851036
Styrene AveCBNZ
d5
8959 +++++34668 91017 177979 0.500 +++++2.00 5.00 10.0
976231 20010075.050.0386630518523501446911
Bromoform AveCBNZ
d5
1793 +++++6489 18293 35879 0.500 +++++2.00 5.00 10.0
197264 20010075.050.0828132407884299136
Isopropylbenzene AveDCBd
4
13041 +++++53638 140156 249901 0.500 +++++2.00 5.00 10.0
1468399 20010075.050.0579234626353132158341
Cyclohexanone AveCBNZ
d5
3690 +++++12299 30391 64738 15.0 +++++60.0 150 300
374284 60003000225015001439379759033490116
1,1,2,2-Tetrachloroethane AveDCBd
4
3841 +++++12475 33236 67032 0.500 +++++2.00 5.00 10.0
348183 20010075.050.01421954719990518669
Bromobenzene AveDCBd
4
3480 +++++12423 32667 63624 0.500 +++++2.00 5.00 10.0
337457 20010075.050.01358808651470505442
trans-1,4-Dichloro-2-butene AveDCBd
4
1051 +++++4153 10550 19897 0.500 +++++2.00 5.00 10.0
114970 20010075.050.0491327240926169380
1,2,3-Trichloropropane AveDCBd
4
++++++++++4492 10027 20682 ++++++++++2.00 5.00 10.0
108709 20010075.050.0444060220919156718
FORM VI 8260C Page 87 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
N-Propylbenzene AveDCBd
4
3824 +++++15271 39240 68969 0.500 +++++2.00 5.00 10.0
406180 20010075.050.01626941734913603493
2-Chlorotoluene AveDCBd
4
3054 +++++13118 34148 61614 0.500 +++++2.00 5.00 10.0
339355 20010075.050.01369999635499503980
1,3,5-Trimethylbenzene AveDCBd
4
11547 +++++48415 121037 227481 0.500 +++++2.00 5.00 10.0
1274955 20010075.050.0499783423457931903986
4-Chlorotoluene AveDCBd
4
3444 +++++13680 33166 63456 0.500 +++++2.00 5.00 10.0
348425 20010075.050.01422841666385524758
tert-Butylbenzene AveDCBd
4
9434 +++++39505 98245 181616 0.500 +++++2.00 5.00 10.0
1047600 20010075.050.0411808318928661548127
1,2,4-Trimethylbenzene AveDCBd
4
13974 +++++48223 126824 239957 0.500 +++++2.00 5.00 10.0
1325846 20010075.050.0513024124685611949027
sec-Butylbenzene AveDCBd
4
2793 +++++10907 28008 51569 0.500 +++++2.00 5.00 10.0
303319 20010075.050.01201966545761441109
1,3-Dichlorobenzene AveDCBd
4
6028 +++++23621 62806 122746 0.500 +++++2.00 5.00 10.0
659986 20010075.050.025847821252404980435
4-Isopropyltoluene AveDCBd
4
11324 +++++48269 121472 226266 0.500 +++++2.00 5.00 10.0
1293839 20010075.050.0503331823540881923431
1,4-Dichlorobenzene AveDCBd
4
7242 +++++26125 62404 124667 0.500 +++++2.00 5.00 10.0
657813 20010075.050.026071671280397984663
n-Butylbenzene AveDCBd
4
9849 +++++42724 106096 197241 0.500 +++++2.00 5.00 10.0
1171415 20010075.050.0455316721144561726850
1,2-Dichlorobenzene AveDCBd
4
5678 +++++22623 60188 116760 0.500 +++++2.00 5.00 10.0
609349 20010075.050.024293561197508922697
FORM VI 8260C Page 88 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC/MS VOA BY INTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VMS_X4
Analy Batch No.:590907
72173Calibration Start Date:Calibration End Date:10/22/2022 11:33
N
10/22/2022 14:18
GC Column:DB-624 (60.25)ID:0.25(mm)
RESPONSE AND CONCENTRATION
ANALYTE CURVE
TYPE
IS
REF
RESPONSE
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
CONCENTRATION (UG/L)
LVL 1 LVL 2 LVL 3 LVL 4 LVL 5
LVL 6 LVL 7 LVL 8 LVL 9 LVL 6 LVL 7 LVL 8 LVL 9
1,2-Dibromo-3-Chloropropane AveDCBd
4
++++++++++2953 7480 14848 ++++++++++2.00 5.00 10.0
76799 20010075.050.0322327166807111865
1,2,4-Trichlorobenzene AveDCBd
4
2986 +++++13764 32935 65815 0.500 +++++2.00 5.00 10.0
348869 20010075.050.01400041705352523644
Hexachlorobutadiene Lin2DCBd
4
455 +++++4737 13212 24315 0.500 +++++2.00 5.00 10.0
139840 20010075.050.0522826255985204592
Naphthalene AveDCBd
4
7886 +++++43685 95811 185477 0.500 +++++2.00 5.00 10.0
940916 20010075.050.0382666520121471371384
1,2,3-Trichlorobenzene AveDCBd
4
2495 +++++12504 28280 53303 0.500 +++++2.00 5.00 10.0
282844 20010075.050.01170329594892426649
Dibromofluoromethane (Surr)AveFB 315183 +++++306223 301779 309832 50.0 +++++50.0 50.0 50.0
311439 50.050.050.050.0325227316253312524
1,2-Dichloroethane-d4 (Surr)AveFB 388967 +++++368638 367877 378855 50.0 +++++50.0 50.0 50.0
370500 50.050.050.050.0396116387057376265
Toluene-d8 (Surr)AveCBNZ
d5
1290952 +++++1225166 1232863 1247068 50.0 +++++50.0 50.0 50.0
1302181 50.050.050.050.0133550112997521284512
4-Bromofluorobenzene (Surr)AveDCBd
4
492031 +++++470839 475045 483270 50.0 +++++50.0 50.0 50.0
489792 50.050.050.050.0509067500214487475
Curve Type Legend
Ave = Average ISTD
Lin1 = Linear 1/conc ISTD
Lin2 = Linear 1/conc^2 ISTD
FORM VI 8260C Page 89 of 349
Calibration / Dichlorodifluoromethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2234
Error Coefficients
Standard Error:580000
Relative Standard Error:12.5
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.982
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.11795 50.0 1334887.0 0.2359 Y
2 STD010 280-590907/14 1.0 0.188945 50.0 1278151.0 0.188945 N
3 STD020 280-590907/15 2.0 0.380289 50.0 1279290.0 0.190145 Y
4 STD050 280-590907/16 5.0 1.279575 50.0 1283629.0 0.255915 Y
5 STD10 280-590907/17 10.0 1.736832 50.0 1310662.0 0.173683 Y
6 ICIS 280-590907/18 50.0 12.186975 50.0 1343824.0 0.24374 Y
7 STD75 280-590907/19 75.0 17.109109 50.0 1323675.0 0.228121 Y
8 STD100 280-590907/20 100.0 22.216415 50.0 1337439.0 0.222164 Y
9 STD200 280-590907/21 200.0 47.529793 50.0 1365088.0 0.237649 Y
RelResp = [0.2234]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 90 of 349
Calibration / Chloromethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2181
Error Coefficients
Standard Error:527000
Relative Standard Error:8.8
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.990
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.127127 50.0 1334887.0 0.254254 Y
2 STD010 280-590907/14 1.0 0.249658 50.0 1278151.0 0.249658 N
3 STD020 280-590907/15 2.0 0.450015 50.0 1279290.0 0.225008 Y
4 STD050 280-590907/16 5.0 1.160849 50.0 1283629.0 0.23217 Y
5 STD10 280-590907/17 10.0 1.902092 50.0 1310662.0 0.190209 Y
6 ICIS 280-590907/18 50.0 10.599974 50.0 1343824.0 0.211999 Y
7 STD75 280-590907/19 75.0 15.647685 50.0 1323675.0 0.208636 Y
8 STD100 280-590907/20 100.0 20.723001 50.0 1337439.0 0.20723 Y
9 STD200 280-590907/21 200.0 43.059092 50.0 1365088.0 0.215295 Y
RelResp = [0.2181]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 91 of 349
Calibration / Vinyl chloride
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2051
Error Coefficients
Standard Error:519000
Relative Standard Error:8.6
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.991
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.106451 50.0 1334887.0 0.212902 Y
2 STD010 280-590907/14 1.0 0.228729 50.0 1278151.0 0.228729 N
3 STD020 280-590907/15 2.0 0.401864 50.0 1279290.0 0.200932 Y
4 STD050 280-590907/16 5.0 1.136154 50.0 1283629.0 0.227231 Y
5 STD10 280-590907/17 10.0 1.667592 50.0 1310662.0 0.166759 Y
6 ICIS 280-590907/18 50.0 10.695076 50.0 1343824.0 0.213902 Y
7 STD75 280-590907/19 75.0 15.347536 50.0 1323675.0 0.204634 Y
8 STD100 280-590907/20 100.0 20.196136 50.0 1337439.0 0.201961 Y
9 STD200 280-590907/21 200.0 42.47217 50.0 1365088.0 0.212361 Y
RelResp = [0.2051]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 92 of 349
Calibration / Bromomethane
Curve Type:Linear
Weighting:Conc
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0.06828
Slope:0.1032
Error Coefficients
Standard Error:309000
Relative Standard Error:13.4
Correlation Coefficient:0.997
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.055136 50.0 1334887.0 0.110272 N
2 STD010 280-590907/14 1.0 0.12209 50.0 1278151.0 0.12209 N
3 STD020 280-590907/15 2.0 0.267023 50.0 1279290.0 0.133512 Y
4 STD050 280-590907/16 5.0 0.704565 50.0 1283629.0 0.140913 Y
5 STD10 280-590907/17 10.0 1.023605 50.0 1310662.0 0.10236 Y
6 ICIS 280-590907/18 50.0 4.386289 50.0 1343824.0 0.087726 Y
7 STD75 280-590907/19 75.0 7.744801 50.0 1323675.0 0.103264 Y
8 STD100 280-590907/20 100.0 10.554799 50.0 1337439.0 0.105548 Y
9 STD200 280-590907/21 200.0 21.416165 50.0 1365088.0 0.107081 Y
RelResp = [0.06828] + [0.1032]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Intercept = -0.662
Page 93 of 349
Calibration / Chloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.138
Error Coefficients
Standard Error:330000
Relative Standard Error:13.3
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.977
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.087985 50.0 1334887.0 0.17597 Y
2 STD010 280-590907/14 1.0 0.148261 50.0 1278151.0 0.148261 N
3 STD020 280-590907/15 2.0 0.252367 50.0 1279290.0 0.126183 Y
4 STD050 280-590907/16 5.0 0.751502 50.0 1283629.0 0.1503 Y
5 STD10 280-590907/17 10.0 1.141675 50.0 1310662.0 0.114167 Y
6 ICIS 280-590907/18 50.0 6.9188 50.0 1343824.0 0.138376 Y
7 STD75 280-590907/19 75.0 10.025384 50.0 1323675.0 0.133672 Y
8 STD100 280-590907/20 100.0 13.204677 50.0 1337439.0 0.132047 Y
9 STD200 280-590907/21 200.0 26.731061 50.0 1365088.0 0.133655 Y
RelResp = [0.138]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 94 of 349
Calibration / Dichlorofluoromethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3629
Error Coefficients
Standard Error:881000
Relative Standard Error:6.6
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.201553 50.0 1334887.0 0.403105 Y
2 STD010 280-590907/14 1.0 0.423815 50.0 1278151.0 0.423815 N
3 STD020 280-590907/15 2.0 0.728881 50.0 1279290.0 0.36444 Y
4 STD050 280-590907/16 5.0 1.921934 50.0 1283629.0 0.384387 Y
5 STD10 280-590907/17 10.0 3.227796 50.0 1310662.0 0.32278 Y
6 ICIS 280-590907/18 50.0 18.371528 50.0 1343824.0 0.367431 Y
7 STD75 280-590907/19 75.0 26.498763 50.0 1323675.0 0.353317 Y
8 STD100 280-590907/20 100.0 34.997858 50.0 1337439.0 0.349979 Y
9 STD200 280-590907/21 200.0 71.485318 50.0 1365088.0 0.357427 Y
RelResp = [0.3629]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 95 of 349
Calibration / Trichlorofluoromethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3082
Error Coefficients
Standard Error:779000
Relative Standard Error:11.0
Correlation Coefficient:0.997
Coefficient of Determination (Adjusted):0.986
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.174397 50.0 1334887.0 0.348794 Y
2 STD010 280-590907/14 1.0 0.346712 50.0 1278151.0 0.346712 N
3 STD020 280-590907/15 2.0 0.624604 50.0 1279290.0 0.312302 Y
4 STD050 280-590907/16 5.0 1.676185 50.0 1283629.0 0.335237 Y
5 STD10 280-590907/17 10.0 2.373839 50.0 1310662.0 0.237384 Y
6 ICIS 280-590907/18 50.0 15.918528 50.0 1343824.0 0.318371 Y
7 STD75 280-590907/19 75.0 22.354845 50.0 1323675.0 0.298065 Y
8 STD100 280-590907/20 100.0 29.395584 50.0 1337439.0 0.293956 Y
9 STD200 280-590907/21 200.0 64.341823 50.0 1365088.0 0.321709 Y
RelResp = [0.3082]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 96 of 349
Calibration / Ethyl ether
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1693
Error Coefficients
Standard Error:412000
Relative Standard Error:7.6
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.993
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.099596 50.0 1334887.0 0.199193 Y
2 STD010 280-590907/14 1.0 0.168329 50.0 1278151.0 0.168329 N
3 STD020 280-590907/15 2.0 0.310915 50.0 1279290.0 0.155457 Y
4 STD050 280-590907/16 5.0 0.81737 50.0 1283629.0 0.163474 Y
5 STD10 280-590907/17 10.0 1.651036 50.0 1310662.0 0.165104 Y
6 ICIS 280-590907/18 50.0 8.282855 50.0 1343824.0 0.165657 Y
7 STD75 280-590907/19 75.0 12.835968 50.0 1323675.0 0.171146 Y
8 STD100 280-590907/20 100.0 16.918716 50.0 1337439.0 0.169187 Y
9 STD200 280-590907/21 200.0 33.066293 50.0 1365088.0 0.165331 Y
RelResp = [0.1693]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 97 of 349
Calibration / Acrolein
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.01235
Error Coefficients
Standard Error:295000
Relative Standard Error:14.8
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.971
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 4.9375 0.082329 50.0 1334887.0 0.016674 Y
2 STD010 280-590907/14 9.875 0.119235 50.0 1278151.0 0.012074 N
3 STD020 280-590907/15 19.75 0.212579 50.0 1279290.0 0.010763 Y
4 STD050 280-590907/16 49.375 0.600836 50.0 1283629.0 0.012169 Y
5 STD10 280-590907/17 98.75 1.121075 50.0 1310662.0 0.011353 Y
6 ICIS 280-590907/18 493.75 5.801727 50.0 1343824.0 0.01175 Y
7 STD75 280-590907/19 740.625 8.541825 50.0 1323675.0 0.011533 Y
8 STD100 280-590907/20 987.5 12.281794 50.0 1337439.0 0.012437 Y
9 STD200 280-590907/21 1975.0 23.870476 50.0 1365088.0 0.012086 Y
RelResp = [0.01235]x
Concentration
0 1000 2000
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 98 of 349
Calibration / 1,1,2-Trichloro-1,2,2-trifluoroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1406
Error Coefficients
Standard Error:366000
Relative Standard Error:10.2
Correlation Coefficient:0.993
Coefficient of Determination (Adjusted):0.989
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.061653 50.0 1334887.0 0.123306 Y
2 STD010 280-590907/14 1.0 0.162383 50.0 1278151.0 0.162383 N
3 STD020 280-590907/15 2.0 0.292506 50.0 1279290.0 0.146253 Y
4 STD050 280-590907/16 5.0 0.739739 50.0 1283629.0 0.147948 Y
5 STD10 280-590907/17 10.0 1.200195 50.0 1310662.0 0.12002 Y
6 ICIS 280-590907/18 50.0 7.814305 50.0 1343824.0 0.156286 Y
7 STD75 280-590907/19 75.0 11.354109 50.0 1323675.0 0.151388 Y
8 STD100 280-590907/20 100.0 12.790939 50.0 1337439.0 0.127909 Y
9 STD200 280-590907/21 200.0 30.271821 50.0 1365088.0 0.151359 Y
RelResp = [0.1406]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 99 of 349
Calibration / 1,1-Dichloroethene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1768
Error Coefficients
Standard Error:460000
Relative Standard Error:8.6
Correlation Coefficient:0.995
Coefficient of Determination (Adjusted):0.992
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.081805 50.0 1334887.0 0.163609 Y
2 STD010 280-590907/14 1.0 0.196651 50.0 1278151.0 0.196651 N
3 STD020 280-590907/15 2.0 0.325102 50.0 1279290.0 0.162551 Y
4 STD050 280-590907/16 5.0 0.964258 50.0 1283629.0 0.192852 Y
5 STD10 280-590907/17 10.0 1.597361 50.0 1310662.0 0.159736 Y
6 ICIS 280-590907/18 50.0 9.599843 50.0 1343824.0 0.191997 Y
7 STD75 280-590907/19 75.0 14.1863 50.0 1323675.0 0.189151 Y
8 STD100 280-590907/20 100.0 16.453423 50.0 1337439.0 0.164534 Y
9 STD200 280-590907/21 200.0 37.988503 50.0 1365088.0 0.189943 Y
RelResp = [0.1768]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 100 of 349
Calibration / Acetone
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.06041
Error Coefficients
Standard Error:620000
Relative Standard Error:8.3
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.990
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 2.0 0.336021 50.0 1334887.0 0.16801 N
2 STD010 280-590907/14 4.0 0.371787 50.0 1278151.0 0.092947 N
3 STD020 280-590907/15 8.0 0.571176 50.0 1279290.0 0.071397 Y
4 STD050 280-590907/16 20.0 1.224536 50.0 1283629.0 0.061227 Y
5 STD10 280-590907/17 40.0 2.2848 50.0 1310662.0 0.05712 Y
6 ICIS 280-590907/18 200.0 11.5674 50.0 1343824.0 0.057837 Y
7 STD75 280-590907/19 300.0 17.456173 50.0 1323675.0 0.058187 Y
8 STD100 280-590907/20 400.0 23.760672 50.0 1337439.0 0.059402 Y
9 STD200 280-590907/21 800.0 46.17314 50.0 1365088.0 0.057716 Y
RelResp = [0.06041]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 101 of 349
Calibration / Iodomethane
Curve Type:Linear
Weighting:Conc
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:-0.1587
Slope:0.2556
Error Coefficients
Standard Error:688000
Relative Standard Error:30.1
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.048993 50.0 1334887.0 0.097986 Y
2 STD010 280-590907/14 1.0 0.15808 50.0 1278151.0 0.15808 N
3 STD020 280-590907/15 2.0 0.278905 50.0 1279290.0 0.139452 Y
4 STD050 280-590907/16 5.0 0.82185 50.0 1283629.0 0.16437 Y
5 STD10 280-590907/17 10.0 1.710204 50.0 1310662.0 0.17102 Y
6 ICIS 280-590907/18 50.0 12.338223 50.0 1343824.0 0.246764 Y
7 STD75 280-590907/19 75.0 20.12182 50.0 1323675.0 0.268291 Y
8 STD100 280-590907/20 100.0 24.498538 50.0 1337439.0 0.244985 Y
9 STD200 280-590907/21 200.0 52.03236 50.0 1365088.0 0.260162 Y
RelResp = [-0.1587] + [0.2556]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Intercept = 0.621
Page 102 of 349
Calibration / Carbon disulfide
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.5643
Error Coefficients
Standard Error:1390000
Relative Standard Error:7.3
Correlation Coefficient:0.996
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.311225 50.0 1334887.0 0.62245 Y
2 STD010 280-590907/14 1.0 0.666979 50.0 1278151.0 0.666979 N
3 STD020 280-590907/15 2.0 1.115853 50.0 1279290.0 0.557927 Y
4 STD050 280-590907/16 5.0 2.902981 50.0 1283629.0 0.580596 Y
5 STD10 280-590907/17 10.0 5.024255 50.0 1310662.0 0.502425 Y
6 ICIS 280-590907/18 50.0 29.739795 50.0 1343824.0 0.594796 Y
7 STD75 280-590907/19 75.0 43.2769 50.0 1323675.0 0.577025 Y
8 STD100 280-590907/20 100.0 50.842057 50.0 1337439.0 0.508421 Y
9 STD200 280-590907/21 200.0 114.189085 50.0 1365088.0 0.570945 Y
RelResp = [0.5643]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
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0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 103 of 349
Calibration / Methyl acetate
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1427
Error Coefficients
Standard Error:676000
Relative Standard Error:14.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.971
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 1.0 0.193949 50.0 1334887.0 0.193949 Y
2 STD010 280-590907/14 2.0 0.328561 50.0 1278151.0 0.16428 N
3 STD020 280-590907/15 4.0 0.512863 50.0 1279290.0 0.128216 Y
4 STD050 280-590907/16 10.0 1.40874 50.0 1283629.0 0.140874 Y
5 STD10 280-590907/17 20.0 2.584648 50.0 1310662.0 0.129232 Y
6 ICIS 280-590907/18 100.0 13.434944 50.0 1343824.0 0.134349 Y
7 STD75 280-590907/19 150.0 20.587229 50.0 1323675.0 0.137248 Y
8 STD100 280-590907/20 200.0 28.358265 50.0 1337439.0 0.141791 Y
9 STD200 280-590907/21 400.0 54.231192 50.0 1365088.0 0.135578 Y
RelResp = [0.1427]x
Concentration
0 100 200 300 400
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
5.5
Re
l
a
t
i
v
e

R
e
s
p
o
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s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 104 of 349
Calibration / 3-Chloro-1-propene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3063
Error Coefficients
Standard Error:732000
Relative Standard Error:8.4
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.991
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.181139 50.0 1334887.0 0.362278 Y
2 STD010 280-590907/14 1.0 0.319681 50.0 1278151.0 0.319681 N
3 STD020 280-590907/15 2.0 0.604632 50.0 1279290.0 0.302316 Y
4 STD050 280-590907/16 5.0 1.501524 50.0 1283629.0 0.300305 Y
5 STD10 280-590907/17 10.0 2.79973 50.0 1310662.0 0.279973 Y
6 ICIS 280-590907/18 50.0 15.799762 50.0 1343824.0 0.315995 Y
7 STD75 280-590907/19 75.0 23.216953 50.0 1323675.0 0.309559 Y
8 STD100 280-590907/20 100.0 28.41509 50.0 1337439.0 0.284151 Y
9 STD200 280-590907/21 200.0 59.159519 50.0 1365088.0 0.295798 Y
RelResp = [0.3063]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 105 of 349
Calibration / Methylene Chloride
Curve Type:Linear
Weighting:Conc_Sq
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0.106
Slope:0.2179
Error Coefficients
Standard Error:581000
Relative Standard Error:2.6
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.215112 50.0 1334887.0 0.430224 Y
2 STD010 280-590907/14 1.0 0.352541 50.0 1278151.0 0.352541 N
3 STD020 280-590907/15 2.0 0.532444 50.0 1279290.0 0.266222 Y
4 STD050 280-590907/16 5.0 1.244246 50.0 1283629.0 0.248849 Y
5 STD10 280-590907/17 10.0 2.240814 50.0 1310662.0 0.224081 Y
6 ICIS 280-590907/18 50.0 11.131406 50.0 1343824.0 0.222628 Y
7 STD75 280-590907/19 75.0 16.712222 50.0 1323675.0 0.22283 Y
8 STD100 280-590907/20 100.0 21.245604 50.0 1337439.0 0.212456 Y
9 STD200 280-590907/21 200.0 43.495071 50.0 1365088.0 0.217475 Y
RelResp = [0.106] + [0.2179]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Intercept = -0.487
Page 106 of 349
Calibration / 2-Methyl-2-propanol
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.0233
Error Coefficients
Standard Error:607000
Relative Standard Error:11.9
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.983
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 5.0 0.142259 50.0 1334887.0 0.028452 Y
2 STD010 280-590907/14 10.0 0.28287 50.0 1278151.0 0.028287 N
3 STD020 280-590907/15 20.0 0.41437 50.0 1279290.0 0.020719 Y
4 STD050 280-590907/16 50.0 1.047304 50.0 1283629.0 0.020946 Y
5 STD10 280-590907/17 100.0 2.053008 50.0 1310662.0 0.02053 Y
6 ICIS 280-590907/18 500.0 11.827256 50.0 1343824.0 0.023655 Y
7 STD75 280-590907/19 750.0 16.630291 50.0 1323675.0 0.022174 Y
8 STD100 280-590907/20 1000.0 25.140997 50.0 1337439.0 0.025141 Y
9 STD200 280-590907/21 2000.0 49.539993 50.0 1365088.0 0.02477 Y
RelResp = [0.0233]x
Concentration
0 1000 2000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 107 of 349
Calibration / Acrylonitrile
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.07449
Error Coefficients
Standard Error:1830000
Relative Standard Error:5.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 5.0 0.417489 50.0 1334887.0 0.083498 Y
2 STD010 280-590907/14 10.0 0.834369 50.0 1278151.0 0.083437 N
3 STD020 280-590907/15 20.0 1.379828 50.0 1279290.0 0.068991 Y
4 STD050 280-590907/16 50.0 3.712755 50.0 1283629.0 0.074255 Y
5 STD10 280-590907/17 100.0 7.101717 50.0 1310662.0 0.071017 Y
6 ICIS 280-590907/18 500.0 37.423204 50.0 1343824.0 0.074846 Y
7 STD75 280-590907/19 750.0 54.996279 50.0 1323675.0 0.073328 Y
8 STD100 280-590907/20 1000.0 76.68189 50.0 1337439.0 0.076682 Y
9 STD200 280-590907/21 2000.0 146.566778 50.0 1365088.0 0.073283 Y
RelResp = [0.07449]x
Concentration
0 1000 2000
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 108 of 349
Calibration / Methyl tert-butyl ether
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.6437
Error Coefficients
Standard Error:1570000
Relative Standard Error:2.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.338643 50.0 1334887.0 0.677286 Y
2 STD010 280-590907/14 1.0 0.651331 50.0 1278151.0 0.651331 N
3 STD020 280-590907/15 2.0 1.238539 50.0 1279290.0 0.619269 Y
4 STD050 280-590907/16 5.0 3.241863 50.0 1283629.0 0.648373 Y
5 STD10 280-590907/17 10.0 6.275302 50.0 1310662.0 0.62753 Y
6 ICIS 280-590907/18 50.0 31.997791 50.0 1343824.0 0.639956 Y
7 STD75 280-590907/19 75.0 49.249476 50.0 1323675.0 0.65666 Y
8 STD100 280-590907/20 100.0 65.047415 50.0 1337439.0 0.650474 Y
9 STD200 280-590907/21 200.0 126.036197 50.0 1365088.0 0.630181 Y
RelResp = [0.6437]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 109 of 349
Calibration / trans-1,2-Dichloroethene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2085
Error Coefficients
Standard Error:519000
Relative Standard Error:4.9
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.105702 50.0 1334887.0 0.211404 Y
2 STD010 280-590907/14 1.0 0.24066 50.0 1278151.0 0.24066 N
3 STD020 280-590907/15 2.0 0.436609 50.0 1279290.0 0.218305 Y
4 STD050 280-590907/16 5.0 1.054822 50.0 1283629.0 0.210964 Y
5 STD10 280-590907/17 10.0 1.900414 50.0 1310662.0 0.190041 Y
6 ICIS 280-590907/18 50.0 10.749622 50.0 1343824.0 0.214992 Y
7 STD75 280-590907/19 75.0 16.160311 50.0 1323675.0 0.215471 Y
8 STD100 280-590907/20 100.0 19.487431 50.0 1337439.0 0.194874 Y
9 STD200 280-590907/21 200.0 42.456933 50.0 1365088.0 0.212285 Y
RelResp = [0.2085]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 110 of 349
Calibration / Hexane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.132
Error Coefficients
Standard Error:692000
Relative Standard Error:10.3
Correlation Coefficient:0.992
Coefficient of Determination (Adjusted):0.988
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.52803 50.0 307369.0 1.05606 Y
2 STD010 280-590907/14 1.0 1.254056 50.0 298631.0 1.254056 N
3 STD020 280-590907/15 2.0 2.261054 50.0 293204.0 1.130527 Y
4 STD050 280-590907/16 5.0 5.63573 50.0 294496.0 1.127146 Y
5 STD10 280-590907/17 10.0 9.548728 50.0 299553.0 0.954873 Y
6 ICIS 280-590907/18 50.0 65.633835 50.0 306665.0 1.312677 Y
7 STD75 280-590907/19 75.0 92.260182 50.0 305763.0 1.230136 Y
8 STD100 280-590907/20 100.0 103.552473 50.0 311262.0 1.035525 Y
9 STD200 280-590907/21 200.0 241.7134 50.0 324180.0 1.208567 Y
RelResp = [1.132]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 111 of 349
Calibration / Vinyl acetate
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.4356
Error Coefficients
Standard Error:2130000
Relative Standard Error:7.3
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 1.0 0.505848 50.0 1334887.0 0.505848 Y
2 STD010 280-590907/14 2.0 0.858584 50.0 1278151.0 0.429292 N
3 STD020 280-590907/15 4.0 1.604875 50.0 1279290.0 0.401219 Y
4 STD050 280-590907/16 10.0 4.226143 50.0 1283629.0 0.422614 Y
5 STD10 280-590907/17 20.0 8.221265 50.0 1310662.0 0.411063 Y
6 ICIS 280-590907/18 100.0 43.54856 50.0 1343824.0 0.435486 Y
7 STD75 280-590907/19 150.0 65.911232 50.0 1323675.0 0.439408 Y
8 STD100 280-590907/20 200.0 88.526019 50.0 1337439.0 0.44263 Y
9 STD200 280-590907/21 400.0 170.537028 50.0 1365088.0 0.426343 Y
RelResp = [0.4356]x
Concentration
0 100 200 300 400
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 112 of 349
Calibration / 1,1-Dichloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3908
Error Coefficients
Standard Error:962000
Relative Standard Error:4.7
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.210879 50.0 1334887.0 0.421759 Y
2 STD010 280-590907/14 1.0 0.429761 50.0 1278151.0 0.429761 N
3 STD020 280-590907/15 2.0 0.771561 50.0 1279290.0 0.38578 Y
4 STD050 280-590907/16 5.0 1.957731 50.0 1283629.0 0.391546 Y
5 STD10 280-590907/17 10.0 3.667956 50.0 1310662.0 0.366796 Y
6 ICIS 280-590907/18 50.0 20.12265 50.0 1343824.0 0.402453 Y
7 STD75 280-590907/19 75.0 29.912592 50.0 1323675.0 0.398835 Y
8 STD100 280-590907/20 100.0 36.656513 50.0 1337439.0 0.366565 Y
9 STD200 280-590907/21 200.0 78.461645 50.0 1365088.0 0.392308 Y
RelResp = [0.3908]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 113 of 349
Calibration / 2-Butanone (MEK)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.08766
Error Coefficients
Standard Error:886000
Relative Standard Error:7.6
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.993
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 2.0 0.198856 50.0 1334887.0 0.099428 Y
2 STD010 280-590907/14 4.0 0.334233 50.0 1278151.0 0.083558 N
3 STD020 280-590907/15 8.0 0.616866 50.0 1279290.0 0.077108 Y
4 STD050 280-590907/16 20.0 1.675718 50.0 1283629.0 0.083786 Y
5 STD10 280-590907/17 40.0 3.34003 50.0 1310662.0 0.083501 Y
6 ICIS 280-590907/18 200.0 17.704365 50.0 1343824.0 0.088522 Y
7 STD75 280-590907/19 300.0 26.045139 50.0 1323675.0 0.086817 Y
8 STD100 280-590907/20 400.0 37.185958 50.0 1337439.0 0.092965 Y
9 STD200 280-590907/21 800.0 71.312765 50.0 1365088.0 0.089141 Y
RelResp = [0.08766]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 114 of 349
Calibration / cis-1,2-Dichloroethene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.238
Error Coefficients
Standard Error:596000
Relative Standard Error:5.9
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.104353 50.0 1334887.0 0.208707 Y
2 STD010 280-590907/14 1.0 0.280209 50.0 1278151.0 0.280209 N
3 STD020 280-590907/15 2.0 0.494337 50.0 1279290.0 0.247168 Y
4 STD050 280-590907/16 5.0 1.253945 50.0 1283629.0 0.250789 Y
5 STD10 280-590907/17 10.0 2.304904 50.0 1310662.0 0.23049 Y
6 ICIS 280-590907/18 50.0 12.28844 50.0 1343824.0 0.245769 Y
7 STD75 280-590907/19 75.0 18.516781 50.0 1323675.0 0.24689 Y
8 STD100 280-590907/20 100.0 23.186441 50.0 1337439.0 0.231864 Y
9 STD200 280-590907/21 200.0 48.470428 50.0 1365088.0 0.242352 Y
RelResp = [0.238]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 115 of 349
Calibration / 2,2-Dichloropropane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3733
Error Coefficients
Standard Error:929000
Relative Standard Error:6.6
Correlation Coefficient:0.997
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.199343 50.0 1334887.0 0.398685 Y
2 STD010 280-590907/14 1.0 0.384031 50.0 1278151.0 0.384031 N
3 STD020 280-590907/15 2.0 0.742482 50.0 1279290.0 0.371241 Y
4 STD050 280-590907/16 5.0 1.92914 50.0 1283629.0 0.385828 Y
5 STD10 280-590907/17 10.0 3.282845 50.0 1310662.0 0.328284 Y
6 ICIS 280-590907/18 50.0 19.555091 50.0 1343824.0 0.391102 Y
7 STD75 280-590907/19 75.0 29.076208 50.0 1323675.0 0.387683 Y
8 STD100 280-590907/20 100.0 34.322126 50.0 1337439.0 0.343221 Y
9 STD200 280-590907/21 200.0 76.119928 50.0 1365088.0 0.3806 Y
RelResp = [0.3733]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 116 of 349
Calibration / sec-Butyl Alcohol
Curve Type:Linear
Weighting:Conc
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:-0.274
Slope:0.01723
Error Coefficients
Standard Error:1210000
Relative Standard Error:9.5
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 12.0 0.185709 50.0 1334887.0 0.015476 N
2 STD010 280-590907/14 24.0 0.494347 50.0 1278151.0 0.020598 N
3 STD020 280-590907/15 48.0 0.681863 50.0 1279290.0 0.014205 Y
4 STD050 280-590907/16 120.0 1.747935 50.0 1283629.0 0.014566 Y
5 STD10 280-590907/17 240.0 3.393171 50.0 1310662.0 0.014138 Y
6 ICIS 280-590907/18 1200.0 20.441888 50.0 1343824.0 0.017035 Y
7 STD75 280-590907/19 1800.0 28.452452 50.0 1323675.0 0.015807 Y
8 STD100 280-590907/20 2400.0 42.798214 50.0 1337439.0 0.017833 Y
9 STD200 280-590907/21 4800.0 83.390558 50.0 1365088.0 0.017373 Y
RelResp = [-0.274] + [0.01723]x
Concentration
0 1000 2000 3000 4000 5000
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Intercept = 15.9
Page 117 of 349
Calibration / Chlorobromomethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1115
Error Coefficients
Standard Error:257000
Relative Standard Error:5.5
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.061279 50.0 1334887.0 0.122557 Y
2 STD010 280-590907/14 1.0 0.126941 50.0 1278151.0 0.126941 N
3 STD020 280-590907/15 2.0 0.225633 50.0 1279290.0 0.112816 Y
4 STD050 280-590907/16 5.0 0.564143 50.0 1283629.0 0.112829 Y
5 STD10 280-590907/17 10.0 1.148237 50.0 1310662.0 0.114824 Y
6 ICIS 280-590907/18 50.0 5.545109 50.0 1343824.0 0.110902 Y
7 STD75 280-590907/19 75.0 8.282207 50.0 1323675.0 0.110429 Y
8 STD100 280-590907/20 100.0 10.458122 50.0 1337439.0 0.104581 Y
9 STD200 280-590907/21 200.0 20.536075 50.0 1365088.0 0.10268 Y
RelResp = [0.1115]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 118 of 349
Calibration / Tetrahydrofuran
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.05888
Error Coefficients
Standard Error:294000
Relative Standard Error:3.7
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 1.0 0.062178 50.0 1334887.0 0.062178 Y
2 STD010 280-590907/14 2.0 0.145718 50.0 1278151.0 0.072859 N
3 STD020 280-590907/15 4.0 0.233411 50.0 1279290.0 0.058353 Y
4 STD050 280-590907/16 10.0 0.586423 50.0 1283629.0 0.058642 Y
5 STD10 280-590907/17 20.0 1.112224 50.0 1310662.0 0.055611 Y
6 ICIS 280-590907/18 100.0 5.86178 50.0 1343824.0 0.058618 Y
7 STD75 280-590907/19 150.0 8.53325 50.0 1323675.0 0.056888 Y
8 STD100 280-590907/20 200.0 12.272709 50.0 1337439.0 0.061364 Y
9 STD200 280-590907/21 400.0 23.762058 50.0 1365088.0 0.059405 Y
RelResp = [0.05888]x
Concentration
0 100 200 300 400
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 119 of 349
Calibration / Chloroform
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3938
Error Coefficients
Standard Error:985000
Relative Standard Error:3.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.18863 50.0 1334887.0 0.37726 Y
2 STD010 280-590907/14 1.0 0.441067 50.0 1278151.0 0.441067 N
3 STD020 280-590907/15 2.0 0.78438 50.0 1279290.0 0.39219 Y
4 STD050 280-590907/16 5.0 2.032012 50.0 1283629.0 0.406402 Y
5 STD10 280-590907/17 10.0 3.790222 50.0 1310662.0 0.379022 Y
6 ICIS 280-590907/18 50.0 20.177419 50.0 1343824.0 0.403548 Y
7 STD75 280-590907/19 75.0 30.684269 50.0 1323675.0 0.409124 Y
8 STD100 280-590907/20 100.0 38.307841 50.0 1337439.0 0.383078 Y
9 STD200 280-590907/21 200.0 79.981181 50.0 1365088.0 0.399906 Y
RelResp = [0.3938]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 120 of 349
Calibration / Dibromofluoromethane (Surr)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2362
Error Coefficients
Standard Error:334000
Relative Standard Error:1.0
Correlation Coefficient:0
Coefficient of Determination (Adjusted):0
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 50.0 11.805606 50.0 1334887.0 0.236112 Y
2 STD010 280-590907/14 50.0 11.958877 50.0 1278151.0 0.239178 N
3 STD020 280-590907/15 50.0 11.968475 50.0 1279290.0 0.239369 Y
4 STD050 280-590907/16 50.0 11.754915 50.0 1283629.0 0.235098 Y
5 STD10 280-590907/17 50.0 11.819676 50.0 1310662.0 0.236394 Y
6 ICIS 280-590907/18 50.0 11.58779 50.0 1343824.0 0.231756 Y
7 STD75 280-590907/19 50.0 11.805164 50.0 1323675.0 0.236103 Y
8 STD100 280-590907/20 50.0 11.823081 50.0 1337439.0 0.236462 Y
9 STD200 280-590907/21 50.0 11.912309 50.0 1365088.0 0.238246 Y
RelResp = [0.2362]x
Concentration
0 10 20 30 40 50
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD010 280-590907/14STD020 280-590907/15STD10 280-590907/17STD100 280-590907/20STD200 280-590907/21
Page 121 of 349
Calibration / 1,1,1-Trichloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.345
Error Coefficients
Standard Error:883000
Relative Standard Error:7.2
Correlation Coefficient:0.996
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.153459 50.0 1334887.0 0.306917 Y
2 STD010 280-590907/14 1.0 0.383132 50.0 1278151.0 0.383132 N
3 STD020 280-590907/15 2.0 0.719227 50.0 1279290.0 0.359614 Y
4 STD050 280-590907/16 5.0 1.793236 50.0 1283629.0 0.358647 Y
5 STD10 280-590907/17 10.0 3.163249 50.0 1310662.0 0.316325 Y
6 ICIS 280-590907/18 50.0 18.264036 50.0 1343824.0 0.365281 Y
7 STD75 280-590907/19 75.0 27.471547 50.0 1323675.0 0.366287 Y
8 STD100 280-590907/20 100.0 32.424507 50.0 1337439.0 0.324245 Y
9 STD200 280-590907/21 200.0 72.529573 50.0 1365088.0 0.362648 Y
RelResp = [0.345]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 122 of 349
Calibration / Cyclohexane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3418
Error Coefficients
Standard Error:877000
Relative Standard Error:9.3
Correlation Coefficient:0.992
Coefficient of Determination (Adjusted):0.990
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.168891 50.0 1334887.0 0.337781 Y
2 STD010 280-590907/14 1.0 0.380589 50.0 1278151.0 0.380589 N
3 STD020 280-590907/15 2.0 0.721103 50.0 1279290.0 0.360552 Y
4 STD050 280-590907/16 5.0 1.749766 50.0 1283629.0 0.349953 Y
5 STD10 280-590907/17 10.0 2.857831 50.0 1310662.0 0.285783 Y
6 ICIS 280-590907/18 50.0 18.780845 50.0 1343824.0 0.375617 Y
7 STD75 280-590907/19 75.0 26.835288 50.0 1323675.0 0.357804 Y
8 STD100 280-590907/20 100.0 30.264221 50.0 1337439.0 0.302642 Y
9 STD200 280-590907/21 200.0 72.846769 50.0 1365088.0 0.364234 Y
RelResp = [0.3418]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 123 of 349
Calibration / 1,1-Dichloropropene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.298
Error Coefficients
Standard Error:782000
Relative Standard Error:8.6
Correlation Coefficient:0.995
Coefficient of Determination (Adjusted):0.992
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.129562 50.0 1334887.0 0.259123 Y
2 STD010 280-590907/14 1.0 0.305089 50.0 1278151.0 0.305089 N
3 STD020 280-590907/15 2.0 0.5949 50.0 1279290.0 0.29745 Y
4 STD050 280-590907/16 5.0 1.531167 50.0 1283629.0 0.306233 Y
5 STD10 280-590907/17 10.0 2.684254 50.0 1310662.0 0.268425 Y
6 ICIS 280-590907/18 50.0 16.211312 50.0 1343824.0 0.324226 Y
7 STD75 280-590907/19 75.0 24.250628 50.0 1323675.0 0.323342 Y
8 STD100 280-590907/20 100.0 28.277551 50.0 1337439.0 0.282776 Y
9 STD200 280-590907/21 200.0 64.495329 50.0 1365088.0 0.322477 Y
RelResp = [0.298]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 124 of 349
Calibration / Carbon tetrachloride
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.295
Error Coefficients
Standard Error:744000
Relative Standard Error:7.3
Correlation Coefficient:0.995
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.143271 50.0 1334887.0 0.286541 Y
2 STD010 280-590907/14 1.0 0.322536 50.0 1278151.0 0.322536 N
3 STD020 280-590907/15 2.0 0.629881 50.0 1279290.0 0.31494 Y
4 STD050 280-590907/16 5.0 1.557031 50.0 1283629.0 0.311406 Y
5 STD10 280-590907/17 10.0 2.573165 50.0 1310662.0 0.257317 Y
6 ICIS 280-590907/18 50.0 15.306431 50.0 1343824.0 0.306129 Y
7 STD75 280-590907/19 75.0 23.046707 50.0 1323675.0 0.307289 Y
8 STD100 280-590907/20 100.0 26.965379 50.0 1337439.0 0.269654 Y
9 STD200 280-590907/21 200.0 61.421754 50.0 1365088.0 0.307109 Y
RelResp = [0.295]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 125 of 349
Calibration / Isobutyl alcohol
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.007122
Error Coefficients
Standard Error:460000
Relative Standard Error:14.4
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.974
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 12.5 0.112744 50.0 1334887.0 0.009019 Y
2 STD010 280-590907/14 25.0 0.270625 50.0 1278151.0 0.010825 N
3 STD020 280-590907/15 50.0 0.307788 50.0 1279290.0 0.006156 Y
4 STD050 280-590907/16 125.0 0.865865 50.0 1283629.0 0.006927 Y
5 STD10 280-590907/17 250.0 1.415163 50.0 1310662.0 0.005661 Y
6 ICIS 280-590907/18 1250.0 9.177727 50.0 1343824.0 0.007342 Y
7 STD75 280-590907/19 1875.0 12.582356 50.0 1323675.0 0.006711 Y
8 STD100 280-590907/20 2500.0 19.170145 50.0 1337439.0 0.007668 Y
9 STD200 280-590907/21 5000.0 37.460296 50.0 1365088.0 0.007492 Y
RelResp = [0.007122]x
Concentration
0 1000 2000 3000 4000 5000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 126 of 349
Calibration / 1,2-Dichloroethane-d4 (Surr)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2868
Error Coefficients
Standard Error:406000
Relative Standard Error:1.7
Correlation Coefficient:0
Coefficient of Determination (Adjusted):0.000000000000000111
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 50.0 14.569286 50.0 1334887.0 0.291386 Y
2 STD010 280-590907/14 50.0 14.384412 50.0 1278151.0 0.287688 N
3 STD020 280-590907/15 50.0 14.407914 50.0 1279290.0 0.288158 Y
4 STD050 280-590907/16 50.0 14.329569 50.0 1283629.0 0.286591 Y
5 STD10 280-590907/17 50.0 14.452811 50.0 1310662.0 0.289056 Y
6 ICIS 280-590907/18 50.0 13.785287 50.0 1343824.0 0.275706 Y
7 STD75 280-590907/19 50.0 14.212892 50.0 1323675.0 0.284258 Y
8 STD100 280-590907/20 50.0 14.470081 50.0 1337439.0 0.289402 Y
9 STD200 280-590907/21 50.0 14.508808 50.0 1365088.0 0.290176 Y
RelResp = [0.2868]x
Concentration
0 10 20 30 40 50
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13STD010 280-590907/14STD020 280-590907/15STD10 280-590907/17STD100 280-590907/20STD200 280-590907/21
Page 127 of 349
Calibration / Benzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.8889
Error Coefficients
Standard Error:2180000
Relative Standard Error:4.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.466257 50.0 1334887.0 0.932513 Y
2 STD010 280-590907/14 1.0 0.923013 50.0 1278151.0 0.923013 N
3 STD020 280-590907/15 2.0 1.778447 50.0 1279290.0 0.889224 Y
4 STD050 280-590907/16 5.0 4.565961 50.0 1283629.0 0.913192 Y
5 STD10 280-590907/17 10.0 8.249419 50.0 1310662.0 0.824942 Y
6 ICIS 280-590907/18 50.0 45.622827 50.0 1343824.0 0.912457 Y
7 STD75 280-590907/19 75.0 68.415094 50.0 1323675.0 0.912201 Y
8 STD100 280-590907/20 100.0 84.21356 50.0 1337439.0 0.842136 Y
9 STD200 280-590907/21 200.0 176.827355 50.0 1365088.0 0.884137 Y
RelResp = [0.8889]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 128 of 349
Calibration / 1,2-Dichloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3292
Error Coefficients
Standard Error:791000
Relative Standard Error:5.1
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.184323 50.0 1334887.0 0.368645 Y
2 STD010 280-590907/14 1.0 0.389547 50.0 1278151.0 0.389547 N
3 STD020 280-590907/15 2.0 0.669121 50.0 1279290.0 0.334561 Y
4 STD050 280-590907/16 5.0 1.635052 50.0 1283629.0 0.32701 Y
5 STD10 280-590907/17 10.0 3.183544 50.0 1310662.0 0.318354 Y
6 ICIS 280-590907/18 50.0 15.971139 50.0 1343824.0 0.319423 Y
7 STD75 280-590907/19 75.0 24.543449 50.0 1323675.0 0.327246 Y
8 STD100 280-590907/20 100.0 31.944709 50.0 1337439.0 0.319447 Y
9 STD200 280-590907/21 200.0 63.824823 50.0 1365088.0 0.319124 Y
RelResp = [0.3292]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 129 of 349
Calibration / n-Heptane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2233
Error Coefficients
Standard Error:557000
Relative Standard Error:12.5
Correlation Coefficient:0.995
Coefficient of Determination (Adjusted):0.980
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.139413 50.0 1334887.0 0.278825 Y
2 STD010 280-590907/14 1.0 0.263036 50.0 1278151.0 0.263036 N
3 STD020 280-590907/15 2.0 0.424181 50.0 1279290.0 0.21209 Y
4 STD050 280-590907/16 5.0 1.057743 50.0 1283629.0 0.211549 Y
5 STD10 280-590907/17 10.0 1.881606 50.0 1310662.0 0.188161 Y
6 ICIS 280-590907/18 50.0 11.852185 50.0 1343824.0 0.237044 Y
7 STD75 280-590907/19 75.0 17.245774 50.0 1323675.0 0.229944 Y
8 STD100 280-590907/20 100.0 19.927937 50.0 1337439.0 0.199279 Y
9 STD200 280-590907/21 200.0 45.977732 50.0 1365088.0 0.229889 Y
RelResp = [0.2233]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 130 of 349
Calibration / Trichloroethene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.9864
Error Coefficients
Standard Error:581000
Relative Standard Error:5.3
Correlation Coefficient:0.997
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.518432 50.0 307369.0 1.036864 Y
2 STD010 280-590907/14 1.0 1.115758 50.0 298631.0 1.115758 N
3 STD020 280-590907/15 2.0 1.889128 50.0 293204.0 0.944564 Y
4 STD050 280-590907/16 5.0 4.916026 50.0 294496.0 0.983205 Y
5 STD10 280-590907/17 10.0 9.072184 50.0 299553.0 0.907218 Y
6 ICIS 280-590907/18 50.0 52.504851 50.0 306665.0 1.050097 Y
7 STD75 280-590907/19 75.0 77.138012 50.0 305763.0 1.028507 Y
8 STD100 280-590907/20 100.0 93.623218 50.0 311262.0 0.936232 Y
9 STD200 280-590907/21 200.0 200.84706 50.0 324180.0 1.004235 Y
RelResp = [0.9864]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 131 of 349
Calibration / 2-Pentanone
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1346
Error Coefficients
Standard Error:1150000
Relative Standard Error:8.3
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.993
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 1.6 0.186046 50.0 1334887.0 0.116279 Y
2 STD010 280-590907/14 3.2 0.4449 50.0 1278151.0 0.139031 N
3 STD020 280-590907/15 6.4 0.818149 50.0 1279290.0 0.127836 Y
4 STD050 280-590907/16 16.0 2.054799 50.0 1283629.0 0.128425 Y
5 STD10 280-590907/17 32.0 4.096212 50.0 1310662.0 0.128007 Y
6 ICIS 280-590907/18 160.0 22.882982 50.0 1343824.0 0.143019 Y
7 STD75 280-590907/19 240.0 33.39498 50.0 1323675.0 0.139146 Y
8 STD100 280-590907/20 320.0 47.70083 50.0 1337439.0 0.149065 Y
9 STD200 280-590907/21 640.0 92.634358 50.0 1365088.0 0.144741 Y
RelResp = [0.1346]x
Concentration
0 100 200 300 400 500 600 700
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
8.0
9.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 132 of 349
Calibration / Methylcyclohexane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2639
Error Coefficients
Standard Error:690000
Relative Standard Error:9.9
Correlation Coefficient:0.992
Coefficient of Determination (Adjusted):0.989
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.129599 50.0 1334887.0 0.259198 Y
2 STD010 280-590907/14 1.0 0.312678 50.0 1278151.0 0.312678 N
3 STD020 280-590907/15 2.0 0.560506 50.0 1279290.0 0.280253 Y
4 STD050 280-590907/16 5.0 1.325928 50.0 1283629.0 0.265186 Y
5 STD10 280-590907/17 10.0 2.132167 50.0 1310662.0 0.213217 Y
6 ICIS 280-590907/18 50.0 14.386147 50.0 1343824.0 0.287723 Y
7 STD75 280-590907/19 75.0 20.882732 50.0 1323675.0 0.278436 Y
8 STD100 280-590907/20 100.0 24.011375 50.0 1337439.0 0.240114 Y
9 STD200 280-590907/21 200.0 57.472192 50.0 1365088.0 0.287361 Y
RelResp = [0.2639]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
5.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 133 of 349
Calibration / 1,2-Dichloropropane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2242
Error Coefficients
Standard Error:559000
Relative Standard Error:4.7
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.118137 50.0 1334887.0 0.236275 Y
2 STD010 280-590907/14 1.0 0.250831 50.0 1278151.0 0.250831 N
3 STD020 280-590907/15 2.0 0.407804 50.0 1279290.0 0.203902 Y
4 STD050 280-590907/16 5.0 1.166381 50.0 1283629.0 0.233276 Y
5 STD10 280-590907/17 10.0 2.148723 50.0 1310662.0 0.214872 Y
6 ICIS 280-590907/18 50.0 11.425008 50.0 1343824.0 0.2285 Y
7 STD75 280-590907/19 75.0 17.182428 50.0 1323675.0 0.229099 Y
8 STD100 280-590907/20 100.0 22.067623 50.0 1337439.0 0.220676 Y
9 STD200 280-590907/21 200.0 45.385426 50.0 1365088.0 0.226927 Y
RelResp = [0.2242]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 134 of 349
Calibration / 1,4-Dioxane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.002902
Error Coefficients
Standard Error:151000
Relative Standard Error:8.1
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.993
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 10.0 0.024534 50.0 1334887.0 0.002453 Y
2 STD010 280-590907/14 20.0 0.098736 50.0 1278151.0 0.004937 N
3 STD020 280-590907/15 40.0 0.118269 50.0 1279290.0 0.002957 Y
4 STD050 280-590907/16 100.0 0.294867 50.0 1283629.0 0.002949 Y
5 STD10 280-590907/17 200.0 0.544992 50.0 1310662.0 0.002725 Y
6 ICIS 280-590907/18 1000.0 3.068817 50.0 1343824.0 0.003069 Y
7 STD75 280-590907/19 1500.0 4.207642 50.0 1323675.0 0.002805 Y
8 STD100 280-590907/20 2000.0 6.401787 50.0 1337439.0 0.003201 Y
9 STD200 280-590907/21 4000.0 12.238478 50.0 1365088.0 0.00306 Y
RelResp = [0.002902]x
Concentration
0 1000 2000 3000 4000
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 135 of 349
Calibration / Dibromomethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1391
Error Coefficients
Standard Error:342000
Relative Standard Error:1.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):1.000
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.071729 50.0 1334887.0 0.143458 Y
2 STD010 280-590907/14 1.0 0.16117 50.0 1278151.0 0.16117 N
3 STD020 280-590907/15 2.0 0.275231 50.0 1279290.0 0.137615 Y
4 STD050 280-590907/16 5.0 0.708499 50.0 1283629.0 0.1417 Y
5 STD10 280-590907/17 10.0 1.367858 50.0 1310662.0 0.136786 Y
6 ICIS 280-590907/18 50.0 6.835828 50.0 1343824.0 0.136717 Y
7 STD75 280-590907/19 75.0 10.503145 50.0 1323675.0 0.140042 Y
8 STD100 280-590907/20 100.0 13.908447 50.0 1337439.0 0.139084 Y
9 STD200 280-590907/21 200.0 27.543426 50.0 1365088.0 0.137717 Y
RelResp = [0.1391]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 136 of 349
Calibration / Dichlorobromomethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3191
Error Coefficients
Standard Error:787000
Relative Standard Error:2.4
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.158927 50.0 1334887.0 0.317855 Y
2 STD010 280-590907/14 1.0 0.340727 50.0 1278151.0 0.340727 N
3 STD020 280-590907/15 2.0 0.656614 50.0 1279290.0 0.328307 Y
4 STD050 280-590907/16 5.0 1.637856 50.0 1283629.0 0.327571 Y
5 STD10 280-590907/17 10.0 3.048536 50.0 1310662.0 0.304854 Y
6 ICIS 280-590907/18 50.0 15.928797 50.0 1343824.0 0.318576 Y
7 STD75 280-590907/19 75.0 24.219842 50.0 1323675.0 0.322931 Y
8 STD100 280-590907/20 100.0 31.410778 50.0 1337439.0 0.314108 Y
9 STD200 280-590907/21 200.0 63.717431 50.0 1365088.0 0.318587 Y
RelResp = [0.3191]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 137 of 349
Calibration / 2-Chloroethyl vinyl ether
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1449
Error Coefficients
Standard Error:349000
Relative Standard Error:8.2
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.992
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.084839 50.0 1334887.0 0.169677 Y
2 STD010 280-590907/14 1.0 0.162305 50.0 1278151.0 0.162305 N
3 STD020 280-590907/15 2.0 0.265812 50.0 1279290.0 0.132906 Y
4 STD050 280-590907/16 5.0 0.770433 50.0 1283629.0 0.154087 Y
5 STD10 280-590907/17 10.0 1.379837 50.0 1310662.0 0.137984 Y
6 ICIS 280-590907/18 50.0 6.958389 50.0 1343824.0 0.139168 Y
7 STD75 280-590907/19 75.0 10.385593 50.0 1323675.0 0.138475 Y
8 STD100 280-590907/20 100.0 14.627359 50.0 1337439.0 0.146274 Y
9 STD200 280-590907/21 200.0 28.121813 50.0 1365088.0 0.140609 Y
RelResp = [0.1449]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 138 of 349
Calibration / cis-1,3-Dichloropropene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.69
Error Coefficients
Standard Error:977000
Relative Standard Error:3.0
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.886231 50.0 307369.0 1.772462 Y
2 STD010 280-590907/14 1.0 1.725373 50.0 298631.0 1.725373 N
3 STD020 280-590907/15 2.0 3.29634 50.0 293204.0 1.64817 Y
4 STD050 280-590907/16 5.0 8.332201 50.0 294496.0 1.66644 Y
5 STD10 280-590907/17 10.0 16.294779 50.0 299553.0 1.629478 Y
6 ICIS 280-590907/18 50.0 86.449709 50.0 306665.0 1.728994 Y
7 STD75 280-590907/19 75.0 130.634838 50.0 305763.0 1.741798 Y
8 STD100 280-590907/20 100.0 166.76594 50.0 311262.0 1.667659 Y
9 STD200 280-590907/21 200.0 333.223672 50.0 324180.0 1.666118 Y
RelResp = [1.69]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 139 of 349
Calibration / 4-Methyl-2-pentanone (MIBK)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1821
Error Coefficients
Standard Error:1860000
Relative Standard Error:4.4
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 2.0 0.367934 50.0 1334887.0 0.183967 Y
2 STD010 280-590907/14 4.0 0.834056 50.0 1278151.0 0.208514 N
3 STD020 280-590907/15 8.0 1.358996 50.0 1279290.0 0.169875 Y
4 STD050 280-590907/16 20.0 3.596055 50.0 1283629.0 0.179803 Y
5 STD10 280-590907/17 40.0 6.874808 50.0 1310662.0 0.17187 Y
6 ICIS 280-590907/18 200.0 37.407168 50.0 1343824.0 0.187036 Y
7 STD75 280-590907/19 300.0 55.072129 50.0 1323675.0 0.183574 Y
8 STD100 280-590907/20 400.0 77.347827 50.0 1337439.0 0.19337 Y
9 STD200 280-590907/21 800.0 149.762396 50.0 1365088.0 0.187203 Y
RelResp = [0.1821]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 140 of 349
Calibration / Toluene-d8 (Surr)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:4.184
Error Coefficients
Standard Error:1370000
Relative Standard Error:0.9
Correlation Coefficient:NA
Coefficient of Determination (Adjusted):0
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 50.0 210.000358 50.0 307369.0 4.200007 Y
2 STD010 280-590907/14 50.0 205.988662 50.0 298631.0 4.119773 N
3 STD020 280-590907/15 50.0 208.927232 50.0 293204.0 4.178545 Y
4 STD050 280-590907/16 50.0 209.317444 50.0 294496.0 4.186349 Y
5 STD10 280-590907/17 50.0 208.154817 50.0 299553.0 4.163096 Y
6 ICIS 280-590907/18 50.0 212.313273 50.0 306665.0 4.246265 Y
7 STD75 280-590907/19 50.0 210.050268 50.0 305763.0 4.201005 Y
8 STD100 280-590907/20 50.0 208.787452 50.0 311262.0 4.175749 Y
9 STD200 280-590907/21 50.0 205.981399 50.0 324180.0 4.119628 Y
RelResp = [4.184]x
Concentration
0 10 20 30 40 50
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13STD050 280-590907/16ICIS 280-590907/18STD75 280-590907/19
Page 141 of 349
Calibration / Toluene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.9734
Error Coefficients
Standard Error:2410000
Relative Standard Error:3.5
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.484723 50.0 1334887.0 0.969445 Y
2 STD010 280-590907/14 1.0 1.034033 50.0 1278151.0 1.034033 N
3 STD020 280-590907/15 2.0 1.946939 50.0 1279290.0 0.97347 Y
4 STD050 280-590907/16 5.0 4.972504 50.0 1283629.0 0.994501 Y
5 STD10 280-590907/17 10.0 9.158502 50.0 1310662.0 0.91585 Y
6 ICIS 280-590907/18 50.0 50.597772 50.0 1343824.0 1.011955 Y
7 STD75 280-590907/19 75.0 75.560504 50.0 1323675.0 1.007473 Y
8 STD100 280-590907/20 100.0 93.381605 50.0 1337439.0 0.933816 Y
9 STD200 280-590907/21 200.0 196.084904 50.0 1365088.0 0.980425 Y
RelResp = [0.9734]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 142 of 349
Calibration / trans-1,3-Dichloropropene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.3631
Error Coefficients
Standard Error:921000
Relative Standard Error:2.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.182562 50.0 1334887.0 0.365125 Y
2 STD010 280-590907/14 1.0 0.365645 50.0 1278151.0 0.365645 N
3 STD020 280-590907/15 2.0 0.698786 50.0 1279290.0 0.349393 Y
4 STD050 280-590907/16 5.0 1.782018 50.0 1283629.0 0.356404 Y
5 STD10 280-590907/17 10.0 3.488733 50.0 1310662.0 0.348873 Y
6 ICIS 280-590907/18 50.0 18.387936 50.0 1343824.0 0.367759 Y
7 STD75 280-590907/19 75.0 28.044648 50.0 1323675.0 0.373929 Y
8 STD100 280-590907/20 100.0 37.062064 50.0 1337439.0 0.370621 Y
9 STD200 280-590907/21 200.0 74.577207 50.0 1365088.0 0.372886 Y
RelResp = [0.3631]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 143 of 349
Calibration / Ethyl methacrylate
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.207
Error Coefficients
Standard Error:722000
Relative Standard Error:6.1
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.583663 50.0 307369.0 1.167327 Y
2 STD010 280-590907/14 1.0 1.29876 50.0 298631.0 1.29876 N
3 STD020 280-590907/15 2.0 2.102973 50.0 293204.0 1.051486 Y
4 STD050 280-590907/16 5.0 6.006533 50.0 294496.0 1.201307 Y
5 STD10 280-590907/17 10.0 12.084005 50.0 299553.0 1.208401 Y
6 ICIS 280-590907/18 50.0 63.299203 50.0 306665.0 1.265984 Y
7 STD75 280-590907/19 75.0 94.49868 50.0 305763.0 1.259982 Y
8 STD100 280-590907/20 100.0 127.891615 50.0 311262.0 1.278916 Y
9 STD200 280-590907/21 200.0 244.909001 50.0 324180.0 1.224545 Y
RelResp = [1.207]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 144 of 349
Calibration / 1,1,2-Trichloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1941
Error Coefficients
Standard Error:488000
Relative Standard Error:2.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.096488 50.0 1334887.0 0.192975 Y
2 STD010 280-590907/14 1.0 0.211829 50.0 1278151.0 0.211829 N
3 STD020 280-590907/15 2.0 0.381383 50.0 1279290.0 0.190692 Y
4 STD050 280-590907/16 5.0 0.910972 50.0 1283629.0 0.182194 Y
5 STD10 280-590907/17 10.0 1.977207 50.0 1310662.0 0.197721 Y
6 ICIS 280-590907/18 50.0 9.806716 50.0 1343824.0 0.196134 Y
7 STD75 280-590907/19 75.0 14.779081 50.0 1323675.0 0.197054 Y
8 STD100 280-590907/20 100.0 19.892384 50.0 1337439.0 0.198924 Y
9 STD200 280-590907/21 200.0 39.466796 50.0 1365088.0 0.197334 Y
RelResp = [0.1941]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 145 of 349
Calibration / Tetrachloroethene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.7262
Error Coefficients
Standard Error:432000
Relative Standard Error:6.5
Correlation Coefficient:0.996
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.334451 50.0 307369.0 0.668903 Y
2 STD010 280-590907/14 1.0 0.796468 50.0 298631.0 0.796468 N
3 STD020 280-590907/15 2.0 1.497933 50.0 293204.0 0.748967 Y
4 STD050 280-590907/16 5.0 3.697164 50.0 294496.0 0.739433 Y
5 STD10 280-590907/17 10.0 6.675113 50.0 299553.0 0.667511 Y
6 ICIS 280-590907/18 50.0 38.99206 50.0 306665.0 0.779841 Y
7 STD75 280-590907/19 75.0 58.149122 50.0 305763.0 0.775322 Y
8 STD100 280-590907/20 100.0 68.013442 50.0 311262.0 0.680134 Y
9 STD200 280-590907/21 200.0 149.824634 50.0 324180.0 0.749123 Y
RelResp = [0.7262]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 146 of 349
Calibration / 1,3-Dichloropropane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.509
Error Coefficients
Standard Error:866000
Relative Standard Error:2.7
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.791394 50.0 307369.0 1.582788 Y
2 STD010 280-590907/14 1.0 1.626924 50.0 298631.0 1.626924 N
3 STD020 280-590907/15 2.0 2.924585 50.0 293204.0 1.462292 Y
4 STD050 280-590907/16 5.0 7.500102 50.0 294496.0 1.50002 Y
5 STD10 280-590907/17 10.0 14.774514 50.0 299553.0 1.477451 Y
6 ICIS 280-590907/18 50.0 76.224708 50.0 306665.0 1.524494 Y
7 STD75 280-590907/19 75.0 115.574808 50.0 305763.0 1.540997 Y
8 STD100 280-590907/20 100.0 151.518335 50.0 311262.0 1.515183 Y
9 STD200 280-590907/21 200.0 293.930841 50.0 324180.0 1.469654 Y
RelResp = [1.509]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 147 of 349
Calibration / 2-Hexanone
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.5448
Error Coefficients
Standard Error:1310000
Relative Standard Error:5.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 2.0 1.01832 50.0 307369.0 0.50916 Y
2 STD010 280-590907/14 4.0 2.64708 50.0 298631.0 0.66177 N
3 STD020 280-590907/15 8.0 4.103798 50.0 293204.0 0.512975 Y
4 STD050 280-590907/16 20.0 10.936651 50.0 294496.0 0.546833 Y
5 STD10 280-590907/17 40.0 20.824695 50.0 299553.0 0.520617 Y
6 ICIS 280-590907/18 200.0 114.773124 50.0 306665.0 0.573866 Y
7 STD75 280-590907/19 300.0 166.704932 50.0 305763.0 0.555683 Y
8 STD100 280-590907/20 400.0 234.252495 50.0 311262.0 0.585631 Y
9 STD200 280-590907/21 800.0 442.881115 50.0 324180.0 0.553601 Y
RelResp = [0.5448]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 148 of 349
Calibration / Chlorodibromomethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.9865
Error Coefficients
Standard Error:573000
Relative Standard Error:5.0
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.544948 50.0 307369.0 1.089895 Y
2 STD010 280-590907/14 1.0 1.0446 50.0 298631.0 1.0446 N
3 STD020 280-590907/15 2.0 1.828249 50.0 293204.0 0.914125 Y
4 STD050 280-590907/16 5.0 4.961358 50.0 294496.0 0.992272 Y
5 STD10 280-590907/17 10.0 9.529032 50.0 299553.0 0.952903 Y
6 ICIS 280-590907/18 50.0 49.337877 50.0 306665.0 0.986758 Y
7 STD75 280-590907/19 75.0 74.480235 50.0 305763.0 0.99307 Y
8 STD100 280-590907/20 100.0 98.201836 50.0 311262.0 0.982018 Y
9 STD200 280-590907/21 200.0 196.19193 50.0 324180.0 0.98096 Y
RelResp = [0.9865]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 149 of 349
Calibration / Ethylene Dibromide
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.8925
Error Coefficients
Standard Error:511000
Relative Standard Error:2.3
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.462148 50.0 307369.0 0.924296 Y
2 STD010 280-590907/14 1.0 0.967749 50.0 298631.0 0.967749 N
3 STD020 280-590907/15 2.0 1.792609 50.0 293204.0 0.896304 Y
4 STD050 280-590907/16 5.0 4.496156 50.0 294496.0 0.899231 Y
5 STD10 280-590907/17 10.0 8.581286 50.0 299553.0 0.858129 Y
6 ICIS 280-590907/18 50.0 44.65508 50.0 306665.0 0.893102 Y
7 STD75 280-590907/19 75.0 67.875282 50.0 305763.0 0.905004 Y
8 STD100 280-590907/20 100.0 89.523938 50.0 311262.0 0.895239 Y
9 STD200 280-590907/21 200.0 173.674193 50.0 324180.0 0.868371 Y
RelResp = [0.8925]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 150 of 349
Calibration / 1-Chlorohexane
Curve Type:Linear
Weighting:Conc_Sq
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0.3115
Slope:1.29
Error Coefficients
Standard Error:666000
Relative Standard Error:6.8
Correlation Coefficient:0.995
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.4 0.827344 50.0 307369.0 2.068361 Y
2 STD010 280-590907/14 0.8 1.549906 50.0 298631.0 1.937383 N
3 STD020 280-590907/15 1.6 2.412996 50.0 293204.0 1.508122 Y
4 STD050 280-590907/16 4.0 5.499226 50.0 294496.0 1.374806 Y
5 STD10 280-590907/17 8.0 9.483964 50.0 299553.0 1.185496 Y
6 ICIS 280-590907/18 40.0 55.59878 50.0 306665.0 1.38997 Y
7 STD75 280-590907/19 60.0 81.78066 50.0 305763.0 1.363011 Y
8 STD100 280-590907/20 80.0 95.837269 50.0 311262.0 1.197966 Y
9 STD200 280-590907/21 160.0 214.713585 50.0 324180.0 1.34196 Y
RelResp = [0.3115] + [1.29]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Intercept = -0.241
Page 151 of 349
Calibration / Chlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.702
Error Coefficients
Standard Error:1510000
Relative Standard Error:5.3
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.493482 50.0 307369.0 2.986964 Y
2 STD010 280-590907/14 1.0 2.904253 50.0 298631.0 2.904253 N
3 STD020 280-590907/15 2.0 5.486965 50.0 293204.0 2.743482 Y
4 STD050 280-590907/16 5.0 13.770476 50.0 294496.0 2.754095 Y
5 STD10 280-590907/17 10.0 25.613164 50.0 299553.0 2.561316 Y
6 ICIS 280-590907/18 50.0 136.260741 50.0 306665.0 2.725215 Y
7 STD75 280-590907/19 75.0 204.024686 50.0 305763.0 2.720329 Y
8 STD100 280-590907/20 100.0 254.221845 50.0 311262.0 2.542218 Y
9 STD200 280-590907/21 200.0 517.153125 50.0 324180.0 2.585766 Y
RelResp = [2.702]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 152 of 349
Calibration / 1,1,1,2-Tetrachloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.9449
Error Coefficients
Standard Error:539000
Relative Standard Error:2.2
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.476138 50.0 307369.0 0.952276 Y
2 STD010 280-590907/14 1.0 1.020992 50.0 298631.0 1.020992 N
3 STD020 280-590907/15 2.0 1.937388 50.0 293204.0 0.968694 Y
4 STD050 280-590907/16 5.0 4.830286 50.0 294496.0 0.966057 Y
5 STD10 280-590907/17 10.0 9.214062 50.0 299553.0 0.921406 Y
6 ICIS 280-590907/18 50.0 47.623139 50.0 306665.0 0.952463 Y
7 STD75 280-590907/19 75.0 71.868408 50.0 305763.0 0.958245 Y
8 STD100 280-590907/20 100.0 91.833889 50.0 311262.0 0.918339 Y
9 STD200 280-590907/21 200.0 184.324758 50.0 324180.0 0.921624 Y
RelResp = [0.9449]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 153 of 349
Calibration / Ethylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.463
Error Coefficients
Standard Error:853000
Relative Standard Error:4.5
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.735598 50.0 307369.0 1.471196 Y
2 STD010 280-590907/14 1.0 1.664261 50.0 298631.0 1.664261 N
3 STD020 280-590907/15 2.0 2.791572 50.0 293204.0 1.395786 Y
4 STD050 280-590907/16 5.0 7.581088 50.0 294496.0 1.516218 Y
5 STD10 280-590907/17 10.0 13.833111 50.0 299553.0 1.383311 Y
6 ICIS 280-590907/18 50.0 77.266887 50.0 306665.0 1.545338 Y
7 STD75 280-590907/19 75.0 114.757345 50.0 305763.0 1.530098 Y
8 STD100 280-590907/20 100.0 139.325873 50.0 311262.0 1.393259 Y
9 STD200 280-590907/21 200.0 293.288142 50.0 324180.0 1.466441 Y
RelResp = [1.463]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 154 of 349
Calibration / m-Xylene & p-Xylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.835
Error Coefficients
Standard Error:1050000
Relative Standard Error:4.5
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.93487 50.0 307369.0 1.86974 Y
2 STD010 280-590907/14 1.0 2.108957 50.0 298631.0 2.108957 N
3 STD020 280-590907/15 2.0 3.758475 50.0 293204.0 1.879238 Y
4 STD050 280-590907/16 5.0 9.39045 50.0 294496.0 1.87809 Y
5 STD10 280-590907/17 10.0 16.884825 50.0 299553.0 1.688483 Y
6 ICIS 280-590907/18 50.0 96.500742 50.0 306665.0 1.930015 Y
7 STD75 280-590907/19 75.0 141.830928 50.0 305763.0 1.891079 Y
8 STD100 280-590907/20 100.0 173.862694 50.0 311262.0 1.738627 Y
9 STD200 280-590907/21 200.0 361.203035 50.0 324180.0 1.806015 Y
RelResp = [1.835]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 155 of 349
Calibration / o-Xylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.782
Error Coefficients
Standard Error:1040000
Relative Standard Error:4.9
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.805058 50.0 307369.0 1.610117 Y
2 STD010 280-590907/14 1.0 1.969822 50.0 298631.0 1.969822 N
3 STD020 280-590907/15 2.0 3.627508 50.0 293204.0 1.813754 Y
4 STD050 280-590907/16 5.0 9.330687 50.0 294496.0 1.866137 Y
5 STD10 280-590907/17 10.0 17.513762 50.0 299553.0 1.751376 Y
6 ICIS 280-590907/18 50.0 92.982081 50.0 306665.0 1.859642 Y
7 STD75 280-590907/19 75.0 139.165955 50.0 305763.0 1.855546 Y
8 STD100 280-590907/20 100.0 173.115896 50.0 311262.0 1.731159 Y
9 STD200 280-590907/21 200.0 354.305016 50.0 324180.0 1.771525 Y
RelResp = [1.782]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 156 of 349
Calibration / Styrene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.028
Error Coefficients
Standard Error:1750000
Relative Standard Error:3.3
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.457369 50.0 307369.0 2.914738 Y
2 STD010 280-590907/14 1.0 3.262722 50.0 298631.0 3.262722 N
3 STD020 280-590907/15 2.0 5.911925 50.0 293204.0 2.955962 Y
4 STD050 280-590907/16 5.0 15.453011 50.0 294496.0 3.090602 Y
5 STD10 280-590907/17 10.0 29.707431 50.0 299553.0 2.970743 Y
6 ICIS 280-590907/18 50.0 159.168963 50.0 306665.0 3.183379 Y
7 STD75 280-590907/19 75.0 236.60662 50.0 305763.0 3.154755 Y
8 STD100 280-590907/20 100.0 297.554793 50.0 311262.0 2.975548 Y
9 STD200 280-590907/21 200.0 596.320717 50.0 324180.0 2.981604 Y
RelResp = [3.028]x
Concentration
0 100 200
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 157 of 349
Calibration / Bromoform
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.6182
Error Coefficients
Standard Error:375000
Relative Standard Error:5.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.291669 50.0 307369.0 0.583338 Y
2 STD010 280-590907/14 1.0 0.707227 50.0 298631.0 0.707227 N
3 STD020 280-590907/15 2.0 1.106567 50.0 293204.0 0.553284 Y
4 STD050 280-590907/16 5.0 3.105815 50.0 294496.0 0.621163 Y
5 STD10 280-590907/17 10.0 5.988757 50.0 299553.0 0.598876 Y
6 ICIS 280-590907/18 50.0 32.162783 50.0 306665.0 0.643256 Y
7 STD75 280-590907/19 75.0 48.916318 50.0 305763.0 0.652218 Y
8 STD100 280-590907/20 100.0 65.521008 50.0 311262.0 0.65521 Y
9 STD200 280-590907/21 200.0 127.727189 50.0 324180.0 0.638636 Y
RelResp = [0.6182]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 158 of 349
Calibration / Isopropylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.824
Error Coefficients
Standard Error:2600000
Relative Standard Error:6.4
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.325437 50.0 491951.0 2.650874 Y
2 STD010 280-590907/14 1.0 3.152124 50.0 472824.0 3.152124 N
3 STD020 280-590907/15 2.0 5.667307 50.0 473223.0 2.833653 Y
4 STD050 280-590907/16 5.0 14.895634 50.0 470460.0 2.979127 Y
5 STD10 280-590907/17 10.0 25.597372 50.0 488138.0 2.559737 Y
6 ICIS 280-590907/18 50.0 152.145203 50.0 482565.0 3.042904 Y
7 STD75 280-590907/19 75.0 224.71249 50.0 480245.0 2.996167 Y
8 STD100 280-590907/20 100.0 266.149681 50.0 495081.0 2.661497 Y
9 STD200 280-590907/21 200.0 573.404226 50.0 505084.0 2.867021 Y
RelResp = [2.824]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
5.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 159 of 349
Calibration / Cyclohexanone
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.03742
Error Coefficients
Standard Error:658000
Relative Standard Error:7.0
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 15.0 0.600256 50.0 307369.0 0.040017 Y
2 STD010 280-590907/14 30.0 2.015531 50.0 298631.0 0.067184 N
3 STD020 280-590907/15 60.0 2.097345 50.0 293204.0 0.034956 Y
4 STD050 280-590907/16 150.0 5.159832 50.0 294496.0 0.034399 Y
5 STD10 280-590907/17 300.0 10.805767 50.0 299553.0 0.036019 Y
6 ICIS 280-590907/18 1500.0 61.024897 50.0 306665.0 0.040683 Y
7 STD75 280-590907/19 2250.0 80.146388 50.0 305763.0 0.035621 Y
8 STD100 280-590907/20 3000.0 121.928311 50.0 311262.0 0.040643 Y
9 STD200 280-590907/21 6000.0 222.003054 50.0 324180.0 0.037001 Y
RelResp = [0.03742]x
Concentration
0 1000 2000 3000 4000 5000 6000
0.0
0.5
1.0
1.5
2.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 160 of 349
Calibration / 4-Bromofluorobenzene (Surr)
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.005
Error Coefficients
Standard Error:522000
Relative Standard Error:0.9
Correlation Coefficient:0
Coefficient of Determination (Adjusted):0
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 50.0 50.008131 50.0 491951.0 1.000163 Y
2 STD010 280-590907/14 50.0 49.634431 50.0 472824.0 0.992689 N
3 STD020 280-590907/15 50.0 49.74811 50.0 473223.0 0.994962 Y
4 STD050 280-590907/16 50.0 50.487289 50.0 470460.0 1.009746 Y
5 STD10 280-590907/17 50.0 49.501371 50.0 488138.0 0.990027 Y
6 ICIS 280-590907/18 50.0 50.748811 50.0 482565.0 1.014976 Y
7 STD75 280-590907/19 50.0 50.752741 50.0 480245.0 1.015055 Y
8 STD100 280-590907/20 50.0 50.5184 50.0 495081.0 1.010368 Y
9 STD200 280-590907/21 50.0 50.394291 50.0 505084.0 1.007886 Y
RelResp = [1.005]x
Concentration
0 10 20 30 40 50
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD050 280-590907/16ICIS 280-590907/18STD75 280-590907/19STD100 280-590907/20STD200 280-590907/21
Page 161 of 349
Calibration / 1,1,2,2-Tetrachloroethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.7132
Error Coefficients
Standard Error:648000
Relative Standard Error:4.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.390384 50.0 491951.0 0.780769 Y
2 STD010 280-590907/14 1.0 0.868082 50.0 472824.0 0.868082 N
3 STD020 280-590907/15 2.0 1.318089 50.0 473223.0 0.659044 Y
4 STD050 280-590907/16 5.0 3.532288 50.0 470460.0 0.706458 Y
5 STD10 280-590907/17 10.0 6.866091 50.0 488138.0 0.686609 Y
6 ICIS 280-590907/18 50.0 36.07628 50.0 482565.0 0.721526 Y
7 STD75 280-590907/19 75.0 54.000458 50.0 480245.0 0.720006 Y
8 STD100 280-590907/20 100.0 72.714364 50.0 495081.0 0.727144 Y
9 STD200 280-590907/21 200.0 140.764111 50.0 505084.0 0.703821 Y
RelResp = [0.7132]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 162 of 349
Calibration / Bromobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.6802
Error Coefficients
Standard Error:615000
Relative Standard Error:3.4
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.353694 50.0 491951.0 0.707388 Y
2 STD010 280-590907/14 1.0 0.815737 50.0 472824.0 0.815737 N
3 STD020 280-590907/15 2.0 1.312595 50.0 473223.0 0.656297 Y
4 STD050 280-590907/16 5.0 3.471815 50.0 470460.0 0.694363 Y
5 STD10 280-590907/17 10.0 6.51701 50.0 488138.0 0.651701 Y
6 ICIS 280-590907/18 50.0 34.964927 50.0 482565.0 0.699299 Y
7 STD75 280-590907/19 75.0 52.623348 50.0 480245.0 0.701645 Y
8 STD100 280-590907/20 100.0 65.794284 50.0 495081.0 0.657943 Y
9 STD200 280-590907/21 200.0 134.513071 50.0 505084.0 0.672565 Y
RelResp = [0.6802]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
1.4
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 163 of 349
Calibration / trans-1,4-Dichloro-2-butene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2276
Error Coefficients
Standard Error:221000
Relative Standard Error:6.4
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.10682 50.0 491951.0 0.213639 Y
2 STD010 280-590907/14 1.0 0.327818 50.0 472824.0 0.327818 N
3 STD020 280-590907/15 2.0 0.438799 50.0 473223.0 0.2194 Y
4 STD050 280-590907/16 5.0 1.121243 50.0 470460.0 0.224249 Y
5 STD10 280-590907/17 10.0 2.038051 50.0 488138.0 0.203805 Y
6 ICIS 280-590907/18 50.0 11.912385 50.0 482565.0 0.238248 Y
7 STD75 280-590907/19 75.0 17.634749 50.0 480245.0 0.23513 Y
8 STD100 280-590907/20 100.0 24.331978 50.0 495081.0 0.24332 Y
9 STD200 280-590907/21 200.0 48.638147 50.0 505084.0 0.243191 Y
RelResp = [0.2276]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 164 of 349
Calibration / 1,2,3-Trichloropropane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.2211
Error Coefficients
Standard Error:217000
Relative Standard Error:3.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.156926 50.0 491951.0 0.313852 N
2 STD010 280-590907/14 1.0 0.291969 50.0 472824.0 0.291969 N
3 STD020 280-590907/15 2.0 0.474618 50.0 473223.0 0.237309 Y
4 STD050 280-590907/16 5.0 1.065659 50.0 470460.0 0.213132 Y
5 STD10 280-590907/17 10.0 2.118458 50.0 488138.0 0.211846 Y
6 ICIS 280-590907/18 50.0 11.263664 50.0 482565.0 0.225273 Y
7 STD75 280-590907/19 75.0 16.316463 50.0 480245.0 0.217553 Y
8 STD100 280-590907/20 100.0 22.3114 50.0 495081.0 0.223114 Y
9 STD200 280-590907/21 200.0 43.959025 50.0 505084.0 0.219795 Y
RelResp = [0.2211]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 165 of 349
Calibration / N-Propylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.7939
Error Coefficients
Standard Error:729000
Relative Standard Error:6.2
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.388657 50.0 491951.0 0.777313 Y
2 STD010 280-590907/14 1.0 0.953103 50.0 472824.0 0.953103 N
3 STD020 280-590907/15 2.0 1.61351 50.0 473223.0 0.806755 Y
4 STD050 280-590907/16 5.0 4.170386 50.0 470460.0 0.834077 Y
5 STD10 280-590907/17 10.0 7.064498 50.0 488138.0 0.70645 Y
6 ICIS 280-590907/18 50.0 42.085522 50.0 482565.0 0.84171 Y
7 STD75 280-590907/19 75.0 62.831784 50.0 480245.0 0.837757 Y
8 STD100 280-590907/20 100.0 74.221491 50.0 495081.0 0.742215 Y
9 STD200 280-590907/21 200.0 161.056478 50.0 505084.0 0.805282 Y
RelResp = [0.7939]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 166 of 349
Calibration / 2-Chlorotoluene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.6742
Error Coefficients
Standard Error:616000
Relative Standard Error:5.7
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.310397 50.0 491951.0 0.620794 Y
2 STD010 280-590907/14 1.0 0.861737 50.0 472824.0 0.861737 N
3 STD020 280-590907/15 2.0 1.386027 50.0 473223.0 0.693014 Y
4 STD050 280-590907/16 5.0 3.629214 50.0 470460.0 0.725843 Y
5 STD10 280-590907/17 10.0 6.311125 50.0 488138.0 0.631113 Y
6 ICIS 280-590907/18 50.0 35.161584 50.0 482565.0 0.703232 Y
7 STD75 280-590907/19 75.0 52.471135 50.0 480245.0 0.699615 Y
8 STD100 280-590907/20 100.0 64.181316 50.0 495081.0 0.641813 Y
9 STD200 280-590907/21 200.0 135.620907 50.0 505084.0 0.678105 Y
RelResp = [0.6742]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
1.4
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 167 of 349
Calibration / 1,3,5-Trimethylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.492
Error Coefficients
Standard Error:2260000
Relative Standard Error:5.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.173592 50.0 491951.0 2.347185 Y
2 STD010 280-590907/14 1.0 2.899388 50.0 472824.0 2.899388 N
3 STD020 280-590907/15 2.0 5.115453 50.0 473223.0 2.557726 Y
4 STD050 280-590907/16 5.0 12.863687 50.0 470460.0 2.572737 Y
5 STD10 280-590907/17 10.0 23.30089 50.0 488138.0 2.330089 Y
6 ICIS 280-590907/18 50.0 132.101893 50.0 482565.0 2.642038 Y
7 STD75 280-590907/19 75.0 198.230695 50.0 480245.0 2.643076 Y
8 STD100 280-590907/20 100.0 236.910021 50.0 495081.0 2.3691 Y
9 STD200 280-590907/21 200.0 494.752754 50.0 505084.0 2.473764 Y
RelResp = [2.492]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 168 of 349
Calibration / 4-Chlorotoluene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.7007
Error Coefficients
Standard Error:640000
Relative Standard Error:3.8
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.350035 50.0 491951.0 0.70007 Y
2 STD010 280-590907/14 1.0 0.795328 50.0 472824.0 0.795328 N
3 STD020 280-590907/15 2.0 1.445407 50.0 473223.0 0.722704 Y
4 STD050 280-590907/16 5.0 3.524848 50.0 470460.0 0.70497 Y
5 STD10 280-590907/17 10.0 6.499801 50.0 488138.0 0.64998 Y
6 ICIS 280-590907/18 50.0 36.101354 50.0 482565.0 0.722027 Y
7 STD75 280-590907/19 75.0 54.634405 50.0 480245.0 0.728459 Y
8 STD100 280-590907/20 100.0 67.300603 50.0 495081.0 0.673006 Y
9 STD200 280-590907/21 200.0 140.851918 50.0 505084.0 0.70426 Y
RelResp = [0.7007]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 169 of 349
Calibration / tert-Butylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.028
Error Coefficients
Standard Error:1850000
Relative Standard Error:5.8
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.958835 50.0 491951.0 1.917671 Y
2 STD010 280-590907/14 1.0 2.342098 50.0 472824.0 2.342098 N
3 STD020 280-590907/15 2.0 4.174036 50.0 473223.0 2.087018 Y
4 STD050 280-590907/16 5.0 10.441377 50.0 470460.0 2.088275 Y
5 STD10 280-590907/17 10.0 18.602936 50.0 488138.0 1.860294 Y
6 ICIS 280-590907/18 50.0 108.544963 50.0 482565.0 2.170899 Y
7 STD75 280-590907/19 75.0 161.18096 50.0 480245.0 2.149079 Y
8 STD100 280-590907/20 100.0 191.167304 50.0 495081.0 1.911673 Y
9 STD200 280-590907/21 200.0 407.663181 50.0 505084.0 2.038316 Y
RelResp = [2.028]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 170 of 349
Calibration / 1,2,4-Trimethylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.628
Error Coefficients
Standard Error:2330000
Relative Standard Error:5.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.420263 50.0 491951.0 2.840527 Y
2 STD010 280-590907/14 1.0 2.950569 50.0 472824.0 2.950569 N
3 STD020 280-590907/15 2.0 5.095167 50.0 473223.0 2.547583 Y
4 STD050 280-590907/16 5.0 13.478723 50.0 470460.0 2.695745 Y
5 STD10 280-590907/17 10.0 24.578808 50.0 488138.0 2.457881 Y
6 ICIS 280-590907/18 50.0 137.374861 50.0 482565.0 2.747497 Y
7 STD75 280-590907/19 75.0 202.920072 50.0 480245.0 2.705601 Y
8 STD100 280-590907/20 100.0 249.3088 50.0 495081.0 2.493088 Y
9 STD200 280-590907/21 200.0 507.860178 50.0 505084.0 2.539301 Y
RelResp = [2.628]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 171 of 349
Calibration / sec-Butylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.5818
Error Coefficients
Standard Error:539000
Relative Standard Error:5.6
Correlation Coefficient:0.998
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.28387 50.0 491951.0 0.567739 Y
2 STD010 280-590907/14 1.0 0.760431 50.0 472824.0 0.760431 N
3 STD020 280-590907/15 2.0 1.152417 50.0 473223.0 0.576208 Y
4 STD050 280-590907/16 5.0 2.976661 50.0 470460.0 0.595332 Y
5 STD10 280-590907/17 10.0 5.282215 50.0 488138.0 0.528222 Y
6 ICIS 280-590907/18 50.0 31.427787 50.0 482565.0 0.628556 Y
7 STD75 280-590907/19 75.0 45.925413 50.0 480245.0 0.612339 Y
8 STD100 280-590907/20 100.0 55.118354 50.0 495081.0 0.551184 Y
9 STD200 280-590907/21 200.0 118.986743 50.0 505084.0 0.594934 Y
RelResp = [0.5818]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 172 of 349
Calibration / 1,3-Dichlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.292
Error Coefficients
Standard Error:1170000
Relative Standard Error:4.2
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.612663 50.0 491951.0 1.225325 Y
2 STD010 280-590907/14 1.0 1.483321 50.0 472824.0 1.483321 N
3 STD020 280-590907/15 2.0 2.495758 50.0 473223.0 1.247879 Y
4 STD050 280-590907/16 5.0 6.674956 50.0 470460.0 1.334991 Y
5 STD10 280-590907/17 10.0 12.572879 50.0 488138.0 1.257288 Y
6 ICIS 280-590907/18 50.0 68.383119 50.0 482565.0 1.367662 Y
7 STD75 280-590907/19 75.0 102.076544 50.0 480245.0 1.361021 Y
8 STD100 280-590907/20 100.0 126.484757 50.0 495081.0 1.264848 Y
9 STD200 280-590907/21 200.0 255.876448 50.0 505084.0 1.279382 Y
RelResp = [1.292]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 173 of 349
Calibration / 4-Isopropyltoluene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.496
Error Coefficients
Standard Error:2280000
Relative Standard Error:6.0
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.150928 50.0 491951.0 2.301855 Y
2 STD010 280-590907/14 1.0 3.132032 50.0 472824.0 3.132032 N
3 STD020 280-590907/15 2.0 5.100027 50.0 473223.0 2.550013 Y
4 STD050 280-590907/16 5.0 12.909918 50.0 470460.0 2.581984 Y
5 STD10 280-590907/17 10.0 23.176438 50.0 488138.0 2.317644 Y
6 ICIS 280-590907/18 50.0 134.058521 50.0 482565.0 2.68117 Y
7 STD75 280-590907/19 75.0 200.255182 50.0 480245.0 2.670069 Y
8 STD100 280-590907/20 100.0 237.747762 50.0 495081.0 2.377478 Y
9 STD200 280-590907/21 200.0 498.265437 50.0 505084.0 2.491327 Y
RelResp = [2.496]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 174 of 349
Calibration / 1,4-Dichlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.346
Error Coefficients
Standard Error:1190000
Relative Standard Error:4.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.997
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.736049 50.0 491951.0 1.472098 Y
2 STD010 280-590907/14 1.0 1.76313 50.0 472824.0 1.76313 N
3 STD020 280-590907/15 2.0 2.760327 50.0 473223.0 1.380163 Y
4 STD050 280-590907/16 5.0 6.632232 50.0 470460.0 1.326446 Y
5 STD10 280-590907/17 10.0 12.769647 50.0 488138.0 1.276965 Y
6 ICIS 280-590907/18 50.0 68.157968 50.0 482565.0 1.363159 Y
7 STD75 280-590907/19 75.0 102.516736 50.0 480245.0 1.36689 Y
8 STD100 280-590907/20 100.0 129.31187 50.0 495081.0 1.293119 Y
9 STD200 280-590907/21 200.0 258.092416 50.0 505084.0 1.290462 Y
RelResp = [1.346]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 175 of 349
Calibration / n-Butylbenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.219
Error Coefficients
Standard Error:2060000
Relative Standard Error:7.1
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.995
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 1.001014 50.0 491951.0 2.002029 Y
2 STD010 280-590907/14 1.0 2.776086 50.0 472824.0 2.776086 N
3 STD020 280-590907/15 2.0 4.514151 50.0 473223.0 2.257075 Y
4 STD050 280-590907/16 5.0 11.275773 50.0 470460.0 2.255155 Y
5 STD10 280-590907/17 10.0 20.203406 50.0 488138.0 2.020341 Y
6 ICIS 280-590907/18 50.0 121.373805 50.0 482565.0 2.427476 Y
7 STD75 280-590907/19 75.0 179.788441 50.0 480245.0 2.397179 Y
8 STD100 280-590907/20 100.0 213.54647 50.0 495081.0 2.135465 Y
9 STD200 280-590907/21 200.0 450.73364 50.0 505084.0 2.253668 Y
RelResp = [2.219]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
STD200 280-590907/21
Page 176 of 349
Calibration / 1,2-Dichlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.223
Error Coefficients
Standard Error:1110000
Relative Standard Error:3.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.57709 50.0 491951.0 1.15418 Y
2 STD010 280-590907/14 1.0 1.611488 50.0 472824.0 1.611488 N
3 STD020 280-590907/15 2.0 2.390311 50.0 473223.0 1.195155 Y
4 STD050 280-590907/16 5.0 6.396718 50.0 470460.0 1.279344 Y
5 STD10 280-590907/17 10.0 11.959733 50.0 488138.0 1.195973 Y
6 ICIS 280-590907/18 50.0 63.136469 50.0 482565.0 1.262729 Y
7 STD75 280-590907/19 75.0 96.065238 50.0 480245.0 1.28087 Y
8 STD100 280-590907/20 100.0 120.940614 50.0 495081.0 1.209406 Y
9 STD200 280-590907/21 200.0 240.490295 50.0 505084.0 1.202451 Y
RelResp = [1.223]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Page 177 of 349
Calibration / 1,2-Dibromo-3-Chloropropane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.1585
Error Coefficients
Standard Error:158000
Relative Standard Error:3.2
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.082325 50.0 491951.0 0.164651 N
2 STD010 280-590907/14 1.0 0.373289 50.0 472824.0 0.373289 N
3 STD020 280-590907/15 2.0 0.312009 50.0 473223.0 0.156005 Y
4 STD050 280-590907/16 5.0 0.794967 50.0 470460.0 0.158993 Y
5 STD10 280-590907/17 10.0 1.520881 50.0 488138.0 0.152088 Y
6 ICIS 280-590907/18 50.0 7.957374 50.0 482565.0 0.159147 Y
7 STD75 280-590907/19 75.0 11.64666 50.0 480245.0 0.155289 Y
8 STD100 280-590907/20 100.0 16.846435 50.0 495081.0 0.168464 Y
9 STD200 280-590907/21 200.0 31.908257 50.0 505084.0 0.159541 Y
RelResp = [0.1585]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD200 280-590907/21
Page 178 of 349
Calibration / 1,2,4-Trichlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.6954
Error Coefficients
Standard Error:639000
Relative Standard Error:5.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.303486 50.0 491951.0 0.606971 Y
2 STD010 280-590907/14 1.0 1.531331 50.0 472824.0 1.531331 N
3 STD020 280-590907/15 2.0 1.454283 50.0 473223.0 0.727141 Y
4 STD050 280-590907/16 5.0 3.500298 50.0 470460.0 0.70006 Y
5 STD10 280-590907/17 10.0 6.741434 50.0 488138.0 0.674143 Y
6 ICIS 280-590907/18 50.0 36.147358 50.0 482565.0 0.722947 Y
7 STD75 280-590907/19 75.0 54.518423 50.0 480245.0 0.726912 Y
8 STD100 280-590907/20 100.0 71.23602 50.0 495081.0 0.71236 Y
9 STD200 280-590907/21 200.0 138.594867 50.0 505084.0 0.692974 Y
RelResp = [0.6954]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
1.4
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 179 of 349
Calibration / Hexachlorobutadiene
Curve Type:Linear
Weighting:Conc_Sq
Origin:None
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:-0.08962
Slope:0.2774
Error Coefficients
Standard Error:259000
Relative Standard Error:6.7
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.996
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.046244 50.0 491951.0 0.092489 Y
2 STD010 280-590907/14 1.0 0.492678 50.0 472824.0 0.492678 N
3 STD020 280-590907/15 2.0 0.500504 50.0 473223.0 0.250252 Y
4 STD050 280-590907/16 5.0 1.404158 50.0 470460.0 0.280832 Y
5 STD10 280-590907/17 10.0 2.490587 50.0 488138.0 0.249059 Y
6 ICIS 280-590907/18 50.0 14.48924 50.0 482565.0 0.289785 Y
7 STD75 280-590907/19 75.0 21.300794 50.0 480245.0 0.284011 Y
8 STD100 280-590907/20 100.0 25.85284 50.0 495081.0 0.258528 Y
9 STD200 280-590907/21 200.0 51.756342 50.0 505084.0 0.258782 Y
RelResp = [-0.08962] + [0.2774]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
4.0
4.5
5.0
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
STD100 280-590907/20
Intercept = 0.323
Page 180 of 349
Calibration / Naphthalene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:1.953
Error Coefficients
Standard Error:1750000
Relative Standard Error:10.1
Correlation Coefficient:0.999
Coefficient of Determination (Adjusted):0.989
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.801503 50.0 491951.0 1.603005 Y
2 STD010 280-590907/14 1.0 7.835474 50.0 472824.0 7.835474 N
3 STD020 280-590907/15 2.0 4.615689 50.0 473223.0 2.307844 Y
4 STD050 280-590907/16 5.0 10.182694 50.0 470460.0 2.036539 Y
5 STD10 280-590907/17 10.0 18.998418 50.0 488138.0 1.899842 Y
6 ICIS 280-590907/18 50.0 97.491115 50.0 482565.0 1.949822 Y
7 STD75 280-590907/19 75.0 142.779623 50.0 480245.0 1.903728 Y
8 STD100 280-590907/20 100.0 203.213919 50.0 495081.0 2.032139 Y
9 STD200 280-590907/21 200.0 378.814712 50.0 505084.0 1.894074 Y
RelResp = [1.953]x
Concentration
0 100 200
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 181 of 349
Calibration / 1,2,3-Trichlorobenzene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ISTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:0.5842
Error Coefficients
Standard Error:533000
Relative Standard Error:7.6
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.994
ID Level Concentration Rel. Resp.IS Amount IS Response RRF Used
1 STD005 280-590907/13 0.5 0.253582 50.0 491951.0 0.507164 Y
2 STD010 280-590907/14 1.0 1.810082 50.0 472824.0 1.810082 N
3 STD020 280-590907/15 2.0 1.321153 50.0 473223.0 0.660577 Y
4 STD050 280-590907/16 5.0 3.005569 50.0 470460.0 0.601114 Y
5 STD10 280-590907/17 10.0 5.459829 50.0 488138.0 0.545983 Y
6 ICIS 280-590907/18 50.0 29.306311 50.0 482565.0 0.586126 Y
7 STD75 280-590907/19 75.0 44.419931 50.0 480245.0 0.592266 Y
8 STD100 280-590907/20 100.0 60.08027 50.0 495081.0 0.600803 Y
9 STD200 280-590907/21 200.0 115.854888 50.0 505084.0 0.579274 Y
RelResp = [0.5842]x
Concentration
0 100 200
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
l
a
t
i
v
e

R
e
s
p
o
n
s
e

(

X

1
0
0
)
STD005 280-590907/13
STD010 280-590907/14
STD020 280-590907/15
STD050 280-590907/16
STD10 280-590907/17
ICIS 280-590907/18
STD75 280-590907/19
Page 182 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
10/22/2022 14:59
10/22/2022 11:33
10/22/2022 14:18
ICV 280-590907/22
DB-624 (60.25)
Eurofins Denver
Lab File ID:X43672.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Dichlorodifluoromethane 0.24030.2234 0.1000 53.8 50.0 7.6 30.0Ave
Chloromethane 0.22640.2181 0.1000 51.9 50.0 3.8 30.0Ave
Vinyl chloride 0.24580.2051 0.0100 59.9 50.0 19.9 30.0Ave
Bromomethane 0.1274 0.0100 61.1 50.0 22.1 30.0Lin1
Chloroethane 0.14050.1380 0.0100 50.9 50.0 1.8 30.0Ave
Dichlorofluoromethane 0.36640.3629 0.0100 50.5 50.0 1.0 30.0Ave
Trichlorofluoromethane 0.34060.3082 0.0100 55.3 50.0 10.5 30.0Ave
Ethyl ether 0.17050.1693 0.0100 50.4 50.0 0.7 30.0Ave
Acrolein 0.01260.0123 0.0010 255 250 1.8 30.0Ave
1,1-Dichloroethene 0.19450.1768 0.0600 55.0 50.0 10.0 30.0Ave
Freon 113 0.15530.1406 0.0500 55.2 50.0 10.5 30.0Ave
Acetone 0.06090.0604 0.0100 202 200 0.8 30.0Ave
Iodomethane 0.2053 0.0100 40.8 50.0 -18.4 30.0Lin1
Carbon disulfide 0.61490.5643 0.1000 54.5 50.0 9.0 30.0Ave
Methyl acetate 0.14630.1427 0.0100 103 100 2.6 30.0Ave
3-Chloro-1-propene 0.31370.3063 0.0100 51.2 50.0 2.4 30.0Ave
Methylene Chloride 0.2268 0.0100 51.6 50.0 3.2 30.0Lin2
2-Methyl-2-propanol 0.02600.0233 0.0010 557 500 11.5 30.0Ave
Acrylonitrile 0.07920.0745 0.0100 531 500 6.3 30.0Ave
Methyl tert-butyl ether 0.66610.6437 0.1000 51.7 50.0 3.5 30.0Ave
trans-1,2-Dichloroethene 0.21560.2085 0.1000 51.7 50.0 3.4 30.0Ave
Hexane 1.2821.132 0.0100 56.6 50.0 13.2 30.0Ave
Vinyl acetate 0.45400.4356 0.0100 104 100 4.2 30.0Ave
1,1-Dichloroethane 0.38930.3908 0.1000 49.8 50.0 -0.4 30.0Ave
2-Butanone (MEK)0.09550.0877 0.0100 218 200 8.9 30.0Ave
cis-1,2-Dichloroethene 0.24830.2380 0.1000 52.2 50.0 4.3 30.0Ave
2,2-Dichloropropane 0.38600.3733 0.0100 51.7 50.0 3.4 30.0Ave
sec-Butyl Alcohol 0.0191 0.0100 1350 1200 12.1 30.0Lin1
Chlorobromomethane 0.11050.1115 0.0500 49.6 50.0 -0.9 30.0Ave
Tetrahydrofuran 0.06330.0589 0.0010 107 100 7.5 30.0Ave
Chloroform 0.40490.3938 0.2000 51.4 50.0 2.8 30.0Ave
1,1,1-Trichloroethane 0.36880.3450 0.0500 53.5 50.0 6.9 30.0Ave
Cyclohexane 0.36590.3418 0.0100 53.5 50.0 7.1 30.0Ave
1,1-Dichloropropene 0.32240.2980 0.0100 54.1 50.0 8.2 30.0Ave
Carbon tetrachloride 0.30280.2950 0.1000 51.3 50.0 2.6 30.0Ave
Isobutyl alcohol 0.00780.0071 0.0010 1380 1250 10.2 30.0Ave
Benzene 0.91640.8889 0.2000 51.6 50.0 3.1 30.0Ave
1,2-Dichloroethane 0.33000.3292 0.0700 50.1 50.0 0.2 30.0Ave
n-Heptane 0.24530.2233 54.9 50.0 9.8Ave
Trichloroethene 1.0360.9864 0.2000 52.5 50.0 5.0 30.0Ave
2-Pentanone 0.15850.1346 0.0010 189 160 17.8 30.0Ave
FORM VII 8260C
Page 183 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
10/22/2022 14:59
10/22/2022 11:33
10/22/2022 14:18
ICV 280-590907/22
DB-624 (60.25)
Eurofins Denver
Lab File ID:X43672.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Methylcyclohexane 0.28400.2639 0.0500 53.8 50.0 7.6 30.0Ave
1,2-Dichloropropane 0.23140.2242 0.1000 51.6 50.0 3.2 30.0Ave
1,4-Dioxane 0.00340.0029 0.0010 1160 1000 15.6 30.0Ave
Dibromomethane 0.14320.1391 0.0100 51.4 50.0 2.9 30.0Ave
Dichlorobromomethane 0.32240.3191 0.2000 50.5 50.0 1.0 30.0Ave
2-Chloroethyl vinyl ether 0.15480.1449 0.0100 53.4 50.0 6.8 30.0Ave
cis-1,3-Dichloropropene 1.6941.690 0.2000 50.1 50.0 0.3 30.0Ave
4-Methyl-2-pentanone (MIBK)0.20050.1821 0.0300 220 200 10.1 30.0Ave
Toluene 1.0050.9734 0.3000 51.6 50.0 3.3 30.0Ave
trans-1,3-Dichloropropene 0.37930.3631 0.2000 52.2 50.0 4.4 30.0Ave
Ethyl methacrylate 1.3201.207 0.0100 54.7 50.0 9.3 30.0Ave
1,1,2-Trichloroethane 0.20470.1941 0.1000 52.7 50.0 5.5 30.0Ave
Tetrachloroethene 0.77830.7262 0.1000 53.6 50.0 7.2 30.0Ave
1,3-Dichloropropane 1.5731.509 0.0100 52.1 50.0 4.2 30.0Ave
Methyl n-butyl ketone (MNBK)0.62180.5448 0.0100 228 200 14.1 30.0Ave
Chlorodibromomethane 1.0090.9865 0.1000 51.1 50.0 2.3 30.0Ave
1,2-Dibromoethane 0.92020.8925 0.1000 51.6 50.0 3.1 30.0Ave
1-Chlorohexane 1.409 0.0100 43.5 40.0 8.7 30.0Lin2
Chlorobenzene 2.7332.702 0.3000 50.6 50.0 1.1 30.0Ave
1,1,1,2-Tetrachloroethane 0.97530.9449 0.0100 51.6 50.0 3.2 30.0Ave
Ethylbenzene 1.5261.463 0.3000 52.2 50.0 4.3 30.0Ave
m-Xylene & p-Xylene 1.9041.835 0.1000 51.9 50.0 3.8 30.0Ave
o-Xylene 1.8581.782 0.2000 52.1 50.0 4.3 30.0Ave
Styrene 3.1443.028 0.2000 51.9 50.0 3.8 30.0Ave
Bromoform 0.65130.6182 0.1000 52.7 50.0 5.4 30.0Ave
Isopropylbenzene 2.9212.824 0.3000 51.7 50.0 3.5 30.0Ave
Cyclohexanone 0.04600.0374 0.0010 1840 1500 23.0 30.0Ave
1,1,2,2-Tetrachloroethane 0.75650.7132 0.3000 53.0 50.0 6.1 30.0Ave
Bromobenzene 0.68800.6802 0.0100 50.6 50.0 1.2 30.0Ave
trans-1,4-Dichloro-2-butene 0.25470.2276 0.0100 56.0 50.0 11.9 30.0Ave
1,2,3-Trichloropropane 0.22940.2211 0.0100 51.9 50.0 3.8 30.0Ave
N-Propylbenzene 0.80690.7939 0.0100 50.8 50.0 1.6 30.0Ave
2-Chlorotoluene 0.67850.6742 0.0100 50.3 50.0 0.6 30.0Ave
1,3,5-Trimethylbenzene 2.5612.492 0.0100 51.4 50.0 2.8 30.0Ave
4-Chlorotoluene 0.72010.7007 0.0100 51.4 50.0 2.8 30.0Ave
tert-Butylbenzene 2.0722.028 0.0100 51.1 50.0 2.2 30.0Ave
1,2,4-Trimethylbenzene 2.6442.628 0.3000 50.3 50.0 0.6 30.0Ave
sec-Butylbenzene 0.61730.5818 0.0100 53.0 50.0 6.1 30.0Ave
1,3-Dichlorobenzene 1.3361.292 0.5000 51.7 50.0 3.4 30.0Ave
4-Isopropyltoluene 2.6412.496 0.0100 52.9 50.0 5.8 30.0Ave
1,4-Dichlorobenzene 1.3721.346 0.5000 51.0 50.0 1.9 30.0Ave
FORM VII 8260C
Page 184 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
10/22/2022 14:59
10/22/2022 11:33
10/22/2022 14:18
ICV 280-590907/22
DB-624 (60.25)
Eurofins Denver
Lab File ID:X43672.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
n-Butylbenzene 2.3462.219 0.0100 52.9 50.0 5.7 30.0Ave
1,2-Dichlorobenzene 1.2731.223 0.5000 52.1 50.0 4.1 30.0Ave
1,2-Dibromo-3-Chloropropane 0.16720.1585 0.0100 52.8 50.0 5.5 30.0Ave
1,2,4-Trichlorobenzene 0.73100.6954 0.2000 52.6 50.0 5.1 30.0Ave
Hexachlorobutadiene 0.2975 0.0100 54.0 50.0 7.9 30.0Lin2
Naphthalene 2.0931.953 0.0100 53.6 50.0 7.2 30.0Ave
1,2,3-Trichlorobenzene 0.61070.5842 0.3000 52.3 50.0 4.5 30.0Ave
Dibromofluoromethane (Surr)0.23580.2362 0.0100 49.9 50.0 -0.2 30.0Ave
1,2-Dichloroethane-d4 (Surr)0.28720.2868 0.0100 50.1 50.0 0.1 30.0Ave
Toluene-d8 (Surr)4.2154.184 0.0100 50.4 50.0 0.7 30.0Ave
4-Bromofluorobenzene (Surr)0.98871.005 0.0100 49.2 50.0 -1.7 30.0Ave
FORM VII 8260C
Page 185 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
10/23/2022 15:09
10/22/2022 11:33
10/22/2022 14:18
ICV 280-590924/12
DB-624 (60.25)
Eurofins Denver
Lab File ID:X43688.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Dibromofluoromethane (Surr)0.23360.2362 0.0100 49.5 50.0 -1.1 30.0Ave
1,2-Dichloroethane-d4 (Surr)0.28180.2868 0.0100 49.1 50.0 -1.8 30.0Ave
Toluene-d8 (Surr)4.0954.184 0.0100 48.9 50.0 -2.1 30.0Ave
4-Bromofluorobenzene (Surr)0.98261.005 0.0100 48.9 50.0 -2.3 30.0Ave
FORM VII 8260C
Page 186 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
10/23/2022 15:09
10/22/2022 15:19
10/22/2022 17:23
ICV 280-590924/12
DB-624 (60.25)
Eurofins Denver
Lab File ID:X43688.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Ethanol 0.00230.0026 0.0100 1280 1500 -14.9 30.0*Ave
Isopropyl alcohol 0.01290.0155 0.0100 209 250 -16.6 30.0Ave
Acetonitrile 0.02500.0279 0.0100 223 250 -10.6 30.0Ave
Isopropyl ether 0.20500.1867 0.0100 27.5 25.0 9.8 30.0Ave
2-Chloro-1,3-butadiene 0.35750.3274 0.0100 27.3 25.0 9.2 30.0Ave
Tert-butyl ethyl ether 0.71100.6465 0.0100 27.5 25.0 10.0 30.0Ave
Ethyl acetate 0.18350.1934 0.0100 47.4 50.0 -5.1 30.0Ave
Propionitrile 0.03060.0311 0.0100 246 250 -1.5 30.0Ave
Methacrylonitrile 0.11730.1216 0.0100 241 250 -3.5 30.0Ave
Tert-amyl methyl ether 0.66090.6244 0.0100 26.5 25.0 5.8 30.0Ave
n-Butanol 0.00560.0061 0.0100 569 625 -8.9 30.0*Ave
Methyl methacrylate 0.06550.0660 0.0100 49.6 50.0 -0.8 30.0Ave
2-Nitropropane 0.06370.0700 0.0100 45.5 50.0 -9.0 30.0Ave
cis-1,4-Dichloro-2-butene 0.17530.1969 0.0100 44.5 50.0 -11.0 30.0Ave
1,2,3-Trimethylbenzene 2.7742.711 0.0100 25.6 25.0 2.3 30.0Ave
1,3,5-Trichlorobenzene 0.86080.8433 0.0100 25.5 25.0 2.1 30.0Ave
FORM VII 8260C
Page 187 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
12/25/2022 09:04
10/22/2022 11:33
10/22/2022 14:18
CCV 280-597688/2
DB-624 (60.25)
Eurofins Denver
Lab File ID:X46337.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Dichlorodifluoromethane 0.21510.2234 0.1000 24.1 25.0 -3.7 20.0Ave
Chloromethane 0.24820.2181 0.1000 28.5 25.0 13.8 20.0Ave
Vinyl chloride 0.23540.2051 0.0100 28.7 25.0 14.8 20.0Ave
Bromomethane 0.1058 0.0100 25.0 25.0 -0.2 20.0Lin1
Chloroethane 0.15030.1380 0.0100 27.2 25.0 8.9 20.0Ave
Dichlorofluoromethane 0.38970.3629 0.0100 26.8 25.0 7.4 20.0Ave
Trichlorofluoromethane 0.29190.3082 0.0100 23.7 25.0 -5.3 20.0Ave
Ethyl ether 0.18810.1693 0.0100 27.8 25.0 11.1 20.0Ave
Acrolein 0.02630.0123 0.0010 526 247 113.0 *20.0Ave
Freon 113 0.12890.1406 0.0500 22.9 25.0 -8.3 20.0Ave
1,1-Dichloroethene 0.18490.1768 0.0600 26.1 25.0 4.6 20.0Ave
Acetone 0.05930.0604 0.0100 98.1 100 -1.9 20.0Ave
Iodomethane 0.2081 0.0100 21.0 25.0 -16.1 20.0Lin1
Carbon disulfide 0.63560.5643 0.1000 28.2 25.0 12.6 20.0Ave
Methyl acetate 0.15680.1427 0.0100 54.9 50.0 9.9 20.0Ave
3-Chloro-1-propene 0.31720.3063 0.0100 25.9 25.0 3.6 20.0Ave
Methylene Chloride 0.2454 0.0100 27.7 25.0 10.7 20.0Lin2
2-Methyl-2-propanol 0.02320.0233 0.0010 249 250 -0.3 20.0Ave
Acrylonitrile 0.08660.0745 0.0100 291 250 16.3 20.0Ave
Methyl tert-butyl ether 0.69700.6437 0.1000 27.1 25.0 8.3 20.0Ave
trans-1,2-Dichloroethene 0.23110.2085 0.1000 27.7 25.0 10.8 20.0Ave
Hexane 1.2031.132 0.0100 26.6 25.0 6.3 20.0Ave
Vinyl acetate 0.45240.4356 0.0100 51.9 50.0 3.9 20.0Ave
1,1-Dichloroethane 0.40800.3908 0.1000 26.1 25.0 4.4 20.0Ave
2-Butanone (MEK)0.09950.0877 0.0100 114 100 13.6 20.0Ave
cis-1,2-Dichloroethene 0.25840.2380 0.1000 27.1 25.0 8.6 20.0Ave
2,2-Dichloropropane 0.34710.3733 0.0100 23.2 25.0 -7.0 20.0Ave
sec-Butyl Alcohol 0.0169 0.0100 603 600 0.5 20.0Lin1
Chlorobromomethane 0.10990.1115 0.0500 24.6 25.0 -1.4 20.0Ave
Tetrahydrofuran 0.06760.0589 0.0010 57.4 50.0 14.7 20.0Ave
Chloroform 0.41620.3938 0.2000 26.4 25.0 5.7 20.0Ave
1,1,1-Trichloroethane 0.34510.3450 0.0500 25.0 25.0 0.0 20.0Ave
Cyclohexane 0.34890.3418 0.0100 25.5 25.0 2.1 20.0Ave
1,1-Dichloropropene 0.32380.2980 0.0100 27.2 25.0 8.7 20.0Ave
Carbon tetrachloride 0.27280.2950 0.1000 23.1 25.0 -7.5 20.0Ave
Isobutyl alcohol 0.00570.0071 0.0010 496 625 -20.6 *20.0Ave
Benzene 1.0030.8889 0.2000 28.2 25.0 12.8 20.0Ave
1,2-Dichloroethane 0.31100.3292 0.0700 23.6 25.0 -5.5 20.0Ave
n-Heptane 0.21790.2233 24.4 25.0 -2.4Ave
Trichloroethene 1.0710.9864 0.2000 27.1 25.0 8.5 20.0Ave
2-Pentanone 0.16230.1346 0.0010 96.5 80.0 20.6 *20.0Ave
FORM VII 8260C
Page 188 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
12/25/2022 09:04
10/22/2022 11:33
10/22/2022 14:18
CCV 280-597688/2
DB-624 (60.25)
Eurofins Denver
Lab File ID:X46337.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
Methylcyclohexane 0.25830.2639 0.0500 24.5 25.0 -2.1 20.0Ave
1,2-Dichloropropane 0.24390.2242 0.1000 27.2 25.0 8.8 20.0Ave
1,4-Dioxane 0.00320.0029 0.0010 547 500 9.4 20.0Ave
Dibromomethane 0.13980.1391 0.0100 25.1 25.0 0.5 20.0Ave
Dichlorobromomethane 0.30990.3191 0.2000 24.3 25.0 -2.9 20.0Ave
2-Chloroethyl vinyl ether 0.15400.1449 0.0100 26.6 25.0 6.3 20.0Ave
cis-1,3-Dichloropropene 1.7601.690 0.2000 26.0 25.0 4.2 20.0Ave
4-Methyl-2-pentanone (MIBK)0.20500.1821 0.0300 113 100 12.6 20.0Ave
Toluene 1.0910.9734 0.3000 28.0 25.0 12.1 20.0Ave
trans-1,3-Dichloropropene 0.35390.3631 0.2000 24.4 25.0 -2.5 20.0Ave
Ethyl methacrylate 1.3621.207 0.0100 28.2 25.0 12.8 20.0Ave
1,1,2-Trichloroethane 0.21160.1941 0.1000 27.2 25.0 9.0 20.0Ave
Tetrachloroethene 0.79250.7262 0.1000 27.3 25.0 9.1 20.0Ave
1,3-Dichloropropane 1.6721.509 0.0100 27.7 25.0 10.8 20.0Ave
Methyl n-butyl ketone (MNBK)0.62220.5448 0.0100 114 100 14.2 20.0Ave
Chlorodibromomethane 0.98300.9865 0.1000 24.9 25.0 -0.4 20.0Ave
1,2-Dibromoethane 0.94310.8925 0.1000 26.4 25.0 5.7 20.0Ave
1-Chlorohexane 1.411 0.0100 21.6 20.0 8.2 20.0Lin2
Chlorobenzene 2.9352.702 0.3000 27.2 25.0 8.6 20.0Ave
1,1,1,2-Tetrachloroethane 0.95450.9449 0.0100 25.3 25.0 1.0 20.0Ave
Ethylbenzene 1.6761.463 0.3000 28.7 25.0 14.6 20.0Ave
m-Xylene & p-Xylene 2.0851.835 0.1000 28.4 25.0 13.6 20.0Ave
o-Xylene 2.0231.782 0.2000 28.4 25.0 13.5 20.0Ave
Styrene 3.3693.028 0.2000 27.8 25.0 11.2 20.0Ave
Bromoform 0.61380.6182 0.1000 24.8 25.0 -0.7 20.0Ave
Isopropylbenzene 3.1252.824 0.3000 27.7 25.0 10.7 20.0Ave
Cyclohexanone 0.05810.0374 0.0010 1160 750 55.2 *20.0Ave
1,1,2,2-Tetrachloroethane 0.79980.7132 0.3000 28.0 25.0 12.1 20.0Ave
Bromobenzene 0.73040.6802 0.0100 26.8 25.0 7.4 20.0Ave
trans-1,4-Dichloro-2-butene 0.21740.2276 0.0100 23.9 25.0 -4.5 20.0Ave
1,2,3-Trichloropropane 0.22320.2211 0.0100 25.2 25.0 0.9 20.0Ave
N-Propylbenzene 0.84350.7939 0.0100 26.6 25.0 6.2 20.0Ave
2-Chlorotoluene 0.71500.6742 0.0100 26.5 25.0 6.1 20.0Ave
1,3,5-Trimethylbenzene 2.7352.492 0.0100 27.4 25.0 9.8 20.0Ave
4-Chlorotoluene 0.74850.7007 0.0100 26.7 25.0 6.8 20.0Ave
tert-Butylbenzene 2.1892.028 0.0100 27.0 25.0 7.9 20.0Ave
1,2,4-Trimethylbenzene 2.8052.628 0.3000 26.7 25.0 6.7 20.0Ave
sec-Butylbenzene 0.62610.5818 0.0100 26.9 25.0 7.6 20.0Ave
1,3-Dichlorobenzene 1.3831.292 0.5000 26.8 25.0 7.0 20.0Ave
4-Isopropyltoluene 2.7942.496 0.0100 28.0 25.0 11.9 20.0Ave
1,4-Dichlorobenzene 1.4011.346 0.5000 26.0 25.0 4.1 20.0Ave
FORM VII 8260C
Page 189 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC/MS VOA CONTINUING CALIBRATION DATA
0.25(mm)
280-170477-1
VMS_X4
12/25/2022 09:04
10/22/2022 11:33
10/22/2022 14:18
CCV 280-597688/2
DB-624 (60.25)
Eurofins Denver
Lab File ID:X46337.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE RRF RRF MIN RRF
n-Butylbenzene 2.4972.219 0.0100 28.1 25.0 12.6 20.0Ave
1,2-Dichlorobenzene 1.2941.223 0.5000 26.5 25.0 5.8 20.0Ave
1,2-Dibromo-3-Chloropropane 0.14920.1585 0.0100 23.5 25.0 -5.9 20.0Ave
1,2,4-Trichlorobenzene 0.72910.6954 0.2000 26.2 25.0 4.8 20.0Ave
Hexachlorobutadiene 0.2739 0.0100 25.0 25.0 0.0 20.0Lin2
Naphthalene 1.9841.953 0.0100 25.4 25.0 1.6 20.0Ave
1,2,3-Trichlorobenzene 0.60070.5842 0.3000 25.7 25.0 2.8 20.0Ave
Dibromofluoromethane (Surr)0.23090.2362 0.0100 48.9 50.0 -2.3 20.0Ave
1,2-Dichloroethane-d4 (Surr)0.25530.2868 0.0100 44.5 50.0 -11.0 20.0Ave
Toluene-d8 (Surr)4.4594.184 0.0100 53.3 50.0 6.6 20.0Ave
4-Bromofluorobenzene (Surr)0.95711.005 0.0100 47.6 50.0 -4.8 20.0Ave
FORM VII 8260C
Page 190 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:MB 280-597688/7
Matrix:X46342.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 10:55
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
15 6.667-64-1 Acetone ND
15 5.978-93-3 2-Butanone (MEK)ND
1.0 0.3171-43-2 Benzene ND
1.0 0.42108-90-7 Chlorobenzene ND
2.0 0.6375-15-0 Carbon disulfide ND
1.0 0.5756-23-5 Carbon tetrachloride ND
1.0 0.44110-82-7 Cyclohexane ND
5.0 1.896-12-8 1,2-Dibromo-3-Chloropropane ND
5.0 2.474-83-9 Bromomethane ND
2.0 1.275-25-2 Bromoform ND
4.0 1.475-00-3 Chloroethane ND
1.0 0.3667-66-3 Chloroform ND
1.0 0.4074-97-5 Chlorobromomethane ND
1.0 0.3975-27-4 Dichlorobromomethane ND
2.0 0.62124-48-1 Chlorodibromomethane ND
1.0 0.3698-82-8 Isopropylbenzene ND
5.0 1.7591-78-6 Methyl n-butyl ketone (MNBK)ND
2.0 0.7574-87-3 Chloromethane ND
3.0 0.9675-71-8 Dichlorodifluoromethane ND
1.0 0.37156-60-5 trans-1,2-Dichloroethene ND
2.0 0.6510061-02-6 trans-1,3-Dichloropropene ND
2.0 0.9475-09-2 Methylene Chloride ND
5.0 1.679-20-9 Methyl acetate ND
5.0 0.251634-04-4 Methyl tert-butyl ether ND
5.0 0.98108-10-1 4-Methyl-2-pentanone (MIBK)ND
1.0 0.31108-87-2 Methylcyclohexane ND
1.0 0.36100-42-5 Styrene ND
1.0 0.2179-34-5 1,1,2,2-Tetrachloroethane ND
2.0 0.7087-61-6 1,2,3-Trichlorobenzene ND
1.0 0.58120-82-1 1,2,4-Trichlorobenzene ND
1.0 0.32108-88-3 Toluene ND
1.0 0.3971-55-6 1,1,1-Trichloroethane ND
1.0 0.2779-00-5 1,1,2-Trichloroethane ND
1.0 0.3079-01-6 Trichloroethene ND
FORM I 8260C
Page 191 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:MB 280-597688/7
Matrix:X46342.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 10:55
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
3.0 0.7376-13-1 Freon 113 ND
2.0 0.5175-01-4 Vinyl chloride ND
2.0 0.36179601-23-1 m-Xylene & p-Xylene ND
1.0 0.3395-47-6 o-Xylene ND
1.0 0.40127-18-4 Tetrachloroethene ND
1.0 0.3795-50-1 1,2-Dichlorobenzene ND
1.0 0.33541-73-1 1,3-Dichlorobenzene ND
1.0 0.39106-46-7 1,4-Dichlorobenzene ND
1.0 0.32156-59-2 cis-1,2-Dichloroethene ND
2.0 0.6310061-01-5 cis-1,3-Dichloropropene ND
1.0 0.2275-34-3 1,1-Dichloroethane ND
1.0 0.2375-35-4 1,1-Dichloroethene ND
1.0 0.54107-06-2 1,2-Dichloroethane ND
1.0 0.5278-87-5 1,2-Dichloropropane ND
150 19123-91-1 1,4-Dioxane ND
1.0 0.30100-41-4 Ethylbenzene ND
1.0 0.40106-93-4 1,2-Dibromoethane ND
2.0 0.5775-69-4 Trichlorofluoromethane ND
%RECCAS NO.LIMITSQSURROGATE
90 70-12717060-07-0 1,2-Dichloroethane-d4 (Surr)
107 80-1252037-26-5 Toluene-d8 (Surr)
96 78-120460-00-4 4-Bromofluorobenzene (Surr)
97 77-1201868-53-7 Dibromofluoromethane (Surr)
FORM I 8260C
Page 192 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCS 280-597688/1002
Matrix:-X46337-LCS.dLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 09:04
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
15 6.667-64-1 Acetone 98.1
15 5.978-93-3 2-Butanone (MEK)114
1.0 0.3171-43-2 Benzene 28.2
1.0 0.42108-90-7 Chlorobenzene 27.2
2.0 0.6375-15-0 Carbon disulfide 28.2
1.0 0.5756-23-5 Carbon tetrachloride 23.1
1.0 0.44110-82-7 Cyclohexane 25.5
5.0 1.896-12-8 1,2-Dibromo-3-Chloropropane 23.5
5.0 2.474-83-9 Bromomethane 25.0
2.0 1.275-25-2 Bromoform 24.8
4.0 1.475-00-3 Chloroethane 27.2
1.0 0.3667-66-3 Chloroform 26.4
1.0 0.4074-97-5 Chlorobromomethane 24.6
1.0 0.3975-27-4 Dichlorobromomethane 24.3
2.0 0.62124-48-1 Chlorodibromomethane 24.9
1.0 0.3698-82-8 Isopropylbenzene 27.7
5.0 1.7591-78-6 Methyl n-butyl ketone (MNBK)114
2.0 0.7574-87-3 Chloromethane 28.5
3.0 0.9675-71-8 Dichlorodifluoromethane 24.1
1.0 0.37156-60-5 trans-1,2-Dichloroethene 27.7
2.0 0.6510061-02-6 trans-1,3-Dichloropropene 24.4
2.0 0.9475-09-2 Methylene Chloride 27.7
5.0 1.679-20-9 Methyl acetate 54.9
5.0 0.251634-04-4 Methyl tert-butyl ether 27.1
5.0 0.98108-10-1 4-Methyl-2-pentanone (MIBK)113
1.0 0.31108-87-2 Methylcyclohexane 24.5
1.0 0.36100-42-5 Styrene 27.8
1.0 0.2179-34-5 1,1,2,2-Tetrachloroethane 28.0
2.0 0.7087-61-6 1,2,3-Trichlorobenzene 25.7
1.0 0.58120-82-1 1,2,4-Trichlorobenzene 26.2
1.0 0.32108-88-3 Toluene 28.0
1.0 0.3971-55-6 1,1,1-Trichloroethane 25.0
1.0 0.2779-00-5 1,1,2-Trichloroethane 27.2
1.0 0.3079-01-6 Trichloroethene 27.1
FORM I 8260C
Page 193 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCS 280-597688/1002
Matrix:-X46337-LCS.dLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 09:04
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
3.0 0.7376-13-1 Freon 113 22.9
2.0 0.5175-01-4 Vinyl chloride 28.7
2.0 0.36179601-23-1 m-Xylene & p-Xylene 28.4
1.0 0.3395-47-6 o-Xylene 28.4
1.0 0.40127-18-4 Tetrachloroethene 27.3
1.0 0.3795-50-1 1,2-Dichlorobenzene 26.5
1.0 0.33541-73-1 1,3-Dichlorobenzene 26.8
1.0 0.39106-46-7 1,4-Dichlorobenzene 26.0
1.0 0.32156-59-2 cis-1,2-Dichloroethene 27.1
2.0 0.6310061-01-5 cis-1,3-Dichloropropene 26.0
1.0 0.2275-34-3 1,1-Dichloroethane 26.1
1.0 0.2375-35-4 1,1-Dichloroethene 26.1
1.0 0.54107-06-2 1,2-Dichloroethane 23.6
1.0 0.5278-87-5 1,2-Dichloropropane 27.2
150 19123-91-1 1,4-Dioxane 547
1.0 0.30100-41-4 Ethylbenzene 28.7
1.0 0.40106-93-4 1,2-Dibromoethane 26.4
2.0 0.5775-69-4 Trichlorofluoromethane 23.7
%RECCAS NO.LIMITSQSURROGATE
89 70-12717060-07-0 1,2-Dichloroethane-d4 (Surr)
107 80-1252037-26-5 Toluene-d8 (Surr)
95 78-120460-00-4 4-Bromofluorobenzene (Surr)
98 77-1201868-53-7 Dibromofluoromethane (Surr)
FORM I 8260C
Page 194 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCSD 280-597688/4
Matrix:X46338.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 09:32
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
15 6.667-64-1 Acetone 106
15 5.978-93-3 2-Butanone (MEK)116
1.0 0.3171-43-2 Benzene 27.7
1.0 0.42108-90-7 Chlorobenzene 26.5
2.0 0.6375-15-0 Carbon disulfide 27.7
1.0 0.5756-23-5 Carbon tetrachloride 23.4
1.0 0.44110-82-7 Cyclohexane 25.1
5.0 1.896-12-8 1,2-Dibromo-3-Chloropropane 23.5
5.0 2.474-83-9 Bromomethane 25.0
2.0 1.275-25-2 Bromoform 24.4
4.0 1.475-00-3 Chloroethane 27.0
1.0 0.3667-66-3 Chloroform 25.8
1.0 0.4074-97-5 Chlorobromomethane 25.0
1.0 0.3975-27-4 Dichlorobromomethane 24.4
2.0 0.62124-48-1 Chlorodibromomethane 24.3
1.0 0.3698-82-8 Isopropylbenzene 27.3
5.0 1.7591-78-6 Methyl n-butyl ketone (MNBK)120
2.0 0.7574-87-3 Chloromethane 27.3
3.0 0.9675-71-8 Dichlorodifluoromethane 24.0
1.0 0.37156-60-5 trans-1,2-Dichloroethene 27.1
2.0 0.6510061-02-6 trans-1,3-Dichloropropene 23.9
2.0 0.9475-09-2 Methylene Chloride 27.7
5.0 1.679-20-9 Methyl acetate 58.6
5.0 0.251634-04-4 Methyl tert-butyl ether 26.9
5.0 0.98108-10-1 4-Methyl-2-pentanone (MIBK)113
1.0 0.31108-87-2 Methylcyclohexane 23.8
1.0 0.36100-42-5 Styrene 27.4
1.0 0.2179-34-5 1,1,2,2-Tetrachloroethane 27.3
2.0 0.7087-61-6 1,2,3-Trichlorobenzene 26.5
1.0 0.58120-82-1 1,2,4-Trichlorobenzene 25.7
1.0 0.32108-88-3 Toluene 27.3
1.0 0.3971-55-6 1,1,1-Trichloroethane 25.2
1.0 0.2779-00-5 1,1,2-Trichloroethane 27.1
1.0 0.3079-01-6 Trichloroethene 26.4
FORM I 8260C
Page 195 of 349
FORM I
GC/MS VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCSD 280-597688/4
Matrix:X46338.DLab File ID:
Date Collected:8260CAnalysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
5(mL)
0.25(mm)
Date Analyzed:12/25/2022 09:32
ID:DB-624 (60.25)
% Solids:
NHeated Purge: (Y/N)Purge Volume:5.0(mL)pH:
Analysis Batch No.:597688 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
3.0 0.7376-13-1 Freon 113 23.6
2.0 0.5175-01-4 Vinyl chloride 27.5
2.0 0.36179601-23-1 m-Xylene & p-Xylene 27.3
1.0 0.3395-47-6 o-Xylene 27.8
1.0 0.40127-18-4 Tetrachloroethene 26.2
1.0 0.3795-50-1 1,2-Dichlorobenzene 26.2
1.0 0.33541-73-1 1,3-Dichlorobenzene 26.4
1.0 0.39106-46-7 1,4-Dichlorobenzene 25.6
1.0 0.32156-59-2 cis-1,2-Dichloroethene 27.8
2.0 0.6310061-01-5 cis-1,3-Dichloropropene 25.3
1.0 0.2275-34-3 1,1-Dichloroethane 26.2
1.0 0.2375-35-4 1,1-Dichloroethene 26.5
1.0 0.54107-06-2 1,2-Dichloroethane 23.0
1.0 0.5278-87-5 1,2-Dichloropropane 26.5
150 19123-91-1 1,4-Dioxane 622
1.0 0.30100-41-4 Ethylbenzene 27.8
1.0 0.40106-93-4 1,2-Dibromoethane 26.1
2.0 0.5775-69-4 Trichlorofluoromethane 23.3
%RECCAS NO.LIMITSQSURROGATE
90 70-12717060-07-0 1,2-Dichloroethane-d4 (Surr)
105 80-1252037-26-5 Toluene-d8 (Surr)
96 78-120460-00-4 4-Bromofluorobenzene (Surr)
98 77-1201868-53-7 Dibromofluoromethane (Surr)
FORM I 8260C
Page 196 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VMS_X4
590907
Start Date:
End Date:10/22/2022 17:23
10/22/2022 11:07
BFB 280-590907/1 DB-624 (60.25) 0.25(mm)110/22/2022 11:07 X43661.D
STD005 280-590907/13
IC
DB-624 (60.25) 0.25(mm)110/22/2022 11:33 X43662.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 11:33
ICIS 280-590907/18 DB-624 (60.25) 0.25(mm)110/22/2022 11:54 X43663.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 11:54
STD010 280-590907/14
IC
DB-624 (60.25) 0.25(mm)110/22/2022 12:14 X43664.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 12:14
STD020 280-590907/15
IC
DB-624 (60.25) 0.25(mm)110/22/2022 12:35 X43665.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 12:35
STD050 280-590907/16
IC
DB-624 (60.25) 0.25(mm)110/22/2022 12:55 X43666.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 12:55
STD10 280-590907/17
IC
DB-624 (60.25) 0.25(mm)110/22/2022 13:16 X43667.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 13:16
STD75 280-590907/19
IC
DB-624 (60.25) 0.25(mm)110/22/2022 13:36 X43668.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 13:36
STD100 280-590907/20
IC
DB-624 (60.25) 0.25(mm)110/22/2022 13:57 X43669.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 13:57
STD200 280-590907/21
IC
DB-624 (60.25) 0.25(mm)110/22/2022 14:18 X43670.D
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 14:18
ICV 280-590907/22 DB-624 (60.25) 0.25(mm)110/22/2022 14:59 X43672.D
STD010 280-590907/23
IC
DB-624 (60.25) 0.25(mm)110/22/2022 15:19
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 15:19
STD020 280-590907/24
IC
DB-624 (60.25) 0.25(mm)110/22/2022 15:40
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 15:40
STD050 280-590907/25
IC
DB-624 (60.25) 0.25(mm)110/22/2022 16:01
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 16:01
STD10 280-590907/26
IC
DB-624 (60.25) 0.25(mm)110/22/2022 16:21
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 16:21
STD50 280-590907/27
IC
DB-624 (60.25) 0.25(mm)110/22/2022 16:42
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 16:42
STD100 280-590907/28
IC
DB-624 (60.25) 0.25(mm)110/22/2022 17:02
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 17:02
STD200 280-590907/29
IC
DB-624 (60.25) 0.25(mm)110/22/2022 17:23
ZZZZZ DB-624 (60.25) 0.25(mm)110/22/2022 17:23
8260C
Page 197 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VMS_X4
590924
Start Date:
End Date:10/23/2022 15:09
10/23/2022 12:37
BFB 280-590924/1 DB-624 (60.25) 0.25(mm)110/23/2022 12:37 X43682.D
ICV 280-590924/12 DB-624 (60.25) 0.25(mm)110/23/2022 15:09 X43688.D
8260C
Page 198 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC/MS VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VMS_X4
597688
Start Date:
End Date:12/25/2022 19:11
12/25/2022 09:04
BFB 280-597688/1 DB-624 (60.25) 0.25(mm)112/25/2022 09:04 X46337A.D
CCV 280-597688/2 DB-624 (60.25) 0.25(mm)112/25/2022 09:04 X46337.D
LCS 280-597688/1002 DB-624 (60.25) 0.25(mm)112/25/2022 09:04 -X46337-LCS.d
LCSD 280-597688/4 DB-624 (60.25) 0.25(mm)112/25/2022 09:32 X46338.D
CCV 280-597688/3 DB-624 (60.25) 0.25(mm)112/25/2022 09:53
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 09:53
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 10:13
MB 280-597688/7 DB-624 (60.25) 0.25(mm)112/25/2022 10:55 X46342.D
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 11:15
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 11:36
ZZZZZ DB-624 (60.25) 0.25(mm)20012/25/2022 11:58
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 12:18
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 12:39
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 13:00
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 13:20
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 13:41
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 14:02
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 14:22
280-170477-1 Offsite A-1 DB-624 (60.25) 0.25(mm)112/25/2022 14:43 X46353.D
280-170477-2 Offsite A-2 DB-624 (60.25) 0.25(mm)112/25/2022 15:04 X46354.D
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 15:24
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 15:45
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 16:05
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 16:26
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 16:47
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 17:07
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 17:28
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 17:49
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 18:09
ZZZZZ DB-624 (60.25) 0.25(mm)112/25/2022 18:30
CCVC 280-597688/34 DB-624 (60.25) 0.25(mm)112/25/2022 18:51
CCVC 280-597688/35 DB-624 (60.25) 0.25(mm)112/25/2022 19:11
8260C
Page 199 of 349
Page 200 of 349
Page 201 of 349
Page 202 of 349
Page 203 of 349
Page 204 of 349
Page 205 of 349
Page 206 of 349
Page 207 of 349
Lab Name:Job No.:
SDG No.:
GC/MS VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Seifert, Judy L10/22/22 11:07590907
Batch Method:
Eurofins Denver
8260C
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Acrolein_A
00015
Cal Dil Std
00104
mv-Cent BFB
00004
MV-Gas A 00136
2 uL 2 uL 5 uL8260CBFB
280-590907/1
5 mL 5 mL 5 uL8260CSTD005
280-590907/13
IC
5 mL 5 mL 10 uL8260CSTD010
280-590907/14
IC
5 mL 5 mL 20 uL8260CSTD020
280-590907/15
IC
5 mL 5 mL 2.5 uL 1 uL8260CSTD050
280-590907/16
IC
5 mL 5 mL 5 uL 2 uL8260CSTD10
280-590907/17
IC
5 mL 5 mL 25 uL 10 uL8260CICIS
280-590907/18
5 mL 5 mL 37.5 uL 15 uL8260CSTD75
280-590907/19
IC
5 mL 5 mL 50 uL 20 uL8260CSTD100
280-590907/20
IC
5 mL 5 mL 100 uL 40 uL8260CSTD200
280-590907/21
IC
5 mL 5 mL8260CICV
280-590907/22
Lab Sample ID Client Sample ID Method Chain Basis MV-Gas B 00120 mv-IS_SS 00049 MV-MegaMain B
00076
MV-MegaMainA
00078
8260CBFB
280-590907/1
5 uL8260CSTD005
280-590907/13
IC
5 uL8260CSTD010
280-590907/14
IC
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 28260C
Page 208 of 349
Lab Name:Job No.:
SDG No.:
GC/MS VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Seifert, Judy L10/22/22 11:07590907
Batch Method:
Eurofins Denver
8260C
Lab Sample ID Client Sample ID Method Chain Basis MV-Gas B 00120 mv-IS_SS 00049 MV-MegaMain B
00076
MV-MegaMainA
00078
5 uL8260CSTD020
280-590907/15
IC
5 uL 2.5 uL8260CSTD050
280-590907/16
IC
5 uL 5 uL8260CSTD10
280-590907/17
IC
5 uL 25 uL8260CICIS
280-590907/18
5 uL 37.5 uL8260CSTD75
280-590907/19
IC
5 uL 50 uL8260CSTD100
280-590907/20
IC
5 uL 100 uL8260CSTD200
280-590907/21
IC
10 uL 5 uL 25 uL8260CICV
280-590907/22
Batch Notes
Basis Basis Description
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 2 of 28260C
Page 209 of 349
Lab Name:Job No.:
SDG No.:
GC/MS VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Pepping, Andrew J10/23/22 12:37590924
Batch Method:
Eurofins Denver
8260C
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount mv-Cent BFB
00004
MV-ETOH_CUS B
00003
mv-IS_SS 00049 MV-Supp B 00054
2 uL 2 uL 5 uL8260CBFB
280-590924/1
5 mL 5 mL 25 uL 5 uL 25 uL8260CICV
280-590924/12
Batch Notes
Basis Basis Description
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 18260C
Page 210 of 349
Lab Name:Job No.:
SDG No.:
GC/MS VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Dobransky, Michael E12/25/22 09:04597688
Batch Method:
Eurofins Denver
8260C
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount mv-Cent BFB
00004
MV-Gas A 00139 mv-IS_SS 00053 MV-MegaMainA
00082
2 uL 2 uL 5 uL8260CBFB
280-597688/1
5 mL 5 mL 5 uL 5 uL 12.5 uL8260CCCV
280-597688/2
5 mL 5 mL 5 uL 5 uL 12.5 uL8260CLCSD
280-597688/4
5 mL 5 mL 5 uL8260CMB 280-597688/7
Offsite A-1 5 mL 5 mL 5 uL8260CT280-170477-D-1
Offsite A-2 5 mL 5 mL 5 uL8260CT280-170477-D-2
5 mL 5 mL 5 uL 5 uL 12.5 uL8260CLCS
280-597688/1002
Batch Notes
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 18260C
Page 211 of 349
Method RSK-175
Dissolved Gases (GC) by Method
RSK_175
Page 212 of 349
GC VOA LAB CONTROL SAMPLE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:J1984.DWater
Lab ID:LCS 280-597520/4 Client ID:
REC
%
REC
QC
LIMITSCONCENTRATION
(ug/L)
SPIKE
ADDED
(ug/L)
#
LCS LCS
COMPOUND
Methane 65.7 66.1 75-125101
FORM III RSK-175
# Column to be used to flag recovery and RPD values
Page 213 of 349
GC VOA LAB CONTROL SAMPLE DUPLICATE RECOVERY
FORM III
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:J1985.DWater
Lab ID:LCSD 280-597520/5 Client ID:
COMPOUND
SPIKE
ADDED CONCENTRATION %
REC
%
RPD
QC LIMITS
RPD REC (ug/L)(ug/L)
#
LCSD LCSD
65.7 65.2 20 75-125Methane199
FORM III RSK-175
# Column to be used to flag recovery and RPD values
Page 214 of 349
GC VOA DUPLICATE SUMMARY
Job No.:Lab Name:280-170477-1Eurofins Denver
SDG No.:
Level:Matrix:Low Lab File ID:J2000.DWater
Lab ID:280-170477-2 DU Client ID:Offsite A-2 DU
COMPOUND #
SAMPLE
CONCENTRATION
(ug/L)
DUPLICATE
(ug/L)%RPD
%RPD
LIMIT
CONCENTRATION
Methane JJ0.9950.92 8 20
RSK-175
# Column to be used to flag %RPD values
Page 215 of 349
FORM IV
GC VOA METHOD BLANK SUMMARY
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Date Analyzed:(1)
Instrument ID:(1)
GC Column:(1)ID:
Instrument ID:(2)
Date Extracted:
Date Analyzed:(2)
GC Column:(2)ID:Rt-Alumina KCl0.53(mm)0.53(mm)
VGC_J
12/21/2022 16:21
Lab File ID:(1)Lab File ID:(2)
Matrix:Water
J1986.D
Lab Sample ID:MB 280-597520/6
J1986.D
12/21/2022 16:21
VGC_J
HP-Plot Q
THIS METHOD BLANK APPLIES TO THE FOLLOWING SAMPLES:
ANALYZED 2
DATEDATE
ANALYZED 1LAB SAMPLE IDCLIENT SAMPLE ID
LCS 280-597520/4 12/21/2022 15:54 12/21/2022 15:54
LCSD 280-597520/5 12/21/2022 16:08 12/21/2022 16:08
280-170477-1Offsite A-1 12/21/2022 19:34 12/21/2022 19:34
280-170477-2Offsite A-2 12/21/2022 20:01 12/21/2022 20:01
280-170477-2 DUOffsite A-2 DU 12/21/2022 20:14 12/21/2022 20:14
FORM IV RSK-175
Page 216 of 349
FORM X
Client Sample ID:
Lab Name:Job No.:
SDG No.:
Lab Sample ID:280-170477-1
Instrument ID (1):Instrument ID (2):
Date Analyzed (1):Date Analyzed (2):
GC Column (1):ID:GC Column (2):ID:
Offsite A-1
Eurofins Denver 280-170477-1
IDENTIFICATION SUMMARY
0.53(mm)0.53(mm)
12/21/2022 19:34 12/21/2022 19:34
VGC_J VGC_J
HP-Plot Q Rt-Alumina KCl
ANALYTE COL PEAK RT RT WINDOW
FROM TO PEAK MEAN
CONCENTRATION RPD
1.691.611.641Methane 4.0 0.4
1.261.181.212 4.0
FORM X RSK-175
Page 217 of 349
FORM X
Client Sample ID:
Lab Name:Job No.:
SDG No.:
Lab Sample ID:280-170477-2
Instrument ID (1):Instrument ID (2):
Date Analyzed (1):Date Analyzed (2):
GC Column (1):ID:GC Column (2):ID:
Offsite A-2
Eurofins Denver 280-170477-1
IDENTIFICATION SUMMARY
0.53(mm)0.53(mm)
12/21/2022 20:01 12/21/2022 20:01
VGC_J VGC_J
HP-Plot Q Rt-Alumina KCl
ANALYTE COL PEAK RT RT WINDOW
FROM TO PEAK MEAN
CONCENTRATION RPD
1.691.611.641Methane 0.92 0.6
1.261.181.212 0.91
FORM X RSK-175
Page 218 of 349
FORM X
Client Sample ID:
Lab Name:Job No.:
SDG No.:
Lab Sample ID:280-170477-2 DU
Instrument ID (1):Instrument ID (2):
Date Analyzed (1):Date Analyzed (2):
GC Column (1):ID:GC Column (2):ID:
Offsite A-2 DU
Eurofins Denver 280-170477-1
IDENTIFICATION SUMMARY
0.53(mm)0.53(mm)
12/21/2022 20:14 12/21/2022 20:14
VGC_J VGC_J
HP-Plot Q Rt-Alumina KCl
ANALYTE COL PEAK RT RT WINDOW
FROM TO PEAK MEAN
CONCENTRATION RPD
1.691.611.651Methane 0.995 7.2
1.261.181.212 0.925
FORM X RSK-175
Page 219 of 349
FORM X
Client Sample ID:
Lab Name:Job No.:
SDG No.:
Lab Sample ID:LCS 280-597520/4
Instrument ID (1):Instrument ID (2):
Date Analyzed (1):Date Analyzed (2):
GC Column (1):ID:GC Column (2):ID:
Eurofins Denver 280-170477-1
IDENTIFICATION SUMMARY
0.53(mm)0.53(mm)
12/21/2022 15:54 12/21/2022 15:54
VGC_J VGC_J
HP-Plot Q Rt-Alumina KCl
ANALYTE COL PEAK RT RT WINDOW
FROM TO PEAK MEAN
CONCENTRATION RPD
1.691.611.651Methane 66.1 1.0
1.261.181.212 66.8
FORM X RSK-175
Page 220 of 349
FORM X
Client Sample ID:
Lab Name:Job No.:
SDG No.:
Lab Sample ID:LCSD 280-597520/5
Instrument ID (1):Instrument ID (2):
Date Analyzed (1):Date Analyzed (2):
GC Column (1):ID:GC Column (2):ID:
Eurofins Denver 280-170477-1
IDENTIFICATION SUMMARY
0.53(mm)0.53(mm)
12/21/2022 16:08 12/21/2022 16:08
VGC_J VGC_J
HP-Plot Q Rt-Alumina KCl
ANALYTE COL PEAK RT RT WINDOW
FROM TO PEAK MEAN
CONCENTRATION RPD
1.691.611.641Methane 65.2 1.9
1.261.181.212 66.4
FORM X RSK-175
Page 221 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-1 Lab Sample ID:280-170477-1
Matrix:J1997.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
12/14/2022 12:45
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 19:34
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.63J74-82-8 Methane 4.0
FORM I RSK-175
Page 222 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-2 Lab Sample ID:280-170477-2
Matrix:J1999.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
12/14/2022 11:00
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 20:01
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.63J74-82-8 Methane 0.92
FORM I RSK-175
Page 223 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VGC_J
Analy Batch No.:594440
73554Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
0.53(mm)GC Column:Rt-Alumina KClID:
RETENTION TIME SUMMARY
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
Level 1 IC 280-594440/4 J1044.D
Level 2 IC 280-594440/5 J1045.D
Level 3 IC 280-594440/6 J1046.D
Level 4 IC 280-594440/7 J1047.D
Level 5 IC 280-594440/8 J1048.D
Level 6 IC 280-594440/9 J1049.D
Level 7 IC 280-594440/10 J1050.D
Level 8 IC 280-594440/11 J1051.D
Level 9 IC 280-594440/12 J1052.D
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 AVG RTRT WINDOW
Methane 1.2081.169 - 1.2491.208 1.208 1.210 1.209 1.209 1.209 1.207 1.207 1.205
Ethane 1.4611.411 - 1.5111.461 1.464 1.462 1.460 1.461 1.460
Ethene 1.7481.696 - 1.7961.748 1.749 1.749 1.747 1.746 1.747
Propane 2.5082.446 - 2.5662.509 2.507 2.509 2.509 2.506 2.507
Acetylene 4.1254.041 - 4.2014.131 4.131 4.130 4.125 4.121 4.112
Butane 4.4094.327 - 4.4874.413 4.411 4.412 4.410 4.407 4.402
isobutylene 5.3245.242 - 5.4025.328 5.326 5.327 5.325 5.322 5.315
FORM VI RSK-175 Page 224 of 349
FORM VI
Lab Name:Job No.:
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:594440
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VGC_J
73554Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
0.53(mm)Rt-Alumina KClID:
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
1Level IC 280-594440/4 J1044.D
2Level IC 280-594440/5 J1045.D
3Level IC 280-594440/6 J1046.D
4Level IC 280-594440/7 J1047.D
5Level IC 280-594440/8 J1048.D
6Level IC 280-594440/9 J1049.D
7Level IC 280-594440/10 J1050.D
8Level IC 280-594440/11 J1051.D
9Level IC 280-594440/12 J1052.D
MIN R^2
OR COD
#R^2
OR COD
MAX
%RSD#%RSD#COEFFICIENT
M2M1B
CURVE
TYPELVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
/RSE /RSE
LVL 5 LVL 6 LVL 7 LVL 8
LVL 9
Methane Lin2 1.0000 0.9900133471868164548439485
38638 38844 40216 38076
37926
78114.372
4
38688.678
4
Ethane Ave 2.4 20.037358381874016038973
38560 38899
38689.692
8
Ethene Ave 2.5 20.038406381944084639737
39510 39552
39374.189
1
Propane Ave 3.0 20.036540376213993339014
38181 38147
38239.422
8
Acetylene Ave 2.5 20.028374295583053229421
29301 28839
29337.567
2
Butane Ave 2.7 20.038432385524125339742
39013 38993
39330.941
2
isobutylene Ave 2.2 20.036454363413843236973
36486 36487
36861.998
0
FORM VI RSK-175
Note: The M1 coefficient is the same as Ave CF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 225 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VGC_J
Analy Batch No.:594440
73554Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
GC Column:Rt-Alumina KClID:0.53(mm)
RESPONSE AND CONCENTRATION
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
Level 1 IC 280-594440/4 J1044.D
Level 2 IC 280-594440/5 J1045.D
Level 3 IC 280-594440/6 J1046.D
Level 4 IC 280-594440/7 J1047.D
Level 5 IC 280-594440/8 J1048.D
Level 6 IC 280-594440/9 J1049.D
Level 7 IC 280-594440/10 J1050.D
Level 8 IC 280-594440/11 J1051.D
Level 9 IC 280-594440/12 J1052.D
CURVE
TYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
LVL 6 LVL 6LVL 7 LVL 7LVL 8 LVL 8LVL 9 LVL 9
Methane Lin2 109618 142601 597693 2594265 5077236 0.821 1.64 13.1 65.7 131
10208583 65400484 247686566 740134626 263 1626 6505 19515
Ethane Ave 57518 117587 989301 4800335 9498907 1.54 3.08 24.6 123 246
19164973 493
Ethene Ave 55161 109711 938642 4565792 9079325 1.44 2.87 23.0 115 230
18178326 460
Propane Ave 82508 169896 1442697 7047561 13794006 2.26 4.52 36.1 181 361
27563548 723
Acetylene Ave 37833 78825 651380 3138327 6251021 1.33 2.67 21.3 107 213
12305009 427
Butane Ave 114370 229454 1964235 9461289 18575547 2.98 5.95 47.6 238 476
37132422 952
isobutylene Ave 104731 208817 1766626 8497786 16772055 2.87 5.75 46.0 230 460
33544265 919
Curve Type Legend
Ave = Average
Lin2 = Linear 1/conc^2
FORM VI RSK-175 Page 226 of 349
Calibration / Methane
Curve Type:Linear
Weighting:Conc_Sq
Origin:None
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:7.811E+04
Slope:3.869E+04
Error Coefficients
Standard Error:5930000
Relative Standard Error:2.2
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):1.000
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 0.821288 109618.0 133470.92218 Y
2 IC 280-594440/5 1.642575 142601.0 86815.518317 Y
3 IC 280-594440/6 13.1406 597693.0 45484.452765 Y
4 IC 280-594440/7 65.703 2594265.0 39484.726725 Y
5 IC 280-594440/8 131.406 5077236.0 38637.779097 Y
6 IC 280-594440/9 262.812 10208583.0 38843.671522 Y
7 IC 280-594440/10 1626.25 65400484.0 40215.516679 Y
8 IC 280-594440/11 6505.0 247686566.0 38076.336049 Y
9 IC 280-594440/12 19515.0 740134626.0 37926.447656 Y
Response = [7.811E+04] + [3.869E+04]x
Concentration
0 10000 20000
0.0
1.0
2.0
3.0
4.0
5.0
6.0
7.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
IC 280-594440/9
IC 280-594440/10
IC 280-594440/11
Intercept = -2.02
Page 227 of 349
Calibration / Ethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.869E+04
Error Coefficients
Standard Error:53400
Relative Standard Error:2.4
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.539625 57518.0 37358.447674 Y
2 IC 280-594440/5 3.07925 117587.0 38186.89616 Y
3 IC 280-594440/6 24.634 989301.0 40159.982139 Y
4 IC 280-594440/7 123.17 4800335.0 38973.248356 Y
5 IC 280-594440/8 246.34 9498907.0 38560.148575 Y
6 IC 280-594440/9 492.68 19164973.0 38899.43371 Y
Response = [3.869E+04]x
Concentration
0 100 200 300 400 500
0.0
0.5
1.0
1.5
2.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6 IC 280-594440/7
IC 280-594440/8
IC 280-594440/9
Page 228 of 349
Calibration / Ethylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.937E+04
Error Coefficients
Standard Error:46000
Relative Standard Error:2.5
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.43625 55161.0 38406.266319 Y
2 IC 280-594440/5 2.8725 109711.0 38193.559617 Y
3 IC 280-594440/6 22.98 938642.0 40846.040035 Y
4 IC 280-594440/7 114.9 4565792.0 39737.093124 Y
5 IC 280-594440/8 229.8 9079325.0 39509.682332 Y
6 IC 280-594440/9 459.6 18178326.0 39552.493473 Y
Response = [3.937E+04]x
Concentration
0 100 200 300 400 500
0.0
0.5
1.0
1.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/9
Page 229 of 349
Calibration / Propane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.824E+04
Error Coefficients
Standard Error:75200
Relative Standard Error:3.0
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.258 82508.0 36540.301151 Y
2 IC 280-594440/5 4.516 169896.0 37620.903454 Y
3 IC 280-594440/6 36.128 1442697.0 39932.932905 Y
4 IC 280-594440/7 180.64 7047561.0 39014.398804 Y
5 IC 280-594440/8 361.28 13794006.0 38180.928919 Y
6 IC 280-594440/9 722.56 27563548.0 38147.071523 Y
Response = [3.824E+04]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
0.5
1.0
1.5
2.0
2.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 230 of 349
Calibration / Acetylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:2.934E+04
Error Coefficients
Standard Error:96000
Relative Standard Error:2.5
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.333375 37833.0 28373.863317 Y
2 IC 280-594440/5 2.66675 78825.0 29558.451298 Y
3 IC 280-594440/6 21.334 651380.0 30532.48336 Y
4 IC 280-594440/7 106.67 3138327.0 29420.896222 Y
5 IC 280-594440/8 213.34 6251021.0 29300.745289 Y
6 IC 280-594440/9 426.68 12305009.0 28838.963626 Y
Response = [2.934E+04]x
Concentration
0 100 200 300 400 500
0.0
0.2
0.4
0.6
0.8
1.0
1.2
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 231 of 349
Calibration / Butane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.933E+04
Error Coefficients
Standard Error:170000
Relative Standard Error:2.7
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.975875 114370.0 38432.393834 Y
2 IC 280-594440/5 5.95175 229454.0 38552.35855 Y
3 IC 280-594440/6 47.614 1964235.0 41253.307851 Y
4 IC 280-594440/7 238.07 9461289.0 39741.626412 Y
5 IC 280-594440/8 476.14 18575547.0 39012.784055 Y
6 IC 280-594440/9 952.28 37132422.0 38993.176377 Y
Response = [3.933E+04]x
Concentration
0 100 200 300 400 500 600 700 800 900 1000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
3.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6 IC 280-594440/7
IC 280-594440/8
Page 232 of 349
Calibration / isobutylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.686E+04
Error Coefficients
Standard Error:176000
Relative Standard Error:2.2
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.873 104731.0 36453.532892 Y
2 IC 280-594440/5 5.746 208817.0 36341.280891 Y
3 IC 280-594440/6 45.968 1766626.0 38431.648103 Y
4 IC 280-594440/7 229.84 8497786.0 36972.615733 Y
5 IC 280-594440/8 459.68 16772055.0 36486.370954 Y
6 IC 280-594440/9 919.36 33544265.0 36486.539549 Y
Response = [3.686E+04]x
Concentration
0 100 200 300 400 500 600 700 800 900 1000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 233 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VGC_J
Analy Batch No.:594440
73555Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
0.53(mm)GC Column:HP-Plot Q ID:
RETENTION TIME SUMMARY
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
Level 1 IC 280-594440/4 J1044.D
Level 2 IC 280-594440/5 J1045.D
Level 3 IC 280-594440/6 J1046.D
Level 4 IC 280-594440/7 J1047.D
Level 5 IC 280-594440/8 J1048.D
Level 6 IC 280-594440/9 J1049.D
Level 7 IC 280-594440/10 J1050.D
Level 8 IC 280-594440/11 J1051.D
Level 9 IC 280-594440/12 J1052.D
ANALYTE LVL 1 LVL 2 LVL 3 LVL 4 LVL 5 LVL 6 LVL 7 LVL 8 LVL 9 AVG RTRT WINDOW
Methane 1.6411.600 - 1.6801.644 1.641 1.645 1.642 1.640 1.642 1.640 1.637 1.635
Ethene 2.5732.520 - 2.6202.574 2.575 2.575 2.572 2.570 2.570
Acetylene 2.7272.644 - 2.8042.726 2.732 2.730 2.727 2.724 2.725
Ethane 2.9932.940 - 3.0402.992 2.997 2.995 2.993 2.990 2.990
Propane 4.9144.854 - 4.9744.912 4.917 4.917 4.913 4.914 4.910
isobutylene 6.2626.180 - 6.3406.264 6.264 6.263 6.262 6.260 6.257
Butane 6.4186.335 - 6.4956.421 6.421 6.420 6.418 6.415 6.412
FORM VI RSK-175 Page 234 of 349
FORM VI
Lab Name:Job No.:
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1 Analy Batch No.:594440
CURVE EVALUATION
SDG No.:
Calibration ID:
Instrument ID:GC Column:Heated Purge: (Y/N)VGC_J
73555Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
0.53(mm)HP-Plot Q ID:
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
1Level IC 280-594440/4 J1044.D
2Level IC 280-594440/5 J1045.D
3Level IC 280-594440/6 J1046.D
4Level IC 280-594440/7 J1047.D
5Level IC 280-594440/8 J1048.D
6Level IC 280-594440/9 J1049.D
7Level IC 280-594440/10 J1050.D
8Level IC 280-594440/11 J1051.D
9Level IC 280-594440/12 J1052.D
MIN R^2
OR COD
#R^2
OR COD
MAX
%RSD#%RSD#COEFFICIENT
M2M1B
CURVE
TYPELVL 4LVL 3LVL 2LVL 1
CFANALYTE MIN CF
/RSE /RSE
LVL 5 LVL 6 LVL 7 LVL 8
LVL 9
Methane Lin2 0.9980 0.9900102690736824067936141
35354 34964 35866 34239
34390
56861.433
4
35362.802
8
Ethene Ave 3.5 20.029622307793281531833
31597 31816
31410.324
9
Acetylene Ave 3.9 20.031635324953530234097
34114 33769
33568.692
0
Ethane Ave 3.1 20.034219336443668435613
35295 35549
35167.435
9
Propane Ave 2.8 20.032741340343573834443
34083 34113
34192.007
6
isobutylene Ave 2.9 20.033763331013374032153
31748 31700
32700.898
5
Butane Ave 3.5 20.038216368623765735891
35304 35169
36516.311
7
FORM VI RSK-175
Note: The M1 coefficient is the same as Ave CF for an Ave curve type. RSD is calculated for Ave curve types. RSE is used for all other types.
Page 235 of 349
FORM VI
Lab Name:Job No.:
Calibration ID:
SDG No.:
Instrument ID:Heated Purge: (Y/N)
GC VOA BY EXTERNAL STANDARD - INITIAL CALIBRATION DATA
Eurofins Denver 280-170477-1
VGC_J
Analy Batch No.:594440
73555Calibration Start Date:Calibration End Date:11/22/2022 16:02
N
11/22/2022 17:53
GC Column:HP-Plot Q ID:0.53(mm)
RESPONSE AND CONCENTRATION
Calibration Files
LEVEL:LAB SAMPLE ID:LAB FILE ID:
Level 1 IC 280-594440/4 J1044.D
Level 2 IC 280-594440/5 J1045.D
Level 3 IC 280-594440/6 J1046.D
Level 4 IC 280-594440/7 J1047.D
Level 5 IC 280-594440/8 J1048.D
Level 6 IC 280-594440/9 J1049.D
Level 7 IC 280-594440/10 J1050.D
Level 8 IC 280-594440/11 J1051.D
Level 9 IC 280-594440/12 J1052.D
CURVE
TYPE
RESPONSEANALYTE CONCENTRATION (UG/L)
LVL 1 LVL 1LVL 2 LVL 2LVL 3 LVL 3LVL 4 LVL 4LVL 5 LVL 5
LVL 6 LVL 6LVL 7 LVL 7LVL 8 LVL 8LVL 9 LVL 9
Methane Lin2 84338 121029 534550 2374559 4645758 0.821 1.64 13.1 65.7 131
9189020 58327040 222721558 671116476 263 1626 6505 19515
Ethene Ave 42544 88414 754091 3657619 7261000 1.44 2.87 23.0 115 230
14622496 460
Acetylene Ave 42181 86657 753138 3637167 7277797 1.33 2.67 21.3 107 213
14408475 427
Ethane Ave 52685 103599 903672 4386486 8694621 1.54 3.08 24.6 123 246
17514088 493
Propane Ave 73929 153698 1291157 6221833 12313361 2.26 4.52 36.1 181 361
24648508 723
isobutylene Ave 97000 190198 1550959 7390142 14593944 2.87 5.75 46.0 230 460
29144072 919
Butane Ave 113725 219395 1792980 8544605 16809482 2.98 5.95 47.6 238 476
33490336 952
Curve Type Legend
Ave = Average
Lin2 = Linear 1/conc^2
FORM VI RSK-175 Page 236 of 349
Calibration / Methane
Curve Type:Linear
Weighting:Conc_Sq
Origin:None
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:5.686E+04
Slope:3.536E+04
Error Coefficients
Standard Error:7720000
Relative Standard Error:4.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 0.821288 84338.0 102689.983715 Y
2 IC 280-594440/5 1.642575 121029.0 73682.480252 Y
3 IC 280-594440/6 13.1406 534550.0 40679.268831 Y
4 IC 280-594440/7 65.703 2374559.0 36140.800268 Y
5 IC 280-594440/8 131.406 4645758.0 35354.2304 Y
6 IC 280-594440/9 262.812 9189020.0 34964.232988 Y
7 IC 280-594440/10 1626.25 58327040.0 35865.973866 Y
8 IC 280-594440/11 6505.0 222721558.0 34238.517756 Y
9 IC 280-594440/12 19515.0 671116476.0 34389.775865 Y
Response = [5.686E+04] + [3.536E+04]x
Concentration
0 10000 20000
0.0
1.0
2.0
3.0
4.0
5.0
6.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
IC 280-594440/9
IC 280-594440/10
IC 280-594440/11
Intercept = -1.61
Page 237 of 349
Calibration / Ethylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.141E+04
Error Coefficients
Standard Error:89400
Relative Standard Error:3.5
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.43625 42544.0 29621.583986 Y
2 IC 280-594440/5 2.8725 88414.0 30779.4604 Y
3 IC 280-594440/6 22.98 754091.0 32815.100087 Y
4 IC 280-594440/7 114.9 3657619.0 31833.063534 Y
5 IC 280-594440/8 229.8 7261000.0 31597.040905 Y
6 IC 280-594440/9 459.6 14622496.0 31815.700609 Y
Response = [3.141E+04]x
Concentration
0 100 200 300 400 500
0.0
0.5
1.0
1.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/9
Page 238 of 349
Calibration / Acetylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.357E+04
Error Coefficients
Standard Error:71200
Relative Standard Error:3.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.333375 42181.0 31634.761414 Y
2 IC 280-594440/5 2.66675 86657.0 32495.35952 Y
3 IC 280-594440/6 21.334 753138.0 35302.240555 Y
4 IC 280-594440/7 106.67 3637167.0 34097.375082 Y
5 IC 280-594440/8 213.34 7277797.0 34113.607387 Y
6 IC 280-594440/9 426.68 14408475.0 33768.808006 Y
Response = [3.357E+04]x
Concentration
0 100 200 300 400 500
0.0
0.5
1.0
1.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
IC 280-594440/9
Page 239 of 349
Calibration / Ethane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.517E+04
Error Coefficients
Standard Error:90200
Relative Standard Error:3.1
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 1.539625 52685.0 34219.3716 Y
2 IC 280-594440/5 3.07925 103599.0 33644.23155 Y
3 IC 280-594440/6 24.634 903672.0 36683.932776 Y
4 IC 280-594440/7 123.17 4386486.0 35613.266217 Y
5 IC 280-594440/8 246.34 8694621.0 35295.205813 Y
6 IC 280-594440/9 492.68 17514088.0 35548.607615 Y
Response = [3.517E+04]x
Concentration
0 100 200 300 400 500
0.0
0.5
1.0
1.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6 IC 280-594440/7
IC 280-594440/9
Page 240 of 349
Calibration / Propane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.419E+04
Error Coefficients
Standard Error:44800
Relative Standard Error:2.8
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.258 73929.0 32740.921169 Y
2 IC 280-594440/5 4.516 153698.0 34034.100974 Y
3 IC 280-594440/6 36.128 1291157.0 35738.402347 Y
4 IC 280-594440/7 180.64 6221833.0 34443.273915 Y
5 IC 280-594440/8 361.28 12313361.0 34082.597985 Y
6 IC 280-594440/9 722.56 24648508.0 34112.749114 Y
Response = [3.419E+04]x
Concentration
0 100 200 300 400 500 600 700 800
0.0
0.5
1.0
1.5
2.0
2.5
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 241 of 349
Calibration / isobutylene
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.27E+04
Error Coefficients
Standard Error:460000
Relative Standard Error:2.9
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.999
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.873 97000.0 33762.617473 Y
2 IC 280-594440/5 5.746 190198.0 33100.939784 Y
3 IC 280-594440/6 45.968 1550959.0 33739.971284 Y
4 IC 280-594440/7 229.84 7390142.0 32153.41977 Y
5 IC 280-594440/8 459.68 14593944.0 31748.050818 Y
6 IC 280-594440/9 919.36 29144072.0 31700.391577 Y
Response = [3.27E+04]x
Concentration
0 100 200 300 400 500 600 700 800 900 1000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 242 of 349
Calibration / Butane
Curve Type:Average
Weighting:Conc_Sq
Origin:Force
Dependency:Response
Calib Mode:ESTD
Response Base:AREA
RF Rounding:0
Curve Coefficients
Intercept:0
Slope:3.652E+04
Error Coefficients
Standard Error:633000
Relative Standard Error:3.5
Correlation Coefficient:1.000
Coefficient of Determination (Adjusted):0.998
ID Level Concentration Response IS Amount IS Response RF Used
1 IC 280-594440/4 2.975875 113725.0 38215.650859 Y
2 IC 280-594440/5 5.95175 219395.0 36862.2674 Y
3 IC 280-594440/6 47.614 1792980.0 37656.571597 Y
4 IC 280-594440/7 238.07 8544605.0 35891.145461 Y
5 IC 280-594440/8 476.14 16809482.0 35303.654387 Y
6 IC 280-594440/9 952.28 33490336.0 35168.58067 Y
Response = [3.652E+04]x
Concentration
0 100 200 300 400 500 600 700 800 900 1000
0.0
0.5
1.0
1.5
2.0
2.5
3.0
Re
s
p
o
n
s
e

(

X

1
0
0
0
0
0
0
0
)
IC 280-594440/4
IC 280-594440/5
IC 280-594440/6
IC 280-594440/7
IC 280-594440/8
Page 243 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
11/22/2022 18:34
11/22/2022 16:02
11/22/2022 17:53
ICV 280-594440/14
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1055.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 38010 62.5 65.7 -4.8 20.0Lin2
Ethane 3561538690 113 123 -7.9 20.0Ave
Ethene 3758339374 110 115 -4.5 20.0Ave
Propane 3858538239 182 181 0.9 20.0Ave
Acetylene 2960729338 108 107 0.9 20.0Ave
Butane 3997239331 242 238 1.6 20.0Ave
isobutylene 3885436862 242 230 5.4 20.0Ave
FORM VII RSK-175
Page 244 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
11/22/2022 18:34
11/22/2022 16:02
11/22/2022 17:53
ICV 280-594440/14
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1055.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.21 1.17 1.25
Ethane 1.46 1.41 1.51
Ethene 1.75 1.70 1.80
Propane 2.51 2.45 2.57
Acetylene 4.13 4.04 4.20
Butane 4.41 4.33 4.49
isobutylene 5.33 5.24 5.40
Form VII RSK-175
Page 245 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
11/22/2022 18:34
11/22/2022 16:02
11/22/2022 17:53
ICV 280-594440/14
HP-Plot Q
Eurofins Denver
Lab File ID:J1055.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 36242 65.7 65.7 0.0 20.0Lin2
Ethene 3166031410 116 115 0.8 20.0Ave
Acetylene 3426133569 109 107 2.1 20.0Ave
Ethane 3408035167 119 123 -3.1 20.0Ave
Propane 3493734192 185 181 2.2 20.0Ave
isobutylene 3307232701 232 230 1.1 20.0Ave
Butane 3547536516 231 238 -2.9 20.0Ave
FORM VII RSK-175
Page 246 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
11/22/2022 18:34
11/22/2022 16:02
11/22/2022 17:53
ICV 280-594440/14
HP-Plot Q
Eurofins Denver
Lab File ID:J1055.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.64 1.60 1.68
Ethene 2.57 2.52 2.62
Acetylene 2.72 2.64 2.80
Ethane 2.99 2.94 3.04
Propane 4.91 4.85 4.97
isobutylene 6.26 6.18 6.34
Butane 6.42 6.34 6.50
Form VII RSK-175
Page 247 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 15:19
11/22/2022 16:02
11/22/2022 17:53
CCVRT 280-597520/2
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1982.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 39992 65.9 65.7 0.3 20.0Lin2
Ethane 3936938690 125 123 1.8 20.0Ave
Ethene 3991939374 116 115 1.4 20.0Ave
Propane 3900838239 184 181 2.0 20.0Ave
Acetylene 2909129338 106 107 -0.8 20.0Ave
Butane 4034939331 244 238 2.6 20.0Ave
isobutylene 3837936862 239 230 4.1 20.0Ave
FORM VII RSK-175
Page 248 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 15:19
11/22/2022 16:02
11/22/2022 17:53
CCVRT 280-597520/2
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1982.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.22 1.18 1.26
Ethane 1.47 1.42 1.52
Ethene 1.74 1.69 1.79
Propane 2.49 2.43 2.55
Acetylene 4.07 3.99 4.15
Butane 4.37 4.29 4.45
isobutylene 5.29 5.21 5.37
Form VII RSK-175
Page 249 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 15:19
11/22/2022 16:02
11/22/2022 17:53
CCVRT 280-597520/2
HP-Plot Q
Eurofins Denver
Lab File ID:J1982.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 35987 65.3 65.7 -0.7 20.0Lin2
Ethene 3197531410 117 115 1.8 20.0Ave
Acetylene 3381133569 107 107 0.7 20.0Ave
Ethane 3596735167 126 123 2.3 20.0Ave
Propane 3509934192 185 181 2.7 20.0Ave
isobutylene 3251332701 229 230 -0.6 20.0Ave
Butane 3631536516 237 238 -0.6 20.0Ave
FORM VII RSK-175
Page 250 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 15:19
11/22/2022 16:02
11/22/2022 17:53
CCVRT 280-597520/2
HP-Plot Q
Eurofins Denver
Lab File ID:J1982.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.65 1.61 1.69
Ethene 2.59 2.54 2.64
Acetylene 2.74 2.66 2.82
Ethane 3.01 2.96 3.06
Propane 4.92 4.86 4.98
isobutylene 6.27 6.19 6.35
Butane 6.42 6.34 6.50
Form VII RSK-175
Page 251 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 19:47
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/18
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1998.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 40146 66.2 65.7 0.7 20.0Lin2
Ethane 3945738690 126 123 2.0 20.0Ave
Ethene 3982739374 116 115 1.1 20.0Ave
Propane 3890138239 184 181 1.7 20.0Ave
Acetylene 2868929338 104 107 -2.2 20.0Ave
Butane 4070539331 246 238 3.5 20.0Ave
isobutylene 3786736862 236 230 2.7 20.0Ave
FORM VII RSK-175
Page 252 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 19:47
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/18
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J1998.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.21 1.18 1.26
Ethane 1.46 1.42 1.52
Ethene 1.75 1.69 1.79
Propane 2.51 2.43 2.55
Acetylene 4.13 3.99 4.15
Butane 4.41 4.29 4.45
isobutylene 5.33 5.21 5.37
Form VII RSK-175
Page 253 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 19:47
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/18
HP-Plot Q
Eurofins Denver
Lab File ID:J1998.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 36071 65.4 65.7 -0.4 20.0Lin2
Ethene 3209931410 117 115 2.2 20.0Ave
Acetylene 3328533569 106 107 -0.8 20.0Ave
Ethane 3625235167 127 123 3.1 20.0Ave
Propane 3556334192 188 181 4.0 20.0Ave
isobutylene 3215432701 226 230 -1.7 20.0Ave
Butane 3607636516 235 238 -1.2 20.0Ave
FORM VII RSK-175
Page 254 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 19:47
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/18
HP-Plot Q
Eurofins Denver
Lab File ID:J1998.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.64 1.61 1.69
Ethene 2.58 2.54 2.64
Acetylene 2.73 2.66 2.82
Ethane 3.00 2.96 3.06
Propane 4.92 4.86 4.98
isobutylene 6.26 6.19 6.35
Butane 6.42 6.34 6.50
Form VII RSK-175
Page 255 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 22:28
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/30
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J2010.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 39697 65.4 65.7 -0.5 20.0Lin2
Ethane 3860438690 123 123 -0.2 20.0Ave
Ethene 3904339374 114 115 -0.8 20.0Ave
Propane 3771138239 178 181 -1.4 20.0Ave
Acetylene 2774929338 101 107 -5.4 20.0Ave
Butane 3783739331 229 238 -3.8 20.0Ave
isobutylene 3564336862 222 230 -3.3 20.0Ave
FORM VII RSK-175
Page 256 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 22:28
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/30
Rt-Alumina KCl
Eurofins Denver
Lab File ID:J2010.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.21 1.18 1.26
Ethane 1.46 1.42 1.52
Ethene 1.75 1.69 1.79
Propane 2.52 2.43 2.55
Acetylene 4.13 3.99 4.15
Butane 4.42 4.29 4.45
isobutylene 5.33 5.21 5.37
Form VII RSK-175
Page 257 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION DATA
0.53(mm)
280-170477-1
VGC_J
12/21/2022 22:28
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/30
HP-Plot Q
Eurofins Denver
Lab File ID:J2010.D Heated Purge: (Y/N)NConc. Units:ug/L
ANALYTE CURVE CALC SPIKE %D MAX
TYPE AMOUNT AMOUNT %D
AVE CF CF MIN CF
Methane 35977 65.2 65.7 -0.7 20.0Lin2
Ethene 3145431410 115 115 0.1 20.0Ave
Acetylene 3259933569 104 107 -2.9 20.0Ave
Ethane 3520235167 123 123 0.1 20.0Ave
Propane 3436134192 182 181 0.5 20.0Ave
isobutylene 3043232701 214 230 -6.9 20.0Ave
Butane 3413136516 223 238 -6.5 20.0Ave
FORM VII RSK-175
Page 258 of 349
FORM VII
Lab Name:Job No.:
SDG No.:
Instrument ID:
Calibration Date:
Calib Start Date:
Lab Sample ID:
Calib End Date:GC Column: ID:
GC VOA CONTINUING CALIBRATION RETENTION TIME SUMMARY
0.53(mm)
280-170477-1
VGC_J
12/21/2022 22:28
11/22/2022 16:02
11/22/2022 17:53
CCV 280-597520/30
HP-Plot Q
Eurofins Denver
Lab File ID:J2010.D Heated Purge: (Y/N)N
Analyte RT TOFROM
RT WINDOW
Methane 1.65 1.61 1.69
Ethene 2.58 2.54 2.64
Acetylene 2.73 2.66 2.82
Ethane 3.00 2.96 3.06
Propane 4.92 4.86 4.98
isobutylene 6.26 6.19 6.35
Butane 6.42 6.34 6.50
Form VII RSK-175
Page 259 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:MB 280-597520/6
Matrix:J1986.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 16:21
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:5.0
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.6374-82-8 Methane ND
FORM I RSK-175
Page 260 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCS 280-597520/4
Matrix:J1984.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 15:54
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:5.0
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.6374-82-8 Methane 66.1
FORM I RSK-175
Page 261 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Lab Sample ID:LCSD 280-597520/5
Matrix:J1985.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 16:08
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:5.0
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.6374-82-8 Methane 65.2
FORM I RSK-175
Page 262 of 349
FORM I
GC VOA ORGANICS ANALYSIS DATA SHEET
Lab Name:Job No.:280-170477-1Eurofins Denver
SDG No.:
Client Sample ID:Offsite A-2 DU Lab Sample ID:280-170477-2 DU
Matrix:J2000.DLab File ID:
Date Collected:RSK-175Analysis Method:
Water
12/14/2022 11:00
Sample wt/vol:
% Moisture:
GC Column:Soil Extract Vol.:
Dilution Factor:Soil Aliquot Vol:1
Level: (low/med)Low
18(mL)
0.53(mm)
Date Analyzed:12/21/2022 20:14
ID:HP-Plot Q
% Solids:
NHeated Purge: (Y/N)Purge Volume:pH:
Analysis Batch No.:597520 ug/LUnits:
CAS NO.COMPOUND NAME RESULT Q MDLRL
5.0 0.63J74-82-8 Methane 0.995
FORM I RSK-175
Page 263 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VGC_J
594440
Start Date:
End Date:11/22/2022 18:34
11/22/2022 14:36
CCVRT 280-594440/1
RTC
Rt-Alumina KCl 0.53(mm)111/22/2022 14:36
CCVRT 280-594440/1
RTC
HP-Plot Q 0.53(mm)111/22/2022 14:36
CCV 280-594440/2 Rt-Alumina KCl 0.53(mm)111/22/2022 14:49
CCV 280-594440/2 HP-Plot Q 0.53(mm)111/22/2022 14:49
ZZZZZ Rt-Alumina KCl 0.53(mm)111/22/2022 15:03
ZZZZZ HP-Plot Q 0.53(mm)111/22/2022 15:03
IC 280-594440/4 Rt-Alumina KCl 0.53(mm)111/22/2022 16:02 J1044.D
IC 280-594440/4 HP-Plot Q 0.53(mm)111/22/2022 16:02 J1044.D
IC 280-594440/5 Rt-Alumina KCl 0.53(mm)111/22/2022 16:16 J1045.D
IC 280-594440/5 HP-Plot Q 0.53(mm)111/22/2022 16:16 J1045.D
IC 280-594440/6 Rt-Alumina KCl 0.53(mm)111/22/2022 16:30 J1046.D
IC 280-594440/6 HP-Plot Q 0.53(mm)111/22/2022 16:30 J1046.D
IC 280-594440/7 Rt-Alumina KCl 0.53(mm)111/22/2022 16:44 J1047.D
IC 280-594440/7 HP-Plot Q 0.53(mm)111/22/2022 16:44 J1047.D
IC 280-594440/8 Rt-Alumina KCl 0.53(mm)111/22/2022 16:57 J1048.D
IC 280-594440/8 HP-Plot Q 0.53(mm)111/22/2022 16:57 J1048.D
IC 280-594440/9 Rt-Alumina KCl 0.53(mm)111/22/2022 17:11 J1049.D
IC 280-594440/9 HP-Plot Q 0.53(mm)111/22/2022 17:11 J1049.D
IC 280-594440/10 Rt-Alumina KCl 0.53(mm)111/22/2022 17:25 J1050.D
IC 280-594440/10 HP-Plot Q 0.53(mm)111/22/2022 17:25 J1050.D
IC 280-594440/11 Rt-Alumina KCl 0.53(mm)111/22/2022 17:39 J1051.D
IC 280-594440/11 HP-Plot Q 0.53(mm)111/22/2022 17:39 J1051.D
IC 280-594440/12 Rt-Alumina KCl 0.53(mm)111/22/2022 17:53 J1052.D
IC 280-594440/12 HP-Plot Q 0.53(mm)111/22/2022 17:53 J1052.D
ZZZZZ Rt-Alumina KCl 0.53(mm)111/22/2022 18:07
ZZZZZ HP-Plot Q 0.53(mm)111/22/2022 18:07
ICV 280-594440/14 Rt-Alumina KCl 0.53(mm)111/22/2022 18:34 J1055.D
ICV 280-594440/14 HP-Plot Q 0.53(mm)111/22/2022 18:34 J1055.D
RSK-175
Page 264 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VGC_J
597520
Start Date:
End Date:12/21/2022 22:28
12/21/2022 15:19
CCVRT 280-597520/2 Rt-Alumina KCl 0.53(mm)112/21/2022 15:19 J1982.D
CCVRT 280-597520/2 HP-Plot Q 0.53(mm)112/21/2022 15:19 J1982.D
LCS 280-597520/4 Rt-Alumina KCl 0.53(mm)112/21/2022 15:54 J1984.D
LCS 280-597520/4 HP-Plot Q 0.53(mm)112/21/2022 15:54 J1984.D
LCSD 280-597520/5 Rt-Alumina KCl 0.53(mm)112/21/2022 16:08 J1985.D
LCSD 280-597520/5 HP-Plot Q 0.53(mm)112/21/2022 16:08 J1985.D
MB 280-597520/6 Rt-Alumina KCl 0.53(mm)112/21/2022 16:21 J1986.D
MB 280-597520/6 HP-Plot Q 0.53(mm)112/21/2022 16:21 J1986.D
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 17:19
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 17:19
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 17:33
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 17:33
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 17:46
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 17:46
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 17:59
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 17:59
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 18:13
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 18:13
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 18:26
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 18:26
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 18:40
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 18:40
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 18:53
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 18:53
ZZZZZ Rt-Alumina KCl 0.53(mm)40012/21/2022 19:07
ZZZZZ HP-Plot Q 0.53(mm)40012/21/2022 19:07
ZZZZZ Rt-Alumina KCl 0.53(mm)40012/21/2022 19:20
ZZZZZ HP-Plot Q 0.53(mm)40012/21/2022 19:20
280-170477-1 Offsite A-1 Rt-Alumina KCl 0.53(mm)112/21/2022 19:34 J1997.D
280-170477-1 Offsite A-1 HP-Plot Q 0.53(mm)112/21/2022 19:34 J1997.D
CCV 280-597520/18 Rt-Alumina KCl 0.53(mm)112/21/2022 19:47 J1998.D
CCV 280-597520/18 HP-Plot Q 0.53(mm)112/21/2022 19:47 J1998.D
280-170477-2 Offsite A-2 Rt-Alumina KCl 0.53(mm)112/21/2022 20:01 J1999.D
280-170477-2 Offsite A-2 HP-Plot Q 0.53(mm)112/21/2022 20:01 J1999.D
280-170477-2 DU Offsite A-2 DU Rt-Alumina KCl 0.53(mm)112/21/2022 20:14 J2000.D
280-170477-2 DU Offsite A-2 DU HP-Plot Q 0.53(mm)112/21/2022 20:14 J2000.D
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 20:27
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 20:27
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 20:41
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 20:41
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 20:54
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 20:54
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 21:08
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 21:08
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 21:21
RSK-175
Page 265 of 349
Lab Name:Job No.:
SDG No.:
Instrument ID:
Analysis Batch Number:
GC VOA ANALYSIS RUN LOG
DILUTION
FACTOR
COLUMN IDDATE ANALYZEDLAB SAMPLE ID CLIENT SAMPLE ID LAB FILE ID
Eurofins Denver 280-170477-1
VGC_J
597520
Start Date:
End Date:12/21/2022 22:28
12/21/2022 15:19
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 21:21
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 21:35
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 21:35
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 21:48
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 21:48
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 22:01
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 22:01
ZZZZZ Rt-Alumina KCl 0.53(mm)112/21/2022 22:15
ZZZZZ HP-Plot Q 0.53(mm)112/21/2022 22:15
CCV 280-597520/30 Rt-Alumina KCl 0.53(mm)112/21/2022 22:28 J2010.D
CCV 280-597520/30 HP-Plot Q 0.53(mm)112/21/2022 22:28 J2010.D
RSK-175
Page 266 of 349
Lab Name:Job No.:
SDG No.:
GC VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Scianna, Charles A11/22/22 14:36594440
Batch Method:
Eurofins Denver
RSK-175
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount RSK175methane
00011
RSK7gasMathes
00034
RSK7gasMathes
00035
20 mL 20 mL 2.5 uLRSK-175IC 280-594440/4
20 mL 20 mL 5 uLRSK-175IC 280-594440/5
20 mL 20 mL 40 uLRSK-175IC 280-594440/6
20 mL 20 mL 200 uLRSK-175IC 280-594440/7
20 mL 20 mL 400 uLRSK-175IC 280-594440/8
20 mL 20 mL 800 uLRSK-175IC 280-594440/9
20 mL 20 mL 50 uLRSK-175IC
280-594440/10
20 mL 20 mL 200 uLRSK-175IC
280-594440/11
20 mL 20 mL 600 uLRSK-175IC
280-594440/12
20 mL 20 mL 200 uLRSK-175ICV
280-594440/14
Batch Notes
Basis Basis Description
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1RSK-175
Page 267 of 349
Lab Name:Job No.:
SDG No.:
GC VOA BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Hiltner, Joseph P12/21/22 15:19597520
Batch Method:
Eurofins Denver
RSK-175
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Initial pH RSK7gasMathes
00035
18 mL 18 mL 5 SU 200 uLRSK-175CCVRT
280-597520/2
18 mL 18 mL 5 SU 200 uLRSK-175LCS
280-597520/4
18 mL 18 mL 5 SU 200 uLRSK-175LCSD
280-597520/5
18 mL 18 mL 5 SURSK-175MB 280-597520/6
Offsite A-1 18 mL 18 mL < 2 SURSK-175 T280-170477-G-1
18 mL 18 mL 5 SU 200 uLRSK-175CCV
280-597520/18
Offsite A-2 18 mL 18 mL < 2 SURSK-175 T280-170477-F-2
Offsite A-2 18 mL 18 mL < 2 SURSK-175 T280-170477-G-2
DU
18 mL 18 mL 5 SU 200 uLRSK-175CCV
280-597520/30
Batch Notes
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1RSK-175
Page 268 of 349
METALS
Page 269 of 349
COVER PAGE
Lab Name: Job Number:
Client Sample ID Lab Sample ID
METALS
Project:GE-Salt Lake City, Utah
SDG No.:
280-170477-1Eurofins Denver
280-170477-1 Offsite A-1
280-170477-2 Offsite A-2
Comments:
Page 270 of 349
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name:Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 280-170477-1
Date Received:12/16/2022 09:15

280-170477-1
Offsite A-1
Water 12/14/2022 12:45Date Sampled:
Reporting Basis:WET
METALS
Eurofins Denver
CAS No.Analyte CUnits Q MethodRLMDLDILResult
7439-89-6 Iron 2400 ug/L5022 1 6020B
FORM IA-IN Page 271 of 349
1A-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name:Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 280-170477-2
Date Received:12/16/2022 09:15

280-170477-1
Offsite A-2
Water 12/14/2022 11:00Date Sampled:
Reporting Basis:WET
METALS
Eurofins Denver
CAS No.Analyte CUnits Q MethodRLMDLDILResult
7439-89-6 Iron 990 ug/L5022 1 6020B
FORM IA-IN Page 272 of 349
2A-IN
Lab Name:Job No.:
SDG No.:
Concentration Units:
CALIBRATION VERIFICATIONS
METALS
ICV Source:
CCV Source:
Eurofins Denver 280-170477-1
ug/Lms 77 icv_02882
ms 77 ccv_02880
Analyte
ICV 280-597704/15
12/22/2022 17:28
Found C True %R
CCV 280-597704/42
12/22/2022 18:18
CCV 280-597704/54
12/22/2022 18:40
Found FoundC CTrue%R True %R
Iron 820 1020 10308001000 1000103102 103
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Italicized analytes were not requested for this sequence.
Page 273 of 349
2A-IN
Lab Name:Job No.:
SDG No.:
Concentration Units:
CALIBRATION VERIFICATIONS
METALS
ICV Source:
CCV Source:
Eurofins Denver 280-170477-1
ug/Lms 77 icv_02882
ms 77 ccv_02880
Analyte
CCV 280-597704/64
12/22/2022 18:59
Found C True %R
CCV 280-597704/74
12/22/2022 19:18
Found FoundC CTrue%R True %R
Iron 1070 10201000 1000107 102
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Italicized analytes were not requested for this sequence.
Page 274 of 349
2B-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
CRQL CHECK STANDARD
METALS
Method:6020B Instrument ID:MT_079
Eurofins Denver
Lab Sample ID:
Analyte True Found Qualifiers %R(1)Limits
CRI 280-597704/25
CRQL Check Standard
CRQL Check Standard Source:MS 77 LLCCV_02699
Concentration Units:ug/L
80-120Iron50.0 51.3 103
FORM IIB-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 275 of 349
Lab Name:Job No.:
Concentration Units:
SDG No.:
INSTRUMENT BLANKS
METALS
Eurofins Denver 280-170477-1
ug/L
CFoundCFoundCFoundCFoundRLAnalyte
ICB 280-597704/16 CCB 280-597704/43 CCB 280-597704/55 CCB 280-597704/65
12/22/2022 17:30 12/22/2022 18:20 12/22/2022 18:42 12/22/2022 19:01
3-IN
Iron ND ND ND ND50
FORM III-IN
Italicized analytes were not requested for this sequence.
Page 276 of 349
Lab Name:Job No.:
Concentration Units:
SDG No.:
INSTRUMENT BLANKS
METALS
Eurofins Denver 280-170477-1
ug/L
CFoundCFoundCFoundCFoundRLAnalyte
CCB 280-597704/75
12/22/2022 19:20
3-IN
Iron ND50
FORM III-IN
Italicized analytes were not requested for this sequence.
Page 277 of 349
Lab Name:Job No.:
SDG No.:
Lab Sample ID: MB 280-597451/1-AConcentration Units:ug/L
CAS No.Analyte Concentration C Q Method
3-IN
Batch No.:

280-170477-1
Instrument Code:MT_079
METHOD BLANK
METALS
597704
Eurofins Denver
7439-89-6 Iron ND 6020B
FORM III-IN
Page 278 of 349
4A-IN
Lab Name:Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
Percent
Recovery
Found
SDG No.:
Lab File ID:
Solution A Solution A
Lab Sample ID:
Eurofins Denver 280-170477-1
ICSA 280-597704/18
091ICSA.d
ug/L
ms 77 icsa_00656
MT_079
INTERFERENCE CHECK STANDARD
METALS
101767Iron100000 102
96294Aluminum100000 96
0.245Antimony
0.324Arsenic
1.65Barium
0.0570Beryllium
57.7Boron
0.231Cadmium
103614Calcium100000 104
1.25Chromium
0.260Cobalt
0.303Copper
0.224Lead
1.04Li
6.35Li
94322Magnesium100000 94
0.359Manganese
2092Molybdenum2000 105
0.293Nickel
94085Potassium100000 94
0.115Selenium
0.0630Silver
96418Sodium100000 96
0.820Strontium
0.104Thallium
0.157Thorium
0.246Tin
0.0560Uranium
0.0790Vanadium
0.998Zinc
686Zirconium
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 279 of 349
4A-IN
Lab Name:Job No.:
Instrument ID:
ICS Source:
Concentration Units:
Analyte
True
Percent
Recovery
Found
SDG No.:
Lab File ID:
Solution AB Solution AB
Lab Sample ID:
Eurofins Denver 280-170477-1
ICSAB 280-597704/19
092ICSB.d
ug/L
ms 77 icsab_00652
MT_079
INTERFERENCE CHECK STANDARD
METALS
104265Iron102000 102
97380Aluminum102000 95
99.7Antimony100 100
94.9Arsenic100 95
98.2Barium100 98
99.9Beryllium100 100
1130Boron1000
96.5Cadmium100 97
113968Calcium107000 107
101Chromium100 101
96.1Cobalt100 96
97.5Copper100 97
99.4Lead100 99
272Li200
197Li200
98116Magnesium107000 92
97.5Manganese100 98
2179Molybdenum2100 104
94.1Nickel100 94
99901Potassium107000 93
104Selenium100 104
95.2Silver100 95
102182Sodium107000 95
198Strontium200 99
99.6Thallium100 100
101Thorium100 101
99.5Tin100 99
101Uranium100 101
98.3Vanadium100 98
97.6Zinc100 98
46.7Zirconium
FORM IVA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 280 of 349
7A-IN
LAB CONTROL SAMPLE
METALS
Lab ID:LCS 280-597451/2-A
Lab Name:Job No.:280-170477-1
Sample Matrix:LCS Source:ms spike 1_00014
Eurofins Denver
Water
Analyte
Water(ug/L)
True Found C %R Limits Q Method
Iron 800 850 106 6020B80120
Calculations are performed before rounding to avoid round-off errors in calculated results.
FORM VIIA - IN
Page 281 of 349
9-IN
Instrument ID:MT_079
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
METALS
Eurofins Denver
DETECTION LIMITS
6020B MDL Date:10/07/2021 19:31Method:
3020APrep Method:
Analyte Wavelength/
Mass
RL MDL
(ug/L)(ug/L)
Iron 21.7250
FORM IX - IN
Page 282 of 349
9-IN
Instrument ID:MT_079
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
METALS
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
6020B XMDL Date:10/07/2021 19:33Method:
Analyte Wavelength/
Mass
XRL XMDL
(ug/L)(ug/L)
Iron 21.7250
FORM IX - IN
Page 283 of 349
11-IN
Lab Name: Eurofins Denver Job No:280-170477-1
Instrument ID:Date:
Analyte
Integ.
Time
(Sec.)
Concentration
Method
LINEAR RANGES
MT_079
SDG No.:
(ug/L)
10/06/2022 14:28
METALS
Iron 72000 6020B
FORM XI - IN
Page 284 of 349
12-IN
PREPARATION LOG
Lab Name:Job No.:
SDG No.:
280-170477-1
METALS
Eurofins Denver
Prep Method:3020A
Lab
Sample
ID
Preparation
Date
Initial
Weight
Final
Volume
Prep
Batch
Initial
Volume
(mL)(mL)
12/22/2022 07:26 597451MB 280-597451/1-A 5050
12/22/2022 07:26 597451LCS 280-597451/2-A 5050
12/22/2022 07:26 597451280-170477-1 5050
12/22/2022 07:26 597451280-170477-2 5050
FORM XII-IN
Page 285 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/22/2022 17:02 12/22/2022 21:41
13-IN
ANALYSIS RUN LOG
METALS
Job No.:280-170477-1
SDG No.:
Eurofins Denver
MT_079 6020B
Analytes
TimeD/FLab Sample Id
F
e
T
y
p
e
17:02RINSE 280-597704/1
17:03RINSE 280-597704/2
17:05RINSE 280-597704/3
17:07RINSE 280-597704/4
17:09RINSE 280-597704/5
17:11RINSE 280-597704/6
17:13RINSE 280-597704/7
17:15RINSE 280-597704/8
17:17RINSE 280-597704/9
17:18RINSE 280-597704/10
17:20RINSE 280-597704/11
X17:22ICIS 280-597704/12
X17:241IC 280-597704/13
X17:261IC 280-597704/14
X17:281ICV 280-597704/15
X17:301ICB 280-597704/16
17:31ZZZZZZ
X17:331ICSA 280-597704/18
X17:351ICSAB 280-597704/19
17:37RINSE 280-597704/20
17:39LRA 280-597704/21
17:40RINSE 280-597704/22
17:42CCV 280-597704/23
17:44CCB 280-597704/24
X17:461CRI 280-597704/25
17:48ZZZZZZ
17:50ZZZZZZ
17:52ZZZZZZ
17:54ZZZZZZ
17:56ZZZZZZ
17:57ZZZZZZ
17:59ZZZZZZ
18:01CCV 280-597704/33
18:03CCB 280-597704/34
18:05ZZZZZZ
18:07ZZZZZZ
18:09ZZZZZZ
18:11ZZZZZZ
18:12ZZZZZZ
18:14ZZZZZZ
18:16ZZZZZZ
X18:181CCV 280-597704/42
FORM XIII-IN
Page 286 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/22/2022 17:02 12/22/2022 21:41
13-IN
ANALYSIS RUN LOG
METALS
Job No.:280-170477-1
SDG No.:
Eurofins Denver
MT_079 6020B
Analytes
TimeD/FLab Sample Id
F
e
T
y
p
e
X18:201CCB 280-597704/43
X18:221MB 280-597451/1-A T
X18:241LCS 280-597451/2-A T
18:25ZZZZZZ
18:27ZZZZZZ
18:29ZZZZZZ
18:31ZZZZZZ
18:33ZZZZZZ
18:35ZZZZZZ
18:37ZZZZZZ
18:39ZZZZZZ
X18:401CCV 280-597704/54
X18:421CCB 280-597704/55
18:44ZZZZZZ
X18:461280-170477-1 T
X18:481280-170477-2 T
18:50ZZZZZZ
18:52ZZZZZZ
18:54ZZZZZZ
18:55ZZZZZZ
18:57ZZZZZZ
X18:591CCV 280-597704/64
X19:011CCB 280-597704/65
19:03ZZZZZZ
19:05ZZZZZZ
19:07ZZZZZZ
19:08ZZZZZZ
19:10ZZZZZZ
19:12ZZZZZZ
19:14ZZZZZZ
19:16ZZZZZZ
X19:181CCV 280-597704/74
X19:201CCB 280-597704/75
19:22ZZZZZZ
19:23ZZZZZZ
19:25ZZZZZZ
19:27ZZZZZZ
19:29ZZZZZZ
19:31ZZZZZZ
19:33ZZZZZZ
19:35ZZZZZZ
19:37ZZZZZZ
FORM XIII-IN
Page 287 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/22/2022 17:02 12/22/2022 21:41
13-IN
ANALYSIS RUN LOG
METALS
Job No.:280-170477-1
SDG No.:
Eurofins Denver
MT_079 6020B
Analytes
TimeD/FLab Sample Id
F
e
T
y
p
e
19:38ZZZZZZ
19:40CCV 280-597704/86
19:42CCB 280-597704/87
19:44ZZZZZZ
19:46ZZZZZZ
19:48ZZZZZZ
19:50ZZZZZZ
19:52ZZZZZZ
19:53ZZZZZZ
19:55ZZZZZZ
19:57ZZZZZZ
19:59ZZZZZZ
20:01ZZZZZZ
20:03CCV 280-597704/98
20:05CCB 280-597704/99
20:07ZZZZZZ
20:08ZZZZZZ
20:10ZZZZZZ
20:12ZZZZZZ
20:14ZZZZZZ
20:16ZZZZZZ
20:18ZZZZZZ
20:20CCV 280-597704/107
20:22CCB 280-597704/108
20:23RINSE 280-597704/109
20:25RINSE 280-597704/110
20:27RINSE 280-597704/111
20:29RINSE 280-597704/112
20:31RINSE 280-597704/113
X20:33ICIS 280-597704/114
X20:35IC 280-597704/115
X20:37IC 280-597704/116
20:38ICV 280-597704/117
20:40CCV 280-597704/118
20:42CCB 280-597704/119
20:44ZZZZZZ
20:46ZZZZZZ
20:48ZZZZZZ
20:50ZZZZZZ
20:51ZZZZZZ
20:53ZZZZZZ
20:55ZZZZZZ
FORM XIII-IN
Page 288 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/22/2022 17:02 12/22/2022 21:41
13-IN
ANALYSIS RUN LOG
METALS
Job No.:280-170477-1
SDG No.:
Eurofins Denver
MT_079 6020B
Analytes
TimeD/FLab Sample Id
F
e
T
y
p
e
20:57ZZZZZZ
20:59ZZZZZZ
21:01ZZZZZZ
21:03ZZZZZZ
21:04CCV 280-597704/131
21:06CCB 280-597704/132
21:08ZZZZZZ
21:10ZZZZZZ
21:12ZZZZZZ
21:14ZZZZZZ
21:15ZZZZZZ
21:17ZZZZZZ
21:19ZZZZZZ
21:21ZZZZZZ
21:23CCV 280-597704/141
21:25CCB 280-597704/142
21:27ZZZZZZ
21:28ZZZZZZ
21:30ZZZZZZ
21:32ZZZZZZ
21:34ZZZZZZ
21:36ZZZZZZ
21:38ZZZZZZ
21:39CCV 280-597704/150
21:41CCB 280-597704/151
Prep Types:
Total/NAT=
FORM XIII-IN
Page 289 of 349
15-IN
Lab Name:Job No.:
METALS
SDG No.:
Eurofins Denver 280-170477-1
ICP-MS INTERNAL STANDARDS RELATIVE INTENSITY SUMMARY
597704Analysis Batch No.:
Lab Sample
ID
Time
Internal Standards %RI For:
Q
ElementElementElementElement
QQQQ
Element
Li-6/1 Li-6/2 Sc/2 Sc/3 Ge/2
ICP-MS Instrument ID:Start Date:End Date:MT_079 12/22/2022 12/22/2022
IC 280-597704/13 17:24 102 98 100 101 101
IC 280-597704/14 17:26 104 98 103 102 104
ICV 280-597704/15 17:28 100 98 104 104 101
ICB 280-597704/16 17:30 100 98 104 102 101
ICSA 280-597704/18 17:33 115 102 109 112 106
ICSAB 280-597704/19 17:35 98 98 110 114 106
CRI 280-597704/25 17:46 101 100 108 109 104
CCV 280-597704/42 18:18 103 100 109 113 107
CCB 280-597704/43 18:20 104 103 110 114 108
MB 280-597451/1-A 18:22 99 97 106 108 102
LCS 280-597451/2-A 18:24 103 98 104 108 103
CCV 280-597704/54 18:40 111 108 112 112 109
CCB 280-597704/55 18:42 113 108 111 113 107
280-170477-1 18:46 111 103 105 111 105
280-170477-2 18:48 104 102 107 109 104
CCV 280-597704/64 18:59 118 107 110 112 106
CCB 280-597704/65 19:01 116 109 111 111 107
CCV 280-597704/74 19:18 116 109 111 115 106
CCB 280-597704/75 19:20 113 110 111 114 105
FORM XV - IN
Page 290 of 349
15A-IN
Lab Name:Job No.:
METALS
SDG No.:
ICP-MS INTERNAL STANDARDS RELATIONS
Analysis Batch No.:
280-170477-1Eurofins Denver
597704
Analyte
Internal Standard Used:
ElementElementElementElementElement
ICP-MS Instrument ID:
Mass
Start Date:End Date:MT_079 12/22/2022 12/22/2022
In Ir Sc/2 Sc/3 Li-6/1
115 193 45 45 6
56Iron
27 XAluminum
121 XAntimony
75Arsenic
137 XBarium
9Beryllium
11Boron
111 XCadmium
40 XCalcium
52Chromium
59Cobalt
63Copper
208 XLead
7 XLi
7Li
24 XMagnesium
55Manganese
95 XMolybdenum
60Nickel
39 XPotassium
78Selenium
107 XSilver
23 XSodium
88Strontium
205 XThallium
232 XThorium
120 XTin
238 XUranium
51Vanadium
66Zinc
90Zirconium
Internal Standard Name on Instrument In
Internal
Standard
Ir (IS)Sc (IS)Sc (IS)Li-6
Internal
standard
FORM XV - IN
Page 291 of 349
15-IN
Lab Name:Job No.:
METALS
SDG No.:
Eurofins Denver 280-170477-1
ICP-MS INTERNAL STANDARDS RELATIVE INTENSITY SUMMARY
597704Analysis Batch No.:
Lab Sample
ID
Time
Internal Standards %RI For:
Q
ElementElementElementElement
QQQQ
Element
Ge/3 In Ir
ICP-MS Instrument ID:Start Date:End Date:MT_079 12/22/2022 12/22/2022
IC 280-597704/13 17:24 104 102 101
IC 280-597704/14 17:26 103 102 100
ICV 280-597704/15 17:28 105 105 99
ICB 280-597704/16 17:30 104 103 101
ICSA 280-597704/18 17:33 112 109 103
ICSAB 280-597704/19 17:35 112 108 101
CRI 280-597704/25 17:46 107 105 99
CCV 280-597704/42 18:18 112 109 99
CCB 280-597704/43 18:20 113 110 99
MB 280-597451/1-A 18:22 109 105 96
LCS 280-597451/2-A 18:24 106 105 98
CCV 280-597704/54 18:40 113 109 103
CCB 280-597704/55 18:42 111 108 105
280-170477-1 18:46 108 105 101
280-170477-2 18:48 108 105 98
CCV 280-597704/64 18:59 113 109 104
CCB 280-597704/65 19:01 107 106 103
CCV 280-597704/74 19:18 111 108 101
CCB 280-597704/75 19:20 110 108 102
FORM XV - IN
Page 292 of 349
15A-IN
Lab Name:Job No.:
METALS
SDG No.:
ICP-MS INTERNAL STANDARDS RELATIONS
Analysis Batch No.:
280-170477-1Eurofins Denver
597704
Analyte
Internal Standard Used:
ElementElementElementElementElement
ICP-MS Instrument ID:
Mass
Start Date:End Date:MT_079 12/22/2022 12/22/2022
Li-6/2 Ge/2 Ge/3
6 72 72
56 XIron
27Aluminum
121Antimony
75 XArsenic
137Barium
9 XBeryllium
11 XBoron
111Cadmium
40Calcium
52 XChromium
59 XCobalt
63 XCopper
208Lead
7Li
7 XLi
24Magnesium
55 XManganese
95Molybdenum
60 XNickel
39Potassium
78 XSelenium
107Silver
23Sodium
88 XStrontium
205Thallium
232Thorium
120Tin
238Uranium
51 XVanadium
66 XZinc
90 XZirconium
Internal Standard Name on Instrument Li-6
Internal
standard
Ge
Internal
standard
Ge
Internal
standard
FORM XV - IN
Page 293 of 349
Lab Name:Job No.:
SDG No.:
METALS BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Sweet, Lydia J12/22/22 07:26597451
Batch Method:
Eurofins Denver
3020A
Lab Sample ID Client Sample ID Method Chain Basis Initial pH InitialAmount FinalAmount ms spike 1
00014
MS spike 2
00103
50 mL 50 mL3020A, 6020BMB 280-597451/1
50 mL 50 mL 0.1 mL 0.1 mL3020A, 6020BLCS
280-597451/2
Offsite A-1 <2 50 mL 50 mL3020A, 6020B T280-170477-B-1
Offsite A-2 <2 50 mL 50 mL3020A, 6020B T280-170477-B-2
Batch Notes
Digestion Tube/Cup ID 2206051
Pipette/Syringe/Dispenser ID MET88
Analyst ID - Spike Analyst LJS
Sufficient Volume for Batch QC YES
Lot # of Nitric Acid 222846-12/23
Digestion Unit ID 14
Thermometer ID V06422
Thermometer Location ID B1
Digestion Start Time 07:26
Temperature - Uncorrected - Start 90 Degrees C
Temperature - Corrected - Start 91 Degrees C
Temperature - Uncorrected - End 92 Degrees C
Temperature - Corrected - End 93 Degrees C
Digestion End Time 13.43
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 16020B
Page 294 of 349
GENERAL CHEMISTRY
Page 295 of 349
COVER PAGE
Lab Name: Job Number:
Client Sample ID Lab Sample ID
GENERAL CHEMISTRY
Project:GE-Salt Lake City, Utah
SDG No.:
280-170477-1Eurofins Denver
280-170477-1 Offsite A-1
280-170477-2 Offsite A-2
Comments:
Page 296 of 349
1B-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name:Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 280-170477-1
Date Received:12/16/2022 09:15

280-170477-1
Offsite A-1
Water 12/14/2022 12:45Date Sampled:
Reporting Basis:WET
GENERAL CHEMISTRY
Eurofins Denver
CAS No.Analyte CUnits Q MethodRLMDLDILResult
14797-55-8 Nitrate as N 2.3 mg/L H0.50 0.090 1 300.0
Alkalinity 410 mg/L B103.1 1 SM 2320B
Ferric Iron 2.4 mg/L0.20 0.021 1 SM 3500
15438-31-0 Ferrous Iron ND mg/L HF0.20 0.021 1 SM 3500
FE B
16887-00-6 Chloride 350 mg/L4014 20 SM 4500
Cl- E
14808-79-8 Sulfate 230 mg/L B507.1 10 SM 4500
SO4 E
FORM IB-IN Page 297 of 349
1B-IN
INORGANIC ANALYSIS DATA SHEET
Client Sample ID:
Lab Name:Job No.:
SDG ID.:
Matrix:
Lab Sample ID: 280-170477-2
Date Received:12/16/2022 09:15

280-170477-1
Offsite A-2
Water 12/14/2022 11:00Date Sampled:
Reporting Basis:WET
GENERAL CHEMISTRY
Eurofins Denver
CAS No.Analyte CUnits Q MethodRLMDLDILResult
14797-55-8 Nitrate as N 2.1 mg/L H0.50 0.090 1 300.0
Alkalinity 470 mg/L B103.1 1 SM 2320B
Ferric Iron 0.89 mg/L0.20 0.021 1 SM 3500
15438-31-0 Ferrous Iron 0.10 Jmg/L HF0.20 0.021 1 SM 3500
FE B
16887-00-6 Chloride 420 mg/L4014 20 SM 4500
Cl- E
14808-79-8 Sulfate 220 mg/L B507.1 10 SM 4500
SO4 E
FORM IB-IN Page 298 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:EJS Batch Start Date:12/13/2022
Reporting Units:mg/L Analytical Batch No.:596556
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
ICV 17:31 Nitrate as N 2.00 2.00 100 90-110 IC ICV 5_00385 8
ICB 17:46 Nitrate as N ND 9
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 299 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:MEC Batch Start Date:12/17/2022
Reporting Units:mg/L Analytical Batch No.:596980
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
CCV 00:42 Nitrate as N 2.40 2.50 96 90-110 IC LCS_01923 29
CCB 00:57 Nitrate as N ND 30
CCV 03:42 Nitrate as N 2.40 2.50 96 90-110 IC LCS_01923 41
CCB 03:57 Nitrate as N ND 42
CCV 05:57 Nitrate as N 2.39 2.50 96 90-110 IC LCS_01923 50
CCB 06:12 Nitrate as N ND 51
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 300 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:KEG Batch Start Date:12/20/2022
Reporting Units:mg/L Analytical Batch No.:597409
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
CCV 13:24 Alkalinity 202 200 101 90-110 Alk daily
lcs_01070
17
CCB 13:30 Alkalinity ND 18
CCV 22:31 Alkalinity 209 200 105 90-110 Alk daily
lcs_01070
81
CCB 22:37 Alkalinity 6.01 J 82
CCV 00:26 Alkalinity 208 200 104 90-110 Alk daily
lcs_01070
95
CCB 00:32 Alkalinity ND 96
CCV 02:55 Alkalinity 210 200 105 90-110 Alk daily
lcs_01070
107
CCB 03:01 Alkalinity ND 108
CCV 04:43 Alkalinity 211 200 106 90-110 Alk daily
lcs_01070
121
CCB 04:48 Alkalinity ND 122
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 301 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:LRB Batch Start Date:12/19/2022
Reporting Units:mg/L Analytical Batch No.:597184
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
ICV 14:06 Ferrous Iron 0.985 1.00 99 90-110 FE ICV INT_00641 7
ICB 14:06 Ferrous Iron ND 8
CCV 14:09 Ferrous Iron 1.00 1.00 100 90-110 FE Cal INT_00644 20
CCB 14:09 Ferrous Iron ND 21
CCV 16:02 Ferrous Iron 1.02 1.00 102 90-110 FE Cal INT_00644 29
CCB 16:02 Ferrous Iron 0.116 J 30
CCV 16:38 Ferrous Iron 1.00 1.00 100 90-110 FE Cal INT_00644 33
CCB 16:38 Ferrous Iron ND 34
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 302 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:LRB Batch Start Date:12/30/2022
Reporting Units:mg/L Analytical Batch No.:598240
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
ICV 15:43 Chloride 20.9 20.0 104 90-110 Cl ICV Int_00039 11
ICB 15:43 Chloride ND 12
CCV 16:07 Chloride 10.4 10.0 104 90-110 Cl ICV Int_00039 20
CCB 16:07 Chloride ND 21
CCV 16:25 Chloride 10.4 10.0 104 90-110 Cl ICV Int_00039 26
CCB 16:26 Chloride ND 27
CCV 16:27 Chloride 10.5 10.0 105 90-110 Cl ICV Int_00039 32
CCB 16:27 Chloride ND 33
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 303 of 349
2-IN
Lab Name:Job No.:
SDG No.:
280-170477-1
Analyst:LRB Batch Start Date:12/30/2022
Reporting Units:mg/L Analytical Batch No.:598232
CALIBRATION QUALITY CONTROL
GENERAL CHEMISTRY
Sample
Number
QC
Type Time Analyte Result Spike
Amount
(%)
Recovery Limits Qual Reagent
Eurofins Denver
ICV 15:38 Sulfate 20.7 20.0 104 90-110 SO4 ICV Int_00042 10
ICB 15:38 Sulfate ND 11
CCV 16:06 Sulfate 21.2 20.0 106 90-110 SO4 Cal Int_00042 19
CCB 16:06 Sulfate ND 20
CCV 16:13 Sulfate 21.1 20.0 105 90-110 SO4 Cal Int_00042 25
CCB 16:13 Sulfate ND 26
CCV 16:25 Sulfate 21.8 20.0 109 90-110 SO4 Cal Int_00042 31
CCB 16:26 Sulfate ND 32
FORM II-IN
Note! Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 304 of 349
Lab Name:Job No.:
SDG No.:
Method Analyte Result Qual Dil
3-IN

280-170477-1
Lab Sample ID Units
Eurofins Denver
METHOD BLANK
GENERAL CHEMISTRY
RL
Batch ID: 596980 Date:12/17/2022 03:12
NDMB 280-596980/39 10.50mg/LNitrate as N300.0
Batch ID: 597409 Date:12/20/2022 11:52
3.47MB 280-597409/6 J 110mg/LAlkalinitySM 2320B
Batch ID: 597409 Date:12/20/2022 22:51
3.78MB 280-597409/84 J 110mg/LAlkalinitySM 2320B
Batch ID: 597409 Date:12/21/2022 03:15
3.37MB 280-597409/110 J 110mg/LAlkalinitySM 2320B
Batch ID: 597184 Date:12/19/2022 14:06
NDMB 280-597184/11 10.20mg/LFerrous IronSM 3500 FE
B
Batch ID: 598240 Date:12/30/2022 15:43
NDMB 280-598240/15 12.0mg/LChlorideSM 4500
Cl- E
Batch ID: 598232 Date:12/30/2022 15:39
0.737MB 280-598232/14 J 15.0mg/LSulfateSM 4500
SO4 E
FORM III-IN
Page 305 of 349
6-IN
Lab Name:Job No.:
SDG No.:
Matrix:
Analyte RPD QualMethod

280-170477-1
Client
Sample ID
Lab
Sample ID Result Unit RPD
Limit
Water
Eurofins Denver
DUPLICATE
GENERAL CHEMISTRY
Batch ID: 597409 Date:12/21/2022 03:31
SM 2320B Offsite A-1 Alkalinity mg/L410280-170477-1
Alkalinity 422 2SM 2320B Offsite A-1 280-170477-1 DU mg/L 10
Calculations are performed before rounding to avoid round-off errors in calculated results.
FORM VI-IN
Page 306 of 349
7A-IN
Job No.:280-170477-1
LAB CONTROL SAMPLE
GENERAL CHEMISTRY
Lab Name:
SDG No.:
QRPD
LimitRPDLimitsPct.
Rec.
Spike
AmountUnitCResultAnalyteLab Sample IDMethod
Matrix:Water
Eurofins Denver
Batch ID: 596980 Date:12/17/2022 02:42
LCS Source:IC LCS_01923
2.50 95 10300.0 LCS
280-596980/37
Nitrate as N 2.38 mg/L 90-110 1
Batch ID: 597409 Date:12/21/2022 03:09
LCS Source:Alk daily lcs_01070
200 105SM
2320B
LCS
280-597409/10
9
Alkalinity 210 mg/L 89-109
Batch ID: 597184 Date:12/19/2022 14:06
LCS Source:FE ICV INT_00641
2.00 99 10SM 3500
FE B
LCS
280-597184/9
Ferrous Iron 1.97 mg/L 85-121 1
Batch ID: 598240 Date:12/30/2022 15:43
LCS Source:Cl Cal Int_00040
20.0 100 10SM 4500
Cl- E
LCS
280-598240/13
Chloride 19.9 mg/L 90-110 0
Batch ID: 598232 Date:12/30/2022 15:39
LCS Source:SO4 ICV Int_00042
25.0 103 10SM 4500
SO4 E
LCS
280-598232/12
Sulfate 25.6 mg/L 90-110 0
FORM VIIA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 307 of 349
7A-IN
Job No.:280-170477-1
LAB CONTROL SAMPLE DUPLICATE
GENERAL CHEMISTRY
Lab Name:
SDG No.:
QRPD
LimitRPDLimitsPct.
Rec.
Spike
AmountUnitCResultAnalyteLab Sample IDMethod
Matrix:Water
Eurofins Denver
Batch ID: 596980 Date:12/17/2022 02:57
LCSD Source:IC LCS_01923
2.50 96 10300.0 LCSD
280-596980/38
Nitrate as N 2.40 mg/L 90-110 1
Batch ID: 597409 Date:12/20/2022 11:46
LCSD Source:Alk daily lcs_01070
200 102 10SM
2320B
LCSD
280-597409/5
Alkalinity 203 mg/L 89-109 2
Batch ID: 597184 Date:12/19/2022 14:06
LCSD Source:FE ICV INT_00641
2.00 100 10SM 3500
FE B
LCSD
280-597184/10
Ferrous Iron 1.99 mg/L 85-121 1
Batch ID: 598240 Date:12/30/2022 15:43
LCSD Source:Cl Cal Int_00040
20.0 100 10SM 4500
Cl- E
LCSD
280-598240/14
Chloride 20.0 mg/L 90-110 0
Batch ID: 598232 Date:12/30/2022 15:39
LCSD Source:SO4 ICV Int_00042
25.0 103 10SM 4500
SO4 E
LCSD
280-598232/13
Sulfate 25.7 mg/L 90-110 0
FORM VIIA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 308 of 349
7A-IN
Job No.:280-170477-1
METHOD REPORTING LIMIT CHECK
GENERAL CHEMISTRY
Lab Name:
SDG No.:
QRPD
LimitRPDLimitsPct.
Rec.
Spike
AmountUnitCResultAnalyteLab Sample IDMethod
Matrix:Water
Eurofins Denver
Batch ID: 596980 Date:12/16/2022 18:11
LCS Source:IC Cal low_00681
0.250 95J300.0 MRL
280-596980/3
Nitrate as N 0.237 mg/L 50-150
FORM VIIA-IN
Calculations are performed before rounding to avoid round-off errors in calculated results.
Page 309 of 349
9-IN
Instrument ID:WC_IonChrom10
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
300.0 MDL Date:06/21/2019 00:00Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Nitrate as N 0.09010.5
FORM IX - IN
Page 310 of 349
9-IN
Instrument ID:WC_IonChrom10
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
300.0 XMDL Date:06/21/2019 00:00Method:
Analyte Wavelength/
Mass
XRL XMDL
(mg/L)(mg/L)
Nitrate as N 0.09010.5
FORM IX - IN
Page 311 of 349
9-IN
Instrument ID:WC_AT4
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
SM 2320B MDL Date:02/03/2019 00:00Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Alkalinity 3.0810
FORM IX - IN
Page 312 of 349
9-IN
Instrument ID:WC_AT4
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
SM 2320B XMDL Date:02/03/2019 00:00Method:
Analyte Wavelength/
Mass
XRL XMDL
(mg/L)(mg/L)
Alkalinity 3.0810
FORM IX - IN
Page 313 of 349
9-IN
Instrument ID:NOEQUIP
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
SM 3500 MDL Date:11/01/2009 00:00Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Ferric Iron 0.0210.2
FORM IX - IN
Page 314 of 349
9-IN
Instrument ID:WC_GAL2
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
SM 3500 FE B MDL Date:03/28/2011 12:11Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Ferrous Iron 0.0210.2
FORM IX - IN
Page 315 of 349
9-IN
Instrument ID:WC_GAL2
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
SM 3500 FE B XMDL Date:03/28/2011 12:11Method:
Analyte Wavelength/
Mass
XRL XMDL
(mg/L)(mg/L)
Ferrous Iron 0.02070.2
FORM IX - IN
Page 316 of 349
9-IN
Instrument ID:WC_GAL1
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
SM 4500 Cl- E MDL Date:04/08/2022 15:24Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Chloride 0.6752
FORM IX - IN
Page 317 of 349
9-IN
Instrument ID:WC_GAL1
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
SM 4500 Cl- E XMDL Date:04/08/2022 15:24Method:
Analyte Wavelength/
Mass
XRL XMDL
(mg/L)(mg/L)
Chloride 0.6752
FORM IX - IN
Page 318 of 349
9-IN
Instrument ID:WC_GAL2
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
DETECTION LIMITS
SM 4500 SO4 E MDL Date:08/06/2020 16:27Method:
Analyte Wavelength/
Mass
RL MDL
(mg/L)(mg/L)
Sulfate 0.7075
FORM IX - IN
Page 319 of 349
9-IN
Instrument ID:WC_GAL2
280-170477-1Job Number:
WaterMatrix:
SDG Number:
Lab Name:
GENERAL CHEMISTRY
Eurofins Denver
CALIBRATION BLANK DETECTION LIMITS
SM 4500 SO4 E XMDL Date:08/06/2020 16:27Method:
Analyte Wavelength/
Mass
XRL XMDL
(mg/L)(mg/L)
Sulfate 15
FORM IX - IN
Page 320 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/13/2022 15:11 12/14/2022 06:21
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_IonChrom10 300.0
Analytes
TimeD/FLab Sample Id
N
O
3
T
y
p
e
15:11RTC 280-596556/1 CCV
X15:26STD 280-596556/2 IC
X15:41STD 280-596556/3 IC
X15:56STD 280-596556/4 IC
X16:11STD 280-596556/5 IC
X16:26STD 280-596556/6 IC
X16:41STD 280-596556/7 IC
X17:311ICV 280-596556/8
X17:461ICB 280-596556/9
18:01ZZZZZZ
18:16ZZZZZZ
18:31ZZZZZZ
18:46ZZZZZZ
19:05ZZZZZZ
19:20ZZZZZZ
19:35ZZZZZZ
19:50ZZZZZZ
20:06ZZZZZZ
20:21ZZZZZZ
20:36ZZZZZZ
20:51ZZZZZZ
21:06ZZZZZZ
21:21ZZZZZZ
21:36CCV 280-596556/24
21:51CCB 280-596556/25
22:06ZZZZZZ
22:21ZZZZZZ
22:36ZZZZZZ
22:51ZZZZZZ
23:06ZZZZZZ
23:21ZZZZZZ
23:36ZZZZZZ
23:51ZZZZZZ
00:06ZZZZZZ
00:21ZZZZZZ
00:36CCV 280-596556/36
00:51CCB 280-596556/37
01:06ZZZZZZ
01:21ZZZZZZ
01:36ZZZZZZ
01:51ZZZZZZ
FORM XIII-IN
Page 321 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/13/2022 15:11 12/14/2022 06:21
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_IonChrom10 300.0
Analytes
TimeD/FLab Sample Id
N
O
3
T
y
p
e
02:06ZZZZZZ
02:22ZZZZZZ
02:36ZZZZZZ
02:51ZZZZZZ
03:06ZZZZZZ
03:21ZZZZZZ
03:36CCV 280-596556/48
03:51CCB 280-596556/49
04:06ZZZZZZ
04:21ZZZZZZ
04:36ZZZZZZ
04:51ZZZZZZ
05:06ZZZZZZ
05:21ZZZZZZ
05:36ZZZZZZ
05:51ZZZZZZ
06:06CCV 280-596556/58
06:21CCB 280-596556/59
Prep Types:
=
FORM XIII-IN
Page 322 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/16/2022 17:41 12/17/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_IonChrom10 300.0
Analytes
TimeD/FLab Sample Id
N
O
3
T
y
p
e
17:41CCV 280-596980/1
17:56CCB 280-596980/2
X18:111MRL 280-596980/3 T
18:26ZZZZZZ
18:41ZZZZZZ
18:56ZZZZZZ
19:11ZZZZZZ
19:26ZZZZZZ
19:41ZZZZZZ
19:56ZZZZZZ
20:11ZZZZZZ
20:26ZZZZZZ
20:41ZZZZZZ
20:56ZZZZZZ
21:11ZZZZZZ
21:26ZZZZZZ
21:41CCV 280-596980/17
21:56CCB 280-596980/18
22:11ZZZZZZ
22:26ZZZZZZ
22:41ZZZZZZ
22:56ZZZZZZ
23:12ZZZZZZ
23:27ZZZZZZ
23:42ZZZZZZ
23:57ZZZZZZ
00:12ZZZZZZ
00:27ZZZZZZ
X00:421CCV 280-596980/29
X00:571CCB 280-596980/30
01:12ZZZZZZ
01:27ZZZZZZ
01:42ZZZZZZ
01:57ZZZZZZ
02:12ZZZZZZ
02:27ZZZZZZ
X02:421LCS 280-596980/37 T
X02:571LCSD 280-596980/38 T
X03:121MB 280-596980/39 T
03:27ZZZZZZ
X03:421CCV 280-596980/41
FORM XIII-IN
Page 323 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/16/2022 17:41 12/17/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_IonChrom10 300.0
Analytes
TimeD/FLab Sample Id
N
O
3
T
y
p
e
X03:571CCB 280-596980/42
04:12ZZZZZZ
X04:271280-170477-1 T
X04:421280-170477-2 T
04:57ZZZZZZ
05:12ZZZZZZ
05:27ZZZZZZ
05:42ZZZZZZ
X05:571CCV 280-596980/50
X06:121CCB 280-596980/51
Prep Types:
Total/NAT=
FORM XIII-IN
Page 324 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/20/2022 11:22 12/21/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_AT4 SM 2320B
Analytes
TimeD/FLab Sample Id
A
l
k
T
y
p
e
11:22RINSE 280-597409/1
11:30ZZZZZZ
11:32ZZZZZZ
11:39ZZZZZZ
X11:461LCSD 280-597409/5 T
X11:521MB 280-597409/6 T
12:01ZZZZZZ
12:10ZZZZZZ
12:18ZZZZZZ
12:26ZZZZZZ
12:34ZZZZZZ
12:43ZZZZZZ
12:52ZZZZZZ
13:00ZZZZZZ
13:09ZZZZZZ
13:17ZZZZZZ
X13:241CCV 280-597409/17
X13:301CCB 280-597409/18
13:37ZZZZZZ
13:46ZZZZZZ
13:55ZZZZZZ
14:04ZZZZZZ
14:10ZZZZZZ
14:18ZZZZZZ
14:24ZZZZZZ
14:29ZZZZZZ
14:39ZZZZZZ
14:46ZZZZZZ
14:53CCV 280-597409/29
14:59CCB 280-597409/30
15:07ZZZZZZ
15:13ZZZZZZ
15:19ZZZZZZ
15:24ZZZZZZ
15:31ZZZZZZ
15:39ZZZZZZ
15:47ZZZZZZ
15:57ZZZZZZ
16:10ZZZZZZ
16:21ZZZZZZ
16:33ZZZZZZ
FORM XIII-IN
Page 325 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/20/2022 11:22 12/21/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_AT4 SM 2320B
Analytes
TimeD/FLab Sample Id
A
l
k
T
y
p
e
16:38ZZZZZZ
16:46CCV 280-597409/43
16:52CCB 280-597409/44
16:58ZZZZZZ
17:05ZZZZZZ
17:11ZZZZZZ
17:26ZZZZZZ
17:36ZZZZZZ
17:47ZZZZZZ
18:06ZZZZZZ
18:12ZZZZZZ
18:17ZZZZZZ
18:22ZZZZZZ
18:30CCV 280-597409/55
18:36CCB 280-597409/56
18:43ZZZZZZ
18:49ZZZZZZ
18:56ZZZZZZ
19:03ZZZZZZ
19:09ZZZZZZ
19:15ZZZZZZ
19:20ZZZZZZ
19:41ZZZZZZ
19:51ZZZZZZ
19:57ZZZZZZ
20:18ZZZZZZ
20:34ZZZZZZ
20:42CCV 280-597409/69
20:48CCB 280-597409/70
21:06ZZZZZZ
21:28ZZZZZZ
21:35ZZZZZZ
21:41ZZZZZZ
21:47ZZZZZZ
21:56ZZZZZZ
22:02ZZZZZZ
22:07ZZZZZZ
22:15ZZZZZZ
22:24ZZZZZZ
X22:311CCV 280-597409/81
X22:371CCB 280-597409/82
FORM XIII-IN
Page 326 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/20/2022 11:22 12/21/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_AT4 SM 2320B
Analytes
TimeD/FLab Sample Id
A
l
k
T
y
p
e
22:45ZZZZZZ
X22:511MB 280-597409/84 T
23:00ZZZZZZ
23:10ZZZZZZ
23:19ZZZZZZ
23:26ZZZZZZ
23:35ZZZZZZ
23:41ZZZZZZ
23:46ZZZZZZ
23:53ZZZZZZ
00:04ZZZZZZ
00:18ZZZZZZ
X00:261CCV 280-597409/95
X00:321CCB 280-597409/96
00:38ZZZZZZ
00:44ZZZZZZ
01:05ZZZZZZ
01:24ZZZZZZ
01:36ZZZZZZ
01:51ZZZZZZ
02:05ZZZZZZ
02:19ZZZZZZ
02:33ZZZZZZ
02:47ZZZZZZ
X02:551CCV 280-597409/107
X03:011CCB 280-597409/108
X03:091LCS 280-597409/109 T
X03:151MB 280-597409/110 T
X03:231280-170477-1 T
X03:311280-170477-1 DU T
X03:391280-170477-2 T
03:47ZZZZZZ
03:56ZZZZZZ
04:04ZZZZZZ
04:11ZZZZZZ
04:19ZZZZZZ
04:27ZZZZZZ
04:35ZZZZZZ
X04:431CCV 280-597409/121
X04:481CCB 280-597409/122
04:56ZZZZZZ
FORM XIII-IN
Page 327 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/20/2022 11:22 12/21/2022 06:12
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_AT4 SM 2320B
Analytes
TimeD/FLab Sample Id
A
l
k
T
y
p
e
05:03ZZZZZZ
05:11ZZZZZZ
05:19ZZZZZZ
05:27ZZZZZZ
05:34ZZZZZZ
05:37ZZZZZZ
05:44ZZZZZZ
05:52ZZZZZZ
05:58ZZZZZZ
06:06CCV 280-597409/133
06:12CCB 280-597409/134
Prep Types:
Total/NAT=
FORM XIII-IN
Page 328 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/29/2022 16:06 12/29/2022 16:06
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
NOEQUIP SM 3500
Analytes
TimeD/FLab Sample Id
F
e
3
T
y
p
e
X16:061280-170477-1 T
X16:061280-170477-2 T
16:06ZZZZZZ
16:06ZZZZZZ
16:06ZZZZZZ
Prep Types:
Total/NAT=
FORM XIII-IN
Page 329 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:10/07/2022 17:40 12/19/2022 16:38
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_GAL2 SM 3500 FE B
Analytes
TimeD/FLab Sample Id
F
e
2
T
y
p
e
17:40ZZZZZZ
17:40ZZZZZZ
17:41ZZZZZZ
17:41ZZZZZZ
17:42ZZZZZZ
17:42ZZZZZZ
X14:061ICV 280-597184/7
X14:061ICB 280-597184/8
X14:061LCS 280-597184/9 T
X14:061LCSD 280-597184/10 T
X14:061MB 280-597184/11 T
14:06ZZZZZZ
14:06ZZZZZZ
14:07ZZZZZZ
14:07ZZZZZZ
14:08ZZZZZZ
14:08ZZZZZZ
X14:091280-170477-1 T
X14:091280-170477-2 T
X14:091CCV1 280-597184/20
X14:091CCB1 280-597184/21
14:59ZZZZZZ
15:00ZZZZZZ
15:00ZZZZZZ
15:00ZZZZZZ
15:00ZZZZZZ
16:01ZZZZZZ
16:02ZZZZZZ
X16:021CCV2 280-597184/29
X16:021CCB2 280-597184/30
16:37ZZZZZZ
16:38ZZZZZZ
X16:381CCV2 280-597184/33
X16:381CCB2 280-597184/34
Prep Types:
Total/NAT=
FORM XIII-IN
Page 330 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/30/2022 14:43 12/30/2022 16:54
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_GAL1 SM 4500 Cl- E
Analytes
TimeD/FLab Sample Id
C
L
-
T
y
p
e
14:43ZZZZZZ
14:43ZZZZZZ
14:43ZZZZZZ
14:44ZZZZZZ
14:44ZZZZZZ
14:44ZZZZZZ
14:45ZZZZZZ
14:45ZZZZZZ
14:45ZZZZZZ
14:45ZZZZZZ
X15:431ICV 280-598240/11
X15:431ICB 280-598240/12
X15:431LCS 280-598240/13 T
X15:431LCSD 280-598240/14 T
X15:431MB 280-598240/15 T
15:45ZZZZZZ
15:53ZZZZZZ
15:54ZZZZZZ
X16:0120280-170477-1 T
X16:071CCV1 280-598240/20
X16:071CCB1 280-598240/21
X16:1720280-170477-2 T
16:18ZZZZZZ
16:18ZZZZZZ
16:18ZZZZZZ
X16:251CCV2 280-598240/26
X16:261CCB2 280-598240/27
16:26ZZZZZZ
16:27ZZZZZZ
16:27ZZZZZZ
16:27ZZZZZZ
X16:271CCV3 280-598240/32
X16:271CCB3 280-598240/33
16:39ZZZZZZ
16:39ZZZZZZ
16:50ZZZZZZ
16:51ZZZZZZ
16:51ZZZZZZ
16:51ZZZZZZ
16:54CCV3 280-598240/40
16:54CCB3 280-598240/41
FORM XIII-IN
Page 331 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/30/2022 14:43 12/30/2022 16:54
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_GAL1 SM 4500 Cl- E
Analytes
TimeD/FLab Sample Id
C
L
-
T
y
p
e
Prep Types:
Total/NAT=
FORM XIII-IN
Page 332 of 349
Lab Name:
Instrument ID:Analysis Method:
Start Date:End Date:12/30/2022 14:46 12/30/2022 16:26
13-IN
ANALYSIS RUN LOG
GENERAL CHEMISTRY
Job No.:280-170477-1
SDG No.:
Eurofins Denver
WC_GAL2 SM 4500 SO4 E
Analytes
TimeD/FLab Sample Id
S
O
4
T
y
p
e
14:46ZZZZZZ
14:47ZZZZZZ
14:47ZZZZZZ
14:48ZZZZZZ
14:48ZZZZZZ
14:49ZZZZZZ
14:49ZZZZZZ
14:50ZZZZZZ
14:50ZZZZZZ
X15:381ICV 280-598232/10
X15:381ICB 280-598232/11
X15:391LCS 280-598232/12 T
X15:391LCSD 280-598232/13 T
X15:391MB 280-598232/14 T
15:43ZZZZZZ
15:48ZZZZZZ
15:49ZZZZZZ
15:49ZZZZZZ
X16:061CCV1 280-598232/19
X16:061CCB1 280-598232/20
X16:0710280-170477-1 T
X16:0810280-170477-2 T
16:08ZZZZZZ
16:09ZZZZZZ
X16:131CCV 280-598232/25
X16:131CCB 280-598232/26
16:24ZZZZZZ
16:24ZZZZZZ
16:25ZZZZZZ
16:25ZZZZZZ
X16:251CCV3 280-598232/31
X16:261CCB3 280-598232/32
Prep Types:
Total/NAT=
FORM XIII-IN
Page 333 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Sherman, Erik J12/13/22 15:11596556
Batch Method:
Eurofins Denver
300.0
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Cl ICV Std
00005
IC ICV 5 00385 IC SO4 ICV
00024
5 mL 5 mL 0.8 mL 0.8 mL 0.8 mL300.0ICV
280-596556/8
5 mL 5 mL300.0ICB
280-596556/9
Batch Notes
Filter ID sf020e
Pipette/Syringe/Dispenser ID arm5000, 1000hex, 200cj, 100cj
Sufficient Volume for Batch QC yes
Eluent 1 ID ic10eluent_00005
Batch Comment mec, reviewed by ejs
Basis Basis Description
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1300.0
Page 334 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Collins, Michael E12/16/22 17:41596980
Batch Method:
Eurofins Denver
300.0
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount IC CAL cl/so4
00457
IC Cal low
00681
IC LCS 01923
5 mL 5 mL 0.2 mL 0.1 mL300.0MRL
280-596980/3
5 mL 5 mL 10 mL300.0CCV
280-596980/29
5 mL 5 mL300.0CCB
280-596980/30
5 mL 5 mL 10 mL300.0LCS
280-596980/37
5 mL 5 mL 10 mL300.0LCSD
280-596980/38
5 mL 5 mL300.0MB
280-596980/39
5 mL 5 mL 10 mL300.0CCV
280-596980/41
5 mL 5 mL300.0CCB
280-596980/42
Offsite A-1 5 mL 5 mL300.0 T280-170477-A-1
Offsite A-2 5 mL 5 mL300.0 T280-170477-A-2
5 mL 5 mL 10 mL300.0CCV
280-596980/50
5 mL 5 mL300.0CCB
280-596980/51
Batch Notes
Filter ID SF020E
Pipette/Syringe/Dispenser ID ARM5000, 1000HEX, 200CJ , 100IC
Sufficient Volume for Batch QC yes
Eluent 1 ID IC10 Eluent_00005
Batch Comment MEC
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1300.0
Page 335 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Guillen, Kristela E12/20/22 11:22597409
Batch Method:
Eurofins Denver
SM 2320B
Lab Sample ID Client Sample ID Method Chain Basis CalcMsg Alk daily lcs
01070
InitialAmount
is blank
10 mLSM 2320BLCSD
280-597409/5
InitialAmount
is blank
SM 2320BMB 280-597409/6
InitialAmount
is blank
10 mLSM 2320BCCV
280-597409/17
InitialAmount
is blank
SM 2320BCCB
280-597409/18
InitialAmount
is blank
10 mLSM 2320BCCV
280-597409/81
InitialAmount
is blank
SM 2320BCCB
280-597409/82
InitialAmount
is blank
SM 2320BMB
280-597409/84
InitialAmount
is blank
10 mLSM 2320BCCV
280-597409/95
InitialAmount
is blank
SM 2320BCCB
280-597409/96
InitialAmount
is blank
10 mLSM 2320BCCV
280-597409/107
InitialAmount
is blank
SM 2320BCCB
280-597409/108
InitialAmount
is blank
10 mLSM 2320BLCS
280-597409/109
InitialAmount
is blank
SM 2320BMB
280-597409/110
Offsite A-1 InitialAmount
is blank
SM 2320B T280-170477-A-1
Offsite A-1 InitialAmount
is blank
SM 2320B T280-170477-A-1
DU
Offsite A-2 InitialAmount
is blank
SM 2320B T280-170477-A-2
InitialAmount
is blank
10 mLSM 2320BCCV
280-597409/121
InitialAmount
is blank
SM 2320BCCB
280-597409/122
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 2SM 2320B
Page 336 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Guillen, Kristela E12/20/22 11:22597409
Batch Method:
Eurofins Denver
SM 2320B
Batch Notes
Nominal Amount Used 10 mL
Acid ID 0.02 H2SO4_00299
Normality of First Titrant 0.02 N
Sodium Carbonate ID Alk Stk Std_00023
pH Buffer 1 ID pH 2.0 buffer_00098
pH Buffer 2 ID pH 4.0 buffer_00209
pH Buffer 3 ID pH 7.0 buffer_00318
pH Buffer 4 ID pH 7.0 buffer_00319
pH Buffer 5 ID pH 10 buffer_00162
pH Buffer 6 ID pH 12 buffer_00180
Probe ID PCE 80 pH 1200D_8918
Batch Comment KG
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 2 of 2SM 2320B
Page 337 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Maddox, Daniel N12/29/22 16:06598094
Batch Method:
Eurofins Denver
SM 3500
Lab Sample ID Client Sample ID Method Chain Basis CalcMsg
Offsite A-1 OKSM 3500 T280-170477-A-1
Offsite A-2 OKSM 3500 T280-170477-A-2
Batch Notes
Perform Calculation (0=No, 1=Yes)1
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1SM 3500
Page 338 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Brock, Lucynda R
12/19/22 16:40
12/19/22 14:00597184
Batch Method:
Eurofins Denver
SM 3500 FE B
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount FE Cal INT
00644
FE ICV INT
00641
100 mL 100 mL 1 mLSM 3500 FE BICV
280-597184/7
2 mL 2 mLSM 3500 FE BICB
280-597184/8
100 mL 100 mL 2 mLSM 3500 FE BLCS
280-597184/9
100 mL 100 mL 2 mLSM 3500 FE BLCSD
280-597184/10
2 mL 2 mLSM 3500 FE BMB
280-597184/11
Offsite A-1 2 mL 2 mLSM 3500 FE B T280-170477-A-1
Offsite A-2 2 mL 2 mLSM 3500 FE B T280-170477-A-2
100 mL 100 mL 1 mLSM 3500 FE BCCV1
280-597184/20
2 mL 2 mLSM 3500 FE BCCB1
280-597184/21
100 mL 100 mL 1 mLSM 3500 FE BCCV2
280-597184/29
2 mL 2 mLSM 3500 FE BCCB2
280-597184/30
100 mL 100 mL 1 mLSM 3500 FE BCCV2
280-597184/33
2 mL 2 mLSM 3500 FE BCCB2
280-597184/34
Batch Notes
Acetate Buffer ID Ferrous R1_00011
Phenanthroline ID Ferrous R2_00009
Batch Comment LRB
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1SM 3500 FE B
Page 339 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Brock, Lucynda R
12/30/22 16:55
12/30/22 14:43598240
Batch Method:
Eurofins Denver
SM 4500 Cl- E
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount Cl Cal Int
00040
Cl ICV Int
00039
2 mL 2 mL 0.2 mLSM 4500 Cl-
E
ICV
280-598240/11
2 mL 2 mLSM 4500 Cl-
E
ICB
280-598240/12
2 mL 2 mL 0.2 mLSM 4500 Cl-
E
LCS
280-598240/13
2 mL 2 mL 0.2 mLSM 4500 Cl-
E
LCSD
280-598240/14
2 mL 2 mLSM 4500 Cl-
E
MB
280-598240/15
Offsite A-1 2 mL 2 mLSM 4500 Cl-
E
T280-170477-A-1
2 mL 2 mL 0.1 mLSM 4500 Cl-
E
CCV1
280-598240/20
2 mL 2 mLSM 4500 Cl-
E
CCB1
280-598240/21
Offsite A-2 2 mL 2 mLSM 4500 Cl-
E
T280-170477-A-2
2 mL 2 mL 0.1 mLSM 4500 Cl-
E
CCV2
280-598240/26
2 mL 2 mLSM 4500 Cl-
E
CCB2
280-598240/27
2 mL 2 mL 0.1 mLSM 4500 Cl-
E
CCV3
280-598240/32
2 mL 2 mLSM 4500 Cl-
E
CCB3
280-598240/33
Batch Notes
Color Reagent ID Chloride R1_00002
Pipette/Syringe/Dispenser ID WC-5000BOD1, 1000SM, 200SM
Batch Comment LRB
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1SM 4500 Cl- E
Page 340 of 349
Lab Name:Job No.:
SDG No.:
GENERAL CHEMISTRY BATCH WORKSHEET
280-170477-1
Batch Number:Batch Analyst:Batch Start Date:
Batch End Date:
Brock, Lucynda R
12/30/22 16:30
12/30/22 14:46598232
Batch Method:
Eurofins Denver
SM 4500 SO4 E
Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SO4 Cal Int
00042
SO4 ICV Int
00042
2 mL 2 mL 0.4 mLSM 4500 SO4
E
ICV
280-598232/10
2 mL 2 mLSM 4500 SO4
E
ICB
280-598232/11
2 mL 2 mL 0.5 mLSM 4500 SO4
E
LCS
280-598232/12
2 mL 2 mL 0.5 mLSM 4500 SO4
E
LCSD
280-598232/13
2 mL 2 mLSM 4500 SO4
E
MB
280-598232/14
2 mL 2 mL 0.4 mLSM 4500 SO4
E
CCV1
280-598232/19
2 mL 2 mLSM 4500 SO4
E
CCB1
280-598232/20
Offsite A-1 2 mL 2 mLSM 4500 SO4
E
T280-170477-A-1
Offsite A-2 2 mL 2 mLSM 4500 SO4
E
T280-170477-A-2
2 mL 2 mL 0.4 mLSM 4500 SO4
E
CCV
280-598232/25
2 mL 2 mLSM 4500 SO4
E
CCB
280-598232/26
2 mL 2 mL 0.4 mLSM 4500 SO4
E
CCV3
280-598232/31
2 mL 2 mLSM 4500 SO4
E
CCB3
280-598232/32
Batch Notes
Barium Chloride ID SO4 Color_00005
Timer ID Gallery 2
Pipette/Syringe/Dispenser ID WC-5000BOD1, 1000SM, 200SM
Batch Comment LRB
Basis Basis Description
T Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated concentration for
this reagent.
Page 1 of 1SM 4500 SO4 E
Page 341 of 349
Shipping and
Receiving
Documents
Page 342 of 349
Page 343 of 349
Page 344 of 349
Page 345 of 349
Page 346 of 349
Page 347 of 349
Page 348 of 349
Login Sample Receipt Checklist
Client: WSP USA Environment & Infrastructure Inc.Job Number: 280-170477-1
Login Number: 170477
Question Answer Comment
Creator: Roehsner, Karen P
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
FalseSamples are received within Holding Time (excluding tests with immediate
HTs)
Refer to Job Narrative for details.
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver Page 349 of 349
The analyses presented on this report were performed in accordance with the
National Environmental Laboratory Accreditation Program (NELAP) unless
noted in the comments, flags, or case narrative. If the report is to be used for
regulatory compliance, it should be presented in its entirety, and not be
altered.
Client Service Contact: 801.262.7299
Wood Environmental & Infrastructure (E&IS)
Attn: Brad Glisson
3800 Ezell Rd #100
Nashville, TN 37211
Work Order: 22L1312
Project: GE - Salt Lake City, Utah
1/9/2023
Approved By:
Mark Broadhead, Project Manager
9632 South 500 West Sandy, Utah 84070
Serving the Intermountain West since 1953
801.262.7299 Main 866.792.0093 Fax www.ChemtechFord.com
Page 1 of 8
_____________________________________________________________________________________________
Wood Environmental & Infrastructure (E&IS)
Project: GE - Salt Lake City, Utah
Project Manager: Brad Glisson
Laboratory ID Sample Name
22L1312-01 Offsite A-1
22L1312-02 Offsite A-2
______________________________________________________________________________________________
Work Order Report Narrative
Sample Preparation
All samples were prepared within method specified holding times. No preparation issues were noted.
Method Blanks
All blank values were within method acceptance criteria. No blank values exceeded the minimum reporting limit for any
analysis in this work order.
Laboratory Control Samples
All laboratory control samples were within method acceptance criteria.
Method Spikes
All method spike recoveries were within method acceptance criteria, except as noted by qualifying flags.
Method Spike Duplicates
All method spike duplicates were within method acceptance criteria, except as noted by qualifying flags.
Corrective Actions
There are no corrective actions associated with this work order.
www.ChemtechFord.com
Project Name: GE - Salt Lake City, Utah CtF WO#: 22L1312
Page 2 of 8
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Wood Environmental & Infrastructure (E&IS)
Brad Glisson
3800 Ezell Rd #100
Nashville, TN 37211
PO#:
Receipt:
Date Reported:
Project Name:
WDP0014.xxxx.xxxx.7362.57300
12/15/22 17:00 @ 1.0 °C
1/9/2023
GE - Salt Lake City, Utah
Sample ID: Offsite A-1
Lab ID: 22L1312-01Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 12/14/22 12:45
Preparation
Date/Time
Sampled By: Corey Buchanan
Minimum
Reporting
Limit MethodResult
1,4-Dioxane by SIM
ug/L 12/17/2212/17/220.2 EPA 8260D /5030A5.2p-Dioxane
Project Name: GE - Salt Lake City, Utah CtF WO#: 22L1312
www.ChemtechFord.com
Page 3 of 8Page 3 of 8
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Wood Environmental & Infrastructure (E&IS)
Brad Glisson
3800 Ezell Rd #100
Nashville, TN 37211
PO#:
Receipt:
Date Reported:
Project Name:
WDP0014.xxxx.xxxx.7362.57300
12/15/22 17:00 @ 1.0 °C
1/9/2023
GE - Salt Lake City, Utah
Sample ID: Offsite A-2
Lab ID: 22L1312-02Matrix: Water
Flag(s)Units
Analysis
Date/Time
Date Sampled: 12/14/22 11:00
Preparation
Date/Time
Sampled By: Corey Buchanan
Minimum
Reporting
Limit MethodResult
1,4-Dioxane by SIM
ug/L 12/17/2212/17/220.2 EPA 8260D /5030A5.1p-Dioxane
Project Name: GE - Salt Lake City, Utah CtF WO#: 22L1312
www.ChemtechFord.com
Page 4 of 8Page 4 of 8
xx
Chemtech-Ford Laboratories
Serving the Intermountain West Since 1953
Certificate of Analysis
9632 South 500 West
Sandy, UT 84070
O:[phone] F: [phone]
www.ChemtechFord.com
Wood Environmental & Infrastructure (E&IS)
Brad Glisson
3800 Ezell Rd #100
Nashville, TN 37211
PO#:
Receipt:
Date Reported:
Project Name:
WDP0014.xxxx.xxxx.7362.57300
12/15/22 17:00 @ 1.0 °C
1/9/2023
GE - Salt Lake City, Utah
Report Footnotes
Abbreviations
ND = Not detected at the corresponding Minimum Reporting Limit (MRL).
1 mg/L = one milligram per liter or 1 mg/kg = one milligram per kilogram = 1 part per million.
1 ug/L = one microgram per liter or 1 ug/kg = one microgram per kilogram = 1 part per billion.
1 ng/L = one nanogram per liter or 1 ng/kg = one nanogram per kilogram = 1 part per trillion.
Project Name: GE - Salt Lake City, Utah CtF WO#: 22L1312
www.ChemtechFord.com
Page 5 of 8Page 5 of 8
Page 6 of 8
QC Report for Work Order (WO) - 22L1312
% Rec RPD RPD Max MRL DFResultSpk ValueLimitsSource ConcAnalyte
Blank - EPA 8260D /5030A
QC Sample ID: BWL0755-BLK1 Batch: BWL0755
Date Prepared: 12/17/2022 Date Analyzed: 12/17/2022
p-Dioxane ND 0.2 1.00
Calibration Check - EPA 8260D /5030A
QC Sample ID: BWL0755-CCV1 Batch: BWL0755
Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022
p-Dioxane 98.8 80 - 120 9.88 10.0 0.2 1.00
LCS - EPA 8260D /5030A
QC Sample ID: BWL0755-BS1 Batch: BWL0755
Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022
p-Dioxane 116 80 - 120 11.6 10.0 0.2 1.00
Matrix Spike - EPA 8260D /5030A
QC Sample ID: BWL0755-MS1 QC Source Sample: 22L1312-01Batch: BWL0755
Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022
p-Dioxane 85.6 70 - 130 48.0 5.21 50.0 1.0 1.00
Matrix Spike Dup - EPA 8260D /5030A
QC Sample ID: BWL0755-MSD1 QC Source Sample: 22L1312-01Batch: BWL0755
Date Prepared: 12/16/2022 Date Analyzed: 12/16/2022
p-Dioxane 99.2 14.7 70 - 130 20 54.8 5.21 50.0 1.0 1.00
CtF WO#: 22L1312
www.ChemtechFord.com Page 7 of 8
Surrogates Report for Work Order (WO) - 22L1312
Spk ValueResultUCL DF BatchLCL% RecAnalyteQC ID
Blank - EPA 8260D /5030A
BWL0755-BLK1 Toluene-d8 101 70 BWL0755 1.0013010.1 10.0
Calibration Check - EPA 8260D /5030A
BWL0755-CCV1 Toluene-d8 103 0 BWL0755 1.0020010.3 10.0
LCS - EPA 8260D /5030A
BWL0755-BS1 Toluene-d8 100 70 BWL0755 1.0013010.0 10.0
Matrix Spike - EPA 8260D /5030A
BWL0755-MS1 Toluene-d8 104 70 BWL0755 1.0013052.1 50.0
Matrix Spike Dup - EPA 8260D /5030A
BWL0755-MSD1 Toluene-d8 108 70 BWL0755 1.0013054.0 50.0
UCLLCL%RecResultAnalyteLabNumber
Surrogate Recoveries (Field Samples)
SpkLvl Qualifier
8260 1,4-Dioxane SIM
22L1312-01 Toluene-d8 10.5 105 70 13010.0
8260 1,4-Dioxane SIM
22L1312-02 Toluene-d8 10.3 103 70 13010.0
CtF WO#: 22L1312
www.ChemtechFord.com Page 8 of 8
ANALYTICAL REPORT
PREPARED FOR
Attn: Brad Glisson
WSP USA Environment & Infrastructure Inc.
3800 Ezell Rd #100
Nashville TN 37211
Generated 12/30/2022 1:37 PM
JOB DESCRIPTION
GE-Salt Lake City, Utah
JOB NUMBER
280-170477-2
See page two for job notes and contact information.
Arvada CO 80002
4955 Yarrow Street
Eurofins Denver
Page 1 of 22
Eurofins Denver
Eurofins Denver is a laboratory within TestAmerica Laboratories, Inc., a company within Eurofins Environment Testing Group of Companies
Job Notes
The test results in this report relate only to the samples in this report and meet all requirements of NELAC, with any
exceptions noted. Pursuant to NELAP, this report shall not be reproduced except in full, without the written approval of the
laboratory. All questions regarding this report should be directed to the Eurofins TestAmerica Denver Project Manager.

The Lab Certification ID# is 4025.

Reporting limits are adjusted for sample size used, dilutions and moisture content if applicable.
The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the
methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written
approval of the laboratory. All questions should be directed to the Eurofins TestAmerica Project Manager.
Authorization
Generated
12/30/2022 1:37 PM
Authorized for release by
Shelby R Turner, Project Manager I
[e-mail]

Page 2 of 22
Table of Contents
Cover Title Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .1
Data Summaries . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Definitions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .4
Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .5
Method Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .6
Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .7
Subcontracted Data . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .8
Shipping and Receiving Documents . . . . . . . . . . . . . . . . . . . . . . . . . . .19
Client Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .20
Sample Receipt Checklist . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .22
Page 3 of 22
Definitions/Glossary
Job ID: 280-170477-2Client: WSP USA Environment & Infrastructure Inc.
Project/Site: GE-Salt Lake City, Utah
Glossary
These commonly used abbreviations may or may not be present in this report.
¤Listed under the "D" column to designate that the result is reported on a dry weight basis
Abbreviation
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoD/DOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative / Absent
POS Positive / Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Eurofins Denver
Page 4 of 22
CASE NARRATIVE
Client: Wood E&I Solutions Inc
Project: GE-Salt Lake City, Utah
Report Number: 280-170477-2
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
RECEIPT
The samples were received at Pace Analytical on 12/16/2022 9:50 AM. Unless otherwise noted below, the samples arrived in good
condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt time was 0.5º C.
The sample summary section of this report notes that samples were received on 12/16/2022 9:15 AM. This is the receipt date/time of
sample volume submitted to the Denver laboratory because the Dissolved Hydrogen analysis was logged in the same job as the Denver
analyses. Dissolved Hydrogen is reported separately from the Denver analyses.
SUBCONTRACTING
The following analysis was subcontracted to Pace Analytical Gulf Coast:
Dissolved Hydrogen
Subcontract Lab non-Sister Lab
See attached subcontract report.
Page 5 of 22
Method Summary
Job ID: 280-170477-2Client: WSP USA Environment & Infrastructure Inc.
Project/Site: GE-Salt Lake City, Utah
Method Method Description LaboratoryProtocol
NoneSubcontractDissolved Hydrogen PAGC
Protocol References:
None = None
Laboratory References:
PAGC = Pace Analytical Gulf Coast, 7979 Innovation Park Drive, Baton Rouge, LA 70820
Eurofins Denver
Page 6 of 22
Sample Summary
Client: WSP USA Environment & Infrastructure Inc.Job ID: 280-170477-2
Project/Site: GE-Salt Lake City, Utah
Lab Sample ID Client Sample ID Matrix Collected Received
280-170477-1 Offsite A-1 Water 12/14/22 12:45 12/16/22 09:15
280-170477-2 Offsite A-2 Water 12/14/22 11:00 12/16/22 09:15
Eurofins DenverPage 7 of 22
Subcontract Data
Page 8 of 22

Cover
ANALYTICAL RESULTS

PERFORMED BY

Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]

Report Date 12/28/2022

Report # 222121712
9999999999

Project 280-170477-1

Samples Collected 12/14/22

Deliver To Additional Recipients
Shelby Turner NONE
Eurofins Test America - Denver
4955 Yarrow St
Arvada, CO 80002
303-736-0165
LELAP Certificate Number: 01955
A2LA Accredited (DoD ELAP-QSM 5.4) Certificate Number: 6429.01

Page 1 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 9 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Laboratory Endorsement

Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or ot her recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.

Common Abbreviations that may be Utilized in this Report

ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub-Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re-analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM

Reporting Flags that may be Utilized in this Report

J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non-compliant QC Result (See Q Flag Application Report)
* Indicates a non-compliant or not applicable QC recovery or RPD – see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk-based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis – when appended to Client Sample ID

Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.

This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in thi s report is prohibited.

I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.

Estimated uncertainty of measurement is available upon request. This report is in compliance with t he DOD QSM as specified in the contract if
applicable.

Authorized Signature
Pace Gulf Coast Report 222121712

Page 2 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 10 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Certifications

Certification Certification Number
A2LA Accredited (DoD ELAP-QSM 5.4) 6429.01
Alabama 01955
Arkansas 88-0655
Colorado 01955
Delaware 01955
Florida E87854
Georgia 01955
Hawaii 01955
Idaho 01955
Illinois 200048
Indiana 01955
Kansas E-10354
Kentucky 95
Louisiana 01955
Maryland 01955
Massachusetts 01955
Michigan 01955
Mississippi 01955
Missouri 01955
Montana N/A
Nebraska 01955
New Mexico 01955
North Carolina 618
North Dakota R-195
Oklahoma 9403
South Carolina 73006001
South Dakota 01955
Tennessee 01955
Texas T104704178
Vermont 01955
Virginia 460215
Washington C929
USDA Soil Permit P330-16-00234

Page 3 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 11 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Case Narrative
Client: Eurofins - Denver Report: 222121712
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).

Page 4 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 12 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Sample Summary
Lab ID Client ID Matrix Collect Date Receive Date
22212171201 OFFSITE A-1 Water 12/14/22 12:45 12/16/22 09:50
22212171202 OFFSITE A-2 Water 12/14/22 11:00 12/16/22 09:50
Page 5 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 13 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Detect Summary
Results and Detection Limits are adjusted for dilution and moisture when applicable

AM20GAX
Lab ID Client ID Parameter Units Result Dil. %Moist
22212171201 OFFSITE A-1 Hydrogen nM 28 1 NA
22212171202 OFFSITE A-2 Hydrogen nM 30 1 NA
Page 6 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 14 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

Sample Results
Sample Results
OFFSITE A-1
OFFSITE A-1 Collect Date 12/14/2022 12:45 Lab ID 22212171201
Receive Date 12/16/2022 09:50 Matrix Water

AM20GAX
AM20GAX

Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/21/22 06:52 756575 LMB NA

CAS# Parameter Result LOQ Units
1333-74-0 Hydrogen 28 15 nM
OFFSITE A-2
OFFSITE A-2 Collect Date 12/14/2022 11:00 Lab ID 22212171202
Receive Date 12/16/2022 09:50 Matrix Water

AM20GAX
AM20GAX

Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 12/21/22 07:14 756575 LMB NA

CAS# Parameter Result LOQ Units
1333-74-0 Hydrogen 30 15 nM
Page 7 of 1012/28/2022 16:56Pace Gulf Coast Report#: 222121712 Page 15 of 22

Report#: 222121712
Project ID: 280-170477-1 Report Date: 12/28/2022

QC Summary
General Chromatography QC Summary
General Chromatography
Analytical Batch
756575

Client ID
Lab ID
Sample Type
Prep Date
Analysis Date
Matrix

MB756575
2435009
MB
NA
12/21/22 06:38
Water

LCS756575
2435010
LCS
NA
12/21/22 06:08
Water

LCSD756575
2435011
LCSD
NA
12/21/22 06:25
Water

AM20GAX Units
Result
nM
LOQ
Spike
Added Result %R Control
Limits%R
Spike
Added Result %R RPD RPD
Limit
Hydrogen 1333-74-0 ND 15 130 160 127 70 - 130 130 160 130 2 20

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SAMPLE RECEIVING CHECKLIST *222121712*
SAMPLE DELIVERY GROUP 222121712
Client PM RWe Transport Method
5577 - Eurofins - Denver FEDEX
Profile Number Received By
300327 McCune, Dodie N.
Line Item(s)Receive Date(s)
1 - Hydrogen 12/16/22
CHECKLIST YES NO
Samples received with proper thermal preservation?
Radioactivity is <1600 cpm? If no, record cpm value in notes section.
COC relinquished and complete (including sampleIDs, collect times, and sampler)?
All containers received in good condition and within hold time?
All sample labels and containers received match the chain of custody?
Preservative added to any containers?
If received, was headspace for VOC water containers < 6mm?
Samples collected in containers provided by Pace Gulf Coast?
COOLERS
Airbill Thermometer ID:E38 Temp oC
392272878334 0.5
DISCREPANCIES
None
LAB PRESERVATIONS
None
NOTES
Revision 1.6 Page 1 of 1
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Shipping and
Receiving
Documents
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Login Sample Receipt Checklist
Client: WSP USA Environment & Infrastructure Inc.Job Number: 280-170477-2
Login Number: 170477
Question Answer Comment
Creator: Roehsner, Karen P
List Source: Eurofins Denver
List Number: 1
TrueRadioactivity wasn't checked or is </= background as measured by a survey
meter.
TrueThe cooler's custody seal, if present, is intact.
TrueSample custody seals, if present, are intact.
TrueThe cooler or samples do not appear to have been compromised or
tampered with.
TrueSamples were received on ice.
TrueCooler Temperature is acceptable.
TrueCooler Temperature is recorded.
TrueCOC is present.
TrueCOC is filled out in ink and legible.
TrueCOC is filled out with all pertinent information.
TrueIs the Field Sampler's name present on COC?
TrueThere are no discrepancies between the containers received and the COC.
TrueSamples are received within Holding Time (excluding tests with immediate
HTs)
TrueSample containers have legible labels.
TrueContainers are not broken or leaking.
TrueSample collection date/times are provided.
TrueAppropriate sample containers are used.
TrueSample bottles are completely filled.
N/ASample Preservation Verified.
TrueThere is sufficient vol. for all requested analyses, incl. any requested
MS/MSDs
TrueContainers requiring zero headspace have no headspace or bubble is
<6mm (1/4").
TrueMultiphasic samples are not present.
TrueSamples do not require splitting or compositing.
N/AResidual Chlorine Checked.
Eurofins Denver Page 22 of 22